Micro 7+ Revision 02/25/14 486691-K Standard Kit Advanced Photometer System IDEAL FOR DRINKING WATER, POOLS AND SPAS, ENVIRONMENTAL, & EDUCATIONAL TESTING USEPA, DIN, & ISO Compliant for Free & Total Chlorine Testing (4500-CL G, DIN Standard 38 408 G4, ISO 7393/2) 863DWHQW1R863DWHQW1R6RXWK$IULFDQ3DWHQW1R (83DWHQWDQG,QWHUQDWLRQDO3DWHQW$SSOQ1R3&786 Index: Parameter Free Chlorine (DPD-1) Permanganate (DPD-1) Combined Chlorine (DPD-3) Ozone (DPD-4) Total Chlorine (DPD-4) pH Bromine (DPD-1) Total Alkalinity (as CaCO3) Total Hardness (as CaCO3) Copper (as Cu+2) Total Iron (as Fe) High Range Chlorine 6SHFL¿FDWLRQV About Your Photometer Tips for Best Accuracy Battery Installation Warranty (2 year) Reorder Information USEPA Compliance Kit Components Page 4 4 5 6 6 6 7 7 8 8 9 9 3 10 11 11 12 3, 12 12 MENU CL1 CL1 CL1 CL1 CL1 PH2 BR3 AL4 TH5 CU6 FE7 HR8 Visit us online at sensafe.com/micro7+ for up-to-date product information and to register your warranty. Manufactured By: Industrial Test Systems, Inc. /DQJVWRQ6WUHHW5RFN+LOO6&86$ Phone: 1-800-861-9712 - INSIDE THE U.S. 1-803-329-9712 - OUTSIDE THE U.S. Fax: 1-803-329-9743 ITS@SENSAFE.COM WWW.SENSAFE.COM www.poolcheckonline.com The eXact® Micro 7+ Advanced Photometer System is designed for use with the eXact® Strip Micro reagent delivery system. eXact® Micro 7+ is Manufactured and tested in an ISO 9001 Facility ,QGXVWULDO7HVW6\VWHPV,QF(;$&7®LVDUHJLVWHUHGWUDGHPDUNRI,QGXVWULDO7HVW6\VWHPV,QF5RFN+LOO6&86$ eXact® Micro 7+ Photometer ITEM PICTURED LETTER B A B C D E C F G H D COMPONENT NAME Mixing Cap/Cell Cover Cell (Built-in Plastic, 4mL) LCD Display READ Button MENU Button ZERO/ON Button Battery Cover with loop for lanyard AAA Batteries (x4) (Not Included) E F A G H (Used for testing outdoors) + – eXact®0LFUR0HWHU6SHFLÀFDWLRQV Measurement Method: Light Source: Wavelength: Automatic Range Selection: Display: CELL Pathlength: Cell Chamber: Custom-molded, proprietary, PET plastic IXVHGLQWRFKDPEHUQRQUHPRYDEOH Sample Required: 4mL (0.13 oz) Operating Temperature Range: 0 - 50°C (32° - 122°F) Power Supply: $$$DONDOLQHEDWWHULHV1RW,QFOXGHG Battery Life: !WHVWVZLWKDONDOLQHEDWWHULHV Electromagnetic Compliance: (PLWWHG,QWHUIHUHQFH(1 (EMC) ,PPXQLW\WR,QWHUIHUHQFH(1 Waterproof Rating: ([FHHGV,3 Weight: ,QVWUXPHQWJR] Dimensions: ,QVWUXPHQW:['[+FP [[LQ Photometric Light Emitting Diode (LED) 525 nm 6HH6SHFL¿FDWLRQVEHORZ 3-digit customized liquid crystal display with annunciators 20mm We offer a “Green” Alternative eXact® Strip Micro 7+ KDVEHHQGHVLJQHGWRRIIHUWKHXVHUDPRUH³*UHHQ´DQGFRVWHIIHFWLYHDOWHUQDWLYHWRWHVWLQJ ,QVWHDGRIXVLQJDP/ZDWHUVDPSOHeXact® Strip Micro 7+ XVHVDP/ZDWHUVDPSOHZKLFKXVHVXSWROHVV FKHPLFDOSHUWHVW7KHDFFXUDF\RIWKHPHWHULVPDLQWDLQHGE\GHVLJQLQJWKHSKRWRFHOOZLWKDPPSDWKOHQJWK eXact®0LFUR6SHFL¿FDWLRQV 0HQX 7HVWVIRU1 5DQJH CL1 )UHH&KORULQH 7RWDO&KORULQH SSP PH2 S+ S+ BR3 Bromine SSP AL4 7RWDO$ONDOLQLW\ DV&D&2) TH5 5HVROXWLRQ Expected Meter2 $FFXUDF\ SSP SSP SSP SSP SSP SSP S+ SSP SSP SSP 1 7RWDO+DUGQHVV DV&D&2) SSP 1 CU6 &RSSHUDV&X) SSP SSP SSP FE7 7RWDO,URQDV)H SSP HR8 +LJK5DQJH&KORULQH SSP 1 SSP SSP SSP SSP R022514 3HUIRUPDQFHYHUL¿HGZLWKYDULRXVVDOWV\VWHPVDQGZDWHUVDPSOHVZLWKRSWLPDOZDWHU WHPSHUDWXUHDWÛ&Û)2SWLPDOZDWHUWHPSHUDWXUHIRU7RWDO$ONDOLQLW\WHVWLV Û&Û)2SWLPDOZDWHUWHPSHUDWXUHIRU+LJK5DQJH&KORULQHWHVWLVÛ&Û) )RUH[DPSOH,IWKHVDPSOHKDVSSPRI)UHH&KORULQHWKHPHWHUPD\UHDGSSPRUSSP 1 2 About Your eXact® Micro 7+ Instrument In order to save power, the meter is designed to turn off after 3 minutes (timed from the last button pressed). Should the meter turn off in the middle of a test, the last stored zero in the meter will remain valid when the meter is turned on again. Also, the test result is stored in memory for easy retrieval. The eXact® Micro 7+ meter is controlled by three buttons: 1. ZERO/ON:KHQ¿UVWSUHVVHGWKLVEXWWRQWXUQVWKHPHWHURQ:KHQWKHPHWHULVRQDQGWKLVEXWWRQLV pressed, it zeroes the sample in the cell. Once the meter is zeroed, this zero value applies to all parameters and is stored and retained even when meter turns off. However, it is recommended that each new water sample analyzed is zeroed before testing, to maximize sensitivity and accuracy. 2. MENU: With each press, the MENU button advances through the tests in the following sequence: CL1, PH2, BR3, AL4, TH5, CU6, FE7, HR8. Each test menu can store up to 20 results. To retrieve the stored results, go to the desired test using the MENU key. When the desired test is displayed, press and hold down the MENU key. Continue holding down the MENU key to scroll the stored results for that test, starting with the most recent result. The meter will display, from memory, the last 20 readings in sequence beginning with -20, which is the latest result, followed by -19, which is the 2ndODWHVWUHVXOWHWFDQG¿QDOO\ZKLFKLV the oldest result retained. Only the last 20 readings are stored in each menu. This meter is able to store 160 results in memory (20 in each menu). 