ESI catalog for PerkinElmer Optima ICP-OES family

ESI catalog for PerkinElmer Optima ICP-OES family
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Evolution of Automation
ICP | ICPMS | AA
Elemental Scientific designs and produces a full range of automation and sample introduction systems
for the determination of trace element concentrations in liquid samples by inductively coupled plasma
instrumentation. Our extensive product line contains sample introduction devices for all models of ICP
instruments, including:
• Fully automated inline and offline
dilution / standardization /
QC systems
• Inert, chemically resistant spray
chambers and end caps
• Demountable o-ring-free injectors
made from platinum, sapphire, or
quartz
• FAST systems
• Innovative SC-DX Series clean,
intelligent autosamplers
• Inert MicroFlow and PolyPro
Nebulizers
• Inert autosampler and manual
sampling probes
• Precision micro peristaltic pumps
and syringe pumps
• Precision and standard quartz ICP
torches
• apex family of high sensitivity,
low contamination sample inlet
systems
• PC3 Peltier-cooled cyclonic spray
chambers
Our years of experience in the laboratory and in the field are at your disposal to help answer your
questions related to elemental analysis. We are pleased to provide our customers complimentary
analytical advice from our on-staff chemists.
Ordering Information:
You may contact us via phone, fax, e-mail, or through our website.
Phone:
1.402.991.7800
E-Mail:
esi@icpms.com
Fax:
1.402.991.7799
Website:
www.icpms.com
TABLE OF CONTENTS
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Nebulizers, Spray Chambers, Torches and Injectors
PFA and polypropylene ST-nebulizers ......................................40-41
Probes and capillaries for ST-nebulizers ....................................... 42
PFA integrated capillary nebulizers ................................................ 43
PFA integrated probe nebulizers .................................................... 44
MEINHARD® quartz and glass nebulizers ................................46-47
PFA FitKit MEINHARD® nebulizer connectors ..........................48-49
pergo nebulizer gas humidifier ..................................................50-51
Cyclonic spray chambers ..........................................................52-54
Torches and injectors ................................................................55-57
Peristaltic and Syringe Pumps
Peristaltic pumps.......................................................................58-59
MP2 peristaltic pump tubing ........................................................... 60
Syringe pumps ............................................................................... 61
High Performance Sample Introduction
apex systems ............................................................................62-63
PC3 Peltier coolers and heaters ..................................................... 64
HF-resistant sample introduction kit............................................... 65
SAMPLE INTRODUCTION
Consumables
FAST valves, stators and rotors ................................................66-67
Autosampler probes and connectors ........................................68-69
Fittings, tubing and loops ..........................................................70-71
High purity HF-resistant sample vials and bottles .....................72-74
Sample vessels .............................................................................. 75
Microtiter plates.........................................................................76-77
Large autosampler racks ............................................................... 78
Heated and micro autosampler racks ............................................ 79
Super autosampler racks ..........................................................80-81
Standards autosampler racks ...................................................82-83
CONSUMABLES
SC-DX Automation for Optima ICP
SC-DX autosamplers and FAST system .......................................... 8
optiFAST DXi system ....................................................................... 9
SC-DX and FAST systems ........................................................10-12
Micro sample and semiconductor autosamplers............................ 13
optiFAST system upgrades ............................................................ 14
oneFAST Systems
oneFAST universal, high-throughput sample
introduction systems................................................................. 15
Autosampler Accessories
Enclosures and ULPA filtered environments .................................. 16
Autosampler stands ....................................................................... 17
Application Systems
prepFAST inline dilution system ................................................18-22
hydrideICP system ....................................................................24-25
hydrideFAST 1 system ..............................................................26-27
hydrideFAST 2 system ..............................................................28-29
brineFAST S4 preconcentration system ...................................30-31
oilFAST high speed wear metals in oil system ..........................32-33
soilFAST high speed soil sample system ..................................34-35
microFAST OSP petrochemical system ....................................36-38
AUTOMATION
Glossary ..............................................................................................4-5
Installation and Training ..................................................................... 84
Page 3
Autosampler Dimensions ..............................................................85-86
Glossary
Application
Clinical
Small volume and high matrix samples such as blood, urine and serum.
Environmental
Drinking water, waste water, seawater, soils and other environmental samples.
Geochemistry
Highly acidified mining samples for transition metals and platinum group elements.
Nuclear
Samples containing Th, U, Pu or other actinides requiring small volumes and careful handling.
Organic Solvents
Sample introduction wear oils and volatile organic samples for petrochemical applications.
Remote Monitoring
Custom online monitoring and high efficiency sample transport for remote chemical baths.
