Second Quarter Groundwater Monitoring Report and Attenuation Analysis

Second Quarter Groundwater Monitoring Report and Attenuation Analysis
ARCADIS U.S., Inc.
1114 Benfield Boulevard
Suite A
Millersville
Maryland 21108
Ms. Jeannette DeBartolomeo
Oil Control Program
Maryland Department of Environment
1800 Washington Boulevard
Baltimore, MD 21230
Tel 410.987.0032
Fax 410.987.4392
www.arcadis-us.com
ENVIRONMENT
Subject:
Second Quarter 2015 Groundwater Monitoring Report and Attenuation Analysis
Former Exxon Facility #14489
285 Old Bayview Road
North East, Cecil County, Maryland
MDE Case No. 1986-1205-CE
Dear Ms. DeBartolomeo:
25 August 2015
Contact:
ARCADIS U.S. (ARCADIS), on behalf of ExxonMobil Environmental Services
Company (EMES) on behalf ExxonMobil Corporation (ExxonMobil), is pleased to
submit the Groundwater Monitoring Report (GMR) for activities performed during
Second Quarter 2015 at the Inactive Exxon Station #14489, located at 285 Old
Bayview Road, North East, Maryland.
Please contact Hillary Goodell of ARCADIS at (919) 415-2268 if you have any
questions regarding the information contained in this report.
Sincerely,
ARCADIS U.S., Inc.
Sarah Matteson
Geologist II
Date:
William R. Kahl, PG
Project Geologist
Copies:
Mr. Mike Meola, ExxonMobil
Imagine the result
g:\prjcts\exxonmobil retail\md-14489 northeast\reports\2015 q2 gmr\md14489 2015q2 gmr.doc
Hillary Goodell
Associate Project Manager
Hillary Goodell
Phone:
919-415-2268
Email:
[email protected]
Our ref:
B0085851.0010
Ms. Jeannette DeBartolomeo
25 August 2015
Second Quarter 2015 Groundwater Monitoring Report
Former Exxon Facility #14489, 285 Old Bayview Road, North East, MD
Regulatory Information
Regulatory Agency:
MDE Case Number:
Agency Contact:
Current Case Status:
Reporting Period:
Last Report:
Maryland Department of the Environment
(MDE)
1986-1205-CE
Ms. Jeannette DeBartolomeo
Quarterly groundwater monitoring and
sampling
1 April 2015 through 30 June 2015
First Quarter 2015 Groundwater Monitoring
Report, April 2015
General Site Information
ExxonMobil Contact:
Consultant Contact:
Facility Status:
Area Property Use:
Monitoring Wells:
Injection Wells:
Site Geology:
Mr. Mike Meola
Ms. Hillary Goodell
Former retail service station currently
operated as an automotive repair facility
See local area map (Figure 1)
MW-1A, MW-2A, MW-3A, MW-5A, MW-8, and
MW-10 through MW-16 (Figure 2)
INJ-1, INJ-2, and INJ-3 (Figure 2)
Micaceous clay and silt with sand and
gravel
Activities Completed this Period
25 June 2015 – Groundwater Gauging and Sampling
Wells Gauged and Sampled:
MW-1A, MW-2A, MW-3A, MW-5A, MW-8,
Well Gauged Only:
MW-10, MW-11, MW-12, MW-13, MW-14,
MW-15, and MW-16.
INJ-1, INJ-2, and INJ-3
Liquid Phase Hydrocarbon:
None Detected
Minimum/Maximum Depth to Water: 2.09 feet (MW-3A) / 7.31 feet (MW-12)
Groundwater Flow Direction:
Southwest
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Ms. Jeannette DeBartolomeo
25 August 2015
Groundwater samples were collected on 25 June 2015 and submitted to
TestAmerica Laboratories of Nashville, Tennessee for analysis of benzene, toluene,
ethylbenzene, and xylenes (BTEX), naphthalene, and fuel oxygenates using
Environmental Protection Agency (EPA) Method 8260B and for biogeochemical
parameters including sulfate (Method 9056A), nitrate (Method 353.2), and dissolved
and total iron (Method 6010B). Monitoring well gauging and sampling data are
summarized on Table 1 and depicted on Figure 3. No liquid phase hydrocarbon
(LPH) was detected during this reporting period. Quality Assurance/Quality Control
(QA/QC) samples collected included a duplicate sample (collected from MW-1A),
daily rinsate blanks, and trip blanks. The TestAmerica laboratory groundwater
analytical reports are attached as Appendix A.
25 June 2015 – Potable Well Sampling
The potable well and POET system at 259 Old Bayview Road and the potable well at
261 Old Bayview Road were sampled on 25 June 2015. Results are summarized on
Table 2 and were submitted to the property owners under separate cover.
Groundwater Sampling Results
Benzene, toluene, ethylbenzene, methyl tertiary butyl ether (MTBE), and
naphthalene were detected at concentrations exceeding MDE Groundwater (GW)
Clean-up Standards at one or more wells:

Benzene was detected at concentrations exceeding the MDE GW standard (5
µg/L) in three samples (MW-1A, MW-2A, and MW-5A) with a maximum
concentration of 147 µg/L in the sample collected from MW-2A.

Toluene was detected at concentrations exceeding the MDE GW standard
(1,000 µg/L) in the sample collected from MW-1A with a concentration of 1,500
µg/L.

Ethylbenzene was detected at concentrations exceeding the MDE GW standard
(700 µg/L) in three samples (MW-1A, MW-2A and MW-5A) with a maximum
concentration of 991 µg/L in the sample collected from MW-2A.

MTBE was detected at concentrations exceeding the MDE GW standard (20
µg/L) in the sample collected from MW-2A with a concentration of 82.0 µg/L.
Page:
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Ms. Jeannette DeBartolomeo
25 August 2015

Naphthalene was detected at concentrations exceeding the MDE GW standard
(0.65 µg/L) in four samples (MW-1A, MW 2A, MW-5A, and MW-11) with a
maximum concentration of 196 µg/L in the sample collected from MW-2A.
Activities Planned for Next Period (Third Quarter 2015)
Activities proposed for the Third Quarter 2015 include quarterly groundwater gauging
and sampling. Groundwater samples will be collected from wells MW-1A, MW-2A,
MW-3A, MW-5A, MW-8, and MW-10 through MW-16 and analyzed for full list volatile
organic compounds (VOCs) and fuel oxygenates using Environmental Protection
Agency (EPA) Method 8260B, sulfate (Method 9056A), nitrate (Method 353.2), and
dissolved and total iron (Method 6010B). Field parameters, such as dissolved oxygen
and pH, will be recorded as part of the standard sampling protocol. Potable wells will
continue to be sampled at 259 and 261 Old Bayview Road properties.
Tables and Figures
Table 1: Groundwater Monitoring and Analytical Data
Table 2: Potable Water Monitoring and Analytical Data
Figure 1: Local Area Map
Figure 2: Site Map
Figure 3: Groundwater Elevation Contours and Analytical Data (25 June 2015)
Appendices
Appendix A: TestAmerica Laboratory Analytical Reports (9 -13 July 2015)
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4/4
Tables
Table 1
Groundwater Monitoring and Analytical Data
Exxon Service Station #14489
285 Old Bayview Drive
North East, Maryland
Gauging Data
Analytical Data
Well ID
Date
Top of
Casing
Elevation
(feet)
Depth
to
Water
(feet)
Depth to
Hydrocarbon
(feet)
Hydrocarbon
Thickness
(feet)
Corrected
GW
Elevation
(feet)
Benzene
(µg/L)
Toluene
(µg/L)
5
MW-1A
6/1/2005
97.65
5.23
ND
ND
92.42
560
12/7/2005
97.65
6.77
ND
ND
90.88
5/24/2006
97.65
6.82
ND
ND
11/7/2006
97.65
5.38
ND
6/21/2007
97.65
6.15
12/11/2007
97.65
3/24/2008
Total
Xylenes
(µg/L)
TAME
(µg/L)
Naphthalene
(µg/L)
Sulfate
(mg/L)
Total
Metals
(mg/L)
Nitrate / Nitrite
(mg/L)
pH (s.u.)
Conductivity
(mS/cm)
Temperature (°C)
DO (mg/L)
1,000
700
10,000
--
20
--
--
5,770
2,360
8,970
17,660
156
<500
NA
--
--
NA
NA
0.65
--
2,600
NA
NS
NS
--
--
--
--
--
--
--
NS
NS
--
--
--
--
252
2,410
2,560
7,500
12,722
149
<500
NA
NA
NA
NA
NS
NS
--
NS
NS
--
--
--
--
90.83
97.7
1,260
1,720
4,870
7,948
114
<500
NA
NA
NA
NA
NS
--
NS
NS
NS
--
--
--
--
ND
92.27
116
703
1,130
2,880
4,829
112
92.2 J
NA
NA
NA
NA
--
NS
NS
NS
NS
--
--
--
--
ND
ND
91.50
145
1,750
1,020
3,220
6,135
53.3
<250
NA
NA
NA
--
NA
NS
NS
NS
NS
--
--
--
--
7.02
ND
ND
90.63
212
3,730
2,380
8,180
14,502
133
<500
NA
NA
--
NA
NA
NS
NS
NS
NS
--
--
--
--
97.65
4.94
ND
ND
92.71
216
3,280
2,270
7,550
13,316
510
<630
NA
--
NA
NA
NA
NS
NS
NS
NS
--
--
--
--
6/29/2008
97.65
6.10
ND
ND
91.55
201
2,970
1,520
5,380
10,071
593
<500
--
<100
<100
<100
378
NS
NS
NS
NS
--
--
--
--
8/14/2008
97.65
7.12
ND
ND
90.53
151
2,300
1,410
4,460
8,321
561
--
<500
<100
<100
59.2 J
345
NS
NS
NS
NS
--
--
--
--
11/20/2008
97.65
7.12
ND
ND
90.53
150
2,330
1,860
6,030
10,370
--
398
<630
<130
<130
58.9 J
497
NS
NS
NS
NS
--
--
--
--
2/11/2009
97.65
5.35
ND
ND
92.30
185
2,720
1,510
5,440
--
9,855
307
<500
<100
<100
<100
375
NS
NS
NS
NS
--
--
--
--
4/21/2009
97.65
5.08
ND
ND
92.57
148
2,700
1,790
--
6,230
10,868
269
<630
<130
<130
44.0 J
402
NS
NS
NS
NS
--
--
--
--
7/31/2009
97.65
6.35
ND
ND
91.30
101
1,460
--
730
2,760
5,051
151
<250
<50
<50
20.1 J
235
NS
NS
NS
NS
--
--
--
--
10/13/2009
97.65
4.80
ND
ND
92.85
NS
--
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
10/27/2009
97.65
5.25
ND
ND
92.40
--
62.8
873
1,080
2,830
4,846
143
<250
<50
<50
17.2 J
263
NS
NS
NS
NS
--
--
--
--
1/12/2010
97.65
4.57
ND
ND
--
93.08
162
2,430
1,350
4,170
8,112
139
<250
<50
<50
24.0 J
355
NS
NS
NS
NS
--
--
--
--
4/21/2010
97.65
4.21
ND
--
ND
93.44
204
3,100
1,610
5,510
10,424
117
<630
<130
<130
<130
369
NS
NS
NS
NS
--
--
--
--
7/22/2010
97.65
6.74
--
ND
ND
90.91
197
2,900
1,340
4,780
9,217
108
<630
<130
<130
31.4 J
225
NS
NS
NS
NS
--
--
--
--
11/23/2010
97.65
--
6.55
ND
ND
91.10
51.2
1,190
1,100
3,530
5,871
54.6
<130
<25
<25
9.0 J
277
NS
NS
NS
NS
--
--
--
--
3/2/2011
--
97.65
4.89
ND
ND
92.76
60.2
1,220
1,120
4,440
6,840
33.8
40.4
<1
<1
<1
218
NS
NS
NS
NS
--
--
--
--
--
5/19/2011
97.65
4.82
ND
ND
92.83
101
1,340
584
2,140
4,165
28.2
<20
<1
<1
7.47
244
NS
NS
NS
NS
--
--
--
--
--
7/12/2011
97.65
6.48
ND
ND
91.17
117
2,450
1,140
3,970
7,677
24.4
<20
<1
<1
<1
234
NS
NS
NS
NS
--
--
--
--
--
10/24/2011
97.65
5.41
ND
ND
92.24
57.6
1,610
1,030
3,660
6,357.6
21
19.1
<1
<1
4.27
198
NS
NS
NS
NS
--
--
--
--
--
2/8/2012
97.65
5.03
ND
ND
92.62
67.5
1,490
956
3,210
5,724
13.8
<10
<1
<1
<1
187
NS
NS
NS
NS
--
--
--
--
--
5/22/2012
97.65
6.83
ND
ND
90.82
76.7
1,910
976
4,140
7,103
13.6
<50
<5
<5
<5
155
NS
NS
NS
NS
--
--
--
--
--
2,180
[2,210]
1,230
1,080
[1,030]
1,010
3,950
[3,700]
7,276
[7,004]
17.7 [<1]
<10 [<10]
<2 [<2]
<1 [<1]
<1 [<1]
182 [192]
NS
NS
NS
NS
--
--
--
--
--
3,860
6,141.9
29.1
11.8
<2
<1
5.72
249
NS
NS
NS
NS
--
--
--
--
--
1,620
2,130
[1,950]
1,880
[1,940]
1,890
[1,870]
1,060
[1,120]
2,060
[1,760]
1,460
[1,580]
1,340
1,290
[1,210]
973
[1,010]
4,290
4,820
[4,510]
3,340
[3,400]
4,010
[4,070]
2,740
[2,810]
4,050
[3,430]
3,300
[3,460]
1,400
[1,520]
2,450
[2,520]
7,313
8,321.3
[7,747.8]
6,285.3
[6,441.1]
6,915.2
[6,955.6]
4,536.6
[4,715.6]
7,153.8
[6,227.6]
5,683.5
[5,973]
2,170.7
[2,367.3]
3,743.4
[3,853.9]
<1
<10
<2
<1
<1
256
NS
NS
NS
NS
6.42
0.236
12.22
0.69
-38
6.88 [<1]
<10 [<10]
<2 [<2]
<1 [<1]
<1 [2.59]
262 [255]
NS
NS
NS
NS
6.15
0.226
14.17
0.25
-27.2
6.25 [6.21] <10 [<10]
<2 [<2]
<1 [<1]
19.3 [<1]
276 [279]
NS
NS
NS
NS
5.85
0.232
17.26
1.49
81.9
7.44 [7.74] <10 [<10]
<2 [<2]
<1 [<1]
<1 [<1]
251 [254]
NS
NS
NS
NS
5.48
0.239
19.48
0.82
30.4
4.70 [4.58] 10.4 [14.3]
<2 [<2]
<1 [<1]
1.61 [1.30] 161 [179]
NS
NS
NS
NS
6.26
0.228
13.22
4.08
-54.2
<20 [<20]
<10 [<10]
<10 [<10]
182 [218]
NS
NS
NS
NS
6.00
0.216
14.73
0.33
-10.6
<20 [<20]
<10 [<10]
<10 [<10]
378 [264]
<1 [<1]
5.85 [5.35]
4.19 [4.30]
<0.1 [<0.1]
6.06
0.172
18.81
0.28
-139.1
3,180
[3,240]
5,447.2
[5,528.4]
8/14/2012
97.65
8.31
ND
ND
89.34
66 [64]
10/4/2012
97.65
8.98
ND
ND
88.67
41.9
2/22/2013
97.65
5.50
ND
ND
92.15
63.2
5/1/2013
97.65
5.21
ND
ND
92.44
81.3 [77.8]
8/6/2013
97.65
4.68
ND
ND
92.97
92.3 [91.1]
10/3/2013
97.65
5.85
ND
ND
91.80
90.2 [90.6]
3/6/2014
97.65
4.25
ND
ND
93.40
47.6 [54.6]
925 [925]
689 [731]
6/12/2014
97.65
4.54
ND
ND
93.11
69.8 [70.6]
9/19/2014
97.65
7.27
ND
ND
90.38
49.5 [51.0]
11/13/2014
97.65
6.09
ND
ND
91.56
10.7 [14.3] 405 [459]
355 [374]
3/25/2015
97.65
4.38
ND
ND
93.27
33.4 [32.9] 743 [762]
517 [539]
6/25/2015
97.65
4.41
ND
ND
93.24
53.2 [54.4]
1,500
[1,510]
974 [967]
874 [882]
714 [724]
Total
BTEX
(µg/L)
Field Parameters
Ethylbenzene
(µg/L)
MTBE
(µg/L)
<10 [<10]
<10 [<10]
TBA
(µg/L)
<100
[<100]
<100
[<100]
DIPE
(µg/L)
ETBE
(µg/L)
Dissolved
Metals
(mg/L)
ORP (mV) Comments
<1 [<1]
<10 [<10]
<2 [<2]
<1 [<1]
<1 [<1]
54.0 [61.6]
<1 [<1]
4.41 [4.47]
3.63 [3.58]
<0.1 [<0.1]
6.10
0.227
19.22
3.04
-17.6
<1 [2.34]
<10 [<10]
<2 [<2]
<1 [<1]
<1 [<1]
133 [133]
<1 [<1]
9.47 [8.89] 1.11 [0.884]
<0.1 [<0.1]
6.03
0.247
11.98
1.06
-61.3
2.31 [2.35] 14.3 [12.6]
<2 [<2]
<1 [<1]
<1 [<1]
153 [157]
<1 [<1]
4.94 [5.43]
<0.1 [<0.1]
6.04
0.263
17.09
1.19
-44.0
page 1 of 13
3.24 [2.43]
Table 1
Groundwater Monitoring and Analytical Data
Exxon Service Station #14489
285 Old Bayview Drive
North East, Maryland
Gauging Data
Analytical Data
Well ID
Date
Top of
Casing
Elevation
(feet)
Depth
to
Water
(feet)
Depth to
Hydrocarbon
(feet)
Hydrocarbon
Thickness
(feet)
Corrected
GW
Elevation
(feet)
Benzene
(µg/L)
Toluene
(µg/L)
5
MW-2A
6/1/2005
97.10
4.74
ND
ND
92.36
1,740
12/7/2005
97.10
5.65
ND
ND
91.45
5/24/2006
97.10
5.71
ND
ND
11/7/2006
97.10
4.35
ND
6/21/2007
97.10
5.26
12/11/2007
97.10
3/24/2008
Total
BTEX
(µg/L)
Field Parameters
Ethylbenzene
(µg/L)
Total
Xylenes
(µg/L)
MTBE
(µg/L)
TBA
(µg/L)
DIPE
(µg/L)
1,000
700
10,000
--
20
--
--
595
2,590
9,200
14,125
829
<500
NA
1,580
2,440
2,660
9,530
16,210
670
<630
NA
91.39
1,570
4,950
2,790
9,990
19,300
599
<630
ND
92.75
964
3,090
2,550
8,730
15,334
413
ND
ND
91.84
456
788
2,290
7,470
11,004
5.77
ND
ND
91.33
216
157
569
1,830
97.10
4.73
ND
ND
92.37
747
529
1,900
6/29/2008
97.10
5.66
ND
ND
91.44
379
4,610
8/14/2008
97.10
5.57
ND
ND
91.53
489
11/20/2008
97.10
5.64
5.63
0.01
91.47
2/11/2009
97.10
4.90
ND
ND
4/21/2009
97.10
1.82
ND
7/31/2009
97.10
5.37
10/13/2009
97.10
10/27/2009
ETBE
(µg/L)
TAME
(µg/L)
Naphthalene
(µg/L)
Sulfate
Total
Metals
--
--
NA
NA
0.65
--
2,600
NA
NS
NS
NA
NA
NA
NS
NS
NA
NA
NA
NA
NS
189 J
NA
NA
NA
NA
198
<250
NA
NA
NA
2,772
86.4
30.0 J
NA
NA
3,920
7,096
568
256 J
NA
2,160
8,620
15,769
457
<630
4,240
3,310
8,760
16,799
531
817
308
1,770
5,450
8,345
92.20
567
1,220
1,330
4,140
ND
95.28
452
4,520
1,860
ND
ND
91.73
191
1,830
3.93
ND
ND
93.17
NS
97.10
4.51
ND
ND
92.59
1/12/2010
97.10
4.36
ND
ND
4/21/2010
97.10
4.04
ND
7/22/2010
97.10
5.10
11/23/2010
97.10
3/2/2011
Dissolved
Metals
Nitrate/Nitrite
pH (s.u.)
Conductivity
(mS/cm)
Temperature (°C)
DO (mg/L)
ORP (mV) Comments
--
--
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
--
--
--
--
--
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NA
NS
NS
NS
NS
--
--
--
--
--
<130
<130
<130
462
NS
NS
NS
NS
--
--
--
--
--
<630
<130
<130
46.4 J
652
NS
NS
NS
NS
--
--
--
--
--
624
<250
<50
<50
55.6
405
NS
NS
NS
NS
--
--
--
--
--
7,257
680
215 J
<50
<50
51.6
306
NS
NS
NS
NS
--
--
--
--
--
7,870
14,702
516
<630
<130
<130
64.0 J
299
NS
NS
NS
NS
--
--
--
--
--
1,270
4,250
7,541
341
<250
<50
<50
38.1 J
316
NS
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
266
656
2,530
7,620
11,072
371
<500
<100
<100
48.5 J
360
NS
NS
NS
NS
--
--
--
--
--
92.74
699
231
2,340
4,360
7,630
532
<500
<100
<100
55.2 J
402
NS
NS
NS
NS
--
--
--
--
--
ND
93.06
858
1,070
1,720
2,690
6,338
538
156 J
<50
<50
43.4 J
325
NS
NS
NS
NS
--
--
--
--
--
ND
ND
92.00
544
865
1,590
5,010
8,009
430
<250
<50
<50
54.8
262
NS
NS
NS
NS
--
--
--
--
--
5.51
ND
ND
91.59
220
367
2,140
3,980
5,807
169
<130
<25
<25
20.2
223
NS
NS
NS
NS
--
--
--
--
--
97.10
4.20
ND
ND
92.90
147
702
1,290
4,920
7,059
151
<20
<1
<1
18.4
232
NS
NS
NS
NS
--
--
--
--
--
5/19/2011
97.10
4.40
ND
ND
92.70
373
1,530
1,300
4,050
7,253
274
<20
1.07
<1
23.8
222
NS
NS
NS
NS
--
--
--
--
--
7/12/2011
97.10
5.45
ND
ND
91.65
316
850
1,460
4,690
7,316
207
<200
<10
<10
16.4
243
NS
NS
NS
NS
--
--
--
--
--
10/24/2011
97.10
4.30
ND
ND
92.80
309
466
1,240
4,070
6,085
171
38.8
<1
<1
16.6
200
NS
NS
NS
NS
--
--
--
--
--
2/8/2012
97.10
4.73
ND
ND
92.37
154
570
1,280
3,580
5,584
115
<10
<1
<1
10.4
201
NS
NS
NS
NS
--
--
--
--
--
5/22/2012
97.10
5.79
ND
ND
91.31
216
443
1,550
4,280
6,489
131
<50
<5
<5
11.9
197
NS
NS
NS
NS
--
--
--
--
--
8/14/2012
97.10
6.61
ND
ND
90.49
221
512
1,220
3,820
5,773
138
<10
<2
<1
13.5
252
NS
NS
NS
NS
--
--
--
--
--
10/4/2012
97.10
6.93
ND
ND
90.17
311
754
1,000
3,990
6,055
179
41.3
<2
<1
17.3
187
NS
NS
NS
NS
--
--
--
--
--
2/22/2013
97.10
4.58
ND
ND
92.52
128
858
1,350
3,930
6,266
73.4
<10
<2
<1
8.71
181
NS
NS
NS
NS
6.49
0.360
12.81
3.42
-49
5/1/2013
97.10
4.77
ND
ND
92.33
153
901
1,220
4,170
6,444
101
<10
<2
<1
10.3
199
NS
NS
NS
NS
6.49
0.328
14.52
0.29
-100.9
8/6/2013
97.10
4.18
ND
ND
92.92
199
651
918
2,510
4,278
117
<10
<2
<1
31.9
179
NS
NS
NS
NS
6.24
0.349
17.34
0.48
9.8
10/3/2013
97.10
4.86
ND
ND
92.24
259
1,080
1,210
4,380
6,929
133
<10
<2
<1
11.3
266
NS
NS
NS
NS
6.22
0.328
20.25
0.24
-63.4
-95.8
3/6/2014
97.10
3.96
ND
ND
93.14
124
372
1,160
2,830
4,486
73.6
22.2
<2
<1
7.44
280
NS
NS
NS
NS
6.71
0.334
11.24
4.37
6/12/2014
97.10
3.90
ND
ND
93.20
153
547
1,590
4,190
6,480
81.4
<100
<20
<10
<10
280
NS
NS
NS
NS
6.37
0.338
15.45
0.31
-66.5
9/19/2014
97.10
5.62
ND
ND
91.48
174
630
1,590
4,450
6,844
82.1
<100
<20
<10
<10
386
1.76
41.0
5.08
<0.1
6.33
0.319
20.17
0.70
-106.3
11/13/2014
97.10
5.16
ND
ND
91.94
163
297
977
2,670
4,107
90.8
21.4
<2
<1
7.78
128
<1
14.1
5.07
<0.1
6.46
0.369
18.97
3.17
-77.4
3/25/2015
97.10
4.10
ND
ND
93.00
117
387
1,420
2,870
4,794
56.2
<10
<2
<1
5.30
174
<1
9.94
1.08
<0.1
6.37
0.315
9.53
2.29
-37.4
6/25/2015
97.10
3.92
ND
ND
93.18
147
415
991
2,450
4,003
82.0
31.5
<2
<1
<1
196
9,990
11.6
1.46
<0.1
6.28
0.291
20.30
1.59
-52.3
page 2 of 13
Table 1
Groundwater Monitoring and Analytical Data
Exxon Service Station #14489
285 Old Bayview Drive
North East, Maryland
Gauging Data
Analytical Data
Date
Top of
Casing
Elevation
(feet)
Depth
to
Water
(feet)
Depth to
Hydrocarbon
(feet)
Hydrocarbon
Thickness
(feet)
Corrected
GW
Elevation
(feet)
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Total
Xylenes
(µg/L)
5
1,000
700
10,000
--
20
--
--
MW-3A
6/1/2005
96.99
2.71
ND
ND
94.28
6.7
18
31
108
163
19.8
<25
NA
12/7/2005
96.99
4.55
ND
ND
92.44
92.0
23.3
99.9
128
343
353
<25
NA
5/24/2006
96.99
2.72
ND
ND
94.27
<1
1.1
5.7
19
26
47.1
<25
11/7/2006
96.99
2.06
ND
ND
94.93
3.4
15.2
36.6
126
181
<1
6/21/2007
96.99
2.45
ND
ND
94.54
278
111
325
991
1,705
12/11/2007
96.99
2.25
ND
ND
94.74
<1
<1
<1
<1
3/24/2008
96.99
2.41
ND
ND
94.58
0.32 J
7.5
14.8
6/29/2008
96.99
NM
NM
NM
NM
NS
NS
8/14/2008
96.99
5.57
ND
ND
91.42
<1
<1
11/20/2008
96.99
2.21
ND
ND
94.78
<1
2/11/2009
96.99
2.75
ND
ND
94.24
28.0
4/21/2009
96.99
1.30
ND
ND
95.69
9.6
7/31/2009
96.99
2.83
ND
ND
94.16
10/13/2009
96.99
2.10
ND
ND
10/27/2009
96.99
1.90
ND
1/12/2010
96.99
2.45
4/21/2010
96.99
7/22/2010
MW-4
Total
BTEX
(µg/L)
Field Parameters
Well ID
MTBE
(µg/L)
TBA
(µg/L)
DIPE
(µg/L)
ETBE
(µg/L)
TAME
(µg/L)
Naphthalene
(µg/L)
Sulfate
Total
Metals
--
--
NA
NA
0.65
--
2,600
NA
NS
NS
NA
NA
NA
NS
NS
NA
NA
NA
NA
NS
<25
NA
NA
NA
NA
17900
<1,300
NA
NA
NA
BRL
23.2
<25
NA
NA
57
79.2 J
0.64 J
<25
NA
NS
NS
NS
NS
NS
<1
<1
BRL
3.7
<1
<1
<1
BRL
13.7
2.8
6
50
7.6
1.8
4
0.25 J
<1
<1
94.89
NS
NS
ND
95.09
<1
ND
ND
94.54
2.26
ND
ND
96.99
2.85
ND
11/23/2010
96.99
4.75
3/2/2011
96.99
5/19/2011
Nitrate/Nitrite
pH (s.u.)
Conductivity
(mS/cm)
Temperature (°C)
DO (mg/L)
--
--
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
--
--
--
--
--
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NA
NS
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
0.60 J
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
67.2
26.0
<5
<5
2.7 J
<5
NS
NS
NS
NS
--
--
--
--
--
23
37.2
21.2 J
<5
<5
1.2 J
<5
NS
NS
NS
NS
--
--
--
--
--
<1
0.25 J
1.4
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
<1
<1
<1
BRL
3.6
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
<1
<1
<1
<1
BRL
18.9
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
94.73
23.8
14.2
5.2
9
52
20.9
7.5 J
<5
<5
0.98 J
<5
NS
NS
NS
NS
--
--
--
--
--
ND
94.14
<1
<1
<1
<1
BRL
10.2
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
ND
ND
92.24
<1
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
2.14
ND
ND
94.85
<1
<1
<1
<3
BRL
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
96.99
2.53
ND
ND
94.46
<1
<1
<1
<3
BRL
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
7/12/2011
96.99
5.76
ND
ND
91.23
<1
<1
<1
<3
BRL
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
10/24/2011
96.99
2.35
ND
ND
94.64
<1
<1
<1
<3
BRL
<1
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
2/8/2012
96.99
2.71
ND
ND
94.28
<1
<1
<1
<3
BRL
<1
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
5/22/2012
96.99
3.30
ND
ND
93.69
<1 [<1]
<1 [<1]
<1 [<1]
<3 [<3]
BRL [BRL]
<1 [<1]
<10 [<10]
<1 [<1]
<1 [<1]
<1 [<1]
<5 [<5]
NS
NS
NS
NS
--
--
--
--
--
8/14/2012
96.99
7.62
ND
ND
89.37
<1
<1
<1
<3
BRL
8.07
<10
<2
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
10/4/2012
96.99
8.63
ND
ND
88.36
8.24
<1
<1
<3
8.24
33.4
14.1
<2
<1
1.12
<5
NS
NS
NS
NS
--
--
--
--
--
2/22/2013
96.99
2.48
ND
ND
94.51
1.31
<1
<1
<3
1.31
1.37
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.91
0.535
13.68
4.10
152
5/1/2013
96.99
4.36
ND
ND
92.63
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.79
0.437
14.45
2.39
125.8
8/6/2013
96.99
2.26
ND
ND
94.73
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.68
0.345
16.84
5.07
273.5
10/3/2013
96.99
2.72
ND
ND
94.27
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
4.96
0.309
18.66
0.45
24.7
3/6/2014
96.99
2.46
ND
ND
94.53
<1
<1
1.41
4.29
5.70
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
7.34
0.269
14.17
8.89
42.7
6/12/2014
96.99
2.42
ND
ND
94.57
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.59
0.351
15.14
4.28
56.5
9/19/2014
96.99
6.08
ND
ND
90.91
<1
<1
<1
<2
BRL
1.16
<10
<2
<1
<1
<5
38.4
0.855
<0.1
0.246
6.49
0.295
17.48
1.02
93.6
11/13/2014
96.99
2.53
ND
ND
94.46
<1
<1
2.49
7.05
9.54
<1
<10
<2
<1
<1
<5
43.6
0.217
<0.1
1.34
6.93
0.293
18.72
6.00
-13.7
3/25/2015
96.99
2.31
ND
ND
94.68
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
22.0
1.10
<0.1
1.20
7.04
0.357
11.53
7.77
205.9
6/25/2015
96.99
2.09
ND
ND
94.90
1.26
<1
<1
<3
1.26
1.75
<10
<2
<1
<1
<5
116
0.736
<0.1
0.722
6.78
0.537
18.47
3.81
99.5
6/1/2005
97.26
2.55
ND
ND
94.71
6.9
3.8
4.7
10.8
26.2
13.8
ND(25)
NA
NA
NA
NA
NS
NS
NS
NS
NS
NS
NS
NS
NS
12/7/2005
97.26
2.77
ND
ND
94.49
2.9
0.81 J
7.6
5.7
17.0 J
5.3
ND(25)
NA
NA
NA
NA
NS
NS
NS
NS
NS
NS
NS
NS
NS
5/24/2006
97.26
2.82
ND
ND
94.44
0.38 J
4.0
16.9
48.1
69.4 J
11.8
ND(25)
NA
NA
NA
NA
NS
NS
NS
NS
NS
NS
NS
NS
NS
11/7/2006
97.26
2.48
ND
ND
94.78
2.1
2.4
9.3
31.8
45.6
291
ND(25)
NA
NA
NA
NA
NS
NS
NS
NS
NS
NS
NS
NS
NS
6/21/2007
97.26
2.73
ND
ND
94.53
22.9
30.8
21.8
81.1
156.6
934
ND(100)
NA
NA
NA
NA
NS
NS
NS
NS
NS
NS
NS
NS
NS
12/11/2007
97.26
NM
NM
NM
NM
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
page 3 of 13
Dissolved
Metals
ORP (mV) Comments
Not accessible
Monitoring well destroyed.
Table 1
Groundwater Monitoring and Analytical Data
Exxon Service Station #14489
285 Old Bayview Drive
North East, Maryland
Gauging Data
Analytical Data
Well ID
Date
Top of
Casing
Elevation
(feet)
Depth
to
Water
(feet)
Depth to
Hydrocarbon
(feet)
Hydrocarbon
Thickness
(feet)
Corrected
GW
Elevation
(feet)
Benzene
(µg/L)
Toluene
(µg/L)
5
MW-5A
6/1/2005
95.02
2.40
ND
ND
92.62
132
12/7/2005
95.02
3.25
ND
ND
91.77
5/24/2006
95.02
3.72
ND
ND
11/7/2006
95.02
2.09
ND
6/21/2007
95.02
5.35
12/11/2007
95.02
3/24/2008
Total
Xylenes
(µg/L)
TAME
(µg/L)
Naphthalene
(µg/L)
Sulfate
Total
Metals
Nitrate/Nitrite
pH (s.u.)