3. READ: When pressed once, this button starts the timer for the parameter being tested. When pressed a second time the meter exits the timer and immediately prepares to colorimetrically measure the sample, and simultaneously stores the measurement in memory. If the parameter being measured is below or above the detection range, the display will show “LO” (Under Range) or “HI´2YHU5DQJHUHVSHFWLYHO\7KLVIHDWXUHLVPHQXVSHFL¿FDQGGRHVQRWDSSO\WRDOOSDUDPHWHUV About The Accuracy / Calibration Of The Micro 7+ System $OOWHVWVKDYHEHHQFDOLEUDWHGXVLQJFHUWL¿HGUHIHUHQFHVWDQGDUGVDQGVWDQGDUGDQDO\WLFDO VSHFWURSKRWRPHWULFPHWKRGV7KHDOJRULWKPVLQWKHVRIWZDUHUHÀHFWWKHEHVWFRUUHODWLRQRIWKHH;DFW® Micro 7+ Systems against the AWWA, US EPA , DIN, and ISO reference test methods for chlorine. Studies show that the eXact® Micro 7+ System repeatedly agrees with an EPA Compliant reference method greater than 99% (R2= 0.9989, 0 - 6.0 ppm - see page 12). The eXact® Micro 7+ Advanced 3KRWRPHWULF6\VWHPKDVEHHQIDFWRU\FDOLEUDWHGIRU\RXUFRQYHQLHQFH<RXFDQH[SHFWWKH¿[HG calibrations in the meter to be valid for the life of the meter because of the quality, Long-Life LED, the photo cell, and the software as written into the meter. This is why the meter comes with a 2-Year Warranty. NOTE: Test algorithms in this meter give accurate results in fresh and salt water (except Nitrate). Compliance VHULÀFDWLRQIRU)UHHDQG7RWDO&KORULQH7HVWLQJ This DPD test system is accepted by most health departments because this test is USEPA (DIN Standard 38 408 G4, ISO 7393/2) accepted for testing requirements for Free and Total Chlorine. The Micro 7+ meter uses a wavelength of 525nm; and the compliance requirement is that the colorimeter wavelength is between 490 and 530nm. The eXact® Strip Micro CL (DPD-1) uses the same reagents and proportions, and the resulting solution pH is maintained between 6.2 and 6.5 as VSHFL¿HGby AWWA (American Water Works Association) method 4500-Cl G. It should be understood that the USEPA does not "approve" commercial DPD delivery systems such as reagent powder pillows, tablets, dispensers, or eXact® Strip DPD delivery devices. The eXact® Strip Micro CL (DPD-1) for Free Chlorine, and the eXact® Strip Micro CL (DPD-3) or the eXact® Strip Micro CL (DPD-4) for Total Chlorine meet your reportable testing requirements because the eXact® Strip Micro CL delivers the same chemicals in identical proportions (see table below); therefore, the system is compliant. Likewise, AWWA proportions are followed as required for Total Chlorine measurements using Potassium Iodide. Component (Free Chlorine) Anhydrous DPD sulfate Anhydrous Na2HPO4 Anhydrous KH2PO4Na2 EDTA 3 AWWA 4500-Cl G eXact® DPD-1 1.5% 33.4% 64.0% 1.1% 1.5% 33.4% 64.0% 1.1% CL1 1 DPD-1 Free Chlorine Test Procedure 1 Remove one (1) eXact Strip Micro CL (DPD-1), Part No. 486637 from the bottle before beginning the test. Set the strip in a dry, convenient place and recap the bottle immediately. TURN METER ON 3 SELECT TEST: CL1 Press the ZERO/ON button to power the meter on; the display will show all annunciators, then the current MENU selection, followed by the last reading. Press and re-press the MENU button until the display shows the parameter CL1. CL1 is also used for testing: Total Chlorine (DPD-4), Ozone (DPD-4), Permanganate (DPD-1), and Total Chlorine (DPD-3). (Contact ITS for specs and details if you are planning on using CL1 for Permanganate or Ozone measurements) 2b 4 3 5 6 5 7 6 CL ® 2 2a 4 REMOVE STRIP RINSE AND FILL CELL WITH SAMPLE Rinse the CELL at least 3 times with the water sample you will be testing - rinsing minimizes the potential for FURVVFRQWDPLQDWLRQIURPDSUHYLRXVWHVW)LQDOO\¿OO cell to capacity (4ml) with the water sample. ZERO METER Press the ZERO/ON button. The cursor will move across the display followed by 0.00 PPM. Sample is ready for testing. DIP STRIP AND PRESS “READ” Dip the eXact® Strip Micro CL (DPD-1), Part No. 486637 into the CELL and immediately press READ. This starts the 20 SECOND countdown timer. During this time move the strip in a gentle back and forth motion. Remove and discard the strip after “1” on the display disappears. RECORD RESULT DISPLAYED The cursor will move across the display while the meter prepares to measure the sample. Record result displayed (this result is automatically stored in CL1). DO NOT discard the sample from the Free Chlorine test if you are planning to run eXact® Strip Micro DPD-3 (Combined Chlorine) Procedure. Move directly to steps 8-10 on page 5. Otherwise, rinse the cell immediately. NOTE: Chlorine reacts with N,N-diethyl-p-phenylenediamine as it is released from the strip to form a magenta color, directly proportional to the Chlorine concentration. 