Semiconductor
Ultra-trace analysis of high matrix samples in clean room environments.
Application Systems
prepFAST
prepFAST is a sample/standard system for FAST inline autodilution, autocalibration, auto QC dilution,
priority sample autodilution and auto MSA. (Pg 18)
hydrideICP / hydrideFAST 1 / hydrideFAST 2
hydrideICP / hydrideFAST utilizes an integrated hydride generator and precision micro peristaltic pump
to obtain sub-ppt ICP detection limits for hydride elements such as As, Se and Sb. (Pg 24 / Pg 26 / Pg
28)
brineFAST S4
For laboratories supporting chlor-alkali process control and other applications requiring the determination
of trace elements in brine. (Pg 30)
oilFAST
oilFAST improves both speed and data quality of wear metal analysis in diesel engines, increasing
throughput by a factor of 2 when compared with other dedicated oil autosamplers. (Pg 32)
soilFAST
Highest throughput soil analysis system with new clog-resistant metal-free valve. (Pg 34)
microFAST OSP
Analyze undiluted volatile organic solvents at low-flow rates using syringe pumps and eliminating
peristaltic pump tubing. Complete sample transport ensures equal response for different analyte species
in volatile solvents. Micro sample loading dramatically reduces waste. (Pg 36)
Function
FAST
Low Sample Consumption
Low Detection Limits
HF Resistant
High Precision / Isotope Ratio
Micro Samples
Preconcentration
High Throughput
Page 4
Elemental Scientific
2013
Materials
CTFE
Ethylene chlorotrifluoroethylene is a fluorocarbon-based polymer. ECTFE is used to minimize wear in
high-friction applications.
PTFE
Polytetrafluoroethylene is a synthetic fluoropolymer of tetrafluoroethylene. PTFE is hydrophobic: neither
water nor water-containing substances wet PTFE.
PEEK/PTFE Composite
Polyether ether ketone (PEEK) is a tan colored organic polymer thermoplastic used to fabricate items for
demanding applications, including bearings, piston parts, and pumps.
PFA
Perfluoroalkoxy is a superior fluoropolymer that is ultra clean, chemically inert and optically transparent.
This material is used for advanced liquid handling, high performance nebulizers and labware.
Polyethylene
Polyethylene is a thermoplastic polymer used for laboratory sample tubes and vessels.
Polypropylene
Polypropylene (PP) is a thermoplastic polymer used in a wide variety of applications. This material is
often chosen for its resistance to corrosion, heat and chemical leaching, and its resilience against most
forms of physical damage, including impact and freezing.
Polystyrene
Polystyrene is an aromatic polymer used for laboratory sample tubes and vessels.
Terminology
DXi - Integrated ESI precision micro peristaltic pump and FAST valve module.
FAST - Valve and loop combination that rapidly loads and injects the sample.
MP2 - Precision micro peristaltic pump.
PC3 - Peltier cooled cyclonic spray chamber.
SC-DX - Inert, chemically resistant autosampler constructed with dual x-rails, large diameter
Z-rail and C6 carriage.
SYRIX - Compact, low-profile, high-precision laboratory syringe pump.
Tubing Sizes
Red
- 0.15 mm i.d.
Yellow - 0.3 mm i.d.
Purple - 0.2 mm i.d.
Orange - 0.5 mm i.d.
Green - 0.25 mm i.d.
Blue
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Gray - 1.0 mm i.d.
- 0.8 mm i.d.
Page 5
prepFAST
The Next Stage of Automation
• FAST Inline Autodilution
• Autocalibration
• Over Range Sample Autodilution and Reanalysis
• Priority Sample Autodilution
• Automated Standard Additions (MSA)
PerkinElmer Optima 8300 ICP
with SC-2 DX and S400V
SC-2 DX
p r e p FA S T w i t h
mobile stand
See page 18 or visit
w w w. p r e p FA S T . c o m
for more information
SC-DX Automation for Optima ICP
SC-DX Autosamplers and FAST System
The SC-DX FAST is a reliable, high-throughput,
automated sample introduction system for the
Optima ICP. The combination of the SC-DX
FAST autosampler with the Optima ICP provides
the perfect platform to introduce even the most
demanding high matrix samples. The SC-DX FAST
is available in four autosampler sizes, holding up to
fourteen large sample racks.