Conductivity
(mS/cm)
Temperature (°C)
DO (mg/L)
1,000
700
10,000
--
20
--
--
1,360
1,670
7,270
10,432
<10
<250
NA
--
--
NA
NA
0.65
--
2,600
NA
NS
NS
--
--
--
--
--
--
--
NS
NS
--
--
--
--
58.2
230
1130
3,420
4,838
<10
<250
NA
NA
NA
NA
NS
NS
--
NS
NS
--
--
--
--
91.30
22.4
144
661
1,840
2,667
<5
<130
NA
NA
NA
NA
NS
--
NS
NS
NS
--
--
--
--
ND
92.93
136
868
1,370
4,780
7,154
<5
<130
NA
NA
NA
NA
--
NS
NS
NS
NS
--
--
--
--
ND
ND
89.67
49.7
460
929
2,750
4,189
<5
<130
NA
NA
NA
--
NA
NS
NS
NS
NS
--
--
--
--
3.63
ND
ND
91.39
20.1
62.3
831
2,520
3,433
<10
<250
NA
NA
--
NA
NA
NS
NS
NS
NS
--
--
--
--
95.02
2.60
ND
ND
92.42
56.2
306
855
1,940
3,157
<5
<130
NA
--
NA
NA
NA
NS
NS
NS
NS
--
--
--
--
6/29/2008
95.02
4.04
ND
ND
90.98
38.5
251
920
3,200
4,410
<10
<250
--
<50
<50
<50
246
NS
NS
NS
NS
--
--
--
--
8/14/2008
95.02
4.32
ND
ND
90.70
26.0
139
766
2,910
3,841
<5
--
<130
<25
<25
<25
242
NS
NS
NS
NS
--
--
--
--
11/20/2008
95.02
2.42
ND
ND
92.60
111
856
1,180
4,070
6,217
--
<20
<500
<100
<100
<100
362
NS
NS
NS
NS
--
--
--
--
2/11/2009
95.02
2.48
ND
ND
92.54
76.0
900
1,170
4,510
--
6,656
<10
<250
<50
<50
<50
347
NS
NS
NS
NS
--
--
--
--
4/21/2009
95.02
4.76
ND
ND
90.26
29.9
236
574
--
1,920
2,760
<5
<130
<25
<25
<25
176
NS
NS
NS
NS
--
--
--
--
7/31/2009
95.02
2.87
ND
ND
92.15
17.3
108
--
488
1,570
2,183
<5
<130
<25
<25
<25
169
NS
NS
NS
NS
--
--
--
--
10/13/2009
95.02
2.57
ND
ND
92.45
NS
--
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
10/27/2009
95.02
2.06
ND
ND
92.96
--
41.3
207
876
2,800
3,924
<10
<250
<50
<50
<50
251
NS
NS
NS
NS
--
--
--
--
1/12/2010
95.02
1.10
ND
ND
--
93.92
54.6
609
1,050
3,800
5,514
<10
<250
<50
<50
<50
269
NS
NS
NS
NS
--
--
--
--
4/21/2010
95.02
1.44
ND
--
ND
93.58
89.3
942
1,230
4,710
6,971
<5
<130
<25
<25
<25
295
NS
NS
NS
NS
--
--
--
--
7/22/2010
95.02
3.87
--
ND
ND
91.15
45.6
306
1,030
3,600
4,982
<10
<250
<50
<50
<50
239
NS
NS
NS
NS
--
--
--
--
11/23/2010
95.02
--
3.53
ND
ND
91.49
86.0
531
1,210
4,070
5,897
<10
<250
<50
<50
<50
294
NS
NS
NS
NS
--
--
--
--
3/2/2011
--
95.02
2.41
ND
ND
92.61
32.1
168
841
2,250
3,291.1
<1
<20
<1
<1
<1
227
NS
NS
NS
NS
--
--
--
--
--
5/19/2011
95.02
2.59
ND
ND
92.43
14.1
162
555
1,730
2,461.1
<1
<20
<1
<1
<1
148
NS
NS
NS
NS
--
--
--
--
--
7/12/2011
95.02
3.92
ND
ND
91.10
35.5
323
898
2,530
3,786.5
<1
<20
<1
<1
<1
267
NS
NS
NS
NS
--
--
--
--
--
10/24/2011
95.02
2.18
ND
ND
92.84
49.1
324
887
2,700
3,960.1
<1
<10
<1
<1
<1
248
NS
NS
NS
NS
--
--
--
--
--
2/8/2012
95.02
2.08
ND
ND
92.94
34.3
425
1,070
3,320
4,849
<1
<10
<1
<1
<1
244
NS
NS
NS
NS
--
--
--
--
--
5/22/2012
95.02
3.41
ND
ND
91.61
20.5
239
805
2,530
3594.5
<5
<50
<5
<5
<5
157
NS
NS
NS
NS
--
--
--
--
--
8/14/2012
95.02
6.23
ND
ND
88.79
21.5
165
726
2,130
3,042.5
<1
<10
<2
<1
<1
189
NS
NS
NS
NS
--
--
--
--
--
10/4/2012
95.02
7.23
ND
ND
87.79
819 [845]
2,460
[2,510]
3,508.4
[3,528.1]
<1 [<1]
<10 [<10]
<2 [<2]
<1 [<1]
<1 [<1]
250 [232]
NS
NS
NS
NS
--
--
--
--
--
2/22/2013
95.02
2.75
ND
ND
92.27
21.1
124
901
2,570
3,616.1
<1
<10
<2
<1
<1
181
NS
NS
NS
NS
6.01
1.11
14.99
3.26
21
5/1/2013
95.02
3.09
ND
ND
91.93
21.1
193
747
2,460
3,421.1
<1
<10
<2
<1
<1
197
NS
NS
NS
NS
5.91
0.716
15.26
0.21
-3.7
41.9
27.4 [26.1] 152 [147]
Total
BTEX
(µg/L)
Field Parameters
Ethylbenzene
(µg/L)
MTBE
(µg/L)
TBA
(µg/L)
DIPE
(µg/L)
ETBE
(µg/L)
Dissolved
Metals
ORP (mV) Comments
8/6/2013
95.02
2.24
ND
ND
92.78
36.2
230
722
2,170
3,158.2
<1
<10
<2
<1
<1
237
NS
NS
NS
NS
5.73
0.938
17.72
3.07
10/3/2013
95.02
2.79
ND
ND
92.23
38.6
242
813
2,300
3,393.6
<1
<10
<2
<1
<1
266
NS
NS
NS
NS
5.55
0.605
18.95
0.55
45.9
3/6/2014
95.02
1.60
ND
ND
93.42
24.3
240
892
2,720
3,876.3
<1
<10
<2
<1
<1
321
NS
NS
NS
NS
6.13
2.081
14.72
2.93
-53.4
6/12/2014
95.02
2.03
ND
ND
92.99
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
9/19/2014
95.02
4.32
ND
ND
90.70
24.2
164
864
2,380
3,432.2
<10
<100
<20
<10
<10
313
<1
8.21
6.39
<0.1
5.68
0.452
20.96
0.25
-53.0
11/13/2014
95.02
3.33
ND
ND
91.69
7.93
42.6
558
1,530
2,138.53
<1
<10
<2
<1
<1
87.4
1.73
15.2
2.02
<0.1
6.19
0.708
18.52
4.87
-25.8
3/25/2015
95.02
1.89
ND
ND
93.13
15.4
157
744
2,260
3,176.4
<1
<10
<2
<1
<1
145
18.9
29.9
16.5
<0.1
5.91
7.116
13.36
1.32
-123.3
6/25/2015
95.02
2.13
ND
ND
92.89
18.9
139
728
1,900
2,785.9
<1
<10
<2
<1
<1
191
<1
17.8
9.50
0.310
5.78
2.245
13.07
1.41
-7.2
page 4 of 13
Inaccessible
Table 1
Groundwater Monitoring and Analytical Data
Exxon Service Station #14489
285 Old Bayview Drive
North East, Maryland
Gauging Data
Analytical Data
Well ID
Date
Top of
Casing
Elevation
(feet)
Depth
to
Water
(feet)
Depth to
Hydrocarbon
(feet)
Hydrocarbon
Thickness
(feet)
Corrected
GW
Elevation
(feet)
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Total
Xylenes
(µg/L)
5
1,000
700
MW-8
12/7/2005
97.04
2.56
ND
ND
94.48
<1
<1
<1
5/24/2006
97.04
2.61
ND
ND
94.43
<1
2.0
11/7/2006
97.04
2.27
ND
ND
94.77
<1
6/21/2007
97.04
2.53
ND
ND
94.51
12/11/2007
97.04
2.28
ND
ND
3/24/2008
97.04
2.46
ND
6/29/2008
97.04
2.92
8/14/2008
97.04
11/20/2008
Field Parameters
Total
BTEX
(µg/L)
MTBE
(µg/L)
TBA
(µg/L)
DIPE
(µg/L)
10,000
--
20
--
--
<1
BRL
<1
<25
NA
10.3
34
46
24.3
<25
NA
4.1
13.9
49
67
<1
<25
104
27.7
130
644
906
8870
94.76
<1
<1
<1
<1
BRL
ND
94.58
<1
0.3 J
0.7 J
2
ND
ND
94.12
<1
<1
<1
3.02
ND
ND
94.02
<1
<1
97.04
2.30
ND
ND
94.74
<1
2/11/2009
97.04
2.67
ND
ND
94.37
4/21/2009
97.04
1.90
ND
ND
7/31/2009
97.04
2.55
ND
10/13/2009
97.04
3.00
10/27/2009
97.04
1/12/2010
ETBE
(µg/L)
TAME
(µg/L)
Naphthalene
(µg/L)
Sulfate
Total
Metals
--
--
NA
NA
0.65
--
2,600
NA
NS
NS
NA
NA
NA
NS
NS
NA
NA
NA
NA
NS
<500
NA
NA
NA
NA
<1
<25
NA
NA
NA
2.9 J
18.9
<25
NA
NA
<1
BRL
13.5
<25
<5
<1
<1
BRL
1.6
<25
<1
<1
<1
BRL
<1
0.34 J
<1
<1
<1
0.34 J
95.14
0.58 J
<1
<1
<1
ND
94.49
0.91 J
9.2
3.3
ND
ND
94.04
NS
NS
4.65
ND
ND
92.39
<1
97.04
2.59
ND
ND
94.45
4/21/2010
97.04
2.46
ND
ND
7/22/2010
97.04
2.65
ND
11/23/2010
97.04
2.90
3/2/2011
97.04
5/19/2011
Nitrate/Nitrite
pH (s.u.)
Conductivity
(mS/cm)
Temperature (°C)
DO (mg/L)
--
--
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
--
--
--
--
--
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NS
NS
NS
NS
--
--
--
--
--
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
86.2
13.8 J
<5
<5
0.84 J
<5
NS
NS
NS
NS
--
--
--
--
--
0.58 J
52.3
86.4
<5
<5
0.95 J
<5
NS
NS
NS
NS
--
--
--
--
--
10
23.0 J
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
2.2
<1
1.3
0.95 J
4.5 J
71.8
<25
<5
<5
3.8 J
<5
NS
NS
NS
NS
--
--
--
--
--
94.58
0.28 J
<1
<1
<1
0.28 J
18.5
20.5 J
<5
<5
0.71 J
<5
NS
NS
NS
NS
--
--
--
--
--
ND
94.39
<1
<1
<1
<1
BRL
0.62 J
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
ND
ND
94.14
<1
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
2.01
ND
ND
95.03
<1
<1
<1
<3
BRL
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
97.04
2.53
ND
ND
94.51
<1
<1
<1
<3
BRL
2.76
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
7/12/2011
97.04
4.65
ND
ND
92.39
<1
11.5
15
56.3
82.8
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
10/24/2011
97.04
2.59
ND
ND
94.45
<1 [<1]
<1 [<1]
<1 [<1]
<3 [<3]
BRL
1.32 [1.45] <10 [<10]
<1 [<1]
<1 [<1]
<1 [<1]
<5 [<5]
NS
NS
NS
NS
--
--
--
--
--
2/8/2012
97.04
2.81
ND
ND
94.23
<1 [<1]
<1 [<1]
<1 [<1]
<3 [<3]
BRL [BRL] 3.46 [3.86] <10 [<10]
<1 [<1]
<1 [<1]
<1 [<1]
<5 [<5]
NS
NS
NS
NS
--
--
--
--
--
5/22/2012
97.04
2.85
ND
ND
94.19
<1
<1
<1
<3
BRL
<1
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
8/14/2012
97.04
3.34
ND
ND
93.70
1.32
<1
<1
<3
1.32
7.33
<10
<2
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
10/4/2012
97.04
5.65
ND
ND
91.39
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
2/22/2013
97.04
2.51
ND
ND
94.53
<1
<1
<1
<3
BRL
1.01
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.91
0.665
7.57
8.55
189
5/1/2013
97.04
2.82
ND
ND
94.22
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
7.10
0.346
13.93
5.03
83.0
8/6/2013
97.04
2.35
ND
ND
94.69
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
7.02
0.361
27.41
5.58
170.7
10/3/2013
97.04
2.74
ND
ND
94.30
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.78
0.386
24.39
1.14
21.9
3/6/2014
97.04
2.46
ND
ND
94.58
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
7.35
0.256
7.11
11.27
22.2
6/12/2014
97.04
2.47
ND
ND
94.57
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.90
0.327
23.30
4.98
47.9
9/19/2014
97.04
4.92
ND
ND
92.12
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
59.5
4.86
<0.1
0.705
7.02
0.328
23.35
1.34
91.4
11/13/2014
97.04
2.61
ND
ND
94.43
<1
<1
<1
2.02
2.02
<1
<10
<2
<1
<1
<5
39.6
0.655
<0.1
1.52
7.03
0.264
18.97
7.81
68.5
3/25/2015
97.04
2.40
ND
ND
94.64
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
37.3
0.813
<0.1
1.59
7.16
0.281
9.04
8.42
218.1
6/25/2015
97.04
2.26
ND
ND
94.78
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
60.6
<0.1
<0.1
1.48
6.83
0.417
26.89
4.62
132.5
page 5 of 13
Dissolved
Metals
ORP (mV) Comments
Table 1
Groundwater Monitoring and Analytical Data
Exxon Service Station #14489
285 Old Bayview Drive
North East, Maryland
Gauging Data
Analytical Data
Well ID
Date
Top of
Casing
Elevation
(feet)
Depth
to
Water
(feet)
Depth to
Hydrocarbon
(feet)
Hydrocarbon
Thickness
(feet)
Corrected
GW
Elevation
(feet)
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Total
Xylenes
(µg/L)
5
1,000
700
MW-10
6/1/2005
93.35
3.82
ND
ND
89.53
9
1
4
12/7/2005
93.35
4.51
ND
ND
88.84
24.7
0.38 J
5/24/2006
93.35
4.67
ND
ND
88.68
13.3
11/7/2006
93.35
4.04
ND
ND
89.31
6/21/2007
93.35
4.54
ND
ND
12/11/2007
93.35
3.73
ND
3/24/2008
93.35
4.10
6/29/2008
93.35
8/14/2008
Field Parameters
Total
BTEX
(µg/L)
MTBE
(µg/L)
TBA
(µg/L)
DIPE
(µg/L)
10,000
--
20
--
--
7
21
9.3
<25
NA
26.8
8
59.4 J
19.6
<25
NA
0.52 J
5.8
4
23.6 J
45.7
25.3
11.2
38.1
83.9
266
399
164
88.81
18.9
7.4
20.1
46
93
ND
89.62
0.85 J
2.6
10.1
28
ND
ND
89.25
0.39 J
3.4
7.9
4.40
ND
ND
88.95
<1
<1
93.35
4.75
ND
ND
88.60
<1
11/20/2008
93.35
4.56
ND
ND
88.79
2/11/2009
93.35
4.27
ND
ND
4/21/2009
93.35
2.72
ND
7/31/2009
93.35
4.31
10/13/2009
93.35
10/27/2009
ETBE
(µg/L)
TAME
(µg/L)
Naphthalene
(µg/L)
Sulfate
Total
Metals
--
--
NA
NA
0.65
--
2,600
NA
NS
NS
NA
NA
NA
NS
NS
NA
NA
NA
NA
NS
127
NA
NA
NA
NA
42.5
<25
NA
NA
NA
41.1 J
22.5
<25
NA
NA
21
32.3 J
6.7
<25
NA
<1
<1
BRL
<1
<25
<1
<1
0.45 J
0.45 J
<1
3.6
<1
2.0
<1
6
89.08
<1
<1
<1
<1
ND
90.63
<1
<1
<1
ND
ND
89.04
<1
0.65 J
3.87
ND
ND
89.48
NS
93.35
3.33
ND
ND
90.02
1/12/2010
93.35
3.41
ND
ND
4/21/2010
93.35
2.94
ND
7/22/2010
93.35
4.41
11/23/2010
93.35
3/2/2011
Nitrate/Nitrite
pH (s.u.)
Conductivity
(mS/cm)
Temperature (°C)
DO (mg/L)
--
--
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
--
--
--
--
--
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NA
NS
NS
NS
NS
--
--
--
--
--
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
11.6
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
BRL
3.0
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
<1
BRL
1.4
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
0.30 J
0.69 J
1.64 J
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
<1
<1
<1
<1
BRL
0.40 J
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
89.94
0.30 J
<1
<1
<1
0.30 J
2.7
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
ND
90.41
<1
0.40 J
1.2
4
5.8 J
0.57 J
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
ND
ND
88.94
<1
0.58 J
0.61 J
2
3.2 J
1.6
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
4.71
ND
ND
88.64
5
0.82 J
13.5
5
24.2 J
40.3
30.4
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
93.35
3.96
ND
ND
89.39
<1
<1
<1
<3
BRL
1.37
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
5/19/2011
93.35
3.55
ND
ND
89.80
<1
<1
<1
<3
BRL
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
7/12/2011
93.35
4.40
ND
ND
88.95
<1
<1
<1
<3
BRL
15.4
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
10/24/2011
93.35
4.07
ND
ND
89.28
<1
<1
<1
<3
BRL
19.3
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
2/8/2012
93.35
4.10
ND
ND
89.25
<1
<1
<1
<3
BRL
2.49
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
5/22/2012
93.35
4.76
ND
ND
88.59
<1
<1
<1
<3
BRL
17
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
8/14/2012
93.35
4.15
ND
ND
89.20
<1
<1
1.07
<3
1.07
27.3
28.7
<2
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
10/4/2012
93.35
4.35
ND
ND
89.00
<1
<1
<1
<3
BRL
10.5
<10
<2
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
2/22/2013
93.35
4.35
ND
ND
89.00
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.70
2.82
9.32
3.09
133
5/1/2013
93.35
4.01
ND
ND
89.34
<1
<1
<1
<3
BRL
1.53
26.6
<2
<1
<1
<5
NS
NS
NS
NS
6.09
4.805
12.34
1.95
89.6
8/6/2013
93.35
3.42
ND
ND
89.93
<1
<1
<1
<2
BRL
5.31
<10
<2
<1
<1
<5
NS
NS
NS
NS
5.98
1.692
21.05
0.59
72.0
10/3/2013
93.35
4.09
ND
ND
89.26
<1
<1
<1
<2
BRL
1.96
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.20
1.502
21.89
0.21
-3.1
3/6/2014
93.35
2.99
ND
ND
90.36
<1
<1
<1
<3
BRL
1.12
<10
<2
<1
<1
<5
NS
NS
NS
NS
5.89
23.39
8.39
2.63
221.0
6/12/2014
93.35
2.81
ND
ND
90.54
1.03
<1
<1
<2
1.03
5.08
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.43
6.873
18.67
0.66
120.7
9/19/2014
93.35
4.31
ND
ND
89.04
1.25
<1
<1
<2
1.25
5.19
<10
<2
<1
<1
<5
1,030
4.97
1.82
<0.1
6.21
3.952
21.29
0.51
-5.6
11/13/2014
93.35
4.54
ND
ND
88.81
<1
<1
<1
<2
BRL
3.79
<10
<2
<1
<1
<5
41.1
2.13
0.470
0.301
6.36
1.508
17.53
2.05
33.4
3/25/2015
93.35
3.16
ND
ND
90.19
<1
<1
<1
<2
BRL
1.89
<10
<2
<1
<1
<5
55.7
2.74
<0.1
0.614
6.16
16.98
6.92
3.80
152.8
6/25/2015
93.35
3.38
ND
ND
89.97
<1
<1
<1
<3
BRL
2.94
<10
<2
<1
<1
<5
21.9
1.40
0.595
0.121
6.31
4.989
15.87
1.72
47.6
page 6 of 13
Dissolved
Metals
ORP (mV) Comments
Table 1
Groundwater Monitoring and Analytical Data
Exxon Service Station #14489
285 Old Bayview Drive
North East, Maryland
Gauging Data
Analytical Data
Well ID
Date
Top of
Casing
Elevation
(feet)
Depth
to
Water
(feet)
Depth to
Hydrocarbon
(feet)
Hydrocarbon
Thickness
(feet)
Corrected
GW
Elevation
(feet)
Benzene
(µg/L)
Toluene
(µg/L)
5
MW-11
6/1/2005
96.64
7.84
ND
ND
88.80
461
12/7/2005
96.64
8.48
ND
ND
88.16
5/24/2006
96.64
8.52
ND
ND
11/7/2006
96.64
6.10
ND
6/21/2007
96.64
8.16
12/11/2007
96.64
3/24/2008
Total
Xylenes
(µg/L)
TAME
(µg/L)
Naphthalene
(µg/L)
Sulfate
Total
Metals
Nitrate/Nitrite
pH (s.u.)
Conductivity
(mS/cm)
Temperature (°C)
DO (mg/L)
1,000
700
10,000
--
20
--
--
1,410
1,690
5,380
8,941
748
185
NA
--
--
NA
NA
0.65
--
2,600
NA
NS
NS
--
--
--
--
--
--
--
NS
NS
--
--
--
--
504
488
839
2,500
4,331
614
<130
NA
NA
NA
NA
NS
NS
--
NS
NS
--
--
--
--
88.12
270
317
729
1,920
3,236
422
<130
NA
NA
NA
NA
NS
--
NS
NS
NS
--
--
--
--
ND
90.54
148
117
463
921
1,649
206
55.8
NA
NA
NA
NA
--
NS
NS
NS
NS
--
--
--
--
ND
ND
88.48
102
64.0
341
423
930
185
<25
NA
NA
NA
--
NA
NS
NS
NS
NS
--
--
--
--
9.15
ND
ND
87.49
275
307
833
2,060
3,475
328
<250
NA
NA
--
NA
NA
NS
NS
NS
NS
--
--
--
--
96.64
6.07
ND
ND
90.57
135
117
443
1,160
1,855
289
69.3 J
NA
--
NA
NA
NA
NS
NS
NS
NS
--
--
--
--
6/29/2008
96.64
7.96
ND
ND
88.68
14.0
12.4
12.7
159
198
65.4
<25
--
<5
<5
4.2 J
19.0
NS
NS
NS
NS
--
--
--
--
8/14/2008
96.64
7.78
ND
ND
88.86
3.0
0.42 J
0.96 J
6
10.5 J
36.7
--
<25
<5
<5
0.92 J
2.1 J
NS
NS
NS
NS
--
--
--
--
11/20/2008
96.64
9.18
ND
ND
87.46
131
89.5
738
1,570
2,529
--
214
<130
<25
<25
<25
212
NS
NS
NS
NS
--
--
--
--
2/11/2009
96.64
6.87
ND
ND
89.77
65.8
63.1
333
781
--
1,243
149
34.8
<5
<5
10.7
87.3
NS
NS
NS
NS
--
--
--
--
4/21/2009
96.64
5.68
ND
ND
90.96
60.6
48.9
360
--
758
1,228
142
34.5 J
<13
<13
10.9 J
84.9
NS
NS
NS
NS
--
--
--
--
7/31/2009
96.64
8.45
ND
ND
88.19
60.4
47.0
--
521
523
1,151
169
<50
<10
<10
11.9
118
NS
NS
NS
NS
--
--
--
--
10/13/2009
96.64
6.73
ND
ND
89.91
NS
--
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
10/27/2009
96.64
6.23
ND
ND
90.41
--
<1
<1
<1
<1
BRL
16.1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
1/12/2010
96.64
5.22
ND
ND
--
91.42
8.9
4.5
70.9
95
180
19.2
<25
<5
<5
1.4 J
16.0
NS
NS
NS
NS
--
--
--
--
4/21/2010
96.64
4.93
ND
--
ND
91.71
29.6
11.3
198
241
480
76.1
16.2 J
<5
<5
4.5 J
51.8
NS
NS
NS
NS
--
--
--
--
7/22/2010
96.64
9.31
--
ND
ND
87.33
78.7
64.2
884
1,210
2,237
206
<63
<13
<13
17.4
213
NS
NS
NS
NS
--
--
--
--
11/23/2010
96.64
--
8.85
ND
ND
87.79
103
65.4
422
566
1,156
176
30.8
<5
<5
11.8
143
NS
NS
NS
NS
--
--
--
--
3/2/2011
--
96.64
5.96
ND
ND
90.68
4.64
4
47
66
121
12.8
<20
<1
<1
<1
9.29
NS
NS
NS
NS
--
--
--
--
--
5/19/2011
96.64
5.99
ND
ND
90.65
16.4
12
126
203
357
41.7
<20
<1
<1
<1
35.2
NS
NS
NS
NS
--
--
--
--
--
7/12/2011
96.64
8.58
ND
ND
88.06
51.6
37.8
432
487
1,008.4
120
<20
<1
<1
8.06
87.5
NS
NS
NS
NS
--
--
--
--
--
10/24/2011
96.64
6.36
ND
ND
90.28
15.6
12
158
218
403.6
36.4
<10
<1
<1
2.31
44.8
NS
NS
NS
NS
--
--
--
--
--
2/8/2012
96.64
5.96
ND
ND
90.68
9.95
10.4
143
228
391
26
<10
<1
<1
<1
41.5
NS
NS
NS
NS
--
--
--
--
--
5/22/2012
96.64
9.10
ND
ND
87.54
31.4
17
291
404
743.4
87.4
13.3
<1
<1
6.17
65.9
NS
NS
NS
NS
--
--
--
--
--
8/14/2012
96.64
10.51
ND
ND
86.13
71.2
56.8
848
1,270
2,246.0
142
<10
<2
<1
9.86
157
NS
NS
NS
NS
--
--
--
--
--
10/4/2012
96.64
10.82
ND
ND
85.82
103
72.9
667
967
1,809.9
148
32.7
<2
<1
12.1
193
NS
NS
NS
NS
--
--
--
--
--
2/22/2013
96.64
6.40
ND
ND
90.24
175.56
[270.71]
<1 [14.1]
<10 [<10]
<2 [<2]
<1 [<1]
<1 [1.1]
24.6 [9.39]
NS
NS
NS
NS
6.20
0.202
12.31
1.87
42
5/1/2013
96.64
6.63
ND
ND
90.01
15.9
15.6
251
455
737.5
52.4
<10
<2
<1
3.87
76
NS
NS
NS
NS
5.70
0.221
13.28
0.74
58.3
8/6/2013
96.64
5.23
ND
ND
91.41
2.91
<1
15
7.81
25.72
8.31
<10
<2
<1
<1
16.3
NS
NS
NS
NS
5.85
0.176
19.14
1.75
100.2
10/3/2013
96.64
6.88
ND
ND
89.76
6.65
1.89
70.8
36.4
115.74
21.0
<10
<2
<1
1.56
42.2
NS
NS
NS
NS
5.72
0.177
21.03
1.00
67.0
3/6/2014
96.64
4.42
ND
ND
92.22
<1
1.05
3.85
7.92
12.82
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.02
2.082
11.57
6.02
39.6
6/12/2014
96.64
5.34
ND
ND
91.30
1.10
1.33
15.2
13.2
30.83
3.44
<10
<2
<1
<1
7.40
NS
NS
NS
NS
6.14
0.593
16.43
4.01
86.4
9/19/2014
96.64
9.59
ND
ND
87.05
12.1
9.91
210
244
476.01
39.1
<10
<2
<1
3.63
77.8
6.27
9.72
7.01
<0.1
5.89
0.626
19.45
0.37
-138.4
11/13/2014
96.64
8.39
ND
ND
88.25
13.8
11.8
304
328
657.6
46.5
<10
<2
<1
3.72
36.1
7.16
76.3
1.20
<0.1
5.97
0.352
18.68
4.29
18.4
3/25/2015
96.64
4.65
ND
ND
91.99
1.06
1.34
36.6
23.3
62.3
2.52
<10
<2
<1
<1
11.2
4.81
12.7
2.99
0.319
5.92
0.257
10.20
4.77
45.6
6/25/2015
96.64
4.91
ND
ND
91.73
1.09
1.36
12.9
15.6
31.0
3.87
<10
<2
<1
<1
8.86
6.85
10.1
3.57
2.26
5.91
0.240
18.52
4.78
88.7
8.17 [10.2] 4.39 [6.51] 92.7 [129] 70.3 [125]
Total
BTEX
(µg/L)
Field Parameters
Ethylbenzene
(µg/L)
MTBE
(µg/L)
TBA
(µg/L)
DIPE
(µg/L)
ETBE
(µg/L)
page 7 of 13
Dissolved
Metals
ORP (mV) Comments
Table 1
Groundwater Monitoring and Analytical Data
Exxon Service Station #14489
285 Old Bayview Drive
North East, Maryland
Gauging Data
Analytical Data
Total
BTEX
(µg/L)
Field Parameters
Well ID
Date
Top of
Casing
Elevation
(feet)
Depth
to
Water
(feet)
Depth to
Hydrocarbon
(feet)
Hydrocarbon
Thickness
(feet)
Corrected
GW
Elevation
(feet)
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Total
Xylenes
(µg/L)
MTBE
(µg/L)
TBA
(µg/L)
DIPE
(µg/L)
5
1,000
700
10,000
--
20
--
--
MW-12
6/1/2005
100.00
10.50
ND
ND
89.50
3.6
<2
<2
<2
3.6
283
<50
NA
12/7/2005
100.00
12.65
ND
ND
87.35
0.45 J
<1
0.72 J
1.3
2.5 J
135
<25
NA
5/24/2006
100.00
13.16
ND
ND
86.84
4.0
25.1
31.7
101
162
198
<50
11/7/2006
100.00
8.19
ND
ND
91.81
1.2
7.6
26.9
75.0
110.7
161
6/21/2007
100.00
12.97
ND
ND
87.03
1.8
7.3
15.4
48.6
73.1
12/11/2007
100.00
15.78
ND
ND
84.22
<1
0.92 J
16.6
56.3
3/24/2008
100.00
7.98
ND
ND
92.02
0.84 J
0.38 J
1.3
6/29/2008
100.00
12.35
ND
ND
87.65
0.85 J
<1
8/14/2008
100.00
13.85
ND
ND
86.15
<1
11/20/2008
100.00
14.53
ND
ND
85.47
2/11/2009
100.00
9.07
ND
ND
4/21/2009
100.00
8.62
ND
7/31/2009
100.00
13.86
10/13/2009
100.00
10/27/2009
ETBE
(µg/L)
TAME
(µg/L)
Naphthalene
(µg/L)
Sulfate
Total
Metals
--
--
NA
NA
0.65
--
2,600
NA
NS
NS
NA
NA
NA
NS
NS
NA
NA
NA
NA
NS
<25
NA
NA
NA
NA
224
<25
NA
NA
NA
73.8 J
25.7
<25
NA
NA
4.1
6.6 J
144
11.2 J
NA
<1
<1
0.85 J
153
9.8 J
<1
<1
<1
BRL
126
<1
<1
<1
<1
BRL
90.93
0.31 J
<1
0.31 J
0.81 J
ND
91.38
<1
<1
<1
ND
ND
86.14
<1
1.5
10.90
ND
ND
89.10
NS
100.00
8.54
ND
ND
91.46
1/12/2010
100.00
7.36
ND
ND
4/21/2010
100.00
7.39
ND
7/22/2010
100.00
15.90
11/23/2010
100.00
3/2/2011
Nitrate/Nitrite
pH (s.u.)
Conductivity
(mS/cm)
Temperature (°C)
DO (mg/L)
--
--
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
--
--
--
--
--
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NA
NS
NS
NS
NS
--
--
--
--
--
<5
<5
27.4
1.4 J
NS
NS
NS
NS
--
--
--
--
--
<25
<5
<5
21.6
<5
NS
NS
NS
NS
--
--
--
--
--
56.0
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
1.43 J
114
<25
<5
<5
14.3
1.4 J
NS
NS
NS
NS
--
--
--
--
--
<1
BRL
96.7
13.2 J
<5
<5
16.6
<5
NS
NS
NS
NS
--
--
--
--
--
0.61 J
1.6
3.7 J
96.7
<25
<5
<5
18.0
<5
NS
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
<1
<1
<1
<1
BRL
38.8
<25
<5
<5
4.9 J
<5
NS
NS
NS
NS
--
--
--
--
--
92.64
0.32 J
<1
<1
<1
0.32 J
90.4
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
ND
92.61
1.4
<1
0.86 J
0.64 J
2.9 J
80.9
9.5 J
<5
<5
13.2
2.6 J
NS
NS
NS
NS
--
--
--
--
--
ND
ND
84.10
<1
1.1
1.3
5.0
7.4
53.0
<25
<5
<5
13.1
<5
NS
NS
NS
NS
--
--
--
--
--
14.50
ND
ND
85.50
<1
<1
0.42 J
1.4
1.8 J
19.1
<25
<5
<5
3.2 J
<5
NS
NS
NS
NS
--
--
--
--
--
100.00
7.72
ND
ND
92.28
<1 [<1]
<1 [<1]
<1 [<1]
<3 [<3]
BRL
36.8 [35.5] <20 [<20]
<1 [<1]
<1 [<1]
6.32 [5.99]
<5 [<5]
NS
NS
NS
NS
--
--
--
--
--
5/19/2011
100.00
8.63
ND
ND
91.37
<1 [<1]
<1 [<1]
1.15 [1.02]
<3 [<3]
BRL
60.9 [54.1] <20 [<20]
<1 [<1]
<1 [<1]
<1 [10.6]
5.01 [<5]
NS
NS
NS
NS
--
--
--
--
--
7/12/2011
100.00
14.09
ND
ND
85.91
<1
<1
<1
<3
BRL
37
<20
<1
<1
6.78
<5
NS
NS
NS
NS
--
--
--
--
--
10/24/2011
100.00
8.48
ND
ND
91.52
<1
1.62
<1
<3
1.62
28.9
<10
<1
<1
4.82
<5
NS
NS
NS
NS
--
--
--
--
--
2/8/2012
100.00
8.33
ND
ND
91.67
<1
<1
<1
<3
BRL
43.9
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
5/22/2012
100.00
14.55
ND
ND
85.45
<1
<1
<1
<3
BRL
27.1
<10
<1
<1
4.11
<5
NS
NS
NS
NS
--
--
--
--
--
8/14/2012
100.00
17.95
ND
ND
82.05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
insufficient volume for sample
10/4/2012
100.00
dry
ND
ND
>100.00
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
insufficient volume for sample
2/22/2013
100.00
8.42
ND
ND
91.58
<1
<1
<1
<3
BRL
9.48
<10
<2
<1
1.41
<5
NS
NS
NS
NS
5.48
0.668
12.76
0.55
148
5/1/2013
100.00
9.13
ND
ND
90.87
<1
<1
<1
<3
BRL
27.4
<10
<2
<1
5.24
<5
NS
NS
NS
NS
4.73
0.485
13.33
0.84
159.4
8/6/2013
100.00
7.25
ND
ND
92.75
<1
<1
<1
<2
BRL
16.7
<10
<2
<1
3.06
<5
NS
NS
NS
NS
4.82
0.394
16.42
0.45
162.1
10/3/2013
100.00
9.83
ND
ND
90.17
<1
<1
<1
<2
BRL
13.7
<10
<2
<1
<1
<5
NS
NS
NS
NS
4.75
0.287
18.58
0.11
132.8
3/6/2014
100.00
6.91
ND
ND
93.09
<1
<1
<1
<3
BRL
15.2
<10
<2
<1
2.46
<5
NS
NS
NS
NS
4.68
0.543
12.61
0.39
230.1
6/12/2014
100.00
8.38
ND
ND
91.62
<1
<1
<1
<2
BRL
9.81
<10
<2
<1
1.86
<5
NS
NS
NS
NS
4.85
0.348
13.60
0.58
170.1
9/19/2014
100.00
16.21
ND
ND
83.79
<1
<1
<1
<2
BRL
7.25
<10
<2
<1
1.16
<5
21.1
18.4
<0.1
0.155
4.98
0.205
16.90
1.29
-34.4
11/13/2014
100.00
13.29
ND
ND
86.71
<1
<1
<1
<2
BRL
3.28
<10
<2
<1
<1
<5
17.1
0.824
0.235
1.29
5.10
0.812
17.94
0.90
227.8
3/25/2015
100.00
6.73
ND
ND
93.27
<1
<1
<1
<2
BRL
4.55
<10
<2
<1
<1
<5
15.1
0.667
<0.1
0.624
5.06
0.750
10.71
4.76
231.9
6/25/2015
100.00
7.31
ND
ND
92.69
<1
<1
<1
<3
BRL
5.87
<10
<2
<1
1.38
<5
19.5
1.78
0.265
0.171
4.95
0.431
14.85
2.49
195.7
page 8 of 13
Dissolved
Metals
ORP (mV) Comments
Table 1
Groundwater Monitoring and Analytical Data
Exxon Service Station #14489
285 Old Bayview Drive
North East, Maryland
Gauging Data
Analytical Data
Well ID
Date
Top of
Casing
Elevation
(feet)
Depth
to
Water
(feet)
Depth to
Hydrocarbon
(feet)
Hydrocarbon
Thickness
(feet)
Corrected
GW
Elevation
(feet)
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Total
Xylenes
(µg/L)
5
1,000
700
MW-13
6/1/2005
94.38
9.60
ND
ND
84.78
0.99 J
11.7
62.3
12/7/2005
94.38
10.93
ND
ND
83.45
<1
<1
5/24/2006
94.38
12.06
ND
ND
82.32
1.4
11/7/2006
94.38
7.87
ND
ND
86.51
6/21/2007
94.38
11.29
ND
ND
12/11/2007
94.38
11.61
ND
3/24/2008
94.38
7.58
6/29/2008
94.38
8/14/2008
Field Parameters
Total
BTEX
(µg/L)
MTBE
(µg/L)
TBA
(µg/L)
DIPE
(µg/L)
10,000
--
20
--
--
225
300 J
2.2
<25
NA
<1
<1
BRL
<1
<25
NA
16.3
25.5
83.9
127.1
<1
<25
<1
1.5
7.3
21.2
30.0
<1
83.09
<1
7.0
15.4
48.0
70.4
ND
82.77
<1
0.76 J
10.5
31.0
ND
ND
86.80
<1
1.8
21.8
11.11
ND
ND
83.27
<1
<1
94.38
12.62
ND
ND
81.76
<1
11/20/2008
94.38
11.97
ND
ND
82.41
2/11/2009
94.38
9.52
ND
ND
4/21/2009
94.38
3.75
ND
7/31/2009
94.38
12.49
10/13/2009
94.38
10/27/2009
ETBE
(µg/L)
TAME
(µg/L)
Naphthalene
(µg/L)
Sulfate
Total
Metals
--
--
NA
NA
0.65
--
2,600
NA
NS
NS
NA
NA
NA
NS
NS
NA
NA
NA
NA
NS
<25
NA
NA
NA
NA
<1
<25
NA
NA
NA
42.3 J
<1
<25
NA
NA
63.7
87.3
2.1
<25
NA
<1
0.91 J
0.91 J
0.46 J
<25
<1
<1
<1
BRL
<1
<1
<1
0.56 J
1.3
1.9 J
84.86
<1
2.0
25.3
73.5
ND
90.63
<1
0.45 J
8.0
ND
ND
81.89
1.2
1.3
10.00
ND
ND
84.38
<1
94.38
NM
NM
NM
NM
1/12/2010
94.38
6.36
ND
ND
4/21/2010
94.38
6.55
ND
7/22/2010
94.38
14.77
11/23/2010
94.38
3/2/2011
Nitrate/Nitrite
pH (s.u.)