4 CL DPD-3 Combined Chlorine Test Procedure CL1 This procedure is only valid when run as a continuation of the eXact® Strip Micro CL (DPD-1 Free Chlorine) Test Procedure located on the previous page. 8 9 10 REMOVE STRIP Remove one (1) eXact® Strip Micro CL (DPD-3), Part No. 486638 from the bottle before beginning the test. Set the strip in a dry, convenient place and recap the bottle immediately. DIP STRIP AND PRESS “READ” Dip the eXact® Strip Micro CL (DPD-3) into the CELL and immediately press READ. This starts the 20 SECOND countdown timer. During this time move the strip in a gentle back and forth motion. Remove and discard the strip when “1” on the display disappears. The cursor will move across the display while the meter prepares to measure the sample. This result is automatically stored in CL1 (NOTE: The Iodide added with DPD-3 will, in the presence of Combined Chlorine or Chloramines, convert into Iodine). PRESS READ AGAIN Press READ again and the meter will count down and display the next reading. If this reading matches the previous result, then record this as the Total Chlorine result. This value is automatically stored in CL1. After testing is completed, rinse cell immediately. Record the Total Chlorine as the highest value the meter displayed. *NOTE: Standard Method (4500-Cl G, procedure for total chlorine) requires the reading to be made after 2 minutes from the time the KI is added. For compliance testing, you must time the two minutes and then make your measurement. NOTE: From testing in our lab, water samples above 70°F (20°C), generally, reach a stabilized reading quicker then 2 minutes. CL1: Chlorine and Iodine react with N,N-diethyl-p-phenylenediamine as it is released from the strip to form a magenta color, directly proportional to the Chlorine concentration. Ozone, Bromine, and Permanganate, and Chlorine Dioxide also form this color. eXact® Strip Micro CL (DPD-1/DPD-3/DPD-4) Interferences (part nos. 486637/486638/486670) Interfering Levels & Treatments If sample has acidity above 150mg/L CaCO3 test may not develop full color. Neutralize to pH 6.0 to 7.0 with 0.5N Sodium hydroxide. If sample has alkalinity above 200mg/L CaCO3 test may not develop Alkalinity full color. Neutralize to pH 6.0 to 7.0 with 0.5N Sulfuric acid. Color similar to free chlorine reaction at all levels. Bromine & Bromamines, Br2 Color similar to free chlorine reaction at all levels. Chlorine Dioxide, ClO2 Color development is reduced above 10 ppm (mg/L). Copper, Cu+2 Color similar to free chlorine reaction at all levels. Iodine, I2 Manganese, oxidized (Mn+4, Mn+7) See AWWA procedure 4500-CL F, 1(d) for removal of interferences. or Chromium, oxidized (Cr+6) Monochloramine interferences are known to occur in free chlorine Monochloramines (NH2Cl) DPD methods. This interference is dependent on temperature and (applies to DPD-1 only) monochloramine concentration. Color similar to free chlorine reaction at all levels. Ozone, O3 Interference is possible. Peroxides Typical pH samples of potable water with a pH of 6.0 to 9.0 are pH OK. If outside this range adjust to pH 6.0 to 7.0 using acid (0.5N Sulfuric acid) or base (0.5N Sodium hydroxide). Interfering Substance Acidity 5 DPD-4 (Total Chlorine or Ozone) Test Procedure CL1 1 REMOVE STRIP Remove one (1) eXact® Strip Micro CL (DPD-4 for Total Chlorine or Ozone), Part No. 486670 from the bottle before beginning the test. Set the strip in a dry, convenient place and recap the bottle immediately. 