SC-DX BENEFITS:
• Robust dual rail system
• Dual flowing rinse station
• Precision micro sampling
• Reset probe - prevents probe damage
• Flexible rack configurations
- micro samples to large bottles
• ULPA filter and cart options
FAST BENEFITS:
• FAST sample loading (0.5 mL sec-1)
• FAST stabilization time
• FAST washout
• FAST probe and loop rinsing
• Flexible for all applications
PerkinElmer Optima with SC-2 FAST DXi
The SC-DX FAST loads the sample loop as the
nebulizer and tubing are cleaned.
Normal Analysis
Load Sample / Rinse Nebulizer
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stabilization and most complete rinse-out of any
sample introduction system, reducing uptake and
wash times while increasing sample throughput.
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The autosampler probe and tubing are rinsed
while the sample is analyzed.
Page 8
Elemental Scientific
2013
optiFAST DXi System
Improve sensitivity, precision, and detection
limits while significantly increasing sample
throughput with the best performing FAST
system for the Optima. The optiFAST DXi
combines the benefits of the integrated MP2
precision micro peristaltic pump, the C2 quartz
dual cyclonic spray chamber, and the new P7
valve.
AUTOMATION
PerkinElmer Optima with FAST DXi
• DXi fully integrates with the Optima
• MP2 peripump improves precision
• C2 spray chamber improves
sensitivity and precision
optiFAST DXi integrated
into the PE Optima
showing a 4 channel
MP2 precision micro
peripump, P7 FAST
valve and quartz C2
spray chamber.
• Improved detection limits
• New P7 valve
- Zero dead volume
- Fastest stabilization time
- In-valve internal standard mixing
- Inert PFA rotor
C2 Quartz Dual Cyclonic
Spray Chamber
OPTIMA
Sample
Gas In
4
5
Vacuum
PFA-ST
Nebulizer
3
V1
2
6
PE Optima
ICP Torch with
Sapphire Injector
SC-2/4DX FAST Autosampler
Waste
Carrier
Diluent IS
Waste ESI DXi Module with
FAST Valve &
4ch Micro Peripump
© 2011 Elemental Scientific
optiFAST DXi System Diagram
www.icpms.com
Page 9
SC-DX and FAST Systems
SC-DX and FAST Systems for the Optima ICP
All SC-DX autosampler components are
composed of inert chemically resistant materials
for extended lifespan. Dual X-rails and large
diameter Z-rail provide precise sampling, virtually
eliminating missed samples–even on microtiter
plates. Reduce uptake and wash times while
increasing sample throughput by upgrading the
SC-DX autosampler to a FAST system.
The SC-DX FAST DXi system offers
enhanced precision and the ability to
add internal standard online at lower
dilution factors. The design of the MP2
minimizes the gaps between rollers,
resulting in even pressure points
along the tubing, which improves
signal stability, data quality and
detection limits.
SC-2 DX FAST
DXi System
SC-DX Systems for the PerkinElmer Optima
System
Description
SC-DX System
SC-DX autosampler
with dual flowing rinse
SC-DX FAST
System
SC-DX autosampler
with FAST for high
throughput and FAST
washout
SC-DX FAST
DXi System
SC-DX autosampler and
integrated MP2 precision
micro peristaltic pump
with FAST
SC-DX optiFAST SC-DX autosampler,
DXi System
integrated MP2 precision
micro peristaltic pump
with P7 FAST valve
and quartz C2 spray
chamber
SC-DX
A/S
FAST
Valve
Module
FAST DXi
Peripump
& Valve
PFA-ST
Nebulizer
Sapphire
Injector
P7
FAST
Valve
Quartz
C2 Spray
Chamber

 
  
     
    
SC-DX System Includes:
• 2 Sample Probes
• Standards Rack (10 positions)
• 4 Large Racks (21, 40, 60, 90 positions)
• Pack (10 ea) 50 mL Standards Vials (10 ea)
• Pack (60 ea) 15 mL Sample Vials (60 ea)
FAST DXi
Integrated MP2 micro
peristaltic pump with FAST
Page 10
Quartz
Cyclonic
Chamber
Elemental Scientific
 
Quartz C2
Spray Chamber
2013
SC-2 DX
SC-2 DX Systems Description
Part Number
SC-2 DX
SC-2 DX autosampler with dual
flowing rinse
2DX
SC-2 DX FAST
SC-2 DX autosampler with FAST for
high throughput and FAST washout 2DXF-57C
SC-2 DX
FAST DXi
SC-2 DX autosampler and
integrated MP2 precision micro
peristaltic pump with FAST
2DXFi-57C
SC-2 DX
optiFAST DXi
SC-2 DX autosampler, integrated
MP2 precision micro peristaltic
pump with P7 FAST valve and
quartz C2 spray chamber
2OPTF-87C
AUTOMATION
The SC-2 DX is a compact autosampler with dual flowing
rinse stations that holds 2 large racks or 4 micro racks.