Conductivity
(mS/cm)
Temperature (°C)
DO (mg/L)
--
--
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
--
--
--
--
--
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NA
NS
NS
NS
NS
--
--
--
--
--
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
0.64 J
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
100.8
3.5
<25
<5
<5
<5
11.8
NS
NS
NS
NS
--
--
--
--
--
18.3
26.8 J
1.7
<25
<5
<5
<5
3.2 J
NS
NS
NS
NS
--
--
--
--
--
2.1
9.3
13.9
5.5
<25
<5
<5
<5
5.3
NS
NS
NS
NS
--
--
--
--
--
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
88.02
<1
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
ND
87.83
<1
<1
<1
<1
BRL
1.5
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
ND
ND
79.61
<1
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
14.40
ND
ND
79.98
<1
<1
0.44 J
1.1
1.5 J
0.46 J
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
94.38
4.58
ND
ND
89.80
<1
<1
5.25
11.8
17
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
5/19/2011
94.38
8.85
ND
ND
85.53
<1
<1
13.9
46.5
60
3.27
<20
<1
<1
<1
7.24
NS
NS
NS
NS
--
--
--
--
--
7/12/2011
94.38
12.63
ND
ND
81.75
<1
<1
14
43
57
5.76
<20
<1
<1
<1
17.1
NS
NS
NS
NS
--
--
--
--
--
10/24/2011
94.38
6.83
ND
ND
87.55
<1
<1
<1
<3
BRL
<1
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
2/8/2012
94.38
5.90
ND
ND
88.48
<1
<1
1.78
3.88
6
<1
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
5/22/2012
94.38
13.05
ND
ND
81.33
<1
<1
2.72
<3
2.72
2.09
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
8/14/2012
94.38
17.93
ND
ND
76.45
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
insufficient volume for sample
10/4/2012
94.38
17.96
ND
ND
76.42
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
insufficient volume for sample
2/22/2013
94.38
6.63
ND
ND
87.75
<1
<1
2.8
5.07
7.87
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.06
1.59
10.80
6.76
143
5/1/2013
94.38
9.34
ND
ND
85.04
<1
<1
9.56
25.6
35.16
1.95
28
<2
<1
<1
<5
NS
NS
NS
NS
5.48
2.006
12.97
3.30
121.0
8/6/2013
94.38
5.22
ND
ND
89.16
<1
<1
3.34
5.64
8.98
1.56
<10
<2
<1
<1
5.24
NS
NS
NS
NS
5.50
1.611
15.24
1.89
140.7
10/3/2013
94.38
8.91
ND
ND
85.47
<1
<1
6.58
19.4
25.98
2.41
<10
<2
<1
<1
<5
NS
NS
NS
NS
5.23
1.840
17.11
0.17
129.9
3/6/2014
94.38
3.95
ND
ND
90.43
<1
<1
1.97
<3
1.97
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
5.41
3.491
11.71
4.91
169.6
6/12/2014
94.38
5.88
ND
ND
88.50
<1
<1
11.9
30.2
42.1
1.98
<10
<2
<1
<1
<5
NS
NS
NS
NS
5.28
3.730
13.42
0.75
155.0
9/19/2014
94.38
14.89
ND
ND
79.49
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
356
26.4
0.189
<0.1
5.33
2.286
15.99
1.31
-36.2
11/13/2014
94.38
11.54
ND
ND
82.84
<1
1.35
<1
<2
1.35
<1
<10
<2
<1
<1
<5
27.1
1.85
0.111
0.523
5.49
3.593
16.50
5.45
65.3
3/25/2015
94.38
4.68
ND
ND
89.70
<1
<1
2.59
<2
2.59
1.29
<10
<2
<1
<1
<5
16.3
1.99
0.762
0.219
5.76
3.890
10.24
4.98
204.9
6/25/2015
94.38
3.94
ND
ND
90.44
<1
<1
<1
<3
BRL
8.19
28.6
<2
<1
<1
<5
14.5
3.56
0.606
0.101
5.40
2.329
10.83
1.59
142.3
page 9 of 13
Dissolved
Metals
ORP (mV) Comments
Table 1
Groundwater Monitoring and Analytical Data
Exxon Service Station #14489
285 Old Bayview Drive
North East, Maryland
Gauging Data
Analytical Data
Date
Top of
Casing
Elevation
(feet)
Depth
to
Water
(feet)
Depth to
Hydrocarbon
(feet)
Hydrocarbon
Thickness
(feet)
Corrected
GW
Elevation
(feet)
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Total
Xylenes
(µg/L)
TAME
(µg/L)
Naphthalene
(µg/L)
Sulfate
Total
Metals
Nitrate/Nitrite
pH (s.u.)
Conductivity
(mS/cm)
Temperature (°C)
DO (mg/L)
5
1,000
700
10,000
--
20
--
--
MW-14
6/1/2005
93.10
11.90
ND
ND
81.20
456
51.1
50.8
144
702
102
<50
NA
--
--
NA
NA
0.65
--
2,600
NA
NS
NS
--
--
--
--
--
--
--
NS
NS
--
--
--
--
12/7/2005
93.10
11.58
ND
ND
81.52
<1
5.3
<1
<1
5.3
<1
<25
NA
NA
NA
NA
NS
NS
--
NS
NS
--
--
--
--
5/24/2006
93.10
12.88
ND
ND
80.22
66.7
14.8
23.5
86.1
191.1
25.9
23.2 J
NA
NA
NA
NA
NS
--
NS
NS
NS
--
--
--
--
11/7/2006
93.10
8.87
ND
ND
84.23
62.9
3.1
8.8
35.9
110.7
28.5
24.4 J
NA
NA
NA
NA
--
NS
NS
NS
NS
--
--
--
--
6/21/2007
93.10
12.69
ND
ND
80.41
580
75.8
87.3
225
968
142
141
NA
NA
NA
--
NA
NS
NS
NS
NS
--
--
--
--
12/11/2007
93.10
10.25
ND
ND
82.85
<1
0.31 J
2.9
9.5
12.7 J
<1
<25
NA
NA
--
NA
NA
NS
NS
NS
NS
--
--
--
--
3/24/2008
93.10
8.40
ND
ND
84.70
4.7
0.41 J
0.47 J
1
7J
5.3
<25
NA
--
NA
NA
NA
NS
NS
NS
NS
--
--
--
--
6/29/2008
93.10
12.50
ND
ND
80.60
27.0
2.8
1.7
19.8
51.3
32.5
11.3 J
--
<5
<5
<5
2.9 J
NS
NS
NS
NS
--
--
--
--
8/14/2008
93.10
14.52
ND
ND
78.58
104
0.33 J
1.3
11.5
117 J
61.7
--
42.2
0.80 J
<5
<5
15.9
NS
NS
NS
NS
--
--
--
--
11/20/2008
93.10
12.32
ND
ND
80.78
0.72 J
<1
<1
<1
0.72 J
--
2.4
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
2/11/2009
93.10
10.33
ND
ND
82.77
19.8
1.1
1.2
2.7
--
24.8
18.2
11.3 J
<5
<5
<5
1.5 J
NS
NS
NS
NS
--
--
--
--
4/21/2009
93.10
7.85
ND
ND
85.25
2.0
<1
<1
--
<1
2.0
3.6
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
7/31/2009
93.10
13.09
ND
ND
80.01
109
4.9
--
1.7
33.1
149
69.6
44.2
1.1 J
<5
<5
11.2
NS
NS
NS
NS
--
--
--
--
10/13/2009
93.10
11.37
ND
ND
81.73
41.7
--
4.4
<1
7.3
53.4
23.7
17.1 J
0.38 J
<5
<5
6.0
NS
NS
NS
NS
--
--
--
--
10/27/2009
93.10
NM
NM
NM
NM
--
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
1/12/2010
93.10
8.54
ND
ND
--
84.56
<1
<1
<1
<1
BRL
7.1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
4/21/2010
93.10
5.98
ND
--
ND
87.12
45
10.1
9.0
38.0
102.1
39.6
21.4 J
0.57 J
<5
<5
10.4
NS
NS
NS
NS
--
--
--
--
7/22/2010
93.10
15.94
--
ND
ND
77.16
118
0.61 J
0.90 J
20.4
140 J
109
100
1.9 J
<5
<5
28.8
NS
NS
NS
NS
--
--
--
--
11/23/2010
93.10
--
17.50
ND
ND
75.60
<1
0.50 J
0.54 J
0.27 J
1.31 J
<1
<25
<5
<5
<5
1.6 J
NS
NS
NS
NS
--
--
--
--
3/2/2011
--
93.10
7.59
ND
ND
85.51
<1
<1
<1
<3
BRL
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
5/19/2011
--
93.10
9.91
ND
ND
83.19
28.1
17.9
22.4
62.7
131
49.4
<20
<1
<1
<1
8.02
NS
NS
NS
NS
--
--
--
--
--
<1 [<1]
<1 [<1]
NS
NS
NS
NS
--
--
--
--
--
11.5 [9.9] 61.9 [52.7]
Total
BTEX
(µg/L)
Field Parameters
Well ID
234.4
[213.6]
18.71
[16.97]
MTBE
(µg/L)
TBA
(µg/L)
79.1 [78.4] 31.7 [31.1]
DIPE
(µg/L)
ETBE
(µg/L)
1.29 [1.27] 42.2 [35.7]
Dissolved
Metals
ORP (mV) Comments
7/12/2011
93.10
13.98
ND
ND
79.12
161 [151]
<1 [<1]
10/24/2011
93.10
9.91
ND
ND
83.19
14.6 [13.3]
<1 [<1]
<1 [<1]
4.11 [3.67]
14.1 [13]
<10 [<10]
<1 [<1]
<1 [<1]
<1 [<1]
<5 [<5]
NS
NS
NS
NS
--
--
--
--
--
2/8/2012
93.10
9.09
ND
ND
84.01
9.79
<1
<1
6.09
16
17.4
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
5/22/2012
93.10
15.07
ND
ND
78.03
22.4
<1
<1
<3
22.4
65.1
13
<1
<1
<1
7.29
NS
NS
NS
NS
--
--
--
--
--
8/14/2012
93.10
18.05
ND
ND
75.05
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
insufficient volume for sample
10/4/2012
93.10
dry
ND
ND
>93.10
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
insufficient volume for sample
2/22/2013
93.10
9.57
ND
ND
83.53
<1
1.32
3.46
12.2
16.98
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.37
0.816
10.90
8.81
162
5/1/2013
93.10
10.82
ND
ND
82.28
<1
<1
<1
<3
BRL
5.7
<10
<2
<1
<1
<5
NS
NS
NS
NS
5.66
1.265
12.97
4.33
107.4
8/6/2013
93.10
7.67
ND
ND
85.43
2.4
<1
<1
8.29
10.69
10.1
<10
<2
<1
<1
<5
NS
NS
NS
NS
5.96
1.005
16.23
2.75
166.6
10/3/2013
93.10
11.24
ND
ND
81.86
10.6
<1
<1
2.58
13.18
24.9
<10
<2
<1
<1
9.44
NS
NS
NS
NS
4.32
1.563
17.88
0.28
176.6
3/6/2014
93.10
7.26
ND
ND
85.84
<1
<1
<1
<3
BRL
1.15
<10
<2
<1
<1
<5
NS
NS
NS
NS
5.85
2.764
11.77
9.10
172.8
6/12/2014
93.10
9.68
ND
ND
83.42
31.2
5.76
9.49
41.8
88.25
41.7
20.7
<2
<1
<1
15.3
NS
NS
NS
NS
5.17
2.267
13.30
1.07
231.8
9/19/2014
93.10
16.21
ND
ND
76.89
22.3
<1
<1
2.93
25.23
39.0
10.3
<2
<1
1.12
7.41
379
139
4.24
<0.1
5.43
2.222
16.40
1.00
-60.3
11/13/2014
93.10
12.59
ND
ND
80.51
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
18.6
7.18
0.391
0.443
6.09
2.282
16.94
3.93
34.9
3/25/2015
93.10
7.83
ND
ND
85.27
1.09
<1
<1
<2
1.09
3.69
<10
<2
<1
<1
<5
12.2
0.860
<0.1
0.255
5.90
2.432
9.35
8.34
118.2
6/25/2015
93.10
7.16
ND
ND
85.94
<1
<1
<1
<3
BRL
1.11
<10
<2
<1
<1
<5
8,850
8.73
1.10
0.287
5.14
1.920
11.37
5.11
136.6
page 10 of 13
Table 1
Groundwater Monitoring and Analytical Data
Exxon Service Station #14489
285 Old Bayview Drive
North East, Maryland
Gauging Data
Analytical Data
Well ID
Date
Top of
Casing
Elevation
(feet)
Depth
to
Water
(feet)
Depth to
Hydrocarbon
(feet)
Hydrocarbon
Thickness
(feet)
Corrected
GW
Elevation
(feet)
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Total
Xylenes
(µg/L)
5
MW-15
6/1/2005
92.40
8.31
ND
ND
84.09
1.6
1,000
700
<1
0.87 J
12/7/2005
92.40
6.02
ND
ND
86.38
<1
<1
5/24/2006
92.40
8.51
ND
ND
83.89
0.68 J
11/7/2006
92.40
5.32
ND
ND
87.08
6/21/2007
92.40
11.29
ND
ND
12/11/2007
92.40
7.31
ND
3/24/2008
92.40
5.22
6/29/2008
92.40
8/14/2008
Field Parameters
Total
BTEX
(µg/L)
MTBE
(µg/L)
TBA
(µg/L)
DIPE
(µg/L)
10,000
--
20
--
--
2.3
4.8 J
<1
<25
NA
<1
<1
BRL
<1
<25
NA
8.5
15.8
51.7
76.7 J
<1
<25
<1
2.7
10.7
31.9
45.3
<1
81.11
1.8
5.0
11.6
35.5
53.9
ND
85.09
<1
<1
1.6
5.3
ND
ND
87.18
0.78 J
<1
<1
7.79
ND
ND
84.61
<1
<1
92.40
9.00
ND
ND
83.40
<1
11/20/2008
92.40
4.84
ND
ND
87.56
2/11/2009
92.40
6.66
ND
ND
4/21/2009
92.40
1.90
ND
7/31/2009
92.40
8.55
10/13/2009
92.40
10/27/2009
ETBE
(µg/L)
TAME
(µg/L)
Naphthalene
(µg/L)
Sulfate
Total
Metals
--
--
NA
NA
0.65
--
2,600
NA
NS
NS
NA
NA
NA
NS
NS
NA
NA
NA
NA
NS
<25
NA
NA
NA
NA
<1
<25
NA
NA
NA
6.9
<1
<25
NA
NA
<1
0.78 J
<1
<25
NA
<1
<1
BRL
<1
<25
<1
<1
<1
BRL
<1
1.2
<1
<1
<1
1.2
85.74
2.3
<1
0.63 J
0.65 J
ND
90.50
0.60 J
<1
<1
ND
ND
83.85
0.55 J
4.7
7.90
ND
ND
84.50
<1
92.40
NM
NM
NM
NM
1/12/2010
92.40
5.21
ND
ND
4/21/2010
92.40
5.88
ND
7/22/2010
92.40
10.31
11/23/2010
92.40
3/2/2011
Dissolved
Metals
Nitrate/Nitrite
pH (s.u.)
Conductivity
(mS/cm)
Temperature (°C)
DO (mg/L)
ORP (mV) Comments
--
--
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
--
--
--
--
--
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NA
NS
NS
NS
NS
--
--
--
--
--
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
3.6 J
<1
<25
<5
<5
<5
2.0 J
NS
NS
NS
NS
--
--
--
--
--
<1
0.60 J
1.1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
1.5
4.6
11.4 J
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
87.19
<1
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
ND
86.52
<1
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
ND
ND
82.09
<1
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
11.14
ND
ND
81.26
1.7
<1
0.34 J
0.27 J
2.3 J
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
92.40
3.94
ND
ND
88.46
<1
<1
<1
<3
BRL
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
5/19/2011
92.40
6.56
ND
ND
85.84
<1
<1
<1
<3
BRL
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
7/12/2011
92.40
8.88
ND
ND
83.52
1.4
<1
<1
<3
1.4
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
10/24/2011
92.40
6.76
ND
ND
85.64
<1
<1
<1
<3
BRL
<1
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
2/8/2012
92.40
7.45
ND
ND
84.95
<1
<1
<1
<3
BRL
<1
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
5/22/2012
92.40
9.45
ND
ND
82.95
1.89
<1
<1
<3
1.89
<1
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
8/14/2012
92.40
11.82
ND
ND
80.58
4.05
<1
1.88
<3
5.93
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
10/4/2012
92.40
13.96
ND
ND
78.44
10.5
<1
8.57
<3
19.07
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
2/22/2013
92.40
6.10
ND
ND
86.30
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
6.21
0.665
11.47
5.88
202
5/1/2013
92.40
7.11
ND
ND
85.29
<1
1.04
2.47
7.96
11.47
<1
15.5
<2
<1
<1
<5
NS
NS
NS
NS
5.62
0.807
12.37
2.98
108.1
8/6/2013
92.40
4.15
ND
ND
88.25
<1
<1
1
2.97
3.97
<1
<10
<2
<1
<1
5.86
NS
NS
NS
NS
5.80
0.523
15.35
0.70
75.7
10/3/2013
92.40
7.41
ND
ND
84.99
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
3.48
0.609
17.73
0.86
237.0
3/6/2014
92.40
4.46
ND
ND
87.94
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
5.77
0.704
11.83
2.83
184.6
6/12/2014
92.40
6.78
ND
ND
85.62
1.78
<1
<1
<2
1.78
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
5.56
0.897
13.00
0.78
231.4
9/19/2014
92.40
10.42
ND
ND
81.98
5.75
<1
1.53
<2
7.28
<1
<10
<2
<1
<1
5.79
232
8.44
<0.1
0.136
5.19
1.243
16.01
1.37
-80.2
11/13/2014
92.40
8.89
ND
ND
83.51
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
22.8
5.97
<0.1
0.277
5.35
1.160
15.85
1.97
173.7
3/25/2015
92.40
4.86
ND
ND
87.54
<1
<1
<1
2.09
2.09
<1
<10
<2
<1
<1
<5
17.0
4.48
<0.1
0.210
5.86
1.102
10.69
5.58
163.8
6/25/2015
92.40
3.78
ND
ND
88.62
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
13.9
2.16
0.286
0.283
5.49
0.893
10.50
1.14
162.2
page 11 of 13
Table 1
Groundwater Monitoring and Analytical Data
Exxon Service Station #14489
285 Old Bayview Drive
North East, Maryland
Gauging Data
Analytical Data
Well ID
Date
Top of
Casing
Elevation
(feet)
Depth
to
Water
(feet)
Depth to
Hydrocarbon
(feet)
Hydrocarbon
Thickness
(feet)
Corrected
GW
Elevation
(feet)
Benzene
(µg/L)
Toluene
(µg/L)
Ethylbenzene
(µg/L)
Total
Xylenes
(µg/L)
5
1,000
700
MW-16
6/1/2005
90.30
7.42
ND
ND
82.88
<1
<1
<1
12/7/2005
90.30
6.12
ND
ND
84.18
<1
<1
5/24/2006
90.30
7.50
ND
ND
82.80
<1
11/7/2006
90.30
5.16
ND
ND
85.14
6/21/2007
90.30
8.50
ND
ND
12/11/2007
90.30
5.84
ND
3/24/2008
90.30
5.13
6/29/2008
90.30
8/14/2008
Field Parameters
Total
BTEX
(µg/L)
MTBE
(µg/L)
TBA
(µg/L)
DIPE
(µg/L)
10,000
--
20
--
--
<1
BRL
<1
<25
NA
<1
<1
BRL
<1
<25
NA
2.0
6.0
31.6
39.6
<1
<25
0.51 J
4.7
17.8
51.1
74.1 J
<1
81.80
<1
9.8
19.8
61.8
91.4
ND
84.46
<1
<1
1.0
3.3
ND
ND
85.17
<1
<1
<1
7.19
ND
ND
83.11
<1
<1
90.30
NM
NM
NM
NM
NS
11/20/2008
90.30
9.43
ND
ND
80.87
2/11/2009
90.30
6.05
ND
ND
4/21/2009
90.30
4.15
ND
ND
7/31/2009
90.30
6.50
ND
10/13/2009
90.30
5.15
10/27/2009
90.30
1/12/2010
ETBE
(µg/L)
TAME
(µg/L)
Naphthalene
(µg/L)
Sulfate
Total
Metals
--
--
NA
NA
0.65
--
2,600
NA
NS
NS
NA
NA
NA
NS
NS
NA
NA
NA
NA
NS
<25
NA
NA
NA
NA
<1
<25
NA
NA
NA
4.3
<1
<25
NA
NA
<1
BRL
<1
<25
NA
<1
<1
BRL
<1
<25
NS
NS
NS
NS
NS
<1
<1
<1
<1
BRL
84.25
86.15
<1
<1
<1
<1
<1
<1
<1
<1
ND
83.80
<1
<1
<1
ND
ND
85.15
NS
NS
3.95
ND
ND
86.35
<1
90.30
5.16
ND
ND
85.14
4/21/2010
90.30
4.96
ND
ND
7/22/2010
90.30
8.49
ND
11/23/2010
90.30
7.49
3/2/2011
90.30
5/19/2011
Nitrate/Nitrite
pH (s.u.)
Conductivity
(mS/cm)
Temperature (°C)
DO (mg/L)
--
--
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
--
--
--
--
--
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
--
--
--
--
--
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NS
NS
NS
NS
--
--
--
--
--
NA
NA
NA
NS
NS
NS
NS
--
--
--
--
--
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
BRL
0.54 J
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
NS
--
--
--
--
--
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
<1
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
85.34
<1
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
ND
81.81
<1
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
ND
ND
82.81
<1
<1
<1
<1
BRL
<1
<25
<5
<5
<5
<5
NS
NS
NS
NS
--
--
--
--
--
4.89
ND
ND
85.41
<1
<1
<1
<3
BRL
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
90.30
5.36
ND
ND
84.94
<1
<1
<1
<3
BRL
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
7/12/2011
90.30
8.84
ND
ND
81.46
<1
<1
<1
<3
BRL
<1
<20
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
10/24/2011
90.30
5.48
ND
ND
84.82
<1
<1
1.3
4.55
BRL
<1
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
2/8/2012
90.30
5.41
ND
ND
84.89
<1
<1
<1
<3
BRL
<1
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
5/22/2012
90.30
8.83
ND
ND
81.47
<1
<1
<1
<3
BRL
<1
<10
<1
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
8/14/2012
90.30
11.87
ND
ND
78.43
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
10/4/2012
90.30
10.99
ND
ND
79.31
<1
<1
1.09
<3
1.09
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
--
--
--
--
--
2/22/2013
90.30
5.70
ND
ND
84.60
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
5.39
0.351
11.38
4.57
298
5/1/2013
90.30
5.94
ND
ND
84.36
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
4.87
0.457
12.01
4.38
128.0
8/6/2013
90.30
4.56
ND
ND
85.74
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
4.99
0.207
15.87
1.96
155.3
10/3/2013
90.30
6.01
ND
ND
84.29
<1
<1
1.12
3.11
4.23
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
4.73
0.402
18.20
2.06
144.8
3/6/2014
90.30
4.83
ND
ND
85.47
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
5.39
0.215
11.43
6.06
212.6
6/12/2014
90.30
5.65
ND
ND
84.65
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
NS
NS
NS
NS
4.97
0.360
13.47
0.32
209.7
9/19/2014
90.30
10.90
ND
ND
79.40
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
21.5
1.18
<0.1
2.94
4.12
0.377
16.60
1.98
5.5
11/13/2014
90.30
8.55
ND
ND
81.75
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
17.8
2.97
<0.1
2.65
4.57
0.338
16.89
1.79
315.6
3/25/2015
90.30
5.22
ND
ND
85.08
<1
<1
<1
<2
BRL
<1
<10
<2
<1
<1
<5
7.46
2.32
<0.1
0.867
5.73
0.239
10.18
7.25
195
6/25/2015
90.30
5.07
ND
ND
85.23
<1
<1
<1
<3
BRL
<1
<10
<2
<1
<1
<5
15.6
2.92
0.390
2.47
4.61
0.395
11.81
2.48
185.5
Notes:
µg/L - micrograms/liter
ETBE - Ethyl Tertiary Butyl Ether
<5 - Not detected at or above the laboratory reporting limit, laboratory reporting limit included.
italic values - MDE Groundwater Clean-Up Standards
GW - Groundwater
NM - Not monitored
0.65 [1.63] - results from duplicate sample listed in brackets
J - Indicates an estimated value
NS - Not sampled
BRL - Below laboratory reporting limits
MTBE - Methyl Tert Butyl Ether
NSVD - Not surveyed to vertical datum
BTEX - Benzene, toluene, ethylbenzene, and total xylenes
NA - Not analyzed
TAME - Tertiary Amyl Methyl Ether
DIPE - Di-Isopropyl Ether
ND - Not detected
TBA - Tertiary Butyl Alcohol
page 12 of 13
Dissolved
Metals
ORP (mV) Comments
Well not located, not sampled
Table 1
Groundwater Monitoring and Analytical Data
Exxon Service Station #14489
285 Old Bayview Drive
North East, Maryland
Gauging Data
Well ID
INJ-1
INJ-2
INJ-3
Date
Top of
Casing
Elevation
(feet)
Depth
to
Water
(feet)
Depth to
Hydrocarbon
(feet)
Hydrocarbon
Thickness
(feet)
Corrected
GW
Elevation
(feet)
2/22/2013
100.49
6.52
ND
ND
93.97
5/1/2013
100.49
NM
ND
ND
NM
8/6/2013
100.49
NM
ND
ND
NM
10/3/2013
100.49
7.01
ND
ND
93.48
3/6/2014
100.49
3.63
ND
ND
96.86
6/12/2014
100.49
5.41
ND
ND
95.08
89.69
9/18/2014
100.49
10.80
ND
ND
11/13/2014
100.49
9.47
ND
ND
91.02
3/25/2015
100.49
4.19
ND
ND
96.30
6/25/2015
100.49
4.65
ND
ND
95.84
2/22/2013
101.50
4.60
ND
ND
96.90
5/1/2013
101.50
NM
ND
ND
NM
8/6/2013
101.50
NM
ND
ND
NM
10/3/2013
101.50
3.38
ND
ND
98.12
3/6/2014
101.50
3.04
ND
ND
98.46
6/12/2014
101.50
3.01
ND
ND
98.49
97.06
9/18/2014
101.50
4.44
ND
ND
11/13/2014
101.50
3.52
ND
ND
97.98
3/25/2015
101.50
2.95
ND
ND
98.55
6/25/2015
101.50
2.81
ND
ND
98.69
2/22/2013
100.49
4.10
ND
ND
96.39
5/1/2013
100.49
NM
ND
ND
NM
8/6/2013
100.49
NM
ND
ND
NM
10/3/2013
100.49
4.41
ND
ND
96.08
3/6/2014
100.49
3.57
ND
ND
96.92
6/12/2014
100.49
3.74
ND
ND
96.75
94.68
9/18/2014
100.49
5.81
ND
ND
11/13/2014
100.49
4.77
ND
ND
95.72
3/25/2015
100.49
3.70
ND
ND
96.79
6/25/2015
100.49
3.65
ND
ND
96.84
Notes:
ND - Not detected
NM - Not monitored
page 13 of 13
Figures
CITY:(Reqd) DIV/GROUP:(Reqd) DB:(Reqd) LD:(Opt) PIC:(Opt) PM:(Reqd) TM:(Opt) LYR:(Opt)ON=*;OFF=*REF*
G:\ENVCAD\BALTIMORE\ACT\B0085851\0010\00002\285 Old Bay View RD-Site-Loc.dwg
LAYOUT: 1 SAVED: 4/28/2011 1:20 PM ACADVER: 18.0S (LMS TECH) PAGESETUP: ---- PLOTSTYLETABLE: ACAD.CTB PLOTTED: 4/29/2011 10:57 AM BY: GOFORTH, JOHN
SITE
FORMER EXXON FACILITY # 14489
285 OLD BAY VIEW ROAD
NORTH EAST, MARYLAND
LOCAL AREA MAP
FIGURE
1
LEGEND:
147
991
P.W.-2
82.0
RESIDENCE
#281
196
90
AUTO
REPAIR
SHOP
FO
R
SP ME
E
N R
IS
LA SE
ND R
(94.78)
ABOVE GROUND
USED FUEL
TANK
FORMER
USED-OIL
TANK
FORMER
MOBILE
SERVICE
STATION
BUILDING
DI
153
(92.69)
2
BI
94
MW-1A
(91.73) MW-11
ME
MO
18.9
P.W.-3
728
RESIDENCE
#280
MW-8
(98.69)
(93.24)
GG
(94.78)
INJ-3
FORMER
DISPENSER
ISLAND
S
FORMER
GASOLINE
TANK PIT
(96.66)
MW-12
JO
SE
PH
9
OLD BAY VIE
W ROAD
53.2
1,500
714
MW-3A
INJ-2
(94.90)
MW-2A
94
DRIVEWAY
MW-5A
(93.18) (92.89)
191
92
INJ-1
RI
AL
(95.84)
90
MW-10
HW
(89.97)
Y
88
MW-13
(90.44)
86
MW-16
90
(85.23)
88
NOTE:
MW-14
86
(85.94)
(M
D
.R
MW-15
PROJECTNAME: ----
(88.62)
86
t. 2
74
)
FORMER EXXON FACILITY # 14489
285 OLD BAY VIEW ROAD
NORTH EAST, MARYLAND
8.86
GROUNDWATER ELEVATION CONTOURS
AND ANALYTICAL DATA
25 JUNE 2015
FIGURE
3
Appendix A
TestAmerica Laboratory
Analytical Reports (9 - 13 July
2015)
1
2
3
4
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: (615)726-0177
TestAmerica Job ID: 490-81527-1
Client Project/Site: 14489 - North East
For:
ARCADIS U.S., Inc.
1114 Benfield Blvd.
Suite A
Millersville, Maryland 21108
Attn: Mr. Rusty Kahl
Authorized for release by:
7/13/2015 12:26:50 PM
Heather Wagner, Project Manager I
(615)301-5763
[email protected]
Designee for
Jennifer Huckaba, Project Manager II
(615)301-5042
[email protected]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
5
6
7
8
9
10
11
12
13
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Table of Contents
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
1
3
1
2
3
4
5
6
36
58
63
68
69
70
74
4
5
6
7
8
9
10
11
12
13
Page 2 of 74
TestAmerica Nashville
7/13/2015
Sample Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
1
2
Lab Sample ID
490-81527-1
490-81527-2
490-81527-3
Client Sample ID
MW1A(062515)
MW2A(062515)
MW3A(062515)
Matrix
Ground Water
Ground Water
Ground Water
Collected
Received
06/25/15 12:45 06/26/15 08:45
06/25/15 11:20 06/26/15 08:45
06/25/15 10:40 06/26/15 08:45
490-81527-4
490-81527-5
490-81527-6
MW5A(062515)
MW8(062515)
MW10(062515)
Ground Water
Ground Water
Ground Water
06/25/15 14:15 06/26/15 08:45
06/25/15 09:30 06/26/15 08:45
06/25/15 13:05 06/26/15 08:45
490-81527-7
490-81527-8
490-81527-9
MW11(062515)
MW12(062515)
MW13(062515)
Ground Water
Ground Water
Ground Water
06/25/15 13:50 06/26/15 08:45
06/25/15 14:55 06/26/15 08:45
06/25/15 11:20 06/26/15 08:45
490-81527-10
490-81527-11
490-81527-12
MW14(062515)
MW15(062515)
MW16(062515)
Ground Water
Ground Water
Ground Water
06/25/15 10:20 06/26/15 08:45
06/25/15 09:35 06/26/15 08:45
06/25/15 15:10 06/26/15 08:45
490-81527-13
490-81527-14
490-81527-15
DUP01(062515)
RB01(062515)
TB01(062515)
Ground Water
Ground Water
Water
06/25/15 12:00 06/26/15 08:45
06/25/15 15:40 06/26/15 08:45
06/25/15 01:00 06/26/15 08:45
3
4
5
6
7
8
9
10
11
12
13
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Page 3 of 74
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Case Narrative
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
1
2
Job ID: 490-81527-1
3
Laboratory: TestAmerica Nashville
4
Narrative
5
Job Narrative
490-81527-1
6
Comments
No additional comments.
7
Receipt
The samples were received on 6/26/2015 8:45 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperatures of the 2 coolers at receipt time were 1.7º C and 2.0º C.
GC/MS VOA
Method(s) 8260B: The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for preparation
batch 260281 recovered outside control limits for the following analytes: Chloroethane.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
9
10
11
12
HPLC/IC
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
13
Metals
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
VOA Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Page 4 of 74
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TestAmerica Nashville
7/13/2015
Definitions/Glossary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Qualifiers
3
GC/MS VOA
Qualifier
F1
*
4
Qualifier Description
MS and/or MSD Recovery is outside acceptance limits.
RPD of the LCS and LCSD exceeds the control limits
5
Metals
Qualifier
4
1
6
Qualifier Description
MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not
applicable.