2 TURN METER ON 3 SELECT TEST: CL1 4 FILL METER WITH SAMPLE 5 6 7 Press the ZERO/ON button to power the meter on; the display will show all annunciators, then the current MENU selection, followed by the last reading. Press and re-press the MENU button until the display shows the parameter CL1. Rinse the CELL at least 3 times with the water sample you will be testing - rinsing PLQLPL]HVWKHSRWHQWLDOIRUFURVVFRQWDPLQDWLRQIURPDSUHYLRXVWHVW)LQDOO\¿OOFHOOWR capacity (4ml) with the water sample. ZERO METER* Press the ZERO/ON button. The cursor will move across the display, followed by 0.00 PPM. Sample is ready for testing. DIP STRIP AND PRESS “READ” Dip the eXact® Strip Micro CL (DPD-4), Part No. 486670 into the CELL and immediately press READ. This starts the 20 SECOND countdown timer. During this time move the strip in a gentle back and forth motion. Remove and discard the strip after “1” on the display disappears*. The cursor will move across the display while the meter prepares to measure the sample. Record result displayed (this result is automatically stored in CL1). PRESS READ AGAIN Press READ again and the meter will count down and display the next Total Chlorine result. If this reading matches the previous result, then record this as Total Chlorine value (this result is stored in CL1). After testing is completed, rinse cell immediately. Record the Total Chlorine as the highest value the meter displayed. NOTE: Standard Method (4500-Cl G, procedure for total chlorine) requires the reading to be made after 2 minutes. 2 minute wait is not necessary for Ozone measurements. PH2 1 pH Test Procedure REMOVE STRIP TURN METER ON 3 SELECT TEST: PH2 5 6 PH Remove one (1) eXact® Strip Micro PH, Part No. 486639 from the bottle before beginning the test. Set the strip in a dry, convenient place and recap the bottle immediately. 2 4 CL Press the ZERO/ON button to power the meter on; the display will show all annunciators, then the current MENU selection, followed by the last reading. Press and re-press the MENU button until the display shows the parameter PH2. FILL METER WITH SAMPLE Rinse the CELL at least 3 times with the water sample you will be testing - rinsing minimizes WKHSRWHQWLDOIRUFURVVFRQWDPLQDWLRQIURPDSUHYLRXVWHVW)LQDOO\¿OOFHOOWRFDSDFLW\POZLWK the water sample. ZERO METER* Press the ZERO/ON button. When the display shows 0.0 PH, the sample is ready for testing. DIP STRIP AND PRESS “READ” Dip the eXact® Strip Micro PH, Part No. 486639 into the CELL and immediately press READ. This starts the 20 SECOND countdown timer. During this time move the strip in a gentle back and forth motion (approx. 2 strokes/sec). Remove and discard the strip after “1” on the display disappears*. The cursor will move across the display while the meter prepares to measure the sample. Record result displayed (this result is automatically stored in PH2). After testing, rinse cell immediately. NOTE: For best results, Total Alkalinity of the sample should be 40-140 ppm. *NOTE: When testing outdoors (sunlight), for best accuracy, use the Mixing Cap/Cell Cover when Zeroing and Reading the sample. 6 Bromine DPD-1 Test Procedure 1 REMOVE STRIP Remove one (1) eXact® Strip Micro CL (DPD-1), Part No. 486637 from the bottle before beginning the test. Set the strip in a dry, convenient place and recap the bottle immediately. 2 TURN METER ON 3 SELECT TEST: bR3 4 FILL METER WITH SAMPLE 5 6 Press the ZERO/ON button to power the meter on; the display will show all annunciators, then the current MENU selection, followed by the last reading. Press and re-press the MENU button until the display shows the parameter bR3. Rinse the CELL at least 3 times with the water sample you will be testing - rinsing minimizes WKHSRWHQWLDOIRUFURVVFRQWDPLQDWLRQIURPDSUHYLRXVWHVW)LQDOO\¿OOFHOOWRFDSDFLW\POZLWK the water sample. ZERO METER* Press the ZERO/ON button. The cursor will move across the display, followed by 0.00 PPM. The sample is ready for testing. DIP STRIP AND PRESS “READ” Dip the eXact® Strip Micro CL (DPD-1), Part No. 486637 into the CELL and immediately press READ. This starts the 20 SECOND countdown timer. During this time move the strip in a gentle back and forth motion (approx. 2 strokes/sec). Remove and discard the strip after “1” on the display disappears*. The cursor will move across the display while the meter prepares to measure the sample. Record result displayed (this result is stored in bR3 memory). After testing is completed, rinse cell immediately. AL 1 2 3 4 5 6 bR3 Total Alkalinity Test Procedure AL4 REMOVE STRIP Remove one (1) eXact® Strip Micro AL, Part No. 486641 from the bottle before beginning the test. Set the strip in a dry, convenient place and recap the bottle immediately. TURN METER ON Press the ZERO/ON button to power the meter on; the display will show all annunciators, then the current MENU selection, followed by the last reading. SELECT TEST: AL4 Press and re-press the MENUEXWWRQXQWLOWKHGLVSOD\VKRZVWKHSDUDPHWHU$/ FILL METER WITH SAMPLE Rinse the CELL at least 3 times with the water sample you will be testing - rinsing minimizes WKHSRWHQWLDOIRUFURVVFRQWDPLQDWLRQIURPDSUHYLRXVWHVW)LQDOO\¿OOFHOOWRFDSDFLW\POZLWK the water sample. ZERO METER* Press the ZERO/ON button. The cursor will move across the display, followed by 0.00 PPM. The sample is ready for testing. DIP STRIP AND PRESS “READ” Dip the eXact® Strip Micro AL, Part No. 486641 into the CELL and immediately press READ. This starts the 20 SECOND countdown timer. During this time move the strip in a gentle back and forth motion (approx. 