7
8
Glossary
Abbreviation
¤
%R
CFL
CNF
These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis
Percent Recovery
Contains Free Liquid
Contains no Free Liquid
DER
Dil Fac
DL, RA, RE, IN
DLC
MDA
EDL
Duplicate error ratio (normalized absolute difference)
Dilution Factor
Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
Decision level concentration
Minimum detectable activity
Estimated Detection Limit
MDC
MDL
ML
NC
ND
PQL
Minimum detectable concentration
Method Detection Limit
Minimum Level (Dioxin)
Not Calculated
Not detected at the reporting limit (or MDL or EDL if shown)
Practical Quantitation Limit
QC
RER
RL
RPD
TEF
TEQ
Quality Control
Relative error ratio
Reporting Limit or Requested Limit (Radiochemistry)
Relative Percent Difference, a measure of the relative difference between two points
Toxicity Equivalent Factor (Dioxin)
Toxicity Equivalent Quotient (Dioxin)
9
10
11
12
13
TestAmerica Nashville
Page 5 of 74
7/13/2015
Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW1A(062515)
Lab Sample ID: 490-81527-1
Date Collected: 06/25/15 12:45
Date Received: 06/26/15 08:45
Matrix: Ground Water
Bromobenzene
ND
RL
25.0
1.00
1.00
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
06/29/15 03:55
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
06/29/15 03:55
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
06/29/15 03:55
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND *
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
06/29/15 03:55
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
06/29/15 03:55
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
06/29/15 03:55
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
06/29/15 03:55
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 03:55
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 03:55
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 03:55
1
Diisopropyl ether
ND
2.00
20.0
1.00
ug/L
ug/L
ug/L
06/29/15 03:55
06/29/15 21:32
06/29/15 03:55
1
20
1
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
06/29/15 03:55
1
1
1
5.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
06/29/15 03:55
1
1
1
5.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
06/29/15 03:55
1
1
1
1.00
ug/L
06/29/15 03:55
1
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
1
1
ug/L
06/29/15 03:55
1
Benzene
Ethylbenzene
Result Qualifier
ND
53.2
714
Ethyl tert-butyl ether
ND
Hexachlorobutadiene
2-Hexanone
ND
ND
Isopropylbenzene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
sec-Butylbenzene
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
1
50.3
ND
ND
2.31
153
ND
111
8.92
12.8
Styrene
ND
1.00
1.00
Tert-amyl methyl ether
ND
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 03:55
06/29/15 03:55
06/29/15 03:55
Dil Fac
1
1
1
TestAmerica Nashville
Page 6 of 74
7/13/2015
5
6
7
8
9
10
11
12
13
Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW1A(062515)
Lab Sample ID: 490-81527-1
Date Collected: 06/25/15 12:45
Date Received: 06/26/15 08:45
Matrix: Ground Water
tert-Butylbenzene
ND
RL
10.0
1.00
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
06/29/15 03:55
1
1
1
1500
tert-Butyl alcohol (TBA)
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
1
Result Qualifier
14.3
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 03:55
06/29/15 03:55
Dil Fac
1
1
5
6
7
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
20.0
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 21:32
06/29/15 03:55
06/29/15 03:55
20
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
06/29/15 03:55
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 03:55
06/29/15 03:55
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 03:55
1
ND
1.00
20.0
ug/L
ug/L
06/29/15 03:55
06/29/15 21:32
1
20
12
13
Toluene
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene (Surr)
1280
375
20.0
ug/L
06/29/15 21:32
20
ND
1.00
ug/L
06/29/15 03:55
1
3180
60.0
ug/L
06/29/15 21:32
20
Analyzed
06/29/15 03:55
Dil Fac
1
06/29/15 21:32
06/29/15 03:55
20
1
%Recovery Qualifier
104
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
97
100
Limits
70 - 130
70 - 130
70 - 130
Prepared
Dibromofluoromethane (Surr)
101
70 - 130
06/29/15 21:32
20
1,2-Dichloroethane-d4 (Surr)
1,2-Dichloroethane-d4 (Surr)
106
99
70 - 130
70 - 130
06/29/15 03:55
06/29/15 21:32
1
20
Toluene-d8 (Surr)
97
70 - 130
06/29/15 03:55
1
Toluene-d8 (Surr)
100
70 - 130
06/29/15 21:32
20
Analyzed
07/03/15 21:49
Dil Fac
1
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
ND
RL
1.00
MDL Unit
mg/L
D
Prepared
Result Qualifier
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 14:11 07/02/15 11:33
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/29/15 16:40 07/01/15 18:24
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Method: 6010B - Metals (ICP)
Analyte
Iron
4.94
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
Result Qualifier
3.24
General Chemistry
Analyte
Nitrate/Nitrite
Result Qualifier
ND
Prepared
Analyzed
07/01/15 10:10
Dil Fac
1
TestAmerica Nashville
Page 7 of 74
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9
Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW2A(062515)
Lab Sample ID: 490-81527-2
Date Collected: 06/25/15 11:20
Date Received: 06/26/15 08:45
Matrix: Ground Water
Bromobenzene
ND
RL
25.0
1.00
1.00
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
06/29/15 04:21
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
06/29/15 04:21
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
06/29/15 04:21
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND *
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
06/29/15 04:21
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
06/29/15 04:21
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
06/29/15 04:21
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
06/29/15 04:21
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 04:21
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 04:21
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 04:21
1
Diisopropyl ether
ND
2.00
20.0
1.00
ug/L
ug/L
ug/L
06/29/15 04:21
06/29/15 21:58
06/29/15 04:21
1
20
1
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
06/29/15 04:21
1
1
1
5.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
06/29/15 04:21
1
1
1
5.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
06/29/15 04:21
1
1
1
1.00
ug/L
06/29/15 04:21
1
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
1
1
ug/L
06/29/15 04:21
1
Benzene
Ethylbenzene
Result Qualifier
ND
147
991
Ethyl tert-butyl ether
ND
Hexachlorobutadiene
2-Hexanone
ND
ND
Isopropylbenzene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
sec-Butylbenzene
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
1
33.0
ND
ND
82.0
196
ND
65.2
2.03
2.81
Styrene
ND
1.00
1.00
Tert-amyl methyl ether
ND
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 04:21
06/29/15 04:21
06/29/15 04:21
Dil Fac
1
1
1
TestAmerica Nashville
Page 8 of 74
7/13/2015
5
6
7
8
9
10
11
12
13
Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW2A(062515)
Lab Sample ID: 490-81527-2
Date Collected: 06/25/15 11:20
Date Received: 06/26/15 08:45
Matrix: Ground Water
tert-Butylbenzene
ND
RL
10.0
1.00
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
06/29/15 04:21
1
1
1
415
tert-Butyl alcohol (TBA)
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
1
Result Qualifier
31.5
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 04:21
06/29/15 04:21
Dil Fac
1
1
5
6
7
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
20.0
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 21:58
06/29/15 04:21
06/29/15 04:21
20
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
06/29/15 04:21
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 04:21
06/29/15 04:21
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 04:21
1
ND
1.00
20.0
ug/L
ug/L
06/29/15 04:21
06/29/15 21:58
1
20
12
13
Toluene
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Total
602
140
1.00
ug/L
06/29/15 04:21
1
ND
1.00
ug/L
06/29/15 04:21
1
2450
60.0
ug/L
06/29/15 21:58
20
Analyzed
06/29/15 04:21
Dil Fac
1
06/29/15 21:58
06/29/15 04:21
20
1
Surrogate
4-Bromofluorobenzene (Surr)
%Recovery Qualifier
101
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
98
97
Limits
70 - 130
70 - 130
70 - 130
Prepared
Dibromofluoromethane (Surr)
100
70 - 130
06/29/15 21:58
20
1,2-Dichloroethane-d4 (Surr)
1,2-Dichloroethane-d4 (Surr)
96
97
70 - 130
70 - 130
06/29/15 04:21
06/29/15 21:58
1
20
Toluene-d8 (Surr)
98
70 - 130
06/29/15 04:21
1
Toluene-d8 (Surr)
97
70 - 130
06/29/15 21:58
20
Analyzed
07/03/15 22:10
Dil Fac
20
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
9990
RL
20.0
MDL Unit
mg/L
D
Prepared
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 14:11 07/02/15 11:29
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/29/15 16:40 07/01/15 18:16
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Method: 6010B - Metals (ICP)
Analyte
Iron
Result Qualifier
11.6
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
Result Qualifier
1.46
General Chemistry
Analyte
Nitrate/Nitrite
Result Qualifier
ND
Prepared
Analyzed
07/01/15 10:12
Dil Fac
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW3A(062515)
Lab Sample ID: 490-81527-3
Date Collected: 06/25/15 10:40
Date Received: 06/26/15 08:45
Matrix: Ground Water
Bromobenzene
ND
RL
25.0
1.00
1.00
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 18:27
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 18:27
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 18:27
1
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
2.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
ND
ND
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
Benzene
Result Qualifier
ND
1.26
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
Dil Fac
1
1
1
1.75
5.00
10.0
1.00
Naphthalene
ND
5.00
ug/L
06/29/15 18:27
1
n-Butylbenzene
N-Propylbenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
1
1
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
Tert-amyl methyl ether
ND
1.00
ug/L
06/29/15 18:27
1
Methyl tert-butyl ether
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
1
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10
11
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13
Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW3A(062515)
Lab Sample ID: 490-81527-3
Date Collected: 06/25/15 10:40
Date Received: 06/26/15 08:45
Matrix: Ground Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
tert-Butyl alcohol (TBA)
tert-Butylbenzene
1
Result Qualifier
ND
ND
RL
10.0
1.00
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 18:27
06/29/15 18:27
Dil Fac
1
1
5
6
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
06/29/15 18:27
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 18:27
1
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 18:27
06/29/15 18:27
1
1
12
1,3,5-Trimethylbenzene
ND
1.00
ug/L
06/29/15 18:27
1
Vinyl chloride
ND
1.00
ug/L
06/29/15 18:27
1
13
Xylenes, Total
ND
3.00
ug/L
06/29/15 18:27
1
Analyzed
06/29/15 18:27
Dil Fac
1
06/29/15 18:27
06/29/15 18:27
1
1
06/29/15 18:27
1
Analyzed
07/03/15 22:31
Dil Fac
1
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
%Recovery Qualifier
97
100
100
Limits
70 - 130
70 - 130
70 - 130
97
70 - 130
Prepared
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
RL
1.00
MDL Unit
mg/L
D
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 14:11 07/02/15 11:24
Dil Fac
1
Result Qualifier
ND
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/29/15 16:40 07/01/15 18:20
Dil Fac
1
Result Qualifier
RL
0.100
MDL Unit
mg/L
D
116
Prepared
Method: 6010B - Metals (ICP)
Analyte
Iron
Result Qualifier
0.736
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
General Chemistry
Analyte
Nitrate/Nitrite
0.722
Prepared
Analyzed
07/01/15 10:13
Dil Fac
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW5A(062515)
Lab Sample ID: 490-81527-4
Date Collected: 06/25/15 14:15
Date Received: 06/26/15 08:45
Matrix: Ground Water
Bromobenzene
ND
RL
25.0
1.00
1.00
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND *
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 05:14
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 05:14
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 05:14
1
Diisopropyl ether
ND
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 22:52
06/29/15 05:14
1
10
1
92.3
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
1
1
1
ND
ND
ND
5.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
1
1
1
Naphthalene
191
n-Butylbenzene
ND
5.00
1.00
10.0
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 22:52
1
1
10
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
1
1
1
ug/L
06/29/15 05:14
1
Benzene
Ethylbenzene
Result Qualifier
ND
18.9
728
Ethyl tert-butyl ether
ND
Hexachlorobutadiene
2-Hexanone
ND
ND
Isopropylbenzene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
N-Propylbenzene
p-Isopropyltoluene
sec-Butylbenzene
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
1
293
13.5
23.2
Styrene
ND
1.00
1.00
1.00
Tert-amyl methyl ether
ND
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
Dil Fac
1
1
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW5A(062515)
Lab Sample ID: 490-81527-4
Date Collected: 06/25/15 14:15
Date Received: 06/26/15 08:45
Matrix: Ground Water
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
tert-Butyl alcohol (TBA)
tert-Butylbenzene
1
Result Qualifier
ND
ND
RL
10.0
1.00
MDL Unit
ug/L
ug/L
ND
ND
ND
1.00
1.00
1.00
139
D
Prepared
Analyzed
06/29/15 05:14
06/29/15 05:14
Dil Fac
1
1
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
1
1
1
5
6
7
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
1
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
06/29/15 05:14
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 05:14
06/29/15 05:14
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 05:14
1
ND
1.00
10.0
ug/L
ug/L
06/29/15 05:14
06/29/15 22:52
1
10
12
13
Toluene
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene (Surr)
1700
458
10.0
ug/L
06/29/15 22:52
10
ND
1.00
ug/L
06/29/15 05:14
1
1900
30.0
ug/L
06/29/15 22:52
10
Analyzed
06/29/15 05:14
Dil Fac
1
06/29/15 22:52
06/29/15 05:14
10
1
%Recovery Qualifier
104
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
100
100
Limits
70 - 130
70 - 130
70 - 130
Prepared
Dibromofluoromethane (Surr)
101
70 - 130
06/29/15 22:52
10
1,2-Dichloroethane-d4 (Surr)
1,2-Dichloroethane-d4 (Surr)
111
102
70 - 130
70 - 130
06/29/15 05:14
06/29/15 22:52
1
10
Toluene-d8 (Surr)
98
70 - 130
06/29/15 05:14
1
Toluene-d8 (Surr)
98
70 - 130
06/29/15 22:52
10
Analyzed
07/07/15 03:46
Dil Fac
1
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
ND
RL
1.00
MDL Unit
mg/L
D
Prepared
Result Qualifier
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 14:11 07/02/15 11:01
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/29/15 16:40 07/01/15 18:29
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Method: 6010B - Metals (ICP)
Analyte
Iron
17.8
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
Result Qualifier
9.50
General Chemistry
Analyte
Nitrate/Nitrite
Result Qualifier
0.310
Prepared
Analyzed
07/01/15 10:14
Dil Fac
1
TestAmerica Nashville
Page 13 of 74
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW8(062515)
Lab Sample ID: 490-81527-5
Date Collected: 06/25/15 09:30
Date Received: 06/26/15 08:45
Matrix: Ground Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
Benzene
Bromobenzene
1
Result Qualifier
ND
ND
ND
RL
25.0
1.00
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
Dil Fac
1
1
1
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 18:54
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 18:54
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 18:54
1
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
2.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
ND
ND
ND
5.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
Naphthalene
n-Butylbenzene
N-Propylbenzene
ND
ND
ND
5.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
Tert-amyl methyl ether
ND
1.00
ug/L
06/29/15 18:54
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW8(062515)
Lab Sample ID: 490-81527-5
Date Collected: 06/25/15 09:30
Date Received: 06/26/15 08:45
Matrix: Ground Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
tert-Butyl alcohol (TBA)
tert-Butylbenzene
1
Result Qualifier
ND
ND
RL
10.0
1.00
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 18:54
06/29/15 18:54
Dil Fac
1
1
5
6
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
06/29/15 18:54
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 18:54
1
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 18:54
06/29/15 18:54
1
1
12
1,3,5-Trimethylbenzene
ND
1.00
ug/L
06/29/15 18:54
1
Vinyl chloride
ND
1.00
ug/L
06/29/15 18:54
1
13
Xylenes, Total
ND
3.00
ug/L
06/29/15 18:54
1
Analyzed
06/29/15 18:54
Dil Fac
1
06/29/15 18:54
06/29/15 18:54
1
1
06/29/15 18:54
1
Analyzed
07/03/15 23:13
Dil Fac
1
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
%Recovery Qualifier
98
101
101
Limits
70 - 130
70 - 130
70 - 130
97
70 - 130
Prepared
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
RL
1.00
MDL Unit
mg/L
D
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 14:11 07/02/15 11:59
Dil Fac
1
Result Qualifier
ND
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/29/15 16:40 07/01/15 16:26
Dil Fac
1
Result Qualifier
RL
0.100
MDL Unit
mg/L
D
60.6
Prepared
Method: 6010B - Metals (ICP)
Analyte
Iron
Result Qualifier
ND
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
General Chemistry
Analyte
Nitrate/Nitrite
1.48
Prepared
Analyzed
07/01/15 10:15
Dil Fac
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW10(062515)
Lab Sample ID: 490-81527-6
Date Collected: 06/25/15 13:05
Date Received: 06/26/15 08:45
Matrix: Ground Water
Result Qualifier
ND
ND
ND
RL
25.0
1.00
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
Dil Fac
1
1
1
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 19:20
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 19:20
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 19:20
1
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
2.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
ND
ND
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
2.94
5.00
10.0
1.00
Naphthalene
ND
5.00
ug/L
06/29/15 19:20
1
n-Butylbenzene
N-Propylbenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
1
1
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
Tert-amyl methyl ether
ND
1.00
ug/L
06/29/15 19:20
1
Methyl tert-butyl ether
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
Benzene
Bromobenzene
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW10(062515)
Lab Sample ID: 490-81527-6
Date Collected: 06/25/15 13:05
Date Received: 06/26/15 08:45
Matrix: Ground Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
tert-Butyl alcohol (TBA)
tert-Butylbenzene
1
Result Qualifier
ND
ND
RL
10.0
1.00
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 19:20
06/29/15 19:20
Dil Fac
1
1
5
6
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
06/29/15 19:20
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 19:20
1
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 19:20
06/29/15 19:20
1
1
12
1,3,5-Trimethylbenzene
ND
1.00
ug/L
06/29/15 19:20
1
Vinyl chloride
ND
1.00
ug/L
06/29/15 19:20
1
13
Xylenes, Total
ND
3.00
ug/L
06/29/15 19:20
1
Analyzed
06/29/15 19:20
Dil Fac
1
06/29/15 19:20
06/29/15 19:20
1
1
06/29/15 19:20
1
Analyzed
07/03/15 23:34
Dil Fac
10
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
%Recovery Qualifier
98
101
101
Limits
70 - 130
70 - 130
70 - 130
98
70 - 130
Prepared
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
21.9
RL
10.0
MDL Unit
mg/L
D
Prepared
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 16:07 07/02/15 15:09
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/30/15 16:23 07/01/15 17:49
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Method: 6010B - Metals (ICP)
Analyte
Iron
Result Qualifier
1.40
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
Result Qualifier
0.595
General Chemistry
Analyte
Nitrate/Nitrite
Result Qualifier
0.121
Prepared
Analyzed
07/01/15 10:16
Dil Fac
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW11(062515)
Lab Sample ID: 490-81527-7
Date Collected: 06/25/15 13:50
Date Received: 06/26/15 08:45
Matrix: Ground Water
Bromobenzene
ND
RL
25.0
1.00
1.00
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 19:47
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 19:47
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 19:47
1
Diisopropyl ether
ND
2.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
5.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
Benzene
Ethylbenzene
Result Qualifier
ND
1.09
12.9
Ethyl tert-butyl ether
ND
Hexachlorobutadiene
2-Hexanone
ND
ND
Isopropylbenzene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
2.65
ND
ND
3.87
8.86
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
Dil Fac
1
1
1
3.83
5.00
1.00
1.00
p-Isopropyltoluene
ND
1.00
ug/L
06/29/15 19:47
1
sec-Butylbenzene
Styrene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
1
1
Tert-amyl methyl ether
ND
1.00
ug/L
06/29/15 19:47
1
n-Butylbenzene
N-Propylbenzene
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
1
ND
TestAmerica Nashville
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13
Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW11(062515)
Lab Sample ID: 490-81527-7
Date Collected: 06/25/15 13:50
Date Received: 06/26/15 08:45
Matrix: Ground Water
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
tert-Butyl alcohol (TBA)
tert-Butylbenzene
1
Result Qualifier
ND
ND
RL
10.0
1.00
MDL Unit
ug/L
ug/L
ND
ND
ND
1.00
1.00
1.00
1.36
D
Prepared
Analyzed
06/29/15 19:47
06/29/15 19:47
Dil Fac
1
1
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
5
6
7
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
06/29/15 19:47
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 19:47
1
ND
1.00
1.00
ug/L
ug/L
06/29/15 19:47
06/29/15 19:47
1
1
12
13
Toluene
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
22.6
2.52
1.00
ug/L
06/29/15 19:47
1
ND
1.00
ug/L
06/29/15 19:47
1
15.6
3.00
ug/L
06/29/15 19:47
1
Analyzed
06/29/15 19:47
Dil Fac
1
06/29/15 19:47
06/29/15 19:47
1
1
06/29/15 19:47
1
Analyzed
07/03/15 23:55
Dil Fac
1
%Recovery Qualifier
98
101
99
Limits
70 - 130
70 - 130
70 - 130
97
70 - 130
Prepared
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
6.85
RL
1.00
MDL Unit
mg/L
D
Prepared
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 16:07 07/02/15 15:14
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/30/15 16:23 07/01/15 17:53
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Method: 6010B - Metals (ICP)
Analyte
Iron
Result Qualifier
10.1
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
Result Qualifier
3.57
General Chemistry
Analyte
Nitrate/Nitrite
Result Qualifier
2.26
Prepared
Analyzed
07/01/15 10:17
Dil Fac
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW12(062515)
Lab Sample ID: 490-81527-8
Date Collected: 06/25/15 14:55
Date Received: 06/26/15 08:45
Matrix: Ground Water
Result Qualifier
ND
ND
ND
RL
25.0
1.00
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
Dil Fac
1
1
1
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND *
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 06:59
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 06:59
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 06:59
1
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
2.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
Hexachlorobutadiene
2-Hexanone
ND
ND
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
5.87
5.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
ND
ND
ND
5.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
1.38
1.00
ug/L
06/29/15 06:59
1
Isopropylbenzene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
Tert-amyl methyl ether
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
Benzene
Bromobenzene
1
3.68
ND
ND
4.19
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13
Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW12(062515)
Lab Sample ID: 490-81527-8
Date Collected: 06/25/15 14:55
Date Received: 06/26/15 08:45
Matrix: Ground Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
tert-Butyl alcohol (TBA)
tert-Butylbenzene
1
Result Qualifier
ND
ND
RL
10.0
1.00
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 06:59
06/29/15 06:59
Dil Fac
1
1
5
6
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
06/29/15 06:59
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 06:59
1
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 06:59
06/29/15 06:59
1
1
12
1,3,5-Trimethylbenzene
ND
1.00
ug/L
06/29/15 06:59
1
Vinyl chloride
ND
1.00
ug/L
06/29/15 06:59
1
13
Xylenes, Total
ND
3.00
ug/L
06/29/15 06:59
1
Analyzed
06/29/15 06:59
Dil Fac
1
06/29/15 06:59
06/29/15 06:59
1
1
06/29/15 06:59
1
Analyzed
07/04/15 00:58
Dil Fac
1
Surrogate
4-Bromofluorobenzene (Surr)
%Recovery Qualifier
99
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
99
97
Limits
70 - 130
70 - 130
70 - 130
Toluene-d8 (Surr)
98
70 - 130
Prepared
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
19.5
RL
1.00
MDL Unit
mg/L
D
Prepared
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 16:07 07/02/15 15:28
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/30/15 16:23 07/01/15 17:58
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Method: 6010B - Metals (ICP)
Analyte
Iron
Result Qualifier
1.78
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
Result Qualifier
0.265
General Chemistry
Analyte
Nitrate/Nitrite
Result Qualifier
0.171
Prepared
Analyzed
07/01/15 10:18
Dil Fac
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW13(062515)
Lab Sample ID: 490-81527-9
Date Collected: 06/25/15 11:20
Date Received: 06/26/15 08:45
Matrix: Ground Water
Result Qualifier
ND
ND
ND
RL
25.0
1.00
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
Dil Fac
1
1
1
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND *
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 07:26
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 07:26
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 07:26
1
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
2.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
ND
ND
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
8.19
5.00
10.0
1.00
Naphthalene
ND
5.00
ug/L
06/29/15 07:26
1
n-Butylbenzene
N-Propylbenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
1
1
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
Tert-amyl methyl ether
ND
1.00
ug/L
06/29/15 07:26
1
Methyl tert-butyl ether
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
Benzene
Bromobenzene
1
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Page 22 of 74
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW13(062515)
Lab Sample ID: 490-81527-9
Date Collected: 06/25/15 11:20
Date Received: 06/26/15 08:45
Matrix: Ground Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
1
Result Qualifier
tert-Butylbenzene
ND
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
06/29/15 07:26
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 07:26
1
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 07:26
06/29/15 07:26
1
1
12
1,3,5-Trimethylbenzene
ND
1.00
ug/L
06/29/15 07:26
1
Vinyl chloride
ND
1.00
ug/L
06/29/15 07:26
1
13
Xylenes, Total
ND
3.00
ug/L
06/29/15 07:26
1
Analyzed
06/29/15 07:26
Dil Fac
1
06/29/15 07:26
06/29/15 07:26
1
1
06/29/15 07:26
1
Analyzed
07/04/15 01:19
Dil Fac
5
28.6
Surrogate
4-Bromofluorobenzene (Surr)
%Recovery Qualifier
99
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
99
97
Limits
70 - 130
70 - 130
70 - 130
Toluene-d8 (Surr)
98
70 - 130
MDL Unit
ug/L
ug/L
D
Prepared
Prepared
Analyzed
06/29/15 07:26
06/29/15 07:26
Dil Fac
1
1
5
RL
10.0
1.00
tert-Butyl alcohol (TBA)
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
14.5
RL
5.00
MDL Unit
mg/L
D
Prepared
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 16:07 07/02/15 15:32
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/30/15 16:23 07/01/15 18:02
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Method: 6010B - Metals (ICP)
Analyte
Iron
Result Qualifier
3.56
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
Result Qualifier
0.606
General Chemistry
Analyte
Nitrate/Nitrite
Result Qualifier
0.101
Prepared
Analyzed
07/01/15 10:19
Dil Fac
1
TestAmerica Nashville
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW14(062515)
Lab Sample ID: 490-81527-10
Date Collected: 06/25/15 10:20
Date Received: 06/26/15 08:45
Matrix: Ground Water
Result Qualifier
ND
ND
ND
RL
25.0
1.00
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
Dil Fac
1
1
1
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND *
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 07:52
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 07:52
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 07:52
1
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
2.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
ND
ND
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
1.11
5.00
10.0
1.00
Naphthalene
ND
5.00
ug/L
06/29/15 07:52
1
n-Butylbenzene
N-Propylbenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
1
1
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
Tert-amyl methyl ether
ND
1.00
ug/L
06/29/15 07:52
1
Methyl tert-butyl ether
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
Benzene
Bromobenzene
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW14(062515)
Lab Sample ID: 490-81527-10
Date Collected: 06/25/15 10:20
Date Received: 06/26/15 08:45
Matrix: Ground Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
tert-Butyl alcohol (TBA)
tert-Butylbenzene
1
Result Qualifier
ND
ND
RL
10.0
1.00
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 07:52
06/29/15 07:52
Dil Fac
1
1
5
6
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
06/29/15 07:52
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 07:52
1
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 07:52
06/29/15 07:52
1
1
12
1,3,5-Trimethylbenzene
ND
1.00
ug/L
06/29/15 07:52
1
Vinyl chloride
ND
1.00
ug/L
06/29/15 07:52
1
13
Xylenes, Total
ND
3.00
ug/L
06/29/15 07:52
1
Analyzed
06/29/15 07:52
Dil Fac
1
06/29/15 07:52
06/29/15 07:52
1
1
06/29/15 07:52
1
Analyzed
07/04/15 01:41
Dil Fac
20
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
%Recovery Qualifier
101
100
98
Limits
70 - 130
70 - 130
70 - 130
97
70 - 130
Prepared
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
8850
RL
20.0
MDL Unit
mg/L
D
Prepared
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 16:07 07/02/15 15:36
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/30/15 16:23 07/01/15 18:06
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Method: 6010B - Metals (ICP)
Analyte
Iron
Result Qualifier
8.73
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
Result Qualifier
1.10
General Chemistry
Analyte
Nitrate/Nitrite
Result Qualifier
0.287
Prepared
Analyzed
07/01/15 10:20
Dil Fac
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW15(062515)
Lab Sample ID: 490-81527-11
Date Collected: 06/25/15 09:35
Date Received: 06/26/15 08:45
Matrix: Ground Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
Benzene
Bromobenzene
1
Result Qualifier
ND
ND
ND
RL
25.0
1.00
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
Dil Fac
1
1
1
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND *
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 08:19
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 08:19
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 08:19
1
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
2.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
ND
ND
ND
5.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
Naphthalene
n-Butylbenzene
N-Propylbenzene
ND
ND
ND
5.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
Tert-amyl methyl ether
ND
1.00
ug/L
06/29/15 08:19
1
TestAmerica Nashville
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW15(062515)
Lab Sample ID: 490-81527-11
Date Collected: 06/25/15 09:35
Date Received: 06/26/15 08:45
Matrix: Ground Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
tert-Butyl alcohol (TBA)
tert-Butylbenzene
1
Result Qualifier
ND
ND
RL
10.0
1.00
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 08:19
06/29/15 08:19
Dil Fac
1
1
5
6
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
06/29/15 08:19
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 08:19
1
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 08:19
06/29/15 08:19
1
1
12
1,3,5-Trimethylbenzene
ND
1.00
ug/L
06/29/15 08:19
1
Vinyl chloride
ND
1.00
ug/L
06/29/15 08:19
1
13
Xylenes, Total
ND
3.00
ug/L
06/29/15 08:19
1
Analyzed
06/29/15 08:19
Dil Fac
1
06/29/15 08:19
06/29/15 08:19
1
1
06/29/15 08:19
1
Analyzed
07/04/15 02:44
Dil Fac
1
Surrogate
4-Bromofluorobenzene (Surr)
%Recovery Qualifier
100
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
99
98
Limits
70 - 130
70 - 130
70 - 130
Toluene-d8 (Surr)
97
70 - 130
Prepared
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
13.9
RL
1.00
MDL Unit
mg/L
D
Prepared
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 16:07 07/02/15 15:40
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/30/15 16:23 07/01/15 18:11
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Method: 6010B - Metals (ICP)
Analyte
Iron
Result Qualifier
2.16
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
Result Qualifier
0.286
General Chemistry
Analyte
Nitrate/Nitrite
Result Qualifier
0.283
Prepared
Analyzed
07/01/15 10:22
Dil Fac
1
TestAmerica Nashville
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW16(062515)
Lab Sample ID: 490-81527-12
Date Collected: 06/25/15 15:10
Date Received: 06/26/15 08:45
Matrix: Ground Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
Benzene
Bromobenzene
1
Result Qualifier
ND
ND
ND
RL
25.0
1.00
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
Dil Fac
1
1
1
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND *
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 08:45
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 08:45
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 08:45
1
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
2.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
ND
ND
ND
5.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
Naphthalene
n-Butylbenzene
N-Propylbenzene
ND
ND
ND
5.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
Tert-amyl methyl ether
ND
1.00
ug/L
06/29/15 08:45
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW16(062515)
Lab Sample ID: 490-81527-12
Date Collected: 06/25/15 15:10
Date Received: 06/26/15 08:45
Matrix: Ground Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
tert-Butyl alcohol (TBA)
tert-Butylbenzene
1
Result Qualifier
ND
ND
RL
10.0
1.00
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 08:45
06/29/15 08:45
Dil Fac
1
1
5
6
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
06/29/15 08:45
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 08:45
1
ND
1.00
1.00
ug/L
ug/L
06/29/15 08:45
06/29/15 08:45
1
1
12
1.14
1,3,5-Trimethylbenzene
ND
1.00
ug/L
06/29/15 08:45
1
Vinyl chloride
ND
1.00
ug/L
06/29/15 08:45
1
13
Xylenes, Total
ND
3.00
ug/L
06/29/15 08:45
1
Analyzed
06/29/15 08:45
Dil Fac
1
06/29/15 08:45
06/29/15 08:45
1
1
06/29/15 08:45
1
Analyzed
07/04/15 03:05
Dil Fac
1
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
%Recovery Qualifier
101
100
97
Limits
70 - 130
70 - 130
70 - 130
97
70 - 130
Prepared
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
15.6
RL
1.00
MDL Unit
mg/L
D
Prepared
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 16:07 07/02/15 15:45
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/30/15 16:23 07/01/15 18:15
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Method: 6010B - Metals (ICP)
Analyte
Iron
Result Qualifier
2.92
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
Result Qualifier
0.390
General Chemistry
Analyte
Nitrate/Nitrite
Result Qualifier
2.47
Prepared
Analyzed
07/01/15 10:24
Dil Fac
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: DUP01(062515)
Lab Sample ID: 490-81527-13
Date Collected: 06/25/15 12:00
Date Received: 06/26/15 08:45
Matrix: Ground Water
Bromobenzene
ND
RL
25.0
1.00
1.00
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
06/29/15 09:12
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
06/29/15 09:12
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
06/29/15 09:12
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND *
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
06/29/15 09:12
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
06/29/15 09:12
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
06/29/15 09:12
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
06/29/15 09:12
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 09:12
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 09:12
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 09:12
1
Diisopropyl ether
ND
2.00
20.0
1.00
ug/L
ug/L
ug/L
06/29/15 09:12
06/29/15 22:25
06/29/15 09:12
1
20
1
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
06/29/15 09:12
1
1
1
5.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
06/29/15 09:12
1
1
1
5.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
06/29/15 09:12
1
1
1
1.00
ug/L
06/29/15 09:12
1
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
1
1
ug/L
06/29/15 09:12
1
Benzene
Ethylbenzene
Result Qualifier
ND
54.4
724
Ethyl tert-butyl ether
ND
Hexachlorobutadiene
2-Hexanone
ND
ND
Isopropylbenzene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
sec-Butylbenzene
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
1
50.4
ND
ND
2.35
157
ND
109
8.28
11.9
Styrene
ND
1.00
1.00
Tert-amyl methyl ether
ND
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 09:12
06/29/15 09:12
06/29/15 09:12
Dil Fac
1
1
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: DUP01(062515)
Lab Sample ID: 490-81527-13
Date Collected: 06/25/15 12:00
Date Received: 06/26/15 08:45
Matrix: Ground Water
tert-Butylbenzene
ND
RL
10.0
1.00
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
06/29/15 09:12
1
1
1
1510
tert-Butyl alcohol (TBA)
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
1
Result Qualifier
12.6
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 09:12
06/29/15 09:12
Dil Fac
1
1
5
6
7
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
20.0
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 22:25
06/29/15 09:12
06/29/15 09:12
20
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
06/29/15 09:12
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 09:12
06/29/15 09:12
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 09:12
1
ND
1.00
20.0
ug/L
ug/L
06/29/15 09:12
06/29/15 22:25
1
20
12
13
Toluene
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene (Surr)
1300
380
20.0
ug/L
06/29/15 22:25
20
ND
1.00
ug/L
06/29/15 09:12
1
3240
60.0
ug/L
06/29/15 22:25
20
Analyzed
06/29/15 09:12
Dil Fac
1
06/29/15 22:25
06/29/15 09:12
20
1
98
101
Limits
70 - 130
70 - 130
70 - 130
Dibromofluoromethane (Surr)
98
70 - 130
06/29/15 22:25
20
1,2-Dichloroethane-d4 (Surr)
1,2-Dichloroethane-d4 (Surr)
106
98
70 - 130
70 - 130
06/29/15 09:12
06/29/15 22:25
1
20
Toluene-d8 (Surr)
98
70 - 130
06/29/15 09:12
1
Toluene-d8 (Surr)
97
70 - 130
06/29/15 22:25
20
Analyzed
07/04/15 03:26
Dil Fac
1
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
%Recovery Qualifier
103
Prepared
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
ND
RL
1.00
MDL Unit
mg/L
D
Prepared
Result Qualifier
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 16:07 07/02/15 15:49
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/30/15 16:23 07/01/15 18:19
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Method: 6010B - Metals (ICP)
Analyte
Iron
5.43
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
Result Qualifier
2.43
General Chemistry
Analyte
Nitrate/Nitrite
Result Qualifier
ND
Prepared
Analyzed
07/01/15 10:25
Dil Fac
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: RB01(062515)
Lab Sample ID: 490-81527-14
Date Collected: 06/25/15 15:40
Date Received: 06/26/15 08:45
Matrix: Ground Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
Benzene
Bromobenzene
1
Result Qualifier
ND
ND
ND
RL
25.0
1.00
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
Dil Fac
1
1
1
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 20:13
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 20:13
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 20:13
1
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
2.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
ND
ND
ND
5.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
Naphthalene
n-Butylbenzene
N-Propylbenzene
ND
ND
ND
5.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
Tert-amyl methyl ether
ND
1.00
ug/L
06/29/15 20:13
1
TestAmerica Nashville
Page 32 of 74
7/13/2015
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13
Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: RB01(062515)
Lab Sample ID: 490-81527-14
Date Collected: 06/25/15 15:40
Date Received: 06/26/15 08:45
Matrix: Ground Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
tert-Butyl alcohol (TBA)
tert-Butylbenzene
1
Result Qualifier
ND
ND
RL
10.0
1.00
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 20:13
06/29/15 20:13
Dil Fac
1
1
5
6
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
06/29/15 20:13
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 20:13
1
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 20:13
06/29/15 20:13
1
1
12
1,3,5-Trimethylbenzene
ND
1.00
ug/L
06/29/15 20:13
1
Vinyl chloride
ND
1.00
ug/L
06/29/15 20:13
1
13
Xylenes, Total
ND
3.00
ug/L
06/29/15 20:13
1
Analyzed
06/29/15 20:13
Dil Fac
1
06/29/15 20:13
06/29/15 20:13
1
1
06/29/15 20:13
1
Analyzed
07/07/15 04:07
Dil Fac
1
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
%Recovery Qualifier
99
101
98
Limits
70 - 130
70 - 130
70 - 130
97
70 - 130
Prepared
Method: 9056A - Anions, Ion Chromatography
Analyte
Sulfate
Result Qualifier
ND
RL
1.00
MDL Unit
mg/L
D
Prepared
Result Qualifier
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
07/01/15 16:07 07/02/15 15:53
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/30/15 16:23 07/01/15 18:23
Dil Fac
1
RL
0.100
MDL Unit
mg/L
D
Method: 6010B - Metals (ICP)
Analyte
Iron
0.115
Method: 6010B - Metals (ICP) - Dissolved
Analyte
Iron
Result Qualifier
0.107
General Chemistry
Analyte
Nitrate/Nitrite
Result Qualifier
0.114
Prepared
Analyzed
07/01/15 10:26
Dil Fac
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: TB01(062515)
Lab Sample ID: 490-81527-15
Date Collected: 06/25/15 01:00
Date Received: 06/26/15 08:45
Matrix: Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS)
Analyte
Acetone
Benzene
Bromobenzene
1
Result Qualifier
ND
ND
ND
RL
25.0
1.00
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
Dil Fac
1
1
1
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
1
1
1,1-Dichloroethane
ND
1.00
ug/L
06/29/15 16:15
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 16:15
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
1
1
1,1-Dichloropropene
ND
1.00
ug/L
06/29/15 16:15
1
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
2.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
ND
ND
ND
5.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
Naphthalene
n-Butylbenzene
N-Propylbenzene
ND
ND
ND
5.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
Tert-amyl methyl ether
ND
1.00
ug/L
06/29/15 16:15
1
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: TB01(062515)
Lab Sample ID: 490-81527-15
Date Collected: 06/25/15 01:00
Date Received: 06/26/15 08:45
Matrix: Water
3
4
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
tert-Butyl alcohol (TBA)
tert-Butylbenzene
1
Result Qualifier
ND
ND
RL
10.0
1.00
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 16:15
06/29/15 16:15
Dil Fac
1
1
5
6
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
06/29/15 16:15
1
1
1
10
1,1,2-Trichloroethane
Trichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
1
1
11
Trichlorofluoromethane
ND
1.00
ug/L
06/29/15 16:15
1
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 16:15
06/29/15 16:15
1
1
12
1,3,5-Trimethylbenzene
ND
1.00
ug/L
06/29/15 16:15
1
Vinyl chloride
ND
1.00
ug/L
06/29/15 16:15
1
13
Xylenes, Total
ND
3.00
ug/L
06/29/15 16:15
1
Analyzed
06/29/15 16:15
Dil Fac
1
06/29/15 16:15
06/29/15 16:15
1
1
06/29/15 16:15
1
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
%Recovery Qualifier
98
101
101
Limits
70 - 130
70 - 130
70 - 130
97
70 - 130
Prepared
TestAmerica Nashville
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QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS)
3
Lab Sample ID: MB 490-260281/8
Matrix: Water
Analysis Batch: 260281
Analyte
Acetone
Benzene
Bromobenzene
1
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Result Qualifier
ND
ND
ND
4
5
RL
25.0
1.00
1.00
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
Dil Fac
1
1
1
6
7
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
Carbon tetrachloride
ND
1.00
ug/L
06/29/15 03:28
1
Chlorobenzene
Chlorodibromomethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
1
1
11
Chloroethane
ND
1.00
ug/L
06/29/15 03:28
1
Chloroform
Chloromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
1
1
12
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
2.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
ND
ND
ND
5.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
Naphthalene
n-Butylbenzene
N-Propylbenzene
ND
ND
ND
5.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
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QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: MB 490-260281/8
Matrix: Water
Analysis Batch: 260281
Client Sample ID: Method Blank
Prep Type: Total/NA
RL
1.00
MDL Unit
ug/L
D
Prepared
Analyzed
06/29/15 03:28
Dil Fac
1
6
7
tert-Butyl alcohol (TBA)
tert-Butylbenzene
ND
ND
10.0
1.00
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
1
1
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
1,2,3-Trichlorobenzene
ND
1.00
ug/L
06/29/15 03:28
1
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
1
1
1,1,2-Trichloroethane
ND
1.00
ug/L
06/29/15 03:28
1
Trichloroethene
Trichlorofluoromethane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
1
1
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
06/29/15 03:28
1
1
1
Vinyl chloride
Xylenes, Total
ND
ND
1.00
3.00
ug/L
ug/L
06/29/15 03:28
06/29/15 03:28
1
1
Analyzed
06/29/15 03:28
06/29/15 03:28
Dil Fac
1
1
MB MB
%Recovery Qualifier
98
101
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
Limits
70 - 130
70 - 130
Prepared
101
70 - 130
06/29/15 03:28
1
98
70 - 130
06/29/15 03:28
1
Lab Sample ID: LCS 490-260281/3
Matrix: Water
Analysis Batch: 260281
Analyte
Acetone
Benzene
Bromobenzene
4
5
MB MB
Result Qualifier
ND
Analyte
Tert-amyl methyl ether
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
250
50.0
50.0
LCS LCS
Result Qualifier
255.9
49.15
47.78
Unit
ug/L
ug/L
ug/L
D
%Rec
102
98
96
%Rec.
Limits
54 - 145
80 - 121
68 - 130
Bromochloromethane
Bromodichloromethane
Bromoform
50.0
50.0
50.0
49.86
51.72
55.37
ug/L
ug/L
ug/L
100
103
111
78 - 129
75 - 129
46 - 145
Bromomethane
2-Butanone (MEK)
Carbon disulfide
50.0
250
50.0
49.08
252.4
49.60
ug/L
ug/L
ug/L
98
101
99
41 - 150
62 - 133
77 - 126
Carbon tetrachloride
Chlorobenzene
50.0
50.0
58.15
48.47
ug/L
ug/L
116
97
64 - 147
80 - 120
Chlorodibromomethane
50.0
54.48
ug/L
109
69 - 133
Chloroethane
Chloroform
Chloromethane
50.0
50.0
50.0
51.07
50.36
47.53
ug/L
ug/L
ug/L
102
101
95
72 - 120
73 - 129
12 - 150
2-Chlorotoluene
50.0
48.19
ug/L
96
75 - 126
TestAmerica Nashville
Page 37 of 74
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QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-260281/3
Matrix: Water
Analysis Batch: 260281
Analyte
4-Chlorotoluene
cis-1,2-Dichloroethene
1
3
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
50.0
50.0
LCS LCS
Result Qualifier
48.16
47.70
Unit
ug/L
ug/L
D
%Rec
96
95
%Rec.
Limits
75 - 130
76 - 125
4
5
6
7
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
50.0
50.0
50.0
50.49
52.24
49.65
ug/L
ug/L
ug/L
101
104
99
74 - 140
54 - 125
80 - 129
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
50.0
50.0
50.0
48.28
47.68
49.04
ug/L
ug/L
ug/L
97
95
98
71 - 125
80 - 121
80 - 122
1,4-Dichlorobenzene
Dichlorodifluoromethane
50.0
50.0
50.10
49.59
ug/L
ug/L
100
99
80 - 120
37 - 127
10
1,1-Dichloroethane
50.0
49.04
ug/L
98
78 - 125
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
50.0
50.0
50.0
48.85
48.73
47.97
ug/L
ug/L
ug/L
98
97
96
77 - 121
79 - 124
75 - 120
11
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
50.0
50.0
50.0
47.52
40.88
48.55
ug/L
ug/L
ug/L
95
82
97
80 - 125
43 - 161
80 - 122
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
50.0
50.0
50.0
48.66
49.27
47.70
ug/L
ug/L
ug/L
97
99
95
61 - 142
80 - 130
63 - 135
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
50.0
250
50.0
48.74
244.4
49.44
ug/L
ug/L
ug/L
97
98
99
49 - 146
60 - 142
80 - 141
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
50.0
250
50.0
51.55
235.4
48.17
ug/L
ug/L
ug/L
103
94
96
79 - 123
60 - 137
72 - 133
Naphthalene
n-Butylbenzene
N-Propylbenzene
50.0
50.0
50.0
54.92
49.25
49.15
ug/L
ug/L
ug/L
110
98
98
62 - 138
68 - 132
75 - 129
p-Isopropyltoluene
sec-Butylbenzene
Styrene
50.0
50.0
50.0
49.45
49.45
49.62
ug/L
ug/L
ug/L
99
99
99
75 - 128
76 - 128
80 - 127
Tert-amyl methyl ether
tert-Butyl alcohol (TBA)
50.0
500
47.41
448.0
ug/L
ug/L
95
90
63 - 135
54 - 150
tert-Butylbenzene
50.0
49.22
ug/L
98
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
50.0
50.0
50.0
52.68
48.14
46.83
ug/L
ug/L
ug/L
105
96
94
76 - 126
74 - 135
69 - 131
80 - 126
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
50.0
50.0
50.0
47.92
49.43
52.06
ug/L
ug/L
ug/L
96
99
104
80 - 126
79 - 126
63 - 134
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
50.0
50.0
50.0
53.16
51.66
49.34
ug/L
ug/L
ug/L
106
103
99
62 - 133
63 - 133
78 - 135
1,1,2-Trichloroethane
50.0
48.06
ug/L
96
Trichloroethene
Trichlorofluoromethane
50.0
50.0
49.90
47.56
ug/L
ug/L
100
95
80 - 124
80 - 123
65 - 124
1,2,3-Trichloropropane
50.0
50.00
ug/L
100
70 - 131
8
9
12
13
TestAmerica Nashville
Page 38 of 74
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QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-260281/3
Matrix: Water
Analysis Batch: 260281
Spike
Added
50.0
50.0
Vinyl chloride
Xylenes, Total
Toluene-d8 (Surr)
50.0
100
LCS LCS
Result Qualifier
49.56
48.88
50.50
97.66
Unit
ug/L
ug/L
D
ug/L
ug/L
%Rec
99
98
%Rec.
Limits
77 - 126
77 - 127
101
98
68 - 120
80 - 132
4
5
6
7
8
LCS LCS
%Recovery Qualifier
99
101
100
Limits
70 - 130
70 - 130
70 - 130
98
70 - 130
9
10
Lab Sample ID: LCSD 490-260281/4
Matrix: Water
Analysis Batch: 260281
Analyte
Acetone
3
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Analyte
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
Added
250
LCSD LCSD
Result Qualifier
258.6
Unit
ug/L
D
%Rec
103
%Rec.
Limits
54 - 145
RPD
1
RPD
Limit
21
Benzene
Bromobenzene
50.0
50.0
48.41
46.67
ug/L
ug/L
97
93
80 - 121
68 - 130
2
2
17
20
Bromochloromethane
Bromodichloromethane
Bromoform
50.0
50.0
50.0
49.57
50.52
54.89
ug/L
ug/L
ug/L
99
101
110
78 - 129
75 - 129
46 - 145
1
2
1
17
18
16
Bromomethane
2-Butanone (MEK)
Carbon disulfide
50.0
250
50.0
42.04
243.8
48.60
ug/L
ug/L
ug/L
84
98
97
41 - 150
62 - 133
77 - 126
15
3
2
50
19
21
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
50.0
50.0
50.0
57.44
47.97
53.86
ug/L
ug/L
ug/L
115
96
108
64 - 147
80 - 120
69 - 133
1
1
1
19
14
15
Chloroethane
Chloroform
Chloromethane
50.0
50.0
50.0
47.87
49.49
34.43 *
ug/L
ug/L
ug/L
96
99
69
72 - 120
73 - 129
12 - 150
6
2
32
20
18
31
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
50.0
50.0
50.0
46.81
47.10
47.50
ug/L
ug/L
ug/L
94
94
95
75 - 126
75 - 130
76 - 125
3
2
0
17
18
17
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
50.0
50.0
50.0
50.15
48.19
49.20
ug/L
ug/L
ug/L
100
96
98
74 - 140
54 - 125
80 - 129
1
8
1
15
24
15
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
50.0
50.0
50.0
47.71
46.59
47.46
ug/L
ug/L
ug/L
95
93
95
71 - 125
80 - 121
80 - 122
1
2
3
16
15
15
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
50.0
50.0
50.0
48.59
49.39
48.64
ug/L
ug/L
ug/L
97
99
97
80 - 120
37 - 127
78 - 125
3
0
1
15
18
17
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
50.0
50.0
50.0
47.85
48.05
47.52
ug/L
ug/L
ug/L
96
96
95
77 - 121
79 - 124
75 - 120
2
1
1
17
17
17
1,3-Dichloropropane
2,2-Dichloropropane
50.0
50.0
46.75
40.30
ug/L
ug/L
94
81
80 - 125
43 - 161
2
1
14
18
TestAmerica Nashville
Page 39 of 74
7/13/2015
11
12
13
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 490-260281/4
Matrix: Water
Analysis Batch: 260281
3
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Analyte
1,1-Dichloropropene
Spike
Added
50.0
%Rec
97
%Rec.
Limits
80 - 122
RPD
0
RPD
Limit
17
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
50.0
50.0
50.0
48.17
48.80
47.45
ug/L
ug/L
ug/L
96
98
95
61 - 142
80 - 130
63 - 135
1
1
1
50
15
19
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
50.0
250
50.0
47.23
239.5
49.32
ug/L
ug/L
ug/L
94
96
99
49 - 146
60 - 142
80 - 141
3
2
0
23
15
16
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
50.0
250
50.0
50.01
230.5
47.45
ug/L
ug/L
ug/L
100
92
95
79 - 123
60 - 137
72 - 133
3
2
2
17
17
16
Naphthalene
n-Butylbenzene
N-Propylbenzene
50.0
50.0
50.0
53.21
47.73
48.11
ug/L
ug/L
ug/L
106
95
96
62 - 138
68 - 132
75 - 129
3
3
2
26
18
17
p-Isopropyltoluene
sec-Butylbenzene
Styrene
50.0
50.0
50.0
48.29
48.13
49.47
ug/L
ug/L
ug/L
97
96
99
75 - 128
76 - 128
80 - 127
2
3
0
16
16
24
Tert-amyl methyl ether
tert-Butyl alcohol (TBA)
tert-Butylbenzene
50.0
500
50.0
48.54
426.1
48.37
ug/L
ug/L
ug/L
97
85
97
63 - 135
54 - 150
76 - 126
2
5
2
15
32
16
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
50.0
50.0
50.0
52.29
46.60
46.35
ug/L
ug/L
ug/L
105
93
93
74 - 135
69 - 131
80 - 126
1
3
1
16
20
16
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
50.0
50.0
50.0
47.49
48.75
51.42
ug/L
ug/L
ug/L
95
97
103
80 - 126
79 - 126
63 - 134
1
1
1
15
16
14
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
50.0
50.0
50.0
50.21
48.92
48.63
ug/L
ug/L
ug/L
100
98
97
62 - 133
63 - 133
78 - 135
6
5
1
25
19
17
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
50.0
50.0
50.0
47.27
48.79
47.99
ug/L
ug/L
ug/L
95
98
96
80 - 124
80 - 123
65 - 124
2
2
1
15
17
18
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
50.0
50.0
50.0
49.13
48.25
47.95
ug/L
ug/L
ug/L
98
97
96
70 - 131
77 - 126
77 - 127
2
3
2
19
16
17
Vinyl chloride
Xylenes, Total
50.0
100
49.05
96.99
ug/L
ug/L
98
97
68 - 120
80 - 132
3
1
17
15
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
1
LCSD LCSD
%Recovery Qualifier
98
102
98
Limits
70 - 130
70 - 130
70 - 130
98
70 - 130
LCSD LCSD
Result Qualifier
48.36
Unit
ug/L
D
TestAmerica Nashville
Page 40 of 74
7/13/2015
4
5
6
7
8
9
10
11
12
13
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-81527-9 MS
Matrix: Ground Water
Analysis Batch: 260281
Analyte
Acetone
Benzene
Bromobenzene
1
3
Client Sample ID: MW13(062515)
Prep Type: Total/NA
Sample Sample
Result Qualifier
ND
ND
ND
Spike
Added
250
50.0
50.0
MS MS
Result Qualifier
225.5
51.36
47.57
Unit
ug/L
ug/L
ug/L
D
%Rec
90
103
95
%Rec.
Limits
45 - 141
75 - 133
60 - 138
4
5
6
7
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
50.0
50.0
50.0
49.57
52.49
52.77
ug/L
ug/L
ug/L
99
105
106
67 - 139
70 - 140
42 - 147
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
50.0
250
50.0
38.46
233.7
55.36
ug/L
ug/L
ug/L
77
93
111
16 - 163
50 - 138
48 - 152
Carbon tetrachloride
ND
50.0
63.61
ug/L
127
62 - 164
Chlorobenzene
Chlorodibromomethane
ND
ND
50.0
50.0
49.45
54.26
ug/L
ug/L
99
109
80 - 129
66 - 140
11
Chloroethane
ND
50.0
50.78
ug/L
102
58 - 137
Chloroform
Chloromethane
ND
ND *
50.0
50.0
50.75
33.31
ug/L
ug/L
102
67
66 - 138
10 - 169
12
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
50.0
50.0
50.0
49.46
49.54
50.74
ug/L
ug/L
ug/L
99
99
101
67 - 138
69 - 138
68 - 138
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
50.0
50.0
50.0
52.97
46.86
48.94
ug/L
ug/L
ug/L
106
94
98
71 - 141
52 - 126
75 - 137
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
50.0
50.0
50.0
47.43
47.27
49.14
ug/L
ug/L
ug/L
95
95
98
58 - 140
79 - 128
77 - 131
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
ND
ND
ND
50.0
50.0
50.0
48.56
58.85
51.43
ug/L
ug/L
ug/L
97
118
103
78 - 126
40 - 127
71 - 139
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
ND
ND
ND
50.0
50.0
50.0
48.38
53.76
48.72
ug/L
ug/L
ug/L
97
108
97
64 - 136
70 - 142
67 - 131
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
ND
ND
ND
50.0
50.0
50.0
46.67
53.49
53.59
ug/L
ug/L
ug/L
93
107
107
72 - 134
37 - 175
76 - 139
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
50.0
50.0
50.0
49.07
51.21
47.98
ug/L
ug/L
ug/L
98
102
96
10 - 200
79 - 139
60 - 138
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
50.0
250
50.0
50.16
227.6
51.54
ug/L
ug/L
ug/L
100
91
103
45 - 155
50 - 150
80 - 153
ND
ND
8.19
50.0
250
50.0
51.94
224.2
55.58
ug/L
ug/L
ug/L
104
90
95
64 - 139
50 - 147
66 - 141
Naphthalene
n-Butylbenzene
ND
ND
50.0
50.0
45.30
51.91
ug/L
ug/L
88
104
55 - 140
66 - 141
N-Propylbenzene
ND
50.0
51.80
ug/L
104
69 - 142
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
50.0
50.0
50.0
51.79
51.76
50.22
ug/L
ug/L
ug/L
104
104
100
71 - 137
73 - 138
61 - 148
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
8
9
10
13
TestAmerica Nashville
Page 41 of 74
7/13/2015
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-81527-9 MS
Matrix: Ground Water
Analysis Batch: 260281
Analyte
Tert-amyl methyl ether
3
Client Sample ID: MW13(062515)
Prep Type: Total/NA
Sample Sample
Result Qualifier
ND
tert-Butyl alcohol (TBA)
tert-Butylbenzene
Spike
Added
50.0
MS MS
Result Qualifier
48.85
Unit
ug/L
D
%Rec
98
%Rec.
Limits
61 - 138
28.6
ND
500
50.0
465.5
50.98
ug/L
ug/L
87
102
50 - 183
70 - 138
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
50.0
50.0
50.0
52.90
47.21
51.16
ug/L
ug/L
ug/L
106
94
102
73 - 141
56 - 143
72 - 145
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
50.0
50.0
50.0
49.95
52.84
53.16
ug/L
ug/L
ug/L
100
106
106
75 - 136
66 - 143
59 - 135
1,2,3-Trichlorobenzene
ND
50.0
40.95
ug/L
82
55 - 138
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
50.0
50.0
46.57
52.93
ug/L
ug/L
93
106
60 - 136
76 - 149
1,1,2-Trichloroethane
ND
50.0
47.34
ug/L
95
Trichloroethene
Trichlorofluoromethane
ND
ND
50.0
50.0
50.92
52.43
ug/L
ug/L
102
105
74 - 134
73 - 144
58 - 139
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
ND
ND
ND
50.0
50.0
50.0
48.03
50.89
50.29
ug/L
ug/L
ug/L
96
101
101
53 - 144
69 - 136
69 - 139
Vinyl chloride
Xylenes, Total
ND
ND
50.0
100
53.03
101.0
ug/L
ug/L
106
101
56 - 129
74 - 141
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
MS MS
%Recovery Qualifier
100
103
Limits
70 - 130
70 - 130
1,2-Dichloroethane-d4 (Surr)
99
70 - 130
Toluene-d8 (Surr)
99
70 - 130
Lab Sample ID: 490-81527-9 MSD
Matrix: Ground Water
Analysis Batch: 260281
Analyte
Acetone
Benzene
Bromobenzene
1
5
6
7
8
9
10
11
12
13
Client Sample ID: MW13(062515)
Prep Type: Total/NA
Sample Sample
Result Qualifier
ND
ND
ND
Spike
Added
250
50.0
50.0
MSD MSD
Result Qualifier
244.2
51.95
49.44
Unit
ug/L
ug/L
ug/L
D
%Rec
98
104
99
%Rec.
Limits
45 - 141
75 - 133
60 - 138
RPD
8
1
4
RPD
Limit
21
17
20
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
50.0
50.0
50.0
50.71
53.26
56.12
ug/L
ug/L
ug/L
101
107
112
67 - 139
70 - 140
42 - 147
2
1
6
17
18
16
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
50.0
250
50.0
46.67
243.4
55.76
ug/L
ug/L
ug/L
93
97
112
16 - 163
50 - 138
48 - 152
19
4
1
50
19
21
Carbon tetrachloride
Chlorobenzene
ND
ND
50.0
50.0
64.65
50.24
ug/L
ug/L
129
100
62 - 164
80 - 129
2
2
19
14
Chlorodibromomethane
ND
50.0
56.00
ug/L
112
66 - 140
3
15
Chloroethane
Chloroform
Chloromethane
ND
ND
ND *
50.0
50.0
50.0
51.53
51.90
36.80
ug/L
ug/L
ug/L
103
104
74
58 - 137
66 - 138
10 - 169
1
2
10
20
18
31
2-Chlorotoluene
ND
50.0
50.64
ug/L
101
67 - 138
2
17
TestAmerica Nashville
Page 42 of 74
4
7/13/2015
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-81527-9 MSD
Matrix: Ground Water
Analysis Batch: 260281
Analyte
4-Chlorotoluene
cis-1,2-Dichloroethene
1
3
Client Sample ID: MW13(062515)
Prep Type: Total/NA
Sample Sample
Result Qualifier
ND
ND
Spike
Added
50.0
50.0
MSD MSD
Result Qualifier
51.16
52.05
Unit
ug/L
ug/L
D
%Rec
102
104
%Rec.
Limits
69 - 138
68 - 138
RPD
3
3
RPD
Limit
18
17
4
5
6
7
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
50.0
50.0
50.0
54.18
50.17
50.76
ug/L
ug/L
ug/L
108
100
102
71 - 141
52 - 126
75 - 137
2
7
4
15
24
15
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
50.0
50.0
50.0
48.68
49.49
50.36
ug/L
ug/L
ug/L
97
99
101
58 - 140
79 - 128
77 - 131
3
5
2
16
15
15
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
50.0
50.0
50.84
59.24
ug/L
ug/L
102
118
78 - 126
40 - 127
5
1
15
18
10
1,1-Dichloroethane
ND
50.0
50.82
ug/L
102
71 - 139
1
17
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
ND
ND
ND
50.0
50.0
50.0
49.46
54.69
49.66
ug/L
ug/L
ug/L
99
109
99
64 - 136
70 - 142
67 - 131
2
2
2
17
17
17
11
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
ND
ND
ND
50.0
50.0
50.0
48.18
53.89
53.86
ug/L
ug/L
ug/L
96
108
108
72 - 134
37 - 175
76 - 139
3
1
0
14
18
17
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
50.0
50.0
50.0
49.88
52.20
49.31
ug/L
ug/L
ug/L
100
104
99
10 - 200
79 - 139
60 - 138
2
2
3
50
15
19
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
50.0
250
50.0
53.86
241.4
52.58
ug/L
ug/L
ug/L
108
97
105
45 - 155
50 - 150
80 - 153
7
6
2
23
15
16
ND
ND
8.19
50.0
250
50.0
52.73
235.6
57.08
ug/L
ug/L
ug/L
105
94
98
64 - 139
50 - 147
66 - 141
2
5
3
17
17
16
Naphthalene
n-Butylbenzene
N-Propylbenzene
ND
ND
ND
50.0
50.0
50.0
53.27
53.87
52.82
ug/L
ug/L
ug/L
104
108
106
55 - 140
66 - 141
69 - 142
16
4
2
26
18
17
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
50.0
50.0
50.0
53.27
53.71
51.04
ug/L
ug/L
ug/L
107
107
102
71 - 137
73 - 138
61 - 148
3
4
2
16
16
24
ND
28.6
50.0
500
50.98
490.2
ug/L
ug/L
102
92
61 - 138
50 - 183
4
5
15
32
tert-Butylbenzene
ND
50.0
52.90
ug/L
106
70 - 138
4
16
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
50.0
50.0
50.0
54.41
49.83
52.18
ug/L
ug/L
ug/L
109
100
104
73 - 141
56 - 143
72 - 145
3
5
2
16
20
16
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
50.0
50.0
50.0
50.98
53.13
55.65
ug/L
ug/L
ug/L
102
106
111
75 - 136
66 - 143
59 - 135
2
1
5
15
16
14
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
50.0
50.0
50.0
50.95
52.26
54.16
ug/L
ug/L
ug/L
102
105
108
55 - 138
60 - 136
76 - 149
22
12
2
25
19
17
1,1,2-Trichloroethane
ND
50.0
48.83
ug/L
98
15
ND
ND
50.0
50.0
52.39
53.42
ug/L
ug/L
105
107
74 - 134
73 - 144
58 - 139
3
Trichloroethene
Trichlorofluoromethane
3
2
17
18
1,2,3-Trichloropropane
ND
50.0
49.72
ug/L
99
53 - 144
3
19
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Tert-amyl methyl ether
tert-Butyl alcohol (TBA)
TestAmerica Nashville
Page 43 of 74
7/13/2015
8
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12
13
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: 490-81527-9 MSD
Matrix: Ground Water
Analysis Batch: 260281
Analyte
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Client Sample ID: MW13(062515)
Prep Type: Total/NA
Sample Sample
Result Qualifier
ND
ND
Vinyl chloride
Xylenes, Total
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
ND
ND
Spike
Added
50.0
50.0
MSD MSD
Result Qualifier
52.22
51.80
50.0
100
54.92
102.8
Unit
ug/L
ug/L
D
ug/L
ug/L
%Rec
104
104
%Rec.
Limits
69 - 136
69 - 139
RPD
3
3
RPD
Limit
16
17
110
103
56 - 129
74 - 141
4
2
17
15
Limits
70 - 130
70 - 130
70 - 130
99
70 - 130
5
6
7
9
10
Lab Sample ID: MB 490-260433/9
Matrix: Water
Analysis Batch: 260433
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Result Qualifier
ND
4
8
MSD MSD
%Recovery Qualifier
99
101
100
Toluene-d8 (Surr)
Analyte
Acetone
1
RL
25.0
MDL Unit
ug/L
D
Prepared
Analyzed
06/29/15 15:21
Dil Fac
1
Benzene
Bromobenzene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
1
1
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
1.00
50.0
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
2-Chlorotoluene
ND
1.00
ug/L
06/29/15 15:21
1
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
1
1
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
1
1
1,2-Dichloropropane
ND
1.00
ug/L
06/29/15 15:21
1
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
1.00
1.00
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
1
1
TestAmerica Nashville
Page 44 of 74
7/13/2015
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QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: MB 490-260433/9
Matrix: Water
Analysis Batch: 260433
Analyte
1,1-Dichloropropene
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Result Qualifier
ND
MDL Unit
ug/L
D
Prepared
Analyzed
06/29/15 15:21
Dil Fac
1
ND
ND
ND
2.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
2.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
ND
ND
ND
5.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
Naphthalene
n-Butylbenzene
N-Propylbenzene
ND
ND
ND
5.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
Tert-amyl methyl ether
tert-Butyl alcohol (TBA)
tert-Butylbenzene
ND
ND
ND
1.00
10.0
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
ND
ND
ND
1.00
1.00
1.00
ug/L
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
1
1
1
Vinyl chloride
Xylenes, Total
ND
ND
1.00
3.00
ug/L
ug/L
06/29/15 15:21
06/29/15 15:21
1
1
Analyzed
06/29/15 15:21
06/29/15 15:21
06/29/15 15:21
Dil Fac
1
1
1
06/29/15 15:21
1
Toluene-d8 (Surr)
4
5
RL
1.00
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
1
MB MB
%Recovery Qualifier
99
98
96
Limits
70 - 130
70 - 130
70 - 130
97
70 - 130
Prepared
TestAmerica Nashville
Page 45 of 74
7/13/2015
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7
8
9
10
11
12
13
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-260433/3
Matrix: Water
Analysis Batch: 260433
Analyte
Acetone
Benzene
Bromobenzene
1
3
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
250
50.0
50.0
LCS LCS
Result Qualifier
261.4
51.32
49.96
Unit
ug/L
ug/L
ug/L
D
%Rec
105
103
100
%Rec.
Limits
54 - 145
80 - 121
68 - 130
4
5
6
7
Bromochloromethane
Bromodichloromethane
Bromoform
50.0
50.0
50.0
51.13
53.27
56.22
ug/L
ug/L
ug/L
102
107
112
78 - 129
75 - 129
46 - 145
Bromomethane
2-Butanone (MEK)
Carbon disulfide
50.0
250
50.0
44.92
250.0
51.82
ug/L
ug/L
ug/L
90
100
104
41 - 150
62 - 133
77 - 126
Carbon tetrachloride
50.0
56.52
ug/L
113
64 - 147
Chlorobenzene
Chlorodibromomethane
50.0
50.0
50.43
55.06
ug/L
ug/L
101
110
80 - 120
69 - 133
11
Chloroethane
50.0
48.36
ug/L
97
Chloroform
Chloromethane
50.0
50.0
51.69
37.73
ug/L
ug/L
103
75
72 - 120
73 - 129
12 - 150
12
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
50.0
50.0
50.0
50.62
50.62
51.18
ug/L
ug/L
ug/L
101
101
102
75 - 126
75 - 130
76 - 125
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
50.0
50.0
50.0
54.26
50.97
50.56
ug/L
ug/L
ug/L
109
102
101
74 - 140
54 - 125
80 - 129
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
50.0
50.0
50.0
49.05
49.72
50.79
ug/L
ug/L
ug/L
98
99
102
71 - 125
80 - 121
80 - 122
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
50.0
50.0
50.0
51.64
46.59
51.10
ug/L
ug/L
ug/L
103
93
102
80 - 120
37 - 127
78 - 125
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
50.0
50.0
50.0
49.66
51.02
49.63
ug/L
ug/L
ug/L
99
102
99
77 - 121
79 - 124
75 - 120
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
50.0
50.0
50.0
48.41
50.69
51.12
ug/L
ug/L
ug/L
97
101
102
80 - 125
43 - 161
80 - 122
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
50.0
50.0
50.0
49.65
51.06
49.34
ug/L
ug/L
ug/L
99
102
99
61 - 142
80 - 130
63 - 135
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
50.0
250
50.0
45.67
235.8
51.79
ug/L
ug/L
ug/L
91
94
104
49 - 146
60 - 142
80 - 141
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
50.0
250
50.0
52.95
229.2
49.01
ug/L
ug/L
ug/L
106
92
98
79 - 123
60 - 137
72 - 133
Naphthalene
n-Butylbenzene
50.0
50.0
57.33
50.60
ug/L
ug/L
115
101
62 - 138
68 - 132
N-Propylbenzene
50.0
51.24
ug/L
102
75 - 129
p-Isopropyltoluene
sec-Butylbenzene
Styrene
50.0
50.0
50.0
51.23
50.95
51.29
ug/L
ug/L
ug/L
102
102
103
75 - 128
76 - 128
80 - 127
8
9
10
13
TestAmerica Nashville
Page 46 of 74
7/13/2015
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-260433/3
Matrix: Water
Analysis Batch: 260433
3
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
50.0
Analyte
Tert-amyl methyl ether
LCS LCS
Result Qualifier
49.72
Unit
ug/L
D
%Rec
99
%Rec.
Limits
63 - 135
tert-Butyl alcohol (TBA)
tert-Butylbenzene
500
50.0
427.6
51.48
ug/L
ug/L
86
103
54 - 150
76 - 126
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
50.0
50.0
50.0
54.06
49.07
49.73
ug/L
ug/L
ug/L
108
98
99
74 - 135
69 - 131
80 - 126
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
50.0
50.0
50.0
49.89
51.83
55.42
ug/L
ug/L
ug/L
100
104
111
80 - 126
79 - 126
63 - 134
1,2,3-Trichlorobenzene
50.0
54.20
ug/L
108
62 - 133
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
50.0
50.0
55.09
50.99
ug/L
ug/L
110
102
63 - 133
78 - 135
1,1,2-Trichloroethane
50.0
49.35
ug/L
99
Trichloroethene
Trichlorofluoromethane
50.0
50.0
50.74
46.97
ug/L
ug/L
101
94
80 - 124
80 - 123
65 - 124
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
50.0
50.0
50.0
49.15
51.71
50.81
ug/L
ug/L
ug/L
98
103
102
70 - 131
77 - 126
77 - 127
Vinyl chloride
Xylenes, Total
50.0
100
49.26
101.8
ug/L
ug/L
99
102
68 - 120
80 - 132
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
LCS LCS
%Recovery Qualifier
99
102
100
70 - 130
99
70 - 130
6
7
8
9
10
11
12
13
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
Added
250
50.0
50.0
LCSD LCSD
Result Qualifier
242.7
50.67
48.84
Unit
ug/L
ug/L
ug/L
D
%Rec
97
101
98
%Rec.
Limits
54 - 145
80 - 121
68 - 130
RPD
7
1
2
RPD
Limit
21
17
20
Bromochloromethane
Bromodichloromethane
Bromoform
50.0
50.0
50.0
50.73
53.82
57.87
ug/L
ug/L
ug/L
101
108
116
78 - 129
75 - 129
46 - 145
1
1
3
17
18
16
Bromomethane
2-Butanone (MEK)
Carbon disulfide
50.0
250
50.0
45.14
253.6
51.87
ug/L
ug/L
ug/L
90
101
104
41 - 150
62 - 133
77 - 126
0
1
0
50
19
21
Carbon tetrachloride
Chlorobenzene
50.0
50.0
56.05
50.13
ug/L
ug/L
112
100
64 - 147
80 - 120
1
1
19
14
Chlorodibromomethane
50.0
56.80
ug/L
114
69 - 133
3
15
Chloroethane
Chloroform
Chloromethane
50.0
50.0
50.0
48.49
51.37
37.89
ug/L
ug/L
ug/L
97
103
76
72 - 120
73 - 129
12 - 150
0
1
0
20
18
31
2-Chlorotoluene
50.0
49.19
ug/L
98
75 - 126
3
17
TestAmerica Nashville
Page 47 of 74
4
5
Limits
70 - 130
70 - 130
Lab Sample ID: LCSD 490-260433/4
Matrix: Water
Analysis Batch: 260433
Analyte
Acetone
Benzene
Bromobenzene
1
7/13/2015
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 490-260433/4
Matrix: Water
Analysis Batch: 260433
Analyte
4-Chlorotoluene
cis-1,2-Dichloroethene
1
3
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
Added
50.0
50.0
LCSD LCSD
Result Qualifier
49.53
51.01
Unit
ug/L
ug/L
D
%Rec
99
102
%Rec.
Limits
75 - 130
76 - 125
RPD
2
0
RPD
Limit
18
17
4
5
6
7
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
50.0
50.0
50.0
54.55
52.29
51.75
ug/L
ug/L
ug/L
109
105
104
74 - 140
54 - 125
80 - 129
1
3
2
15
24
15
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
50.0
50.0
50.0
50.32
49.09
50.19
ug/L
ug/L
ug/L
101
98
100
71 - 125
80 - 121
80 - 122
3
1
1
16
15
15
1,4-Dichlorobenzene
Dichlorodifluoromethane
50.0
50.0
51.52
45.47
ug/L
ug/L
103
91
80 - 120
37 - 127
0
2
15
18
10
1,1-Dichloroethane
50.0
50.73
ug/L
101
78 - 125
1
17
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
50.0
50.0
50.0
50.59
50.36
49.53
ug/L
ug/L
ug/L
101
101
99
77 - 121
79 - 124
75 - 120
2
1
0
17
17
17
11
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
50.0
50.0
50.0
49.66
49.80
50.55
ug/L
ug/L
ug/L
99
100
101
80 - 125
43 - 161
80 - 122
3
2
1
14
18
17
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
50.0
50.0
50.0
50.56
50.55
50.50
ug/L
ug/L
ug/L
101
101
101
61 - 142
80 - 130
63 - 135
2
1
2
50
15
19
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
50.0
250
50.0
45.26
248.7
51.45
ug/L
ug/L
ug/L
91
99
103
49 - 146
60 - 142
80 - 141
1
5
1
23
15
16
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
50.0
250
50.0
52.64
240.8
50.26
ug/L
ug/L
ug/L
105
96
101
79 - 123
60 - 137
72 - 133
1
5
3
17
17
16
Naphthalene
n-Butylbenzene
N-Propylbenzene
50.0
50.0
50.0
60.09
49.65
50.27
ug/L
ug/L
ug/L
120
99
101
62 - 138
68 - 132
75 - 129
5
2
2
26
18
17
p-Isopropyltoluene
sec-Butylbenzene
Styrene
50.0
50.0
50.0
50.38
49.80
51.81
ug/L
ug/L
ug/L
101
100
104
75 - 128
76 - 128
80 - 127
2
2
1
16
16
24
Tert-amyl methyl ether
tert-Butyl alcohol (TBA)
50.0
500
51.30
418.6
ug/L
ug/L
103
84
63 - 135
54 - 150
3
2
15
32
tert-Butylbenzene
50.0
50.08
ug/L
100
76 - 126
3
16
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
50.0
50.0
50.0
53.84
50.54
49.39
ug/L
ug/L
ug/L
108
101
99
74 - 135
69 - 131
80 - 126
0
3
1
16
20
16
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
50.0
50.0
50.0
49.38
51.21
56.40
ug/L
ug/L
ug/L
99
102
113
80 - 126
79 - 126
63 - 134
1
1
2
15
16
14
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
50.0
50.0
50.0
57.84
55.84
50.58
ug/L
ug/L
ug/L
116
112
101
62 - 133
63 - 133
78 - 135
6
1
1
25
19
17
1,1,2-Trichloroethane
50.0
50.18
ug/L
100
80 - 124
2
15
Trichloroethene
Trichlorofluoromethane
50.0
50.0
49.75
46.44
ug/L
ug/L
99
93
80 - 123
65 - 124
2
1
17
18
1,2,3-Trichloropropane
50.0
49.94
ug/L
100
70 - 131
2
19
TestAmerica Nashville
Page 48 of 74
7/13/2015
8
9
12
13
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 490-260433/4
Matrix: Water
Analysis Batch: 260433
Vinyl chloride
Xylenes, Total
50.0
100
LCSD LCSD
Result Qualifier
50.71
50.02
48.26
101.5
Unit
ug/L
ug/L
ug/L
ug/L
Limits
70 - 130
70 - 130
70 - 130
%Rec
101
100
%Rec.
Limits
77 - 126
77 - 127
RPD
2
2
RPD
Limit
16
17
97
101
68 - 120
80 - 132
2
0
17
15
98
70 - 130
6
7
10
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Sample Sample
Result Qualifier
ND
5
9
Lab Sample ID: 490-81477-A-2 MS
Matrix: Water
Analysis Batch: 260433
Analyte
Acetone
D
4
8
LCSD LCSD
%Recovery Qualifier
97
101
99
Toluene-d8 (Surr)
3
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
Added
50.0
50.0
Analyte
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
1
Spike
Added
250
MS MS
Result Qualifier
175.8
Unit
ug/L
D
%Rec
70
%Rec.
Limits
45 - 141
Benzene
Bromobenzene
ND
ND
50.0
50.0
49.21
44.61
ug/L
ug/L
98
89
75 - 133
60 - 138
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
50.0
50.0
50.0
48.44
49.68
49.18
ug/L
ug/L
ug/L
97
99
98
67 - 139
70 - 140
42 - 147
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
50.0
250
50.0
45.61
196.9
53.37
ug/L
ug/L
ug/L
91
79
107
16 - 163
50 - 138
48 - 152
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
ND
ND
ND
50.0
50.0
50.0
60.49
47.68
51.01
ug/L
ug/L
ug/L
121
95
102
62 - 164
80 - 129
66 - 140
Chloroethane
Chloroform
Chloromethane
ND
ND
ND
50.0
50.0
50.0
47.94
49.15
45.42
ug/L
ug/L
ug/L
96
98
91
58 - 137
66 - 138
10 - 169
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
50.0
50.0
50.0
46.51
46.95
48.42
ug/L
ug/L
ug/L
93
94
97
67 - 138
69 - 138
68 - 138
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
50.0
50.0
50.0
49.63
41.28
46.03
ug/L
ug/L
ug/L
99
83
92
71 - 141
52 - 126
75 - 137
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
50.0
50.0
50.0
45.37
45.66
46.72
ug/L
ug/L
ug/L
91
91
93
58 - 140
79 - 128
77 - 131
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
ND
ND
ND
50.0
50.0
50.0
46.63
45.15
49.81
ug/L
ug/L
ug/L
93
90
100
78 - 126
40 - 127
71 - 139
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
ND
ND
ND
50.0
50.0
50.0
46.65
50.63
47.22
ug/L
ug/L
ug/L
93
101
94
64 - 136
70 - 142
67 - 131
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
50.0
50.0
44.43
47.51
ug/L
ug/L
89
95
72 - 134
37 - 175
12
13
TestAmerica Nashville
Page 49 of 74
11
7/13/2015
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-81477-A-2 MS
Matrix: Water
Analysis Batch: 260433
Analyte
1,1-Dichloropropene
3
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Sample Sample
Result Qualifier
ND
Spike
Added
50.0
MS MS
Result Qualifier
50.19
Unit
ug/L
D
%Rec
100
%Rec.
Limits
76 - 139
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
50.0
50.0
50.0
46.50
49.51
44.47
ug/L
ug/L
ug/L
93
99
89
10 - 200
79 - 139
60 - 138
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
50.0
250
50.0
39.99
192.4
50.02
ug/L
ug/L
ug/L
80
77
100
45 - 155
50 - 150
80 - 153
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
ND
ND
ND
50.0
250
50.0
50.58
197.1
43.46
ug/L
ug/L
ug/L
101
79
87
64 - 139
50 - 147
66 - 141
Naphthalene
n-Butylbenzene
N-Propylbenzene
ND
ND
ND
50.0
50.0
50.0
44.49
46.68
48.31
ug/L
ug/L
ug/L
88
93
97
55 - 140
66 - 141
69 - 142
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
50.0
50.0
50.0
48.03
48.05
49.18
ug/L
ug/L
ug/L
96
96
98
71 - 137
73 - 138
61 - 148
Tert-amyl methyl ether
tert-Butyl alcohol (TBA)
tert-Butylbenzene
ND
ND F1
ND
50.0
500
50.0
43.66
237.8 F1
48.22
ug/L
ug/L
ug/L
87
48
96
61 - 138
50 - 183
70 - 138
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
50.0
50.0
50.0
50.37
43.71
48.93
ug/L
ug/L
ug/L
101
87
98
73 - 141
56 - 143
72 - 145
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
50.0
50.0
50.0
48.16
51.09
49.56
ug/L
ug/L
ug/L
96
102
99
75 - 136
66 - 143
59 - 135
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
ND
50.0
50.0
50.0
41.23
44.60
50.94
ug/L
ug/L
ug/L
82
89
102
55 - 138
60 - 136
76 - 149
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
ND
ND
ND
50.0
50.0
50.0
44.79
48.51
46.40
ug/L
ug/L
ug/L
90
97
93
74 - 134
73 - 144
58 - 139
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
ND
ND
ND
50.0
50.0
50.0
43.43
47.81
47.58
ug/L
ug/L
ug/L
87
96
95
53 - 144
69 - 136
69 - 139
Vinyl chloride
Xylenes, Total
ND
ND
50.0
100
47.19
97.55
ug/L
ug/L
94
98
56 - 129
74 - 141
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
1
MS MS
%Recovery Qualifier
97
101
97
Limits
70 - 130
70 - 130
70 - 130
99
70 - 130
5
6
7
8
9
10
11
12
13
TestAmerica Nashville
Page 50 of 74
4
7/13/2015
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-81477-A-2 MSD
Matrix: Water
Analysis Batch: 260433
Analyte
Acetone
Benzene
Bromobenzene
1
Sample Sample
Result Qualifier
ND
ND
ND
3
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Spike
Added
250
50.0
50.0
MSD MSD
Result Qualifier
195.0
50.24
46.91
Unit
ug/L
ug/L
ug/L
D
%Rec
78
100
94
%Rec.