2 strokes/sec). Remove and discard the strip after “1” on the display disappears*. NOTE: For water temperatures above 95°F/35°C (hot tubs), remove and discard the strip when the timer displays “10”, countdown continues. For the hot water samples, a 10-second dip time is best. The cursor will move across the display while the meter prepares to measure the sample. Record result displayed WKLVUHVXOWLVDXWRPDWLFDOO\VWRUHGLQ$/$IWHUWHVWLQJLVFRPSOHWHGULQVHFHOOLPPHGLDWHO\ NOTE: Total Alkalinity reacts with the Alizarin Red S and citric acid as it is released from the strip to form a red color, directly proportional to the alkalinity present in the sample. *NOTE: When testing outdoors (sunlight), for best accuracy, use the Mixing Cap/Cell Cover when Zeroing and Reading the sample. 7 TH5 1 Total Hardness Test Procedure REMOVE STRIP Remove one (1) eXact® Strip Micro TH, Part No. 486673 from the bottle before beginning the test. Set the strip in a dry, convenient place and recap the bottle immediately. 2 TURN METER ON 3 SELECT TEST: TH5 4 FILL METER WITH SAMPLE 5 6 TH Press the ZERO/ON button to power the meter on; the display will show all annunciators, then the current MENU selection, followed by the last reading. Press and re-press the MENU button until the display shows the parameter TH5. Rinse the CELL 2 or 3 times with the water sample you will be testing - rinsing minimizes WKHSRWHQWLDOIRUFURVVFRQWDPLQDWLRQIURPDSUHYLRXVWHVW)LQDOO\¿OOFHOOWRFDSDFLW\PO with the water sample. ZERO METER Press the ZERO/ON button. The cursor will move across the display, followed by 0.00 PPM. The sample is ready for testing. DIP STRIP AND PRESS “READ” Dip the eXact® Strip Micro TH, Part No. 486673 into the CELL and immediately press READ. This starts the 20 SECOND countdown timer. During this time move the strip in a gentle back and forth motion. Remove and discard the strip after “1” on the display disappears. The cursor will move across the display while the meter prepares to measure the sample. Record result displayed (this result is automatically stored in TH5). After testing is completed, rinse cell immediately. INTERFERENCES: Positive interferences are observed if the test sample contains Barium. Interferences also observed if the test sample contains Copper, Lead, Cobalt or Nickel. NOTE: The Calcium and Magnesium ions react with Phthalein purple to form a purple color depending on the concentration. CU6 1 Copper Test Procedure REMOVE STRIP Remove one (1) eXact® Strip Micro CU, Part No. 486632 from the bottle before beginning the test. Set the strip in a dry, convenient place and recap the bottle immediately. 2 TURN METER ON 3 SELECT TEST: CU6 4 5 6 CU Press the ZERO/ON button to power the meter on; the display will show all annunciators, then the current MENU selection, followed by the last reading. Press and re-press the MENU button until the display shows the parameter CU6. FILL METER WITH SAMPLE Rinse the CELL at least 3 times with the water sample you will be testing - rinsing PLQLPL]HVWKHSRWHQWLDOIRUFURVVFRQWDPLQDWLRQIURPDSUHYLRXVWHVW)LQDOO\¿OOFHOOWR FDSDFLW\POZLWKWKHZDWHUVDPSOH ZERO METER* Press the ZERO/ON button. The cursor will move across the display, followed by 0.00 PPM. The sample is ready for testing. DIP STRIP AND PRESS “READ” Dip the eXact® Strip Micro CU, Part No. 486632 into the CELL and immediately press READ. This starts the 20 SECOND countdown timer. During this time move the strip in a gentle back and forth motion. Remove and discard the strip after “1” on the display disappears*. The display will immediately start counting up from 1 to 20 (this extra time allows more thorough color development). At 20 sec, the cursor will move across the display while the meter prepares to measure the sample. Record result displayed (this result is automatically stored in CU6). After testing is completed, rinse cell immediately. NOTE: Copper reacts with Biquinoline or Bicinchoninic Acid as it is released from the strip to form a purple color, directly proportional to the copper concentration. *NOTE: When testing outdoors (sunlight), for best accuracy, use the Mixing Cap/Cell Cover when Zeroing and Reading the sample. 8 FE Total Iron, TPTZ (Fe+2/Fe+3) Test Procedure 7RWDO,URQ.LW5HGXFHUDQG6WULSV 1 TURN METER ON 2 SELECT TEST: FE7 3 FILL METER WITH SAMPLE 4 5 6 FE7 Press the ZERO/ON button to power the meter on; the display will show all annunciators, then the current MENU selection, followed by the last reading. Press and re-press the MENU button until the display shows the parameter FE7. Rinse the CELL at least 3 times with the water sample you will be testing - rinsing minimizes WKHSRWHQWLDOIRUFURVVFRQWDPLQDWLRQIURPDSUHYLRXVWHVW)LOOFHOOWRFDSDFLW\POZLWKWKH water sample. NOTE: For accurate results (<0.3 ppm) it is recommended to rinse the CELL with diluted HCl (diluted Muriatic acid) or White Distilled Vinegar solution. ADD REAGENT, CAP, AND MIX Tilt meter to discard about 0.2 mL water in order to leave room for powder reagent. Add the contents of one eXact® Reagent EZ Open REDUCER, Part No. 486601 to the CELL and cap meter cell with mixing cap. Press READ to start the 20 SECOND countdown timer, place thumb over cap to keep cap securely in place, and mix the sample by turning the meter upside-down repetitively. When time displays 1KROGWKHPHWHUXSULJKWDQGWKHFXUVRUZLOOÀDVKDQGWKHPHWHUZLOOEHJLQWRFRXQW XSWRVHFRQGV$IWHUWKHVHFRQGVDUHVXOWZLOOEHGLVSOD\HGLJQRUHWKLVUHVXOW ZERO METER Press the ZERO/ON button. The cursor will move across the display, followed by 0.00 PPM. Sample is ready for testing. DIP STRIP AND PRESS “READ” Dip the eXact® Strip Micro FE (TPTZ), Part No. 486631 into the CELL and immediately press READ. This starts the 20 SECOND countdown timer. During this time, move the strip in a gentle back and forth motion. Remove and discard the strip after “1” on the display disappears. The meter will DXWRPDWLFDOO\FRXQWXSIRUVHFRQGVThe cursor will move across the display, informing you that it is about to measure the sample. Record result displayed (this result is automatically stored in FE7). NOTE: Reducer will reduce Iron and the Iron will react with TPTZ to form a blue color. HR 1 2 3 4 5 6 High Range Chlorine Test Procedure HR8 REMOVE STRIP Remove one (1) eXact® Strip Micro HR, Part No. 486672 from the bottle before beginning the test. Set the strip in a dry, convenient place and recap the bottle immediately. TURN METER ON Press the ZERO/ON button to power the meter on; the display will show all annunciators, then the current MENU selection, followed by the last reading. SELECT TEST: HR8 Press and re-press the MENU button until the display shows the parameter HR8. FILL METER WITH SAMPLE Rinse the CELL at least 3 times with the water sample you will be testing - rinsing minimizes the potential IRUFURVVFRQWDPLQDWLRQIURPDSUHYLRXVWHVW)LQDOO\¿OOFHOOWRFDSDFLW\POZLWKWKHZDWHUVDPSOH ZERO METER* Press the ZERO/ON button. The cursor will move across the display, followed by 0.0 PPM. The sample is ready for testing. DIP STRIP - (read carefully and follow procedure closely) Dip the eXact® Strip Micro HR, Part No. 486672 into the CELL and immediately press READ. This starts the 20 SECOND countdown timer. During this time move the strip in a gentle back and forth motion. Remove and discard the strip after “1” on the display disappears*. The display will immediately start counting up from 1 to 120 (this extra time allows more thorough color development). At 120 sec, the cursor will move across the display while the meter prepares to measure the sample. Record result displayed (this result is automatically stored in HR8). After testing is completed, rinse cell immediately with brush and water. *Note: Use a 10 second dip time if water temperature is above 113°F / 40°C. INTERFERENCES: Oxidizers such as Chloramine, Chlorine Dioxide, Bromine, Iodine, Ozone, Bromamines, and Permanganate will give false positive readings. *NOTE: When testing outdoors (sunlight), for best accuracy, use the Mixing Cap/Cell Cover when Zeroing and Reading the sample. 9 eXact® Micro 7+ Tips For Best Accuracy 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. Become familiar with the meter and the different tests by reading the instructions carefully. The Free Chlorine, Combined Chlorine, and Total Chlorine reagents are compliant for meeting USEPA (4500-Cl G); ISO 7393/2; and German DIN 38408 G4-2 requirements. Observe the dip time (as required for the test) for accurate results. 