Limits
45 - 141
75 - 133
60 - 138
RPD
10
2
5
RPD
Limit
21
17
20
4
5
6
7
Bromochloromethane
Bromodichloromethane
Bromoform
ND
ND
ND
50.0
50.0
50.0
51.24
51.64
53.82
ug/L
ug/L
ug/L
102
103
108
67 - 139
70 - 140
42 - 147
6
4
9
17
18
16
Bromomethane
2-Butanone (MEK)
Carbon disulfide
ND
ND
ND
50.0
250
50.0
52.01
207.2
54.18
ug/L
ug/L
ug/L
104
83
108
16 - 163
50 - 138
48 - 152
13
5
2
50
19
21
Carbon tetrachloride
ND
50.0
62.49
ug/L
125
62 - 164
3
19
Chlorobenzene
Chlorodibromomethane
ND
ND
50.0
50.0
49.63
54.30
ug/L
ug/L
99
109
80 - 129
66 - 140
4
6
14
15
11
Chloroethane
ND
50.0
51.20
ug/L
102
58 - 137
7
20
Chloroform
Chloromethane
ND
ND
50.0
50.0
50.87
48.79
ug/L
ug/L
102
98
66 - 138
10 - 169
3
7
18
31
12
2-Chlorotoluene
4-Chlorotoluene
cis-1,2-Dichloroethene
ND
ND
ND
50.0
50.0
50.0
48.33
48.73
49.95
ug/L
ug/L
ug/L
97
97
100
67 - 138
69 - 138
68 - 138
4
4
3
17
18
17
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
ND
ND
ND
50.0
50.0
50.0
51.79
45.58
48.28
ug/L
ug/L
ug/L
104
91
97
71 - 141
52 - 126
75 - 137
4
10
5
15
24
15
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
ND
ND
ND
50.0
50.0
50.0
47.44
47.67
49.17
ug/L
ug/L
ug/L
95
95
98
58 - 140
79 - 128
77 - 131
4
4
5
16
15
15
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
ND
ND
ND
50.0
50.0
50.0
49.05
46.50
50.70
ug/L
ug/L
ug/L
98
93
101
78 - 126
40 - 127
71 - 139
5
3
2
15
18
17
1,2-Dichloroethane
1,1-Dichloroethene
1,2-Dichloropropane
ND
ND
ND
50.0
50.0
50.0
48.38
52.12
48.40
ug/L
ug/L
ug/L
97
104
97
64 - 136
70 - 142
67 - 131
4
3
2
17
17
17
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
ND
ND
ND
50.0
50.0
50.0
46.86
48.13
51.37
ug/L
ug/L
ug/L
94
96
103
72 - 134
37 - 175
76 - 139
5
1
2
14
18
17
Diisopropyl ether
Ethylbenzene
Ethyl tert-butyl ether
ND
ND
ND
50.0
50.0
50.0
48.52
51.19
47.14
ug/L
ug/L
ug/L
97
102
94
10 - 200
79 - 139
60 - 138
4
3
6
50
15
19
Hexachlorobutadiene
2-Hexanone
Isopropylbenzene
ND
ND
ND
50.0
250
50.0
44.74
215.0
51.71
ug/L
ug/L
ug/L
89
86
103
45 - 155
50 - 150
80 - 153
11
11
3
23
15
16
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
ND
ND
ND
50.0
250
50.0
52.42
217.3
46.48
ug/L
ug/L
ug/L
105
87
93
64 - 139
50 - 147
66 - 141
4
10
7
17
17
16
Naphthalene
n-Butylbenzene
ND
ND
50.0
50.0
53.59
49.56
ug/L
ug/L
107
99
55 - 140
66 - 141
19
6
26
18
N-Propylbenzene
ND
50.0
50.67
ug/L
101
69 - 142
5
17
p-Isopropyltoluene
sec-Butylbenzene
Styrene
ND
ND
ND
50.0
50.0
50.0
50.12
50.40
50.60
ug/L
ug/L
ug/L
100
101
101
71 - 137
73 - 138
61 - 148
4
5
3
16
16
24
TestAmerica Nashville
Page 51 of 74
7/13/2015
8
9
10
13
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: 490-81477-A-2 MSD
Matrix: Water
Analysis Batch: 260433
Analyte
Tert-amyl methyl ether
3
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Sample Sample
Result Qualifier
ND
Spike
Added
50.0
MSD MSD
Result Qualifier
47.00
Unit
ug/L
D
%Rec
94
%Rec.
Limits
61 - 138
RPD
7
RPD
Limit
15
tert-Butyl alcohol (TBA)
tert-Butylbenzene
ND F1
ND
500
50.0
291.1
50.17
ug/L
ug/L
58
100
50 - 183
70 - 138
20
4
32
16
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
ND
ND
ND
50.0
50.0
50.0
53.22
45.98
50.50
ug/L
ug/L
ug/L
106
92
101
73 - 141
56 - 143
72 - 145
5
5
3
16
20
16
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
ND
ND
ND
50.0
50.0
50.0
49.76
52.20
52.48
ug/L
ug/L
ug/L
100
104
105
75 - 136
66 - 143
59 - 135
3
2
6
15
16
14
1,2,3-Trichlorobenzene
ND
50.0
51.47
ug/L
103
55 - 138
22
25
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
ND
ND
50.0
50.0
51.13
52.23
ug/L
ug/L
102
104
60 - 136
76 - 149
14
2
19
17
1,1,2-Trichloroethane
ND
50.0
47.39
ug/L
95
15
ND
ND
50.0
50.0
49.93
49.13
ug/L
ug/L
100
98
74 - 134
73 - 144
58 - 139
6
Trichloroethene
Trichlorofluoromethane
3
6
17
18
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
ND
ND
ND
50.0
50.0
50.0
46.47
49.73
49.26
ug/L
ug/L
ug/L
93
99
99
53 - 144
69 - 136
69 - 139
7
4
3
19
16
17
Vinyl chloride
Xylenes, Total
ND
ND
50.0
100
50.33
100.9
ug/L
ug/L
101
101
56 - 129
74 - 141
6
3
17
15
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
MSD MSD
%Recovery Qualifier
96
103
Limits
70 - 130
70 - 130
1,2-Dichloroethane-d4 (Surr)
98
70 - 130
Toluene-d8 (Surr)
99
70 - 130
Method: 9056A - Anions, Ion Chromatography
Lab Sample ID: MB 490-262167/3
Matrix: Water
Analysis Batch: 262167
Analyte
Sulfate
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Result Qualifier
ND
RL
1.00
MDL Unit
mg/L
Lab Sample ID: LCS 490-262167/4
Matrix: Water
Analysis Batch: 262167
Analyte
Sulfate
1
D
Prepared
Analyzed
07/03/15 21:07
Dil Fac
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
100
LCS LCS
Result Qualifier
98.98
Unit
mg/L
D
%Rec
99
%Rec.
Limits
80 - 120
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5
6
7
8
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13
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 9056A - Anions, Ion Chromatography (Continued)
3
Lab Sample ID: 490-81527-7 MS
Matrix: Ground Water
Analysis Batch: 262167
Analyte
Sulfate
Client Sample ID: MW11(062515)
Prep Type: Total/NA
Sample Sample
Result Qualifier
6.85
Spike
Added
100
MS MS
Result Qualifier
103.4
Unit
mg/L
D
Lab Sample ID: 490-81527-7 MSD
Matrix: Ground Water
Analysis Batch: 262167
Analyte
Sulfate
%Rec
97
Sample Sample
Result Qualifier
6.85
Spike
Added
100
MSD MSD
Result Qualifier
102.9
Unit
mg/L
D
%Rec
96
%Rec.
Limits
80 - 120
6
RPD
0
RPD
Limit
20
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Analyte
Sulfate
Result Qualifier
ND
RL
1.00
MDL Unit
mg/L
Lab Sample ID: LCS 490-262376/4
Matrix: Water
Analysis Batch: 262376
LCS LCS
Result Qualifier
98.14
Lab Sample ID: LCSD 490-262376/5
Matrix: Water
Analysis Batch: 262376
Unit
mg/L
LCSD LCSD
Result Qualifier
98.14
Unit
mg/L
Lab Sample ID: 490-81437-M-6 MS
Matrix: Water
Analysis Batch: 262376
Sample Sample
Result Qualifier
3.14
Sample Sample
Result Qualifier
3.14
Dil Fac
1
D
%Rec
98
%Rec.
Limits
80 - 120
D
%Rec
98
%Rec.
Limits
80 - 120
RPD
0
RPD
Limit
20
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Spike
Added
100
MS MS
Result Qualifier
94.94
Lab Sample ID: 490-81437-M-6 MSD
Matrix: Water
Analysis Batch: 262376
Analyte
Sulfate
Analyzed
07/06/15 21:48
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
Added
100
Analyte
Sulfate
Prepared
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
100
Analyte
Sulfate
D
Unit
mg/L
D
%Rec
92
%Rec.
Limits
80 - 120
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Spike
Added
100
MSD MSD
Result Qualifier
102.7
Unit
mg/L
D
%Rec
100
%Rec.
Limits
80 - 120
RPD
8
RPD
Limit
20
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5
%Rec.
Limits
80 - 120
Client Sample ID: MW11(062515)
Prep Type: Total/NA
Lab Sample ID: MB 490-262376/3
Matrix: Water
Analysis Batch: 262376
Analyte
Sulfate
1
7/13/2015
7
8
9
10
11
12
13
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 6010B - Metals (ICP)
3
Lab Sample ID: MB 490-261246/1-A
Matrix: Water
Analysis Batch: 261558
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 261246
MB MB
Result Qualifier
ND
Analyte
Iron
RL
0.100
MDL Unit
mg/L
Lab Sample ID: LCS 490-261246/2-A
Matrix: Water
Analysis Batch: 261558
LCS LCS
Result Qualifier
0.9843
Lab Sample ID: LCSD 490-261246/3-A
Matrix: Water
Analysis Batch: 261558
Unit
mg/L
D
Unit
mg/L
D
Spike
Added
1.00
MS MS
Result Qualifier
29.18 4
Unit
mg/L
D
Spike
Added
1.00
MSD MSD
Result Qualifier
29.84 4
RPD
RPD
2
Limit
20
%Rec
-982
%Rec.
Limits
75 - 125
Unit
mg/L
D
%Rec
-916
%Rec.
Limits
75 - 125
RPD
2
RPD
Limit
20
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 261295
MB MB
Result Qualifier
ND
RL
0.100
MDL Unit
mg/L
Lab Sample ID: LCS 490-261295/2-A
Matrix: Water
Analysis Batch: 262048
Analyte
Iron
D
Prepared
Analyzed
07/01/15 16:07 07/02/15 13:46
Dil Fac
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 261295
Spike
Added
1.00
LCS LCS
Result Qualifier
1.020
Lab Sample ID: LCSD 490-261295/3-A
Matrix: Water
Analysis Batch: 262048
Analyte
Iron
Limits
80 - 120
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Prep Batch: 261246
Lab Sample ID: MB 490-261295/1-A
Matrix: Water
Analysis Batch: 262048
Analyte
Iron
%Rec
101
Unit
mg/L
D
%Rec
102
%Rec.
Limits
80 - 120
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 261295
Spike
Added
1.00
LCSD LCSD
Result Qualifier
1.071
Unit
mg/L
D
%Rec
107
%Rec.
Limits
80 - 120
RPD
5
RPD
Limit
20
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5
6
7
8
9
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Prep Batch: 261246
Lab Sample ID: 490-81484-G-6-E MSD
Matrix: Water
Analysis Batch: 261558
Sample Sample
Result Qualifier
39.0
Dil Fac
1
%Rec.
Limits
80 - 120
%Rec.
Result Qualifier
1.008
Lab Sample ID: 490-81484-G-6-D MS
Matrix: Water
Analysis Batch: 261558
Analyte
Iron
%Rec
98
LCSD LCSD
Added
1.00
Sample Sample
Result Qualifier
39.0
Prepared
Analyzed
07/01/15 14:11 07/02/15 10:08
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Prep Batch: 261246
Spike
Analyte
Iron
D
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 261246
Spike
Added
1.00
Analyte
Iron
Analyte
Iron
1
7/13/2015
10
11
12
13
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Lab Sample ID: 490-81516-A-1-B MS
Matrix: Water
Analysis Batch: 262048
Analyte
Iron
Client Sample ID: Matrix Spike
Prep Type: Total/NA
Prep Batch: 261295
Sample Sample
Result Qualifier
71.0
Spike
Added
1.00
MS MS
Result Qualifier
61.15 4
Lab Sample ID: 490-81516-A-1-C MSD
Matrix: Water
Analysis Batch: 262048
Analyte
Iron
Unit
mg/L
D
Sample Sample
Result Qualifier
71.0
Spike
Added
1.00
MSD MSD
Result Qualifier
62.69 4
Unit
mg/L
D
RL
0.100
MDL Unit
mg/L
Lab Sample ID: LCS 490-260600/2-B
Matrix: Water
Analysis Batch: 261386
RPD
2
RPD
Limit
20
D
Prepared
Analyzed
06/29/15 16:40 07/01/15 16:14
Dil Fac
1
Client Sample ID: Lab Control Sample
Prep Type: Dissolved
Prep Batch: 260607
Spike
Added
1.00
Analyte
Iron
LCS LCS
Result Qualifier
0.9471
Lab Sample ID: LCSD 490-260600/3-B
Matrix: Water
Analysis Batch: 261386
Unit
mg/L
D
%Rec
95
%Rec.
Limits
80 - 120
Client Sample ID: Lab Control Sample Dup
Prep Type: Dissolved
Prep Batch: 260607
Spike
Added
1.00
Analyte
Iron
LCSD LCSD
Result Qualifier
1.020
Unit
mg/L
D
Lab Sample ID: 490-81527-5 MS
Matrix: Ground Water
Analysis Batch: 261386
%Rec
102
%Rec.
Limits
80 - 120
RPD
7
RPD
Limit
20
Client Sample ID: MW8(062515)
Prep Type: Dissolved
Prep Batch: 260607
Sample Sample
Result Qualifier
ND
Spike
Added
1.00
MS MS
Result Qualifier
1.034
Unit
mg/L
D
Lab Sample ID: 490-81527-5 MSD
Matrix: Ground Water
Analysis Batch: 261386
Analyte
Iron
%Rec
-827
%Rec.
Limits
75 - 125
%Rec
103
%Rec.
Limits
75 - 125
Client Sample ID: MW8(062515)
Prep Type: Dissolved
Prep Batch: 260607
Sample Sample
Result Qualifier
ND
Spike
Added
1.00
MSD MSD
Result Qualifier
1.032
Unit
mg/L
D
Lab Sample ID: MB 490-260941/1-B
Matrix: Water
Analysis Batch: 261387
%Rec
103
%Rec.
Limits
75 - 125
RPD
0
RPD
Limit
20
Client Sample ID: Method Blank
Prep Type: Dissolved
Prep Batch: 260945
MB MB
Analyte
Iron
Result Qualifier
ND
RL
0.100
MDL Unit
mg/L
D
Prepared
Analyzed
06/30/15 16:23 07/01/15 17:06
Dil Fac
1
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4
5
Client Sample ID: Method Blank
Prep Type: Dissolved
Prep Batch: 260607
MB MB
Result Qualifier
ND
Analyte
Iron
%Rec
-981
%Rec.
Limits
75 - 125
Client Sample ID: Matrix Spike Duplicate
Prep Type: Total/NA
Prep Batch: 261295
Lab Sample ID: MB 490-260600/1-B
Matrix: Water
Analysis Batch: 261386
Analyte
Iron
1
7/13/2015
6
7
8
9
10
11
12
13
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 6010B - Metals (ICP) (Continued)
3
Lab Sample ID: LCS 490-260941/2-B
Matrix: Water
Analysis Batch: 261387
Client Sample ID: Lab Control Sample
Prep Type: Dissolved
Prep Batch: 260945
Spike
Added
1.00
Analyte
Iron
LCS LCS
Result Qualifier
0.9985
Lab Sample ID: LCSD 490-260941/3-C
Matrix: Water
Analysis Batch: 261387
Unit
mg/L
D
LCSD LCSD
Result Qualifier
1.011
Unit
mg/L
D
Lab Sample ID: 490-81525-P-1-E MS
Matrix: Water
Analysis Batch: 261387
Sample Sample
Result Qualifier
ND
Sample Sample
Result Qualifier
ND
%Rec
101
%Rec.
Limits
80 - 120
Spike
MS MS
Added
1.00
RPD
1
RPD
Limit
20
%Rec.
Result Qualifier
0.9610
Unit
mg/L
D
%Rec
96
MSD MSD
Result Qualifier
0.9377
Unit
mg/L
D
%Rec
94
%Rec.
Limits
75 - 125
RPD
2
RPD
Limit
20
Method: 353.2 - Nitrogen, Nitrate-Nitrite
Lab Sample ID: MB 490-261101/6
Matrix: Water
Analysis Batch: 261101
Analyte
Nitrate/Nitrite
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Result Qualifier
ND
RL
0.100
MDL Unit
mg/L
Lab Sample ID: LCS 490-261101/7
Matrix: Water
Analysis Batch: 261101
Analyte
Nitrate/Nitrite
Prepared
Analyzed
07/01/15 10:07
Dil Fac
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
0.996
LCS LCS
Result Qualifier
1.055
Lab Sample ID: LCSD 490-261101/8
Matrix: Water
Analysis Batch: 261101
Analyte
Nitrate/Nitrite
D
Unit
mg/L
D
%Rec
106
%Rec.
Limits
90 - 110
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
Added
0.996
LCSD LCSD
Result Qualifier
1.050
Unit
mg/L
D
%Rec
105
%Rec.
Limits
90 - 110
RPD
0
RPD
Limit
20
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7
8
9
10
11
12
Limits
75 - 125
Client Sample ID: Matrix Spike Duplicate
Prep Type: Dissolved
Prep Batch: 260945
Spike
Added
1.00
4
6
Client Sample ID: Matrix Spike
Prep Type: Dissolved
Prep Batch: 260945
Lab Sample ID: 490-81525-P-1-F MSD
Matrix: Water
Analysis Batch: 261387
Analyte
Iron
%Rec
100
%Rec.
Limits
80 - 120
Client Sample ID: Lab Control Sample Dup
Prep Type: Dissolved
Prep Batch: 260945
Spike
Added
1.00
Analyte
Iron
Analyte
Iron
1
7/13/2015
13
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Method: 353.2 - Nitrogen, Nitrate-Nitrite (Continued)
3
Lab Sample ID: 490-81527-1 MS
Matrix: Ground Water
Analysis Batch: 261101
Analyte
Nitrate/Nitrite
Client Sample ID: MW1A(062515)
Prep Type: Total/NA
Sample Sample
Result Qualifier
ND
Spike
Added
0.996
MS MS
Result Qualifier
1.051
Unit
mg/L
Lab Sample ID: 490-81527-1 MSD
Matrix: Ground Water
Analysis Batch: 261101
Analyte
Nitrate/Nitrite
Sample Sample
Result Qualifier
ND
Sample Sample
Result Qualifier
0.283
D
%Rec
106
Spike
Added
0.996
MSD MSD
Result Qualifier
1.054
Unit
mg/L
D
%Rec
106
%Rec.
Limits
90 - 110
6
RPD
0
RPD
Limit
20
Client Sample ID: MW15(062515)
Prep Type: Total/NA
Spike
Added
0.996
MS MS
Result Qualifier
1.321
%Rec.
Unit
mg/L
D
%Rec
104
7
8
9
10
11
12
Limits
90 - 110
13
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Page 57 of 74
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5
%Rec.
Limits
90 - 110
Client Sample ID: MW1A(062515)
Prep Type: Total/NA
Lab Sample ID: 490-81527-11 MS
Matrix: Ground Water
Analysis Batch: 261101
Analyte
Nitrate/Nitrite
1
7/13/2015
QC Association Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
1
2
GC/MS VOA
3
Analysis Batch: 260281
Prep Batch
4
Lab Sample ID
490-81527-1
490-81527-2
490-81527-4
Client Sample ID
MW1A(062515)
MW2A(062515)
MW5A(062515)
Prep Type
Total/NA
Total/NA
Total/NA
Matrix
Ground Water
Ground Water
Ground Water
Method
8260B
8260B
8260B
490-81527-8
490-81527-9
490-81527-9 MS
MW12(062515)
MW13(062515)
MW13(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
8260B
8260B
8260B
490-81527-9 MSD
490-81527-10
490-81527-11
MW13(062515)
MW14(062515)
MW15(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
8260B
8260B
8260B
490-81527-12
490-81527-13
LCS 490-260281/3
MW16(062515)
DUP01(062515)
Lab Control Sample
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Water
8260B
8260B
8260B
10
LCSD 490-260281/4
MB 490-260281/8
Lab Control Sample Dup
Method Blank
Total/NA
Total/NA
Water
Water
8260B
8260B
11
Lab Sample ID
490-81477-A-2 MS
490-81477-A-2 MSD
490-81527-1
Client Sample ID
Matrix Spike
Matrix Spike Duplicate
MW1A(062515)
Prep Type
Total/NA
Total/NA
Total/NA
Matrix
Water
Water
Ground Water
Method
8260B
8260B
8260B
490-81527-2
490-81527-3
490-81527-4
MW2A(062515)
MW3A(062515)
MW5A(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
8260B
8260B
8260B
490-81527-5
490-81527-6
490-81527-7
MW8(062515)
MW10(062515)
MW11(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
8260B
8260B
8260B
490-81527-13
490-81527-14
490-81527-15
DUP01(062515)
RB01(062515)
TB01(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Water
8260B
8260B
8260B
LCS 490-260433/3
LCSD 490-260433/4
MB 490-260433/9
Lab Control Sample
Lab Control Sample Dup
Method Blank
Total/NA
Total/NA
Total/NA
Water
Water
Water
8260B
8260B
8260B
Lab Sample ID
490-81527-1
490-81527-2
490-81527-3
Client Sample ID
MW1A(062515)
MW2A(062515)
MW3A(062515)
Prep Type
Total/NA
Total/NA
Total/NA
Matrix
Ground Water
Ground Water
Ground Water
Method
9056A
9056A
9056A
490-81527-5
490-81527-6
MW8(062515)
MW10(062515)
Total/NA
Total/NA
Ground Water
Ground Water
9056A
9056A
490-81527-7
MW11(062515)
Total/NA
Ground Water
9056A
490-81527-7 MS
490-81527-7 MSD
490-81527-8
MW11(062515)
MW11(062515)
MW12(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
9056A
9056A
9056A
490-81527-9
490-81527-10
490-81527-11
MW13(062515)
MW14(062515)
MW15(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
9056A
9056A
9056A
490-81527-12
MW16(062515)
Total/NA
Ground Water
9056A
5
6
7
8
9
Analysis Batch: 260433
Prep Batch
13
HPLC/IC
Analysis Batch: 262167
Prep Batch
TestAmerica Nashville
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7/13/2015
QC Association Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
1
2
HPLC/IC (Continued)
3
Analysis Batch: 262167 (Continued)
Lab Sample ID
490-81527-13
LCS 490-262167/4
Client Sample ID
DUP01(062515)
Lab Control Sample
Prep Type
Total/NA
Total/NA
Matrix
Ground Water
Water
Method
9056A
9056A
MB 490-262167/3
Method Blank
Total/NA
Water
9056A
Lab Sample ID
490-81437-M-6 MS
490-81437-M-6 MSD
490-81527-4
Client Sample ID
Matrix Spike
Matrix Spike Duplicate
MW5A(062515)
Prep Type
Total/NA
Total/NA
Total/NA
Matrix
Water
Water
Ground Water
Method
9056A
9056A
9056A
490-81527-14
LCS 490-262376/4
LCSD 490-262376/5
RB01(062515)
Lab Control Sample
Lab Control Sample Dup
Total/NA
Total/NA
Total/NA
Ground Water
Water
Water
9056A
9056A
9056A
MB 490-262376/3
Method Blank
Total/NA
Water
9056A
Prep Batch
4
5
6
Analysis Batch: 262376
Prep Batch
7
8
9
10
11
Metals
12
Filtration Batch: 260600
Lab Sample ID
490-81527-1
Client Sample ID
MW1A(062515)
Prep Type
Dissolved
Matrix
Ground Water
Method
Filtration
Prep Batch
490-81527-2
490-81527-3
MW2A(062515)
MW3A(062515)
Dissolved
Dissolved
Ground Water
Ground Water
Filtration
Filtration
490-81527-4
490-81527-5
490-81527-5 MS
MW5A(062515)
MW8(062515)
MW8(062515)
Dissolved
Dissolved
Dissolved
Ground Water
Ground Water
Ground Water
Filtration
Filtration
Filtration
490-81527-5 MSD
LCS 490-260600/2-B
LCSD 490-260600/3-B
MW8(062515)
Lab Control Sample
Lab Control Sample Dup
Dissolved
Dissolved
Dissolved
Ground Water
Water
Water
Filtration
Filtration
Filtration
MB 490-260600/1-B
Method Blank
Dissolved
Water
Filtration
Lab Sample ID
490-81527-1
490-81527-2
490-81527-3
Client Sample ID
MW1A(062515)
MW2A(062515)
MW3A(062515)
Prep Type
Dissolved
Dissolved
Dissolved
Matrix
Ground Water
Ground Water
Ground Water
Method
3005A
3005A
3005A
490-81527-4
490-81527-5
MW5A(062515)
MW8(062515)
Dissolved
Dissolved
Ground Water
Ground Water
3005A
3005A
260600
260600
490-81527-5 MS
MW8(062515)
Dissolved
Ground Water
3005A
260600
490-81527-5 MSD
LCS 490-260600/2-B
LCSD 490-260600/3-B
MW8(062515)
Lab Control Sample
Lab Control Sample Dup
Dissolved
Dissolved
Dissolved
Ground Water
Water
Water
3005A
3005A
3005A
260600
260600
260600
MB 490-260600/1-B
Method Blank
Dissolved
Water
3005A
260600
Lab Sample ID
490-81525-P-1-E MS
490-81525-P-1-F MSD
490-81527-6
Client Sample ID
Matrix Spike
Matrix Spike Duplicate
MW10(062515)
Prep Type
Dissolved
Dissolved
Dissolved
Matrix
Water
Water
Ground Water
Method
Filtration
Filtration
Filtration
490-81527-7
490-81527-8
MW11(062515)
MW12(062515)
Dissolved
Dissolved
Ground Water
Ground Water
Filtration
Filtration
490-81527-9
MW13(062515)
Dissolved
Ground Water
Filtration
Prep Batch: 260607
Prep Batch
260600
260600
260600
Filtration Batch: 260941
Prep Batch
TestAmerica Nashville
Page 59 of 74
7/13/2015
13
QC Association Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
1
2
Metals (Continued)
3
Filtration Batch: 260941 (Continued)
Lab Sample ID
490-81527-10
490-81527-11
490-81527-12
Client Sample ID
MW14(062515)
MW15(062515)
MW16(062515)
Prep Type
Dissolved
Dissolved
Dissolved
Matrix
Ground Water
Ground Water
Ground Water
Method
Filtration
Filtration
Filtration
Prep Batch
490-81527-13
490-81527-14
LCS 490-260941/2-B
DUP01(062515)
RB01(062515)
Lab Control Sample
Dissolved
Dissolved
Dissolved
Ground Water
Ground Water
Water
Filtration
Filtration
Filtration
LCSD 490-260941/3-C
MB 490-260941/1-B
Lab Control Sample Dup
Method Blank
Dissolved
Dissolved
Water
Water
Filtration
Filtration
Lab Sample ID
490-81525-P-1-E MS
490-81525-P-1-F MSD
490-81527-6
Client Sample ID
Matrix Spike
Matrix Spike Duplicate
MW10(062515)
Prep Type
Dissolved
Dissolved
Dissolved
Matrix
Water
Water
Ground Water
Method
3005A
3005A
3005A
490-81527-7
490-81527-8
490-81527-9
MW11(062515)
MW12(062515)
MW13(062515)
Dissolved
Dissolved
Dissolved
Ground Water
Ground Water
Ground Water
3005A
3005A
3005A
260941
260941
260941
490-81527-10
490-81527-11
490-81527-12
MW14(062515)
MW15(062515)
MW16(062515)
Dissolved
Dissolved
Dissolved
Ground Water
Ground Water
Ground Water
3005A
3005A
3005A
260941
260941
260941
490-81527-13
490-81527-14
LCS 490-260941/2-B
DUP01(062515)
RB01(062515)
Lab Control Sample
Dissolved
Dissolved
Dissolved
Ground Water
Ground Water
Water
3005A
3005A
3005A
260941
260941
260941
LCSD 490-260941/3-C
MB 490-260941/1-B
Lab Control Sample Dup
Method Blank
Dissolved
Dissolved
Water
Water
3005A
3005A
260941
260941
Lab Sample ID
490-81484-G-6-D MS
490-81484-G-6-E MSD
490-81527-1
Client Sample ID
Matrix Spike
Matrix Spike Duplicate
MW1A(062515)
Prep Type
Total/NA
Total/NA
Total/NA
Matrix
Water
Water
Ground Water
Method
3010A
3010A
3010A
490-81527-2
490-81527-3
MW2A(062515)
MW3A(062515)
Total/NA
Total/NA
Ground Water
Ground Water
3010A
3010A
490-81527-4
MW5A(062515)
Total/NA
Ground Water
3010A
490-81527-5
LCS 490-261246/2-A
LCSD 490-261246/3-A
MW8(062515)
Lab Control Sample
Lab Control Sample Dup
Total/NA
Total/NA
Total/NA
Ground Water
Water
Water
3010A
3010A
3010A
MB 490-261246/1-A
Method Blank
Total/NA
Water
3010A
Lab Sample ID
490-81516-A-1-B MS
490-81516-A-1-C MSD
490-81527-6
Client Sample ID
Matrix Spike
Matrix Spike Duplicate
MW10(062515)
Prep Type
Total/NA
Total/NA
Total/NA
Matrix
Water
Water
Ground Water
Method
3010A
3010A
3010A
490-81527-7
490-81527-8
490-81527-9
MW11(062515)
MW12(062515)
MW13(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
3010A
3010A
3010A
490-81527-10
490-81527-11
490-81527-12
MW14(062515)
MW15(062515)
MW16(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
3010A
3010A
3010A
490-81527-13
DUP01(062515)
Total/NA
Ground Water
3010A
4
5
6
7
8
Prep Batch: 260945
9
Prep Batch
260941
260941
260941
Prep Batch: 261246
Prep Batch
Prep Batch: 261295
Prep Batch
TestAmerica Nashville
Page 60 of 74
7/13/2015
10
11
12
13
QC Association Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Metals (Continued)
3
Prep Batch: 261295 (Continued)
Lab Sample ID
490-81527-14
LCS 490-261295/2-A
Client Sample ID
RB01(062515)
Lab Control Sample
Prep Type
Total/NA
Total/NA
Matrix
Ground Water
Water
Method
3010A
3010A
LCSD 490-261295/3-A
MB 490-261295/1-A
Lab Control Sample Dup
Method Blank
Total/NA
Total/NA
Water
Water
3010A
3010A
Prep Batch
4
5
6
7
Analysis Batch: 261386
Lab Sample ID
490-81527-1
490-81527-2
490-81527-3
Client Sample ID
MW1A(062515)
MW2A(062515)
MW3A(062515)
Prep Type
Dissolved
Dissolved
Dissolved
Matrix
Ground Water
Ground Water
Ground Water
Method
6010B
6010B
6010B
490-81527-4
490-81527-5
490-81527-5 MS
MW5A(062515)
MW8(062515)
MW8(062515)
Dissolved
Dissolved
Dissolved
Ground Water
Ground Water
Ground Water
6010B
6010B
6010B
260607
260607
260607
490-81527-5 MSD
LCS 490-260600/2-B
LCSD 490-260600/3-B
MW8(062515)
Lab Control Sample
Lab Control Sample Dup
Dissolved
Dissolved
Dissolved
Ground Water
Water
Water
6010B
6010B
6010B
260607
260607
260607
MB 490-260600/1-B
Method Blank
Dissolved
Water
6010B
260607
Prep Batch
260607
260607
260607
8
9
10
11
12
13
Analysis Batch: 261387
Lab Sample ID
490-81525-P-1-E MS
490-81525-P-1-F MSD
490-81527-6
Client Sample ID
Matrix Spike
Matrix Spike Duplicate
MW10(062515)
Prep Type
Dissolved
Dissolved
Dissolved
Matrix
Water
Water
Ground Water
Method
6010B
6010B
6010B
490-81527-7
490-81527-8
490-81527-9
MW11(062515)
MW12(062515)
MW13(062515)
Dissolved
Dissolved
Dissolved
Ground Water
Ground Water
Ground Water
6010B
6010B
6010B
260945
260945
260945
490-81527-10
490-81527-11
490-81527-12
MW14(062515)
MW15(062515)
MW16(062515)
Dissolved
Dissolved
Dissolved
Ground Water
Ground Water
Ground Water
6010B
6010B
6010B
260945
260945
260945
490-81527-13
490-81527-14
LCS 490-260941/2-B
DUP01(062515)
RB01(062515)
Lab Control Sample
Dissolved
Dissolved
Dissolved
Ground Water
Ground Water
Water
6010B
6010B
6010B
260945
260945
260945
LCSD 490-260941/3-C
MB 490-260941/1-B
Lab Control Sample Dup
Method Blank
Dissolved
Dissolved
Water
Water
6010B
6010B
260945
260945
Prep Batch
260945
260945
260945
Lab Sample ID
490-81484-G-6-D MS
490-81484-G-6-E MSD
490-81527-1
Client Sample ID
Matrix Spike
Matrix Spike Duplicate
MW1A(062515)
Prep Type
Total/NA
Total/NA
Total/NA
Matrix
Water
Water
Ground Water
Method
6010B
6010B
6010B
490-81527-2
490-81527-3
490-81527-4
MW2A(062515)
MW3A(062515)
MW5A(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
6010B
6010B
6010B
261246
261246
261246
490-81527-5
LCS 490-261246/2-A
LCSD 490-261246/3-A
MW8(062515)
Lab Control Sample
Lab Control Sample Dup
Total/NA
Total/NA
Total/NA
Ground Water
Water
Water
6010B
6010B
6010B
261246
261246
261246
MB 490-261246/1-A
Method Blank
Total/NA
Water
6010B
261246
Client Sample ID
Matrix Spike
Prep Type
Total/NA
Matrix
Water
Method
6010B
Analysis Batch: 261558
Prep Batch
261246
261246
261246
Analysis Batch: 262048
Lab Sample ID
490-81516-A-1-B MS
1
Prep Batch
261295
TestAmerica Nashville
Page 61 of 74
7/13/2015
QC Association Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
1
2
Metals (Continued)
3
Analysis Batch: 262048 (Continued)
Lab Sample ID
490-81516-A-1-C MSD
490-81527-6
Client Sample ID
Matrix Spike Duplicate
MW10(062515)
Prep Type
Total/NA
Total/NA
Matrix
Water
Ground Water
Method
6010B
6010B
Prep Batch
261295
261295
490-81527-7
490-81527-8
490-81527-9
MW11(062515)
MW12(062515)
MW13(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
6010B
6010B
6010B
261295
261295
261295
490-81527-10
490-81527-11
490-81527-12
MW14(062515)
MW15(062515)
MW16(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
6010B
6010B
6010B
261295
261295
261295
490-81527-13
490-81527-14
LCS 490-261295/2-A
DUP01(062515)
RB01(062515)
Lab Control Sample
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Water
6010B
6010B
6010B
261295
261295
261295
LCSD 490-261295/3-A
MB 490-261295/1-A
Lab Control Sample Dup
Method Blank
Total/NA
Total/NA
Water
Water
6010B
6010B
261295
261295
4
5
6
7
8
9
10
11
General Chemistry
12
Analysis Batch: 261101
Lab Sample ID
490-81527-1
490-81527-1 MS
490-81527-1 MSD
Client Sample ID
MW1A(062515)
MW1A(062515)
MW1A(062515)
Prep Type
Total/NA
Total/NA
Total/NA
Matrix
Ground Water
Ground Water
Ground Water
Method
353.2
353.2
353.2
490-81527-2
490-81527-3
490-81527-4
MW2A(062515)
MW3A(062515)
MW5A(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
353.2
353.2
353.2
490-81527-5
490-81527-6
490-81527-7
MW8(062515)
MW10(062515)
MW11(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
353.2
353.2
353.2
490-81527-8
490-81527-9
490-81527-10
MW12(062515)
MW13(062515)
MW14(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
353.2
353.2
353.2
490-81527-11
490-81527-11 MS
490-81527-12
MW15(062515)
MW15(062515)
MW16(062515)
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Ground Water
353.2
353.2
353.2
490-81527-13
490-81527-14
LCS 490-261101/7
DUP01(062515)
RB01(062515)
Lab Control Sample
Total/NA
Total/NA
Total/NA
Ground Water
Ground Water
Water
353.2
353.2
353.2
LCSD 490-261101/8
Lab Control Sample Dup
Total/NA
Water
353.2
MB 490-261101/6
Method Blank
Total/NA
Water
353.2
Prep Batch
TestAmerica Nashville
Page 62 of 74
7/13/2015
13
Lab Chronicle
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW1A(062515)
Lab Sample ID: 490-81527-1
Date Collected: 06/25/15 12:45
Date Received: 06/26/15 08:45
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
8260B
Total/NA
Analysis
8260B
1
Matrix: Ground Water
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260281
Prepared
or Analyzed Analyst
06/29/15 03:55 RP
Lab
TAL NSH
20
10 mL
10 mL
260433
06/29/15 21:32 EML
TAL NSH
3
4
5
6
Total/NA
Analysis
9056A
1
10 mL
262167
07/03/15 21:49 JHS
TAL NSH
7
Dissolved
Dissolved
Dissolved
Prep
Filtration
Analysis
3005A
Filtration
6010B
50 mL
50 mL
50 mL
260607
260600
261386
06/29/15 16:40 ZLN
06/29/15 16:40 ZLN
07/01/15 18:24 LEG
TAL NSH
TAL NSH
TAL NSH
8
1
50 mL
50 mL
50 mL
Total/NA
Total/NA
Prep
Analysis
3010A
6010B
1
50 mL
50 mL
50 mL
50 mL
261246
261558
07/01/15 14:11 ZLN
07/02/15 11:33 LEG
TAL NSH
TAL NSH
Total/NA
Analysis
353.2
1
50 mL
50 mL
261101
07/01/15 10:10 MJA
TAL NSH
Client Sample ID: MW2A(062515)
Lab Sample ID: 490-81527-2
Date Collected: 06/25/15 11:20
Date Received: 06/26/15 08:45
Batch
Batch
Prep Type
Total/NA
Type
Analysis
Method
8260B
Total/NA
Analysis
8260B
Total/NA
Analysis
9056A
Dissolved
Dissolved
Dissolved
Prep
Filtration
Analysis
Total/NA
Total/NA
Total/NA
Matrix: Ground Water
Dil
Final
Amount
10 mL
Number
260281
or Analyzed Analyst
06/29/15 04:21 RP
Lab
TAL NSH
20
10 mL
10 mL
260433
06/29/15 21:58 EML
TAL NSH
20
10 mL
262167
07/03/15 22:10 JHS
TAL NSH
3005A
Filtration
6010B
1
50 mL
50 mL
50 mL
50 mL
50 mL
50 mL
260607
260600
261386
06/29/15 16:40 ZLN
06/29/15 16:40 ZLN
07/01/15 18:16 LEG
TAL NSH
TAL NSH
TAL NSH
Prep
Analysis
3010A
6010B
1
50 mL
50 mL
50 mL
50 mL
261246
261558
07/01/15 14:11 ZLN
07/02/15 11:29 LEG
TAL NSH
TAL NSH
Analysis
353.2
1
50 mL
50 mL
261101
07/01/15 10:12 MJA
TAL NSH
Factor
1
Batch
Client Sample ID: MW3A(062515)
Prepared
Lab Sample ID: 490-81527-3
Date Collected: 06/25/15 10:40
Date Received: 06/26/15 08:45
Matrix: Ground Water
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
8260B
Total/NA
Analysis
9056A
1
10 mL
Dissolved
Dissolved
Dissolved
Prep
Filtration
Analysis
3005A
Filtration
6010B
1
50 mL
50 mL
50 mL
50 mL
50 mL
50 mL
Total/NA
Total/NA
Prep
Analysis
3010A
6010B
1
50 mL
50 mL
Total/NA
Analysis
353.2
1
50 mL
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260433
Prepared
or Analyzed Analyst
06/29/15 18:27 EML
Lab
TAL NSH
262167
07/03/15 22:31 JHS
TAL NSH
260607
260600
261386
06/29/15 16:40 ZLN
06/29/15 16:40 ZLN
07/01/15 18:20 LEG
TAL NSH
TAL NSH
TAL NSH
50 mL
50 mL
261246
261558
07/01/15 14:11 ZLN
07/02/15 11:24 LEG
TAL NSH
TAL NSH
50 mL
261101
07/01/15 10:13 MJA
TAL NSH
TestAmerica Nashville
Page 63 of 74
10
11
12
13
Initial
Amount
10 mL
Run
9
7/13/2015
Lab Chronicle