7HVWLPPHGLDWHO\DIWHU¿OOLQJWKHCELL with water sample when testing for oxidizers such as Chlorine and Bromine (Ozone can be measured in CL3 MENU). Be sure the CELL LV¿OOHGWRFDSDFLW\POXQOHVVPHQWLRQHGLQWKHSURFHGXUH Rinse the CELL with clean water immediately after completing each test. Some reagents may stain the CELL if not rinsed shortly after use. It is recommended, after these tests, to use the Cell Cleaning Brush with water to clean the CELL. Just before testing, rinse the sample CELL with the sample water several times to get a representative sample. (Use deionized or distilled water for rinsing if you have a limited amount of sample). Store the meter and all test materials out of direct sunlight and away from chemical storage areas. Minimize exposure of meter and test reagents to heat above 38°C (100°F). Dry the outside of the meter when testing is complete or before storage of the meter. When running a DPD-1 Free Chlorine test AFTER a Total Chlorine DPD-3, a Total Chlorine DPD-4, or a HR Chlorine test, rinsing is very important to remove residual KI, which may interfere. Each eXact® Strip Micro is valid for ONLY one test. Discard strip after single use in regular refuse that is inaccessible to children and pets. Each bottle of eXact® Strip Micro contains the quantity of strips notated on the bottle. Due to the VWULSVOLWWLQJSURFHVV\RXPD\¿QGRQHRUWZRVWULSVWKDWDUHQRWLFHDEO\VPDOOHURUODUJHULQZLGWK than the normal strips in the bottle. These should be discarded. Using these strips may give unreliable results. Each table supplied has a unique revision number located in the bottom right corner of the table. It is recommended that you visit www.sensafe.com at least every 6 months to check for any updated revisions. The eXact® Micro 7+ Meter is not compatible for use with DPD-1, DPD-3, and DPD-4 powder pillows, tablets, and liquids available from other manufacturers. Accurate results can only be guaranteed by using genuine eXact® Micro strips or reagents (reorder information on page 19). Our lab testing with the Micro 7+ meter has shown that zeroing and measuring of the sample normally does not require any cell cover for accurate results, except in sunlight. To obtain optimal accuracy when testing with the meter outdoors (sunlight), use the Mixing Cap/Cell Cover when zeroing and reading the sample. Remove batteries when meter is not used for more than a month (Warranty Requirement). It is recommended that Pool and Spa samples for oxidizers (such as Chlorine) be taken 18 inches below the surface as follows: submerge meter with open cell facing down 18 inches, and then turn PHWHUXSULJKWDWWKDWGHSWKWR¿OOWKHFHOO5HPRYHPHWHUIURPZDWHUZLWKWKHVDPSOHIRUWHVWLQJ When there is a question about the quality of a ReagentStrip™, your test method, or the photometer you are using, then it is recommended to test the SYSTEM (reagent, you, and photometer) by using the appropriate READY SNAP™ solution. Follow the procedure for the test you are running. If you get the acceptible result using the READY SNAP™VROXWLRQWKHQ\RXFDQEHFRQ¿GHQWWKDWWKHUHDJHQW\RXDQGWKHSKRWRPHWHUDUHZRUNLQJ as a SYSTEM correctly. ™ Assigned Value for READY SNAP 3 (lot 505) Solution Parameter Free Chlorine Desired Acceptable Value Value (ppm) (ppm) 1.52 1.46 - 1.59 56;,!=HS\LZYLÅLJ[J\YYLU[JVUJLU[YH[PVUZHZ MV\UKH[[PTLVMTHU\MHJ[\YLHUKTH`JOHUNL ^P[OJVUZLJ\[P]LSV[Z 10 R020713 eXact® Micro 7+ Meter Messages The following are some common messages that may be displayed, including error messages. LCD Message Description HI In READ mode: test sample concentration is above WKHPHDVXUHPHQWUDQJHWHVWVSHFL¿F LO In READ mode: test sample concentration is below WKHPHDVXUHPHQWUDQJHWHVWVSHFL¿F LO In ZERO mode: sample absorbance (due to a cloudy or colored sample or a dirty cell) is too high to zero, the meter will read “LO”. ER ([FHVVLYHVWUD\OLJKWGHWHFWHG1RUPDOO\WKLV does not occur, even when testing in sunlight. TR9 &/ Low battery indication. Quality control of meter used by ITS. Clear memory. Contact ITS for more info. Corrective Action Dilute and retest. Sample value is below measurement range. 'LOXWHVDPSOH¿OWHUVDPSOHRUFOHDQFHOO2QHRI these options should remedy the problem. Place the LIGHT BLOCKING CAP over the CELL for zeroing and for reading result. Moving WRDVKDGHGDUHDFDQDOVR¿[WKLVSUREOHP Replace the batteries. Unscrew and rescrew battery cover to reset. Unscrew and rescrew battery cover to reset. About The Built-In Cell The built-in CELLLVWUDQVSDUHQWSODVWLFDQGZKHQ¿OOHGWRWKHWRSFRQWDLQVPO7KHVWXUG\CELL design will last for over 20,000 readings. Scratches on the CELL will not interfere or compromise the accuracy of WKHUHDGLQJVEHFDXVHRILWV¿[HGSRVLWLRQ)RUEHVWDFFXUDF\ULQVHFHOOZLWKFOHDQZDWHULPPHGLDWHO\DIWHU a test is completed. Do not use solvents, such as acetone, to clean the cell. When the CELL becomes stained or cloudy from repeated testing, or when the meter does not blank when you press the ZERO/ON button, the cell needs to be cleaned. Clean as follows)LOOFHOOZLWKFOHDQZDWHUDQGPRYHWKHCell cleaning brush up-and-down and back-and-forth along the walls of the cell. Afterwards, rinse the cell and the meter is ready for use again. Cleaning the cell regularly is especially recommended after you run a test that is using turbidity or precipitation chemistry for analysis (Calcium Hardness and Cyanuric Acid). To Install/Replace “AAA” Batteries: 1. Unscrew the O-ring sealed battery cover counter-clockwise. Use proper sized pliers if necessary. Do not disturb the sealing O-ring. Batteries are not included. 5HPRYHWKHXVHGEDWWHULHVDQGLQVWDOOQHZ$$$EDWWHULHVIROORZLQJWKHGLDJUDPIRU correct polarity (see diagram). We recommend high quality AAA alkaline batteries be used. 5HSODFHWKHEDWWHU\FRYHU%HVXUHWRWLJKWHQWKHFRYHUVHFXUHO\GRQRWRYHUWLJKWHQ7KLVLV necessary for meter to be waterproof. 'LVSRVHRIWKHXVHGEDWWHULHVLQDFFRUGDQFHZLWK\RXU local regulations. 3UHVV=(5221EXWWRQWRFRQ¿UPWKHPHWHUWXUQVRQ The meter is now ready for operation. 7. Meter will not work if battery orientation is incorrect. TOP VIEW eXact® Photometer 2-Year Limited Warranty Registration of your eXact® photometer must be received within 30 days from date of purchase to activate the warranty. The eXact® photometer is warranted to be free from defects in materials and workmanship for a period of two (2) years from the date of purchase by the customer. ITS will repair or replace any part of the product which is deemed to be faulty or otherwise defective. The non-transferable warranty does not cover product damage caused by abuse (such as crushing a tablet in the cell) or LPSURSHUXVH,IWKHPHWHULVIDXOW\RURWKHUZLVHGHIHFWLYHFRQWDFW,76E\SKRQH([W or email (its@sensafe.com) to describe the problem and obtain a return authorization form before returning the photometer to ITS. Damage caused by improper packing of the photometer for return shipment to ITS will not be covered by the warranty. Customer is responsible for shipping charges to ,76KRZHYHU,76SD\VUHWXUQSRVWDJH$PD[LPXPSURFHVVLQJIHHRIZLOOEHFKDUJHGIRUUHSDLURU replacement of non-registered photometers and damages not covered by this warranty. Registration is DYDLODEOHRYHUWKHSKRQH([WRURQOLQHDW http://www.sensafe.com/micro7+/warranty/3HUVRQDOGDWDLVNHSWFRQ¿GHQWLDO 11 eXact® Strip Micro DPD-1 Accuracy Free Chlorine results are compared using the eXact® Strip Micro CL (DPD-1) with the eXact® Micro 7+ Meter in Menu CL1 and Hach® DR890 Colorimeter in Program 9 and Program 12 using Hach® powder pillows. 0.00 0.41 0.92 0.79 1.28 2.70 3.20 4.45 5.30 Meter Menu Micro 7+ CL1 DR890 Program 9 Program 12 6.0 Micro 7+ 0 0.39 0.96 0.73 1.32 2.73 3.22 4.75 5.53 5.5 DPD Free Chlorine study January 21, 2011 Hach vs ITS y = 1.0402x R2 = 0.9989 Linear (Hach vs ITS) 5.0 4.5 ITS Free Chlorine, ppm DR890 Range (PPM) Resolution 0 to 5.99 6.0 to 11.0 0.00 to 2.20 0.0 to 11.0 0.01 0.1 0.01 0.1 Hach® is a registered trademark of Danaher Corporation 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0 0.0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 Hach Free Chlorine, ppm eXact® Strip Micro 7+ Reagent Reorder Information eXact® Strip Micro (4mL ) Reagent SpeciÀcations - For use with eXact® Micro 7+, Part no. 486691 No. PARAMETER eXact® Micro Carrying Case w/ foam* Dilution Kit Reference Standard Mini Dilution Kit II 1 Alkalinity, Total (as CaCO3)* 2 Bromine* 3 Total Hardness (as CaCO3)* 4 Chlorine, Free* Chlorine, Free 5 Chlorine, High Range* 6 Chlorine, Combined* ** Chlorine, Combined* ** 7 Chlorine, Total* Chlorine, Total 8 Copper (as Cu+2)* 9 Ozone 10 Permanganate 11 pH* 12 Total Iron, TPTZ (as Fe+2/Fe+3)* PART NO. 486001 487200 486602 487202 486641 486637 486673 486637 484051 486672 486638 484053 486670 484054 486632 486670 486637 486639 486650 # OF TESTS DETECTION RANGE N/A N/A 15 N/A 100 100 50 100 100 Foils 50 100 100 Foils 100 100 Foils 50 100 100 100 50 *Included in the Standard Kit (486691-K) &RPELQHG&KORULQH7HVWUHTXLUHV)UHH&KORULQHWREHUXQ¿UVW N/A N/A N/A N/A 5 - 200 ppm 0 - 14 ppm 1 - 200 ppm 0 - 11 ppm 0 - 11 ppm 1 - 300 ppm 0 - 11 ppm 0 - 11 ppm 0 - 11 ppm 0 - 11 ppm 0.04 - 8 ppm 0 - 11 ppm 0 - 11 ppm 6.2 - 8.4 pH 0.03 - 5 ppm Contact Information 12 CHEMISTRY N/A N/A N/A N/A Alizarin Red S + Citrate DPD Phthalein Purple DPD DPD KI + Buffer Kl KI DPD + Kl DPD + KI Biquinoline DPD + Kl DPD Phenol Red TPTZ + PP