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW5A(062515)
Lab Sample ID: 490-81527-4
Date Collected: 06/25/15 14:15
Date Received: 06/26/15 08:45
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
8260B
Total/NA
Analysis
8260B
Total/NA
Analysis
9056A
Dissolved
Dissolved
Prep
Filtration
3005A
Filtration
Dissolved
Analysis
6010B
Total/NA
Total/NA
Prep
Analysis
Total/NA
Analysis
1
Matrix: Ground Water
3
4
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260281
Prepared
or Analyzed Analyst
06/29/15 05:14 RP
Lab
TAL NSH
10
10 mL
10 mL
260433
06/29/15 22:52 EML
TAL NSH
1
10 mL
262376
07/07/15 03:46 JHS
TAL NSH
5
6
7
50 mL
50 mL
50 mL
50 mL
260607
260600
06/29/15 16:40 ZLN
06/29/15 16:40 ZLN
TAL NSH
TAL NSH
1
50 mL
50 mL
261386
07/01/15 18:29 LEG
TAL NSH
3010A
6010B
1
50 mL
50 mL
50 mL
50 mL
261246
261558
07/01/15 14:11 ZLN
07/02/15 11:01 LEG
TAL NSH
TAL NSH
9
353.2
1
50 mL
50 mL
261101
07/01/15 10:14 MJA
TAL NSH
10
Client Sample ID: MW8(062515)
Lab Sample ID: 490-81527-5
Date Collected: 06/25/15 09:30
Date Received: 06/26/15 08:45
Matrix: Ground Water
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
8260B
Total/NA
Analysis
9056A
1
10 mL
Dissolved
Dissolved
Dissolved
Prep
Filtration
Analysis
3005A
Filtration
6010B
1
50 mL
50 mL
50 mL
50 mL
50 mL
50 mL
Total/NA
Total/NA
Prep
Analysis
3010A
6010B
1
50 mL
50 mL
Total/NA
Analysis
353.2
1
50 mL
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260433
Prepared
or Analyzed Analyst
06/29/15 18:54 EML
Lab
TAL NSH
262167
07/03/15 23:13 JHS
TAL NSH
260607
260600
261386
06/29/15 16:40 ZLN
06/29/15 16:40 ZLN
07/01/15 16:26 LEG
TAL NSH
TAL NSH
TAL NSH
50 mL
50 mL
261246
261558
07/01/15 14:11 ZLN
07/02/15 11:59 LEG
TAL NSH
TAL NSH
50 mL
261101
07/01/15 10:15 MJA
TAL NSH
Client Sample ID: MW10(062515)
Lab Sample ID: 490-81527-6
Date Collected: 06/25/15 13:05
Date Received: 06/26/15 08:45
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
8260B
Total/NA
Analysis
9056A
Dissolved
Dissolved
Dissolved
Prep
Filtration
Analysis
Total/NA
Total/NA
Total/NA
Matrix: Ground Water
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260433
Prepared
or Analyzed Analyst
06/29/15 19:20 EML
Lab
TAL NSH
262167
07/03/15 23:34 JHS
TAL NSH
10
10 mL
3005A
Filtration
6010B
1
50 mL
50 mL
50 mL
50 mL
50 mL
50 mL
260945
260941
261387
06/30/15 16:23 ZLN
06/30/15 16:23 ZLN
07/01/15 17:49 LEG
TAL NSH
TAL NSH
TAL NSH
Prep
Analysis
3010A
6010B
1
50 mL
50 mL
50 mL
50 mL
261295
262048
07/01/15 16:07 ZLN
07/02/15 15:09 LEG
TAL NSH
TAL NSH
Analysis
353.2
1
50 mL
50 mL
261101
07/01/15 10:16 MJA
TAL NSH
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Lab Chronicle
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW11(062515)
Lab Sample ID: 490-81527-7
Date Collected: 06/25/15 13:50
Date Received: 06/26/15 08:45
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
8260B
Total/NA
Analysis
9056A
Dissolved
Dissolved
Dissolved
Prep
Filtration
Analysis
3005A
Filtration
6010B
Total/NA
Total/NA
Prep
Analysis
3010A
6010B
Total/NA
Analysis
353.2
1
Matrix: Ground Water
3
4
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260433
Prepared
or Analyzed Analyst
06/29/15 19:47 EML
Lab
TAL NSH
262167
07/03/15 23:55 JHS
TAL NSH
1
10 mL
1
50 mL
50 mL
50 mL
50 mL
50 mL
50 mL
260945
260941
261387
06/30/15 16:23 ZLN
06/30/15 16:23 ZLN
07/01/15 17:53 LEG
TAL NSH
TAL NSH
TAL NSH
1
50 mL
50 mL
50 mL
50 mL
261295
262048
07/01/15 16:07 ZLN
07/02/15 15:14 LEG
TAL NSH
TAL NSH
1
50 mL
50 mL
261101
07/01/15 10:17 MJA
TAL NSH
5
6
7
8
9
10
Client Sample ID: MW12(062515)
Lab Sample ID: 490-81527-8
Date Collected: 06/25/15 14:55
Date Received: 06/26/15 08:45
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
8260B
Total/NA
Analysis
9056A
Matrix: Ground Water
Run
Dil
Factor
1
Initial
Amount
10 mL
1
10 mL
Final
Amount
10 mL
12
Batch
Number
260281
Prepared
or Analyzed Analyst
06/29/15 06:59 RP
Lab
TAL NSH
262167
07/04/15 00:58 JHS
TAL NSH
Dissolved
Prep
3005A
50 mL
50 mL
260945
06/30/15 16:23 ZLN
TAL NSH
Dissolved
Dissolved
Filtration
Analysis
Filtration
6010B
1
50 mL
50 mL
50 mL
50 mL
260941
261387
06/30/15 16:23 ZLN
07/01/15 17:58 LEG
TAL NSH
TAL NSH
Total/NA
Total/NA
Prep
Analysis
3010A
6010B
1
50 mL
50 mL
50 mL
50 mL
261295
262048
07/01/15 16:07 ZLN
07/02/15 15:28 LEG
TAL NSH
TAL NSH
Total/NA
Analysis
353.2
1
50 mL
50 mL
261101
07/01/15 10:18 MJA
TAL NSH
Client Sample ID: MW13(062515)
Lab Sample ID: 490-81527-9
Date Collected: 06/25/15 11:20
Date Received: 06/26/15 08:45
Matrix: Ground Water
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
8260B
Total/NA
Analysis
9056A
5
10 mL
Dissolved
Dissolved
Dissolved
Prep
Filtration
Analysis
3005A
Filtration
6010B
1
50 mL
50 mL
50 mL
50 mL
50 mL
50 mL
Total/NA
Total/NA
Prep
Analysis
3010A
6010B
1
50 mL
50 mL
Total/NA
Analysis
353.2
1
50 mL
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260281
Prepared
or Analyzed Analyst
06/29/15 07:26 RP
Lab
TAL NSH
262167
07/04/15 01:19 JHS
TAL NSH
260945
260941
261387
06/30/15 16:23 ZLN
06/30/15 16:23 ZLN
07/01/15 18:02 LEG
TAL NSH
TAL NSH
TAL NSH
50 mL
50 mL
261295
262048
07/01/15 16:07 ZLN
07/02/15 15:32 LEG
TAL NSH
TAL NSH
50 mL
261101
07/01/15 10:19 MJA
TAL NSH
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Lab Chronicle
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: MW14(062515)
Lab Sample ID: 490-81527-10
Date Collected: 06/25/15 10:20
Date Received: 06/26/15 08:45
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
8260B
Total/NA
Analysis
9056A
Dissolved
Dissolved
Dissolved
Prep
Filtration
Analysis
3005A
Filtration
6010B
Total/NA
Total/NA
Prep
Analysis
3010A
6010B
Total/NA
Analysis
353.2
1
Matrix: Ground Water
3
4
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260281
Prepared
or Analyzed Analyst
06/29/15 07:52 RP
Lab
TAL NSH
262167
07/04/15 01:41 JHS
TAL NSH
20
10 mL
1
50 mL
50 mL
50 mL
50 mL
50 mL
50 mL
260945
260941
261387
06/30/15 16:23 ZLN
06/30/15 16:23 ZLN
07/01/15 18:06 LEG
TAL NSH
TAL NSH
TAL NSH
1
50 mL
50 mL
50 mL
50 mL
261295
262048
07/01/15 16:07 ZLN
07/02/15 15:36 LEG
TAL NSH
TAL NSH
1
50 mL
50 mL
261101
07/01/15 10:20 MJA
TAL NSH
5
6
7
8
9
10
Client Sample ID: MW15(062515)
Lab Sample ID: 490-81527-11
Date Collected: 06/25/15 09:35
Date Received: 06/26/15 08:45
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
8260B
Total/NA
Analysis
9056A
Matrix: Ground Water
Run
Dil
Factor
1
Initial
Amount
10 mL
1
10 mL
Final
Amount
10 mL
12
Batch
Number
260281
Prepared
or Analyzed Analyst
06/29/15 08:19 RP
Lab
TAL NSH
262167
07/04/15 02:44 JHS
TAL NSH
Dissolved
Prep
3005A
50 mL
50 mL
260945
06/30/15 16:23 ZLN
TAL NSH
Dissolved
Dissolved
Filtration
Analysis
Filtration
6010B
1
50 mL
50 mL
50 mL
50 mL
260941
261387
06/30/15 16:23 ZLN
07/01/15 18:11 LEG
TAL NSH
TAL NSH
Total/NA
Total/NA
Prep
Analysis
3010A
6010B
1
50 mL
50 mL
50 mL
50 mL
261295
262048
07/01/15 16:07 ZLN
07/02/15 15:40 LEG
TAL NSH
TAL NSH
Total/NA
Analysis
353.2
1
50 mL
50 mL
261101
07/01/15 10:22 MJA
TAL NSH
Client Sample ID: MW16(062515)
Lab Sample ID: 490-81527-12
Date Collected: 06/25/15 15:10
Date Received: 06/26/15 08:45
Matrix: Ground Water
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
8260B
Total/NA
Analysis
9056A
1
10 mL
Dissolved
Dissolved
Dissolved
Prep
Filtration
Analysis
3005A
Filtration
6010B
1
50 mL
50 mL
50 mL
50 mL
50 mL
50 mL
Total/NA
Total/NA
Prep
Analysis
3010A
6010B
1
50 mL
50 mL
Total/NA
Analysis
353.2
1
50 mL
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260281
Prepared
or Analyzed Analyst
06/29/15 08:45 RP
Lab
TAL NSH
262167
07/04/15 03:05 JHS
TAL NSH
260945
260941
261387
06/30/15 16:23 ZLN
06/30/15 16:23 ZLN
07/01/15 18:15 LEG
TAL NSH
TAL NSH
TAL NSH
50 mL
50 mL
261295
262048
07/01/15 16:07 ZLN
07/02/15 15:45 LEG
TAL NSH
TAL NSH
50 mL
261101
07/01/15 10:24 MJA
TAL NSH
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Lab Chronicle
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Client Sample ID: DUP01(062515)
Lab Sample ID: 490-81527-13
Date Collected: 06/25/15 12:00
Date Received: 06/26/15 08:45
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
8260B
Total/NA
Analysis
8260B
Total/NA
Analysis
9056A
Dissolved
Dissolved
Prep
Filtration
3005A
Filtration
Dissolved
Analysis
6010B
Total/NA
Total/NA
Prep
Analysis
Total/NA
Analysis
Matrix: Ground Water
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260281
Prepared
or Analyzed Analyst
06/29/15 09:12 RP
Lab
TAL NSH
20
10 mL
10 mL
260433
06/29/15 22:25 EML
TAL NSH
1
10 mL
262167
07/04/15 03:26 JHS
TAL NSH
5
6
7
50 mL
50 mL
50 mL
50 mL
260945
260941
06/30/15 16:23 ZLN
06/30/15 16:23 ZLN
TAL NSH
TAL NSH
1
50 mL
50 mL
261387
07/01/15 18:19 LEG
TAL NSH
3010A
6010B
1
50 mL
50 mL
50 mL
50 mL
261295
262048
07/01/15 16:07 ZLN
07/02/15 15:49 LEG
TAL NSH
TAL NSH
9
353.2
1
50 mL
50 mL
261101
07/01/15 10:25 MJA
TAL NSH
10
Lab Sample ID: 490-81527-14
Date Collected: 06/25/15 15:40
Date Received: 06/26/15 08:45
Matrix: Ground Water
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
8260B
Total/NA
Analysis
9056A
1
10 mL
Dissolved
Dissolved
Dissolved
Prep
Filtration
Analysis
3005A
Filtration
6010B
1
50 mL
50 mL
50 mL
50 mL
50 mL
50 mL
Total/NA
Total/NA
Prep
Analysis
3010A
6010B
1
50 mL
50 mL
Total/NA
Analysis
353.2
1
50 mL
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260433
Prepared
or Analyzed Analyst
06/29/15 20:13 EML
Lab
TAL NSH
262376
07/07/15 04:07 JHS
TAL NSH
260945
260941
261387
06/30/15 16:23 ZLN
06/30/15 16:23 ZLN
07/01/15 18:23 LEG
TAL NSH
TAL NSH
TAL NSH
50 mL
50 mL
261295
262048
07/01/15 16:07 ZLN
07/02/15 15:53 LEG
TAL NSH
TAL NSH
50 mL
261101
07/01/15 10:26 MJA
TAL NSH
Client Sample ID: TB01(062515)
Lab Sample ID: 490-81527-15
Date Collected: 06/25/15 01:00
Date Received: 06/26/15 08:45
Batch
Type
Analysis
3
4
Client Sample ID: RB01(062515)
Prep Type
Total/NA
1
Batch
Method
8260B
Matrix: Water
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260433
Prepared
or Analyzed Analyst
06/29/15 16:15 EML
Lab
TAL NSH
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177
TestAmerica Nashville
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Method Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
1
2
Method
8260B
9056A
6010B
Method Description
Volatile Organic Compounds (GC/MS)
Anions, Ion Chromatography
Metals (ICP)
Protocol
SW846
SW846
SW846
Laboratory
TAL NSH
TAL NSH
TAL NSH
353.2
Nitrogen, Nitrate-Nitrite
MCAWW
TAL NSH
3
4
5
6
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
7
8
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177
9
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11
12
13
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Page 68 of 74
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Certification Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81527-1
2
Laboratory: TestAmerica Nashville
3
The certifications listed below are applicable to this report.
Authority
Maryland
1
Program
State Program
EPA Region
3
Certification ID
316
4
Expiration Date
03-31-16
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6
7
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10
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13
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Page 72 of 74
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Page 73 of 74
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Login Sample Receipt Checklist
Client: ARCADIS U.S., Inc.
2
Job Number: 490-81527-1
Login Number: 81527
List Number: 1
Creator: McBride, Mike
List Source: TestAmerica Nashville
3
4
5
Question
Answer
Radioactivity wasn't checked or is </= background as measured by a
survey meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time.
True
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
True
6
Comment
7
True
8
9
True
10
1.7/2.0
11
12
13
True
True
TestAmerica Nashville
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ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: (615)726-0177
TestAmerica Job ID: 490-81555-1
Client Project/Site: 14489 - North East
For:
ARCADIS U.S., Inc.
1114 Benfield Blvd.
Suite A
Millersville, Maryland 21108
Attn: Mr. Rusty Kahl
Authorized for release by:
7/9/2015 10:34:50 PM
Jennifer Huckaba, Project Manager II
(615)301-5042
[email protected]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Table of Contents
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
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Page 2 of 25
TestAmerica Nashville
7/9/2015
Sample Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
1
2
Lab Sample ID
490-81555-1
490-81555-2
490-81555-3
Client Sample ID
2590BINF(062515)
2590BMID(062515)
2590BEFF(062515)
Matrix
Water
Water
Water
Collected
Received
06/25/15 12:05 06/26/15 08:45
06/25/15 12:10 06/26/15 08:45
06/25/15 12:15 06/26/15 08:45
490-81555-4
TB01(062515)
Water
06/25/15 01:00 06/26/15 08:45
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4
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7
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Page 3 of 25
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Case Narrative
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
1
2
Job ID: 490-81555-1
3
Laboratory: TestAmerica Nashville
4
Narrative
5
Job Narrative
490-81555-1
6
Comments
No additional comments.
7
Receipt
The samples were received on 6/26/2015 8:45 AM; the samples arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 1.7º C.
GC/MS VOA
Method(s) 524.2: The laboratory control sample (LCS) for batch analytical batch 490-260431 recovered outside control limits for the
following analytes: Dichlorodifluoromethane and Bromomethane. These analytes were biased high in the LCS and were not detected in
the associated samples; therefore, the data have been reported.
Method(s) 524.2: The laboratory control sample duplicate (LCSD) for batch analytical batch 490-260431 recovered outside control limits
for the following analyte: Dichlorodifluoromethane. This analyte was biased high in the LCSD and was not detected in the associated
samples; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Page 4 of 25
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7/9/2015
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Definitions/Glossary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Qualifiers
3
GC/MS VOA
Qualifier
*
J
1
4
Qualifier Description
LCS or LCSD is outside acceptance limits.
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
5
6
Glossary
Abbreviation
¤
%R
CFL
CNF
DER
These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis
Percent Recovery
Contains Free Liquid
Contains no Free Liquid
Duplicate error ratio (normalized absolute difference)
Dil Fac
DL, RA, RE, IN
DLC
Dilution Factor
Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
Decision level concentration
MDA
EDL
MDC
MDL
ML
NC
ND
Minimum detectable activity
Estimated Detection Limit
Minimum detectable concentration
Method Detection Limit
Minimum Level (Dioxin)
Not Calculated
Not detected at the reporting limit (or MDL or EDL if shown)
PQL
QC
RER
RL
RPD
TEF
Practical Quantitation Limit
Quality Control
Relative error ratio
Reporting Limit or Requested Limit (Radiochemistry)
Relative Percent Difference, a measure of the relative difference between two points
Toxicity Equivalent Factor (Dioxin)
TEQ
Toxicity Equivalent Quotient (Dioxin)
7
8
9
10
11
12
13
TestAmerica Nashville
Page 5 of 25
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Client Sample ID: 2590BINF(062515)
Lab Sample ID: 490-81555-1
Date Collected: 06/25/15 12:05
Date Received: 06/26/15 08:45
Matrix: Water
Result Qualifier
ND
ND
ND
RL
0.500
0.500
0.500
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
Dil Fac
1
1
1
Bromodichloromethane
Bromoform
Bromomethane
ND
ND
ND *
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
Chlorodibromomethane
Chloroethane
Chloroform
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
ND
ND
ND
0.500
0.500
2.00
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
ND *
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
1,1-Dichloroethane
1,2-Dichloroethane
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
1
1
1,1-Dichloroethene
ND
0.500
ug/L
06/29/15 15:05
1
1,2-Dichloropropane
1,3-Dichloropropane
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
1
1
2,2-Dichloropropane
ND
0.500
ug/L
06/29/15 15:05
1
1,1-Dichloropropene
ND
1.49
0.500
0.500
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
1
1
Ethylbenzene
ND
0.500
ug/L
06/29/15 15:05
1
Ethyl tert-butyl ether
Hexachlorobutadiene
Isopropylbenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
ND
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 17:41
06/29/15 15:05
1
5
1
Diisopropyl ether
Methylene Chloride
Naphthalene
ND
5.00
2.50
5.00
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
sec-Butylbenzene
Styrene
Tert-amyl methyl ether
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
135
Methyl tert-butyl ether
59.3
tert-Butylbenzene
1,1,1,2-Tetrachloroethane
ND
ND
10.0
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
1,1,2,2-Tetrachloroethane
ND
0.500
ug/L
06/29/15 15:05
1
tert-Butyl alcohol
3
4
Method: 524.2 - Volatile Organic Compounds (GC/MS)
Analyte
Benzene
Bromobenzene
Bromochloromethane
1
TestAmerica Nashville
Page 6 of 25
7/9/2015
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7
8
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10
11
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13
Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Client Sample ID: 2590BINF(062515)
Lab Sample ID: 490-81555-1
Date Collected: 06/25/15 12:05
Date Received: 06/26/15 08:45
Matrix: Water
3
4
Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Tetrachloroethene
Toluene
1
Result Qualifier
ND
ND
RL
0.500
0.500
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 15:05
06/29/15 15:05
Dil Fac
1
1
5
6
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1,2,3-Trichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
06/29/15 15:05
1
1
1
10
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 15:05
06/29/15 15:05
1
1
11
Vinyl chloride
ND
0.500
ug/L
06/29/15 15:05
1
Xylenes, Total
ND
1.00
ug/L
06/29/15 15:05
1
12
Analyzed
06/29/15 15:05
06/29/15 17:41
06/29/15 15:05
Dil Fac
1
5
1
13
Surrogate
4-Bromofluorobenzene (Surr)
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
%Recovery Qualifier
106
104
102
Limits
70 - 130
70 - 130
70 - 130
Prepared
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
103
102
70 - 130
70 - 130
06/29/15 17:41
06/29/15 15:05
5
1
1,2-Dichloroethane-d4 (Surr)
101
70 - 130
06/29/15 17:41
5
98
98
70 - 130
70 - 130
06/29/15 15:05
06/29/15 17:41
1
5
Toluene-d8 (Surr)
Toluene-d8 (Surr)
TestAmerica Nashville
Page 7 of 25
7/9/2015
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9
Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Client Sample ID: 2590BMID(062515)
Lab Sample ID: 490-81555-2
Date Collected: 06/25/15 12:10
Date Received: 06/26/15 08:45
Matrix: Water
3
4
Method: 524.2 - Volatile Organic Compounds (GC/MS)
Analyte
Benzene
Bromobenzene
Bromochloromethane
1
Result Qualifier
ND
ND
ND
RL
0.500
0.500
0.500
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
Dil Fac
1
1
1
Bromodichloromethane
Bromoform
Bromomethane
ND
ND
ND *
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
Chlorodibromomethane
Chloroethane
Chloroform
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
ND
ND
ND
0.500
0.500
2.00
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
ND *
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
1,1-Dichloroethane
1,2-Dichloroethane
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
1
1
1,1-Dichloroethene
ND
0.500
ug/L
06/29/15 14:39
1
1,2-Dichloropropane
1,3-Dichloropropane
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
1
1
2,2-Dichloropropane
ND
0.500
ug/L
06/29/15 14:39
1
1,1-Dichloropropene
Diisopropyl ether
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
1
1
Ethylbenzene
ND
0.500
ug/L
06/29/15 14:39
1
Ethyl tert-butyl ether
Hexachlorobutadiene
Isopropylbenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
Methylene Chloride
Methyl tert-butyl ether
Naphthalene
ND
ND
ND
5.00
0.500
5.00
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
sec-Butylbenzene
Styrene
Tert-amyl methyl ether
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
tert-Butyl alcohol
tert-Butylbenzene
1,1,1,2-Tetrachloroethane
ND
ND
ND
10.0
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
1,1,2,2-Tetrachloroethane
ND
0.500
ug/L
06/29/15 14:39
1
TestAmerica Nashville
Page 8 of 25
7/9/2015
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Client Sample ID: 2590BMID(062515)
Lab Sample ID: 490-81555-2
Date Collected: 06/25/15 12:10
Date Received: 06/26/15 08:45
Matrix: Water
3
4
Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Tetrachloroethene
Toluene
1
Result Qualifier
ND
ND
RL
0.500
0.500
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 14:39
06/29/15 14:39
Dil Fac
1
1
5
6
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1,2,3-Trichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
1
1
1
10
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 14:39
06/29/15 14:39
1
1
11
Vinyl chloride
ND
0.500
ug/L
06/29/15 14:39
1
Xylenes, Total
ND
1.00
ug/L
06/29/15 14:39
1
12
Analyzed
06/29/15 14:39
06/29/15 14:39
06/29/15 14:39
Dil Fac
1
1
1
13
06/29/15 14:39
1
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
%Recovery Qualifier
105
102
101
Limits
70 - 130
70 - 130
70 - 130
97
70 - 130
Prepared
TestAmerica Nashville
Page 9 of 25
7/9/2015
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Client Sample ID: 2590BEFF(062515)
Lab Sample ID: 490-81555-3
Date Collected: 06/25/15 12:15
Date Received: 06/26/15 08:45
Matrix: Water
3
4
Method: 524.2 - Volatile Organic Compounds (GC/MS)
Analyte
Benzene
Bromobenzene
Bromochloromethane
1
Result Qualifier
ND
ND
ND
RL
0.500
0.500
0.500
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
Dil Fac
1
1
1
Bromodichloromethane
Bromoform
Bromomethane
ND
ND
ND *
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
Chlorodibromomethane
Chloroethane
Chloroform
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
ND
ND
ND
0.500
0.500
2.00
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
ND *
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
1,1-Dichloroethane
1,2-Dichloroethane
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
1
1
1,1-Dichloroethene
ND
0.500
ug/L
06/29/15 14:13
1
1,2-Dichloropropane
1,3-Dichloropropane
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
1
1
2,2-Dichloropropane
ND
0.500
ug/L
06/29/15 14:13
1
1,1-Dichloropropene
Diisopropyl ether
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
1
1
Ethylbenzene
ND
0.500
ug/L
06/29/15 14:13
1
Ethyl tert-butyl ether
Hexachlorobutadiene
Isopropylbenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
Methylene Chloride
Methyl tert-butyl ether
Naphthalene
ND
ND
ND
5.00
0.500
5.00
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
sec-Butylbenzene
Styrene
Tert-amyl methyl ether
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
tert-Butyl alcohol
tert-Butylbenzene
1,1,1,2-Tetrachloroethane
ND
ND
ND
10.0
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
1,1,2,2-Tetrachloroethane
ND
0.500
ug/L
06/29/15 14:13
1
TestAmerica Nashville
Page 10 of 25
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Client Sample ID: 2590BEFF(062515)
Lab Sample ID: 490-81555-3
Date Collected: 06/25/15 12:15
Date Received: 06/26/15 08:45
Matrix: Water
3
4
Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Tetrachloroethene
Toluene
1
Result Qualifier
ND
ND
RL
0.500
0.500
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 14:13
06/29/15 14:13
Dil Fac
1
1
5
6
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1,2,3-Trichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
1
1
1
10
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 14:13
06/29/15 14:13
1
1
11
Vinyl chloride
ND
0.500
ug/L
06/29/15 14:13
1
Xylenes, Total
ND
1.00
ug/L
06/29/15 14:13
1
12
Analyzed
06/29/15 14:13
06/29/15 14:13
06/29/15 14:13
Dil Fac
1
1
1
13
06/29/15 14:13
1
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
%Recovery Qualifier
100
103
102
Limits
70 - 130
70 - 130
70 - 130
97
70 - 130
Prepared
TestAmerica Nashville
Page 11 of 25
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Client Sample ID: TB01(062515)
Lab Sample ID: 490-81555-4
Date Collected: 06/25/15 01:00
Date Received: 06/26/15 08:45
Matrix: Water
3
4
Method: 524.2 - Volatile Organic Compounds (GC/MS)
Analyte
Benzene
Bromobenzene
Bromochloromethane
1
Result Qualifier
ND
ND
ND
RL
0.500
0.500
0.500
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
Dil Fac
1
1
1
Bromodichloromethane
Bromoform
Bromomethane
ND
ND
ND *
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
Chlorodibromomethane
Chloroethane
Chloroform
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
ND
ND
ND
0.500
0.500
2.00
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
ND *
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
1,1-Dichloroethane
1,2-Dichloroethane
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
1
1
1,1-Dichloroethene
ND
0.500
ug/L
06/29/15 13:21
1
1,2-Dichloropropane
1,3-Dichloropropane
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
1
1
2,2-Dichloropropane
ND
0.500
ug/L
06/29/15 13:21
1
1,1-Dichloropropene
Diisopropyl ether
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
1
1
Ethylbenzene
ND
0.500
ug/L
06/29/15 13:21
1
Ethyl tert-butyl ether
Hexachlorobutadiene
Isopropylbenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
Methylene Chloride
Methyl tert-butyl ether
Naphthalene
ND
ND
ND
5.00
0.500
5.00
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
sec-Butylbenzene
Styrene
Tert-amyl methyl ether
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
tert-Butyl alcohol
tert-Butylbenzene
1,1,1,2-Tetrachloroethane
ND
ND
ND
10.0
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
1,1,2,2-Tetrachloroethane
ND
0.500
ug/L
06/29/15 13:21
1
TestAmerica Nashville
Page 12 of 25
7/9/2015
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Client Sample ID: TB01(062515)
Lab Sample ID: 490-81555-4
Date Collected: 06/25/15 01:00
Date Received: 06/26/15 08:45
Matrix: Water
3
4
Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Tetrachloroethene
Toluene
1
Result Qualifier
ND
ND
RL
0.500
0.500
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 13:21
06/29/15 13:21
Dil Fac
1
1
5
6
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1,2,3-Trichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
1
1
1
10
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 13:21
06/29/15 13:21
1
1
11
Vinyl chloride
ND
0.500
ug/L
06/29/15 13:21
1
Xylenes, Total
ND
1.00
ug/L
06/29/15 13:21
1
12
Analyzed
06/29/15 13:21
06/29/15 13:21
06/29/15 13:21
Dil Fac
1
1
1
13
06/29/15 13:21
1
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
%Recovery Qualifier
105
102
100
Limits
70 - 130
70 - 130
70 - 130
97
70 - 130
Prepared
TestAmerica Nashville
Page 13 of 25
7/9/2015
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QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Method: 524.2 - Volatile Organic Compounds (GC/MS)
3
Lab Sample ID: MB 490-260431/6
Matrix: Water
Analysis Batch: 260431
Analyte
Benzene
Bromobenzene
Bromochloromethane
1
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Result Qualifier
ND
ND
ND
4
5
RL
0.500
0.500
0.500
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
Dil Fac
1
1
1
6
7
Bromodichloromethane
Bromoform
Bromomethane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
Chlorodibromomethane
ND
0.500
ug/L
06/29/15 12:55
1
Chloroethane
Chloroform
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
1
1
11
Chloromethane
ND
0.500
ug/L
06/29/15 12:55
1
2-Chlorotoluene
4-Chlorotoluene
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
1
1
12
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
ND
ND
ND
0.500
0.500
2.00
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
Ethyl tert-butyl ether
Hexachlorobutadiene
Isopropylbenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
Methylene Chloride
Methyl tert-butyl ether
Naphthalene
ND
ND
ND
5.00
0.500
5.00
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
sec-Butylbenzene
Styrene
Tert-amyl methyl ether
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
tert-Butyl alcohol
tert-Butylbenzene
1,1,1,2-Tetrachloroethane
ND
ND
ND
10.0
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
TestAmerica Nashville
Page 14 of 25
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QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: MB 490-260431/6
Matrix: Water
Analysis Batch: 260431
Client Sample ID: Method Blank
Prep Type: Total/NA
RL
0.500
MDL Unit
ug/L
D
Prepared
Analyzed
06/29/15 12:55
Dil Fac
1
6
7
Tetrachloroethene
Toluene
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
1
1
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1,2,3-Trichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
Trichloroethene
ND
0.500
ug/L
06/29/15 12:55
1
Trichlorofluoromethane
1,2,3-Trichloropropane
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
1
1
1,2,4-Trimethylbenzene
ND
0.500
ug/L
06/29/15 12:55
1
1,3,5-Trimethylbenzene
Vinyl chloride
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
1
1
Xylenes, Total
ND
1.00
ug/L
06/29/15 12:55
1
Analyzed
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
Dil Fac
1
1
1
06/29/15 12:55
1
MB MB
%Recovery Qualifier
104
101
100
Limits
70 - 130
70 - 130
70 - 130
98
70 - 130
Toluene-d8 (Surr)
Prepared
Lab Sample ID: LCS 490-260431/3
Matrix: Water
Analysis Batch: 260431
Analyte
Benzene
Bromobenzene
4
5
MB MB
Result Qualifier
ND
Analyte
1,1,2,2-Tetrachloroethane
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
5.00
5.00
LCS LCS
Result Qualifier
5.149
4.937
Unit
ug/L
ug/L
D
%Rec
103
99
%Rec.
Limits
70 - 130
70 - 130
Bromochloromethane
5.00
4.956
ug/L
99
70 - 130
Bromodichloromethane
Bromoform
Bromomethane
5.00
5.00
5.00
4.909
4.813
6.723 *
ug/L
ug/L
ug/L
98
96
134
70 - 130
70 - 130
70 - 130
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
5.00
5.00
5.00
5.369
4.889
5.038
ug/L
ug/L
ug/L
107
98
101
70 - 130
70 - 130
70 - 130
Chlorodibromomethane
Chloroethane
Chloroform
5.00
5.00
5.00
4.874
5.381
5.418
ug/L
ug/L
ug/L
97
108
108
70 - 130
70 - 130
70 - 130
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
5.00
5.00
5.00
6.456
4.705
5.236
ug/L
ug/L
ug/L
129
94
105
70 - 130
70 - 130
70 - 130
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
5.00
5.00
5.00
5.262
4.742
4.527
ug/L
ug/L
ug/L
105
95
91
70 - 130
70 - 130
70 - 130
1,2-Dibromoethane (EDB)
Dibromomethane
5.00
5.00
4.693
4.939
ug/L
ug/L
94
99
70 - 130
70 - 130
TestAmerica Nashville
Page 15 of 25
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QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-260431/3
Matrix: Water
Analysis Batch: 260431
3
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
5.00
Analyte
1,2-Dichlorobenzene
LCS LCS
Result Qualifier
5.261
Unit
ug/L
D
%Rec
105
%Rec.
Limits
70 - 130
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
5.00
5.00
5.00
4.966
4.995
7.929 *
ug/L
ug/L
ug/L
99
100
159
70 - 130
70 - 130
70 - 130
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
5.00
5.00
5.00
5.267
5.044
5.255
ug/L
ug/L
ug/L
105
101
105
70 - 130
70 - 130
70 - 130
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
5.00
5.00
5.00
5.068
5.021
5.186
ug/L
ug/L
ug/L
101
100
104
70 - 130
70 - 130
70 - 130
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
5.00
5.00
5.00
5.126
4.999
5.093
ug/L
ug/L
ug/L
103
100
102
70 - 130
70 - 130
70 - 130
Ethyl tert-butyl ether
Hexachlorobutadiene
Isopropylbenzene
5.00
5.00
5.00
5.097
4.981
5.087
ug/L
ug/L
ug/L
102
100
102
70 - 130
70 - 130
70 - 130
Methylene Chloride
Methyl tert-butyl ether
Naphthalene
5.00
5.00
5.00
4.990 J
5.075
4.459 J
ug/L
ug/L
ug/L
100
102
89
70 - 130
70 - 130
70 - 130
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
5.00
5.00
5.00
4.544
5.124
5.111
ug/L
ug/L
ug/L
91
102
102
70 - 130
70 - 130
70 - 130
sec-Butylbenzene
Styrene
Tert-amyl methyl ether
5.00
5.00
5.00
5.257
4.760
5.113
ug/L
ug/L
ug/L
105
95
102
70 - 130
70 - 130
70 - 130
tert-Butyl alcohol
tert-Butylbenzene
1,1,1,2-Tetrachloroethane
50.0
5.00
5.00
46.29
5.082
4.863
ug/L
ug/L
ug/L
93
102
97
70 - 130
70 - 130
70 - 130
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
5.00
5.00
5.00
5.168
4.808
4.936
ug/L
ug/L
ug/L
103
96
99
70 - 130
70 - 130
70 - 130
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1,2,3-Trichlorobenzene
5.00
5.00
5.00
5.138
4.607
5.119
ug/L
ug/L
ug/L
103
92
102
70 - 130
70 - 130
70 - 130
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
5.00
5.00
5.00
5.047
5.101
4.981
ug/L
ug/L
ug/L
101
102
100
70 - 130
70 - 130
70 - 130
Trichloroethene
Trichlorofluoromethane
5.00
5.00
5.092
5.441
ug/L
ug/L
102
109
70 - 130
70 - 130
1,2,3-Trichloropropane
5.00
4.673
ug/L
93
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
5.00
5.00
5.00
5.307
5.104
6.054
ug/L
ug/L
ug/L
106
102
121
70 - 130
70 - 130
70 - 130
70 - 130
Xylenes, Total
10.0
10.35
ug/L
104
70 - 130
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
LCS LCS
%Recovery Qualifier
101
102
1
5
6
7
8
9
10
11
12
13
Limits
70 - 130
70 - 130
TestAmerica Nashville
Page 16 of 25
4
7/9/2015
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-260431/3
Matrix: Water
Analysis Batch: 260431
Surrogate
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
3
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS
%Recovery Qualifier
104
97
4
5
Limits
70 - 130
70 - 130
6
7
Lab Sample ID: LCSD 490-260431/4
Matrix: Water
Analysis Batch: 260431
Analyte
Benzene
Bromobenzene
Bromochloromethane
1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
Added
5.00
5.00
5.00
LCSD LCSD
Result Qualifier
5.101
5.054
4.996
Unit
ug/L
ug/L
ug/L
D
%Rec
102
101
100
%Rec.
Limits
70 - 130
70 - 130
70 - 130
RPD
1
2
1
RPD
Limit
20
20
20
Bromodichloromethane
Bromoform
Bromomethane
5.00
5.00
5.00
4.837
4.721
6.482
ug/L
ug/L
ug/L
97
94
130
70 - 130
70 - 130
70 - 130
1
2
4
20
20
20
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
5.00
5.00
5.00
5.497
4.946
5.060
ug/L
ug/L
ug/L
110
99
101
70 - 130
70 - 130
70 - 130
2
1
0
20
20
20
Chlorodibromomethane
Chloroethane
Chloroform
5.00
5.00
5.00
4.833
5.682
5.522
ug/L
ug/L
ug/L
97
114
110
70 - 130
70 - 130
70 - 130
1
5
2
20
20
20
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
5.00
5.00
5.00
6.491
5.149
5.139
ug/L
ug/L
ug/L
130
103
103
70 - 130
70 - 130
70 - 130
1
9
2
20
20
20
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
5.00
5.00
5.00
4.948
4.732
4.191
ug/L
ug/L
ug/L
99
95
84
70 - 130
70 - 130
70 - 130
6
0
8
20
20
20
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
5.00
5.00
5.00
4.849
4.943
5.138
ug/L
ug/L
ug/L
97
99
103
70 - 130
70 - 130
70 - 130
3
0
2
20
20
20
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
5.00
5.00
5.00
5.021
5.148
7.795 *
ug/L
ug/L
ug/L
100
103
156
70 - 130
70 - 130
70 - 130
1
3
2
20
20
20
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
5.00
5.00
5.00
5.115
5.065
5.350
ug/L
ug/L
ug/L
102
101
107
70 - 130
70 - 130
70 - 130
3
0
2
20
20
20
1,2-Dichloropropane
1,3-Dichloropropane
5.00
5.00
5.182
5.065
ug/L
ug/L
104
101
70 - 130
70 - 130
2
1
20
20
2,2-Dichloropropane
5.00
5.389
ug/L
108
70 - 130
4
20
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
5.00
5.00
5.00
5.091
5.060
5.258
ug/L
ug/L
ug/L
102
101
105
70 - 130
70 - 130
70 - 130
1
1
3
20
20
20
Ethyl tert-butyl ether
Hexachlorobutadiene
Isopropylbenzene
5.00
5.00
5.00
5.110
4.901
5.134
ug/L
ug/L
ug/L
102
98
103
70 - 130
70 - 130
70 - 130
0
2
1
20
20
20
Methylene Chloride
Methyl tert-butyl ether
Naphthalene
5.00
5.00
5.00
5.028
5.075
4.260 J
ug/L
ug/L
ug/L
101
102
85
70 - 130
70 - 130
70 - 130
1
0
5
20
20
20
n-Butylbenzene
5.00
4.632
ug/L
93
70 - 130
2
20
TestAmerica Nashville
Page 17 of 25
7/9/2015
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10
11
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13
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
1
2
Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 490-260431/4
Matrix: Water
Analysis Batch: 260431
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
Added
5.00
5.00
Analyte
N-Propylbenzene
p-Isopropyltoluene
3
LCSD LCSD
Result Qualifier
5.195
5.081
Unit
ug/L
ug/L
D
%Rec
104
102
%Rec.
Limits
70 - 130
70 - 130
RPD
1
1
RPD
Limit
20
20
4
5
6
7
sec-Butylbenzene
Styrene
Tert-amyl methyl ether
5.00
5.00
5.00
5.283
4.679
4.996
ug/L
ug/L
ug/L
106
94
100
70 - 130
70 - 130
70 - 130
0
2
2
20
20
20
tert-Butyl alcohol
tert-Butylbenzene
1,1,1,2-Tetrachloroethane
50.0
5.00
5.00
44.13
5.034
4.902
ug/L
ug/L
ug/L
88
101
98
70 - 130
70 - 130
70 - 130
5
1
1
20
20
20
1,1,2,2-Tetrachloroethane
Tetrachloroethene
5.00
5.00
5.075
4.958
ug/L
ug/L
102
99
70 - 130
70 - 130
2
3
20
20
10
Toluene
5.00
5.043
ug/L
101
70 - 130
2
20
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1,2,3-Trichlorobenzene
5.00
5.00
5.00
5.285
4.549
4.794
ug/L
ug/L
ug/L
106
91
96
70 - 130
70 - 130
70 - 130
3
1
7
20
20
20
11
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
5.00
5.00
5.00
4.634
5.149
4.857
ug/L
ug/L
ug/L
93
103
97
70 - 130
70 - 130
70 - 130
9
1
3
20
20
20
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
5.00
5.00
5.00
5.138
5.541
4.818
ug/L
ug/L
ug/L
103
111
96
70 - 130
70 - 130
70 - 130
1
2
3
20
20
20
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
5.00
5.00
5.00
5.299
5.160
6.118
ug/L
ug/L
ug/L
106
103
122
70 - 130
70 - 130
70 - 130
0
1
1
20
20
20
Xylenes, Total
10.0
10.60
ug/L
106
70 - 130
2
20
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
LCSD LCSD
%Recovery Qualifier
102
100
100
Limits
70 - 130
70 - 130
70 - 130
98
70 - 130
TestAmerica Nashville
Page 18 of 25
7/9/2015
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9
12
13
QC Association Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
1
2
GC/MS VOA
3
Analysis Batch: 260431
Lab Sample ID
490-81555-1
490-81555-1
490-81555-2
Client Sample ID
2590BINF(062515)
2590BINF(062515)
2590BMID(062515)
Prep Type
Total/NA
Total/NA
Total/NA
Matrix
Water
Water
Water
Method
524.2
524.2
524.2
490-81555-3
490-81555-4
LCS 490-260431/3
2590BEFF(062515)
TB01(062515)
Lab Control Sample
Total/NA
Total/NA
Total/NA
Water
Water
Water
524.2
524.2
524.2
LCSD 490-260431/4
MB 490-260431/6
Lab Control Sample Dup
Method Blank
Total/NA
Total/NA
Water
Water
524.2
524.2
Prep Batch
4
5
6
7
8
9
10
11
12
13
TestAmerica Nashville
Page 19 of 25
7/9/2015
Lab Chronicle
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Client Sample ID: 2590BINF(062515)
Lab Sample ID: 490-81555-1
Date Collected: 06/25/15 12:05
Date Received: 06/26/15 08:45
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
524.2
Total/NA
Analysis
524.2
Matrix: Water
Run
Dil
Factor
1
5
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260431
Prepared
or Analyzed Analyst
06/29/15 15:05 NC
Lab
TAL NSH
10 mL
10 mL
260431
06/29/15 17:41 NC
TAL NSH
Client Sample ID: 2590BMID(062515)
Lab Sample ID: 490-81555-2
Date Collected: 06/25/15 12:10
Date Received: 06/26/15 08:45
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
524.2
Matrix: Water
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260431
Client Sample ID: 2590BEFF(062515)
Prepared
or Analyzed Analyst
06/29/15 14:39 NC
Batch
Type
Analysis
Batch
Method
524.2
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260431
Client Sample ID: TB01(062515)
Prepared
or Analyzed Analyst
06/29/15 14:13 NC
Batch
Batch
Type
Analysis
Method
524.2
Matrix: Water
Dil
Run
Factor
1
Initial
Final
Amount
10 mL
Amount
10 mL
Batch
Number
260431
Prepared
or Analyzed Analyst
06/29/15 13:21 NC
Lab
TAL NSH
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177
TestAmerica Nashville
Page 20 of 25
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5
6
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10
11
12
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Lab
TAL NSH
Lab Sample ID: 490-81555-4
Date Collected: 06/25/15 01:00
Date Received: 06/26/15 08:45
Prep Type
Total/NA
Lab
TAL NSH
Matrix: Water
Run
3
9
Lab Sample ID: 490-81555-3
Date Collected: 06/25/15 12:15
Date Received: 06/26/15 08:45
Prep Type
Total/NA
1
7/9/2015
Method Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
Method
524.2
TestAmerica Job ID: 490-81555-1
1
2
Method Description
Volatile Organic Compounds (GC/MS)
Protocol
EPA-DW
Laboratory
TAL NSH
Protocol References:
EPA-DW = "Methods For The Determination Of Organic Compounds In Drinking Water", EPA/600/4-88/039, December 1988 And Its Supplements.
3
4
5
6
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177
7
8
9
10
11
12
13
TestAmerica Nashville
Page 21 of 25
7/9/2015
Certification Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81555-1
2
Laboratory: TestAmerica Nashville
3
Unless otherwise noted, all analytes for this laboratory were covered under each certification below.
Authority
Maryland
Program
State Program
EPA Region
3
Certification ID
316
4
Expiration Date
03-31-16
5
The following analytes are included in this report, but certification is not offered by the governing authority:
Analysis Method
524.2
524.2
524.2
524.2
524.2
524.2
524.2
524.2
524.2
1
Prep Method
Matrix
Water
Water
Water
Water
Water
Water
Water
Water
Water
Analyte
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
1,1-Dichloroethane
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
524.2
524.2
524.2
524.2
524.2
Water
Water
Water
Water
Water
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
2,2-Dichloropropane
2-Chlorotoluene
524.2
524.2
524.2
524.2
524.2
524.2
Water
Water
Water
Water
Water
Water
4-Chlorotoluene
Bromobenzene
Bromochloromethane
Bromomethane
Carbon disulfide
Chloroethane
524.2
524.2
524.2
524.2
524.2
524.2
524.2
Water
Water
Water
Water
Water
Water
Water
Chloromethane
cis-1,3-Dichloropropene
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethyl tert-butyl ether
Hexachlorobutadiene
524.2
524.2
524.2
524.2
524.2
524.2
524.2
524.2
Water
Water
Water
Water
Water
Water
Water
Water
Isopropylbenzene
Methyl tert-butyl ether
Naphthalene
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
sec-Butylbenzene
Tert-amyl methyl ether
524.2
524.2
524.2
524.2
Water
Water
Water
Water
tert-Butyl alcohol
tert-Butylbenzene
trans-1,3-Dichloropropene
Trichlorofluoromethane
6
7
8
9
10
11
12
13
TestAmerica Nashville
Page 22 of 25
7/9/2015
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4
5
6
7
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13
Page 23 of 25
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4
5
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9
10
11
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13
Page 24 of 25
7/9/2015
1
Login Sample Receipt Checklist
Client: ARCADIS U.S., Inc.
2
Job Number: 490-81555-1
Login Number: 81555
List Number: 1
Creator: McBride, Mike
List Source: TestAmerica Nashville
3
4
5
Question
Answer
Radioactivity wasn't checked or is </= background as measured by a
survey meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time.
True
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
6
Comment
7
True
8
9
True
10
1.7
11
12
13
True
True
TestAmerica Nashville
Page 25 of 25
7/9/2015
1
2
3
4
ANALYTICAL REPORT
TestAmerica Laboratories, Inc.
TestAmerica Nashville
2960 Foster Creighton Drive
Nashville, TN 37204
Tel: (615)726-0177
TestAmerica Job ID: 490-81552-1
Client Project/Site: 14489 - North East
For:
ARCADIS U.S., Inc.
1114 Benfield Blvd.
Suite A
Millersville, Maryland 21108
Attn: Mr. Rusty Kahl
Authorized for release by:
7/9/2015 10:02:17 PM
Jennifer Huckaba, Project Manager II
(615)301-5042
[email protected]
The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accredited
parameters, exceptions are noted in this report. This report may not be reproduced except in full,
and with written approval from the laboratory. For questions please contact the Project Manager
at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
5
6
7
8
9
10
11
12
13
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81552-1
2
Table of Contents
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
1
3
1
2
3
4
5
6
8
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14
15
16
17
19
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5
6
7
8
9
10
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Page 2 of 19
TestAmerica Nashville
7/9/2015
Sample Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
Lab Sample ID
490-81552-1
TestAmerica Job ID: 490-81552-1
1
2
Client Sample ID
2610BEFF(062515)
Matrix
Water
Collected
Received
06/25/15 12:20 06/26/15 08:45
3
4
5
6
7
8
9
10
11
12
13
TestAmerica Nashville
Page 3 of 19
7/9/2015
Case Narrative
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81552-1
1
2
Job ID: 490-81552-1
3
Laboratory: TestAmerica Nashville
4
Narrative
5
Job Narrative
490-81552-1
6
Comments
No additional comments.
7
Receipt
The sample was received on 6/26/2015 8:45 AM; the sample arrived in good condition, properly preserved and, where required, on ice.
The temperature of the cooler at receipt was 1.7º C.
GC/MS VOA
Method(s) 524.2: The laboratory control sample (LCS) for batch analytical batch 490-260431 recovered outside control limits for the
following analytes: Dichlorodifluoromethane and Bromomethane. These analytes were biased high in the LCS and were not detected in
the associated samples; therefore, the data have been reported.
Method(s) 524.2: The laboratory control sample duplicate (LCSD) for batch analytical batch 490-260431 recovered outside control limits
for the following analyte: Dichlorodifluoromethane. This analyte was biased high in the LCSD and was not detected in the associated
samples; therefore, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Page 4 of 19
TestAmerica Nashville
7/9/2015
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Definitions/Glossary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81552-1
2
Qualifiers
3
GC/MS VOA
Qualifier
*
J
1
4
Qualifier Description
LCS or LCSD is outside acceptance limits.
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
5
6
Glossary
Abbreviation
¤
%R
CFL
CNF
DER
These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis
Percent Recovery
Contains Free Liquid
Contains no Free Liquid
Duplicate error ratio (normalized absolute difference)
Dil Fac
DL, RA, RE, IN
DLC
Dilution Factor
Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
Decision level concentration
MDA
EDL
MDC
MDL
ML
NC
ND
Minimum detectable activity
Estimated Detection Limit
Minimum detectable concentration
Method Detection Limit
Minimum Level (Dioxin)
Not Calculated
Not detected at the reporting limit (or MDL or EDL if shown)
PQL
QC
RER
RL
RPD
TEF
Practical Quantitation Limit
Quality Control
Relative error ratio
Reporting Limit or Requested Limit (Radiochemistry)
Relative Percent Difference, a measure of the relative difference between two points
Toxicity Equivalent Factor (Dioxin)
TEQ
Toxicity Equivalent Quotient (Dioxin)
7
8
9
10
11
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81552-1
2
Client Sample ID: 2610BEFF(062515)
Lab Sample ID: 490-81552-1
Date Collected: 06/25/15 12:20
Date Received: 06/26/15 08:45
Matrix: Water
Result Qualifier
ND
ND
ND
RL
0.500
0.500
0.500
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
Dil Fac
1
1
1
Bromodichloromethane
Bromoform
Bromomethane
ND
ND
ND *
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
Chlorodibromomethane
Chloroethane
Chloroform
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
ND
ND
ND
0.500
0.500
2.00
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
ND *
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
1,1-Dichloroethane
1,2-Dichloroethane
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
1
1
1,1-Dichloroethene
ND
0.500
ug/L
06/29/15 13:47
1
1,2-Dichloropropane
1,3-Dichloropropane
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
1
1
2,2-Dichloropropane
ND
0.500
ug/L
06/29/15 13:47
1
1,1-Dichloropropene
Diisopropyl ether
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
1
1
Ethylbenzene
ND
0.500
ug/L
06/29/15 13:47
1
Ethyl tert-butyl ether
Hexachlorobutadiene
Isopropylbenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
ND
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
Methylene Chloride
Naphthalene
ND
5.00
0.500
5.00
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
sec-Butylbenzene
Styrene
Tert-amyl methyl ether
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
29.6
Methyl tert-butyl ether
9.79
tert-Butylbenzene
1,1,1,2-Tetrachloroethane
ND
ND
10.0
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
1,1,2,2-Tetrachloroethane
ND
0.500
ug/L
06/29/15 13:47
1
tert-Butyl alcohol
3
4
Method: 524.2 - Volatile Organic Compounds (GC/MS)
Analyte
Benzene
Bromobenzene
Bromochloromethane
1
TestAmerica Nashville
Page 6 of 19
7/9/2015
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Client Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81552-1
2
Client Sample ID: 2610BEFF(062515)
Lab Sample ID: 490-81552-1
Date Collected: 06/25/15 12:20
Date Received: 06/26/15 08:45
Matrix: Water
3
4
Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued)
Analyte
Tetrachloroethene
Toluene
1
Result Qualifier
ND
ND
RL
0.500
0.500
MDL Unit
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 13:47
06/29/15 13:47
Dil Fac
1
1
5
6
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1,2,3-Trichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
1
1
1
10
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 13:47
06/29/15 13:47
1
1
11
Vinyl chloride
ND
0.500
ug/L
06/29/15 13:47
1
Xylenes, Total
ND
1.00
ug/L
06/29/15 13:47
1
12
Analyzed
06/29/15 13:47
06/29/15 13:47
06/29/15 13:47
Dil Fac
1
1
1
13
06/29/15 13:47
1
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
%Recovery Qualifier
107
103
101
Limits
70 - 130
70 - 130
70 - 130
99
70 - 130
Prepared
TestAmerica Nashville
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7/9/2015
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QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81552-1
2
Method: 524.2 - Volatile Organic Compounds (GC/MS)
3
Lab Sample ID: MB 490-260431/6
Matrix: Water
Analysis Batch: 260431
Analyte
Benzene
Bromobenzene
Bromochloromethane
1
Client Sample ID: Method Blank
Prep Type: Total/NA
MB MB
Result Qualifier
ND
ND
ND
4
5
RL
0.500
0.500
0.500
MDL Unit
ug/L
ug/L
ug/L
D
Prepared
Analyzed
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
Dil Fac
1
1
1
6
7
Bromodichloromethane
Bromoform
Bromomethane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
Chlorodibromomethane
ND
0.500
ug/L
06/29/15 12:55
1
Chloroethane
Chloroform
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
1
1
11
Chloromethane
ND
0.500
ug/L
06/29/15 12:55
1
2-Chlorotoluene
4-Chlorotoluene
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
1
1
12
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
ND
ND
ND
0.500
0.500
2.00
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
Ethyl tert-butyl ether
Hexachlorobutadiene
Isopropylbenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
Methylene Chloride
Methyl tert-butyl ether
Naphthalene
ND
ND
ND
5.00
0.500
5.00
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
sec-Butylbenzene
Styrene
Tert-amyl methyl ether
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
tert-Butyl alcohol
tert-Butylbenzene
1,1,1,2-Tetrachloroethane
ND
ND
ND
10.0
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
TestAmerica Nashville
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7/9/2015
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QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81552-1
2
Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued)
3
Lab Sample ID: MB 490-260431/6
Matrix: Water
Analysis Batch: 260431
Client Sample ID: Method Blank
Prep Type: Total/NA
RL
0.500
MDL Unit
ug/L
D
Prepared
Analyzed
06/29/15 12:55
Dil Fac
1
6
7
Tetrachloroethene
Toluene
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
1
1
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1,2,3-Trichlorobenzene
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
ND
ND
ND
0.500
0.500
0.500
ug/L
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
1
1
1
Trichloroethene
ND
0.500
ug/L
06/29/15 12:55
1
Trichlorofluoromethane
1,2,3-Trichloropropane
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
1
1
1,2,4-Trimethylbenzene
ND
0.500
ug/L
06/29/15 12:55
1
1,3,5-Trimethylbenzene
Vinyl chloride
ND
ND
0.500
0.500
ug/L
ug/L
06/29/15 12:55
06/29/15 12:55
1
1
Xylenes, Total
ND
1.00
ug/L
06/29/15 12:55
1
Analyzed
06/29/15 12:55
06/29/15 12:55
06/29/15 12:55
Dil Fac
1
1
1
06/29/15 12:55
1
MB MB
%Recovery Qualifier
104
101
100
Limits
70 - 130
70 - 130
70 - 130
98
70 - 130
Toluene-d8 (Surr)
Prepared
Lab Sample ID: LCS 490-260431/3
Matrix: Water
Analysis Batch: 260431
Analyte
Benzene
Bromobenzene
4
5
MB MB
Result Qualifier
ND
Analyte
1,1,2,2-Tetrachloroethane
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
5.00
5.00
LCS LCS
Result Qualifier
5.149
4.937
Unit
ug/L
ug/L
D
%Rec
103
99
%Rec.
Limits
70 - 130
70 - 130
Bromochloromethane
5.00
4.956
ug/L
99
70 - 130
Bromodichloromethane
Bromoform
Bromomethane
5.00
5.00
5.00
4.909
4.813
6.723 *
ug/L
ug/L
ug/L
98
96
134
70 - 130
70 - 130
70 - 130
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
5.00
5.00
5.00
5.369
4.889
5.038
ug/L
ug/L
ug/L
107
98
101
70 - 130
70 - 130
70 - 130
Chlorodibromomethane
Chloroethane
Chloroform
5.00
5.00
5.00
4.874
5.381
5.418
ug/L
ug/L
ug/L
97
108
108
70 - 130
70 - 130
70 - 130
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
5.00
5.00
5.00
6.456
4.705
5.236
ug/L
ug/L
ug/L
129
94
105
70 - 130
70 - 130
70 - 130
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
5.00
5.00
5.00
5.262
4.742
4.527
ug/L
ug/L
ug/L
105
95
91
70 - 130
70 - 130
70 - 130
1,2-Dibromoethane (EDB)
Dibromomethane
5.00
5.00
4.693
4.939
ug/L
ug/L
94
99
70 - 130
70 - 130
TestAmerica Nashville
Page 9 of 19
7/9/2015
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QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81552-1
2
Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-260431/3
Matrix: Water
Analysis Batch: 260431
3
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike
Added
5.00
Analyte
1,2-Dichlorobenzene
LCS LCS
Result Qualifier
5.261
Unit
ug/L
D
%Rec
105
%Rec.
Limits
70 - 130
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
5.00
5.00
5.00
4.966
4.995
7.929 *
ug/L
ug/L
ug/L
99
100
159
70 - 130
70 - 130
70 - 130
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
5.00
5.00
5.00
5.267
5.044
5.255
ug/L
ug/L
ug/L
105
101
105
70 - 130
70 - 130
70 - 130
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
5.00
5.00
5.00
5.068
5.021
5.186
ug/L
ug/L
ug/L
101
100
104
70 - 130
70 - 130
70 - 130
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
5.00
5.00
5.00
5.126
4.999
5.093
ug/L
ug/L
ug/L
103
100
102
70 - 130
70 - 130
70 - 130
Ethyl tert-butyl ether
Hexachlorobutadiene
Isopropylbenzene
5.00
5.00
5.00
5.097
4.981
5.087
ug/L
ug/L
ug/L
102
100
102
70 - 130
70 - 130
70 - 130
Methylene Chloride
Methyl tert-butyl ether
Naphthalene
5.00
5.00
5.00
4.990 J
5.075
4.459 J
ug/L
ug/L
ug/L
100
102
89
70 - 130
70 - 130
70 - 130
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
5.00
5.00
5.00
4.544
5.124
5.111
ug/L
ug/L
ug/L
91
102
102
70 - 130
70 - 130
70 - 130
sec-Butylbenzene
Styrene
Tert-amyl methyl ether
5.00
5.00
5.00
5.257
4.760
5.113
ug/L
ug/L
ug/L
105
95
102
70 - 130
70 - 130
70 - 130
tert-Butyl alcohol
tert-Butylbenzene
1,1,1,2-Tetrachloroethane
50.0
5.00
5.00
46.29
5.082
4.863
ug/L
ug/L
ug/L
93
102
97
70 - 130
70 - 130
70 - 130
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
5.00
5.00
5.00
5.168
4.808
4.936
ug/L
ug/L
ug/L
103
96
99
70 - 130
70 - 130
70 - 130
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1,2,3-Trichlorobenzene
5.00
5.00
5.00
5.138
4.607
5.119
ug/L
ug/L
ug/L
103
92
102
70 - 130
70 - 130
70 - 130
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
5.00
5.00
5.00
5.047
5.101
4.981
ug/L
ug/L
ug/L
101
102
100
70 - 130
70 - 130
70 - 130
Trichloroethene
Trichlorofluoromethane
5.00
5.00
5.092
5.441
ug/L
ug/L
102
109
70 - 130
70 - 130
1,2,3-Trichloropropane
5.00
4.673
ug/L
93
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
5.00
5.00
5.00
5.307
5.104
6.054
ug/L
ug/L
ug/L
106
102
121
70 - 130
70 - 130
70 - 130
70 - 130
Xylenes, Total
10.0
10.35
ug/L
104
70 - 130
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
LCS LCS
%Recovery Qualifier
101
102
1
5
6
7
8
9
10
11
12
13
Limits
70 - 130
70 - 130
TestAmerica Nashville
Page 10 of 19
4
7/9/2015
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81552-1
2
Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCS 490-260431/3
Matrix: Water
Analysis Batch: 260431
Surrogate
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
3
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
LCS LCS
%Recovery Qualifier
104
97
4
5
Limits
70 - 130
70 - 130
6
7
Lab Sample ID: LCSD 490-260431/4
Matrix: Water
Analysis Batch: 260431
Analyte
Benzene
Bromobenzene
Bromochloromethane
1
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
Added
5.00
5.00
5.00
LCSD LCSD
Result Qualifier
5.101
5.054
4.996
Unit
ug/L
ug/L
ug/L
D
%Rec
102
101
100
%Rec.
Limits
70 - 130
70 - 130
70 - 130
RPD
1
2
1
RPD
Limit
20
20
20
Bromodichloromethane
Bromoform
Bromomethane
5.00
5.00
5.00
4.837
4.721
6.482
ug/L
ug/L
ug/L
97
94
130
70 - 130
70 - 130
70 - 130
1
2
4
20
20
20
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
5.00
5.00
5.00
5.497
4.946
5.060
ug/L
ug/L
ug/L
110
99
101
70 - 130
70 - 130
70 - 130
2
1
0
20
20
20
Chlorodibromomethane
Chloroethane
Chloroform
5.00
5.00
5.00
4.833
5.682
5.522
ug/L
ug/L
ug/L
97
114
110
70 - 130
70 - 130
70 - 130
1
5
2
20
20
20
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
5.00
5.00
5.00
6.491
5.149
5.139
ug/L
ug/L
ug/L
130
103
103
70 - 130
70 - 130
70 - 130
1
9
2
20
20
20
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
1,2-Dibromo-3-Chloropropane
5.00
5.00
5.00
4.948
4.732
4.191
ug/L
ug/L
ug/L
99
95
84
70 - 130
70 - 130
70 - 130
6
0
8
20
20
20
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
5.00
5.00
5.00
4.849
4.943
5.138
ug/L
ug/L
ug/L
97
99
103
70 - 130
70 - 130
70 - 130
3
0
2
20
20
20
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
5.00
5.00
5.00
5.021
5.148
7.795 *
ug/L
ug/L
ug/L
100
103
156
70 - 130
70 - 130
70 - 130
1
3
2
20
20
20
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
5.00
5.00
5.00
5.115
5.065
5.350
ug/L
ug/L
ug/L
102
101
107
70 - 130
70 - 130
70 - 130
3
0
2
20
20
20
1,2-Dichloropropane
1,3-Dichloropropane
5.00
5.00
5.182
5.065
ug/L
ug/L
104
101
70 - 130
70 - 130
2
1
20
20
2,2-Dichloropropane
5.00
5.389
ug/L
108
70 - 130
4
20
1,1-Dichloropropene
Diisopropyl ether
Ethylbenzene
5.00
5.00
5.00
5.091
5.060
5.258
ug/L
ug/L
ug/L
102
101
105
70 - 130
70 - 130
70 - 130
1
1
3
20
20
20
Ethyl tert-butyl ether
Hexachlorobutadiene
Isopropylbenzene
5.00
5.00
5.00
5.110
4.901
5.134
ug/L
ug/L
ug/L
102
98
103
70 - 130
70 - 130
70 - 130
0
2
1
20
20
20
Methylene Chloride
Methyl tert-butyl ether
Naphthalene
5.00
5.00
5.00
5.028
5.075
4.260 J
ug/L
ug/L
ug/L
101
102
85
70 - 130
70 - 130
70 - 130
1
0
5
20
20
20
n-Butylbenzene
5.00
4.632
ug/L
93
70 - 130
2
20
TestAmerica Nashville
Page 11 of 19
7/9/2015
8
9
10
11
12
13
QC Sample Results
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81552-1
1
2
Method: 524.2 - Volatile Organic Compounds (GC/MS) (Continued)
Lab Sample ID: LCSD 490-260431/4
Matrix: Water
Analysis Batch: 260431
Client Sample ID: Lab Control Sample Dup
Prep Type: Total/NA
Spike
Added
5.00
5.00
Analyte
N-Propylbenzene
p-Isopropyltoluene
3
LCSD LCSD
Result Qualifier
5.195
5.081
Unit
ug/L
ug/L
D
%Rec
104
102
%Rec.
Limits
70 - 130
70 - 130
RPD
1
1
RPD
Limit
20
20
4
5
6
7
sec-Butylbenzene
Styrene
Tert-amyl methyl ether
5.00
5.00
5.00
5.283
4.679
4.996
ug/L
ug/L
ug/L
106
94
100
70 - 130
70 - 130
70 - 130
0
2
2
20
20
20
tert-Butyl alcohol
tert-Butylbenzene
1,1,1,2-Tetrachloroethane
50.0
5.00
5.00
44.13
5.034
4.902
ug/L
ug/L
ug/L
88
101
98
70 - 130
70 - 130
70 - 130
5
1
1
20
20
20
1,1,2,2-Tetrachloroethane
Tetrachloroethene
5.00
5.00
5.075
4.958
ug/L
ug/L
102
99
70 - 130
70 - 130
2
3
20
20
10
Toluene
5.00
5.043
ug/L
101
70 - 130
2
20
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
1,2,3-Trichlorobenzene
5.00
5.00
5.00
5.285
4.549
4.794
ug/L
ug/L
ug/L
106
91
96
70 - 130
70 - 130
70 - 130
3
1
7
20
20
20
11
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
5.00
5.00
5.00
4.634
5.149
4.857
ug/L
ug/L
ug/L
93
103
97
70 - 130
70 - 130
70 - 130
9
1
3
20
20
20
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
5.00
5.00
5.00
5.138
5.541
4.818
ug/L
ug/L
ug/L
103
111
96
70 - 130
70 - 130
70 - 130
1
2
3
20
20
20
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
5.00
5.00
5.00
5.299
5.160
6.118
ug/L
ug/L
ug/L
106
103
122
70 - 130
70 - 130
70 - 130
0
1
1
20
20
20
Xylenes, Total
10.0
10.60
ug/L
106
70 - 130
2
20
Surrogate
4-Bromofluorobenzene (Surr)
Dibromofluoromethane (Surr)
1,2-Dichloroethane-d4 (Surr)
Toluene-d8 (Surr)
LCSD LCSD
%Recovery Qualifier
102
100
100
Limits
70 - 130
70 - 130
70 - 130
98
70 - 130
TestAmerica Nashville
Page 12 of 19
7/9/2015
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9
12
13
QC Association Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81552-1
1
2
GC/MS VOA
3
Analysis Batch: 260431
Lab Sample ID
490-81552-1
LCS 490-260431/3
LCSD 490-260431/4
Client Sample ID
2610BEFF(062515)
Lab Control Sample
Lab Control Sample Dup
Prep Type
Total/NA
Total/NA
Total/NA
Matrix
Water
Water
Water
Method
524.2
524.2
524.2
MB 490-260431/6
Method Blank
Total/NA
Water
524.2
Prep Batch
4
5
6
7
8
9
10
11
12
13
TestAmerica Nashville
Page 13 of 19
7/9/2015
Lab Chronicle
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81552-1
2
Client Sample ID: 2610BEFF(062515)
Lab Sample ID: 490-81552-1
Date Collected: 06/25/15 12:20
Date Received: 06/26/15 08:45
Prep Type
Total/NA
Batch
Type
Analysis
Batch
Method
524.2
1
Matrix: Water
Run
Dil
Factor
1
Initial
Amount
10 mL
Final
Amount
10 mL
Batch
Number
260431
Prepared
or Analyzed Analyst
06/29/15 13:47 NC
Lab
TAL NSH
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177
3
4
5
6
7
8
9
10
11
12
13
TestAmerica Nashville
Page 14 of 19
7/9/2015
Method Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
Method
524.2
TestAmerica Job ID: 490-81552-1
1
2
Method Description
Volatile Organic Compounds (GC/MS)
Protocol
EPA-DW
Laboratory
TAL NSH
Protocol References:
EPA-DW = "Methods For The Determination Of Organic Compounds In Drinking Water", EPA/600/4-88/039, December 1988 And Its Supplements.
3
4
5
6
Laboratory References:
TAL NSH = TestAmerica Nashville, 2960 Foster Creighton Drive, Nashville, TN 37204, TEL (615)726-0177
7
8
9
10
11
12
13
TestAmerica Nashville
Page 15 of 19
7/9/2015
Certification Summary
Client: ARCADIS U.S., Inc.
Project/Site: 14489 - North East
TestAmerica Job ID: 490-81552-1
2
Laboratory: TestAmerica Nashville
3
Unless otherwise noted, all analytes for this laboratory were covered under each certification below.
Authority
Maryland
Program
State Program
EPA Region
3
Certification ID
316
4
Expiration Date
03-31-16
5
The following analytes are included in this report, but certification is not offered by the governing authority:
Analysis Method
524.2
524.2
524.2
524.2
524.2
524.2
524.2
524.2
524.2
1
Prep Method
Matrix
Water
Water
Water
Water
Water
Water
Water
Water
Water
Analyte
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
1,1-Dichloroethane
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane (EDB)
524.2
524.2
524.2
524.2
524.2
Water
Water
Water
Water
Water
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
2,2-Dichloropropane
2-Chlorotoluene
524.2
524.2
524.2
524.2
524.2
524.2
Water
Water
Water
Water
Water
Water
4-Chlorotoluene
Bromobenzene
Bromochloromethane
Bromomethane
Carbon disulfide
Chloroethane
524.2
524.2
524.2
524.2
524.2
524.2
524.2
Water
Water
Water
Water
Water
Water
Water
Chloromethane
cis-1,3-Dichloropropene
Dibromomethane
Dichlorodifluoromethane
Diisopropyl ether
Ethyl tert-butyl ether
Hexachlorobutadiene
524.2
524.2
524.2
524.2
524.2
524.2
524.2
524.2
Water
Water
Water
Water
Water
Water
Water
Water
Isopropylbenzene
Methyl tert-butyl ether
Naphthalene
n-Butylbenzene
N-Propylbenzene
p-Isopropyltoluene
sec-Butylbenzene
Tert-amyl methyl ether
524.2
524.2
524.2
524.2
Water
Water
Water
Water
tert-Butyl alcohol
tert-Butylbenzene
trans-1,3-Dichloropropene
Trichlorofluoromethane
6
7
8
9
10
11
12
13
TestAmerica Nashville
Page 16 of 19
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1
2
3
4
5
6
7
8
9
10
11
12
13
Page 17 of 19
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2
3
4
5
6
7
8
9
10
11
12
13
Page 18 of 19
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1
Login Sample Receipt Checklist
Client: ARCADIS U.S., Inc.
2
Job Number: 490-81552-1
Login Number: 81552
List Number: 1
Creator: McBride, Mike
List Source: TestAmerica Nashville
3
4
5
Question
Answer
Radioactivity wasn't checked or is </= background as measured by a
survey meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
N/A
The cooler or samples do not appear to have been compromised or
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time.
True
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
6
Comment
7
True
8
9
True
10
1.7
11
12
13
True
True
TestAmerica Nashville
Page 19 of 19
7/9/2015
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