See page 85 for SC-2 DX dimensions.
SC-4 DX
The SC-4 DX is an autosampler with dual flowing rinse
stations that holds 4 large racks or 6 micro racks. It is ideal
for labs with moderate sample throughput needs.
SC-4 DX Systems Description
Part Number
SC-4 DX
SC-4 DX autosampler with dual
flowing rinse
4DX
SC-4 DX FAST
SC-4 DX autosampler with FAST for
high throughput and FAST washout 4DXF-57C
SC-4 DX
FAST DXi
SC-4 DX autosampler and
integrated MP2 precision micro
peristaltic pump with FAST
4DXFi-57C
SC-4 DX
optiFAST DXi
SC-4 DX autosampler, integrated
MP2 precision micro peristaltic
pump with P7 FAST valve and
quartz C2 spray chamber
4OPTF-87C
See page 85 for SC-4 DX dimensions.
EXAMPLES OF SC-2 DX RACK CONFIGURATIONS
1 Large Rack 1 Microtiter Plate
1 Micro Rack
2 x 10
3x7
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Micro 90
4 Micro Racks
2 Large Racks
3x7
3x7
3x7
3x7
3x7
3x7
Page 11
SC-DX and FAST Systems
SC-8 DXS
The high capacity SC-8 DXS holds 8 large sample racks and
up to 40 standards/QC solutions (50 mL vials). It has the
smallest footprint of any 8 rack autosampler and is ideal for
labs with high sample throughput needs.
SC-8 DXS
Systems
Description
Benchtop
Cart Version Version
Part Number Part Number
SC-8 DXS
SC-8 DXS autosampler
with dual flowing rinse
8DX
8DX-BT
SC-8 DXS
FAST
SC-8 DXS autosampler
with FAST for high
throughput and FAST
washout
8DXF-57C
8DXF-BT-57C
SC-8 DXS
FAST DXi
SC-8 DXS autosampler
and integrated MP2
precision micro peristaltic
pump with FAST
8DXFi-57C
8DXFi-BT-57C
SC-8 DXS
optiFAST
DXi
SC-8 DXS autosampler,
integrated MP2 precision
micro peristaltic pump
with P7 FAST valve and
quartz C2 spray chamber
8OPTF-87C
8OPTF-BT-87C
See page 86 for SC-8 DX dimensions.
SC-8 DXS benchtop version
SC-14 DXS
The high capacity SC-14 DXS holds 14 large sample racks
and up to 10 standards/QC solutions (50 mL vials). It is ideal
for labs with the highest sample throughput needs.
SC-14 DXS
Systems
Description
Benchtop
Cart Version Version
Part Number Part Number
SC-14 DXS
SC-14 DXS autosampler
with dual flowing rinse
14DX
14DX-BT
SC-14 DXS
FAST
SC-14 DXS autosampler
with FAST for high
throughput and FAST
washout
14DXF-57C
14DXF-BT-57C
SC-14 DXS
FAST DXi
SC-14 DXS autosampler
and integrated MP2
precision micro peristaltic 14DXFi-57C
pump with FAST
14DXFi-BT-57C
SC-14 DXS
optiFAST
DXi
SC-14 DXS autosampler,
integrated MP2 precision
micro peristaltic pump
14OPTF-87C 14OPTF-BT-87C
with P7 FAST valve and
quartz C2 spray chamber
See page 86 for SC-14 DX dimensions.
Page 12
Elemental Scientific
2013
Micro Sample and Semiconductor Autosamplers
SC-Micro DX
AUTOMATION
The SC-Micro DX is a small-footprint (330mm x 223mm),
low-cost autosampler with instrument pumped dual
flowing rinse stations. It holds 2 microtiter plates or 2
micro racks and 10 standards vials.
SC-Micro DX System Includes:
2 Sample Probes
Standards Rack (10 positions)
3 Microtiter Plates (24, 48, 96 positions)
3 Micro Racks (21, 40, 90 positions)
Pk (10 ea) 20 mL PFA Standards Vials
Pk (10 ea) 2 mL PFA Sample Vials
Part Number
Description
m-DX
SC-Micro DX autosampler with dual flowing rinse
Contact a sales representative to discuss customizing the SC-Micro DX with an
optional diaphragm rinse pump or for glovebox applications.
SC-2 DX Semiconductor
The SC-2 DX Semiconductor autosampler with a
PTFE top is designed for ultra-pure semiconductor
applications where the lowest possible background
levels and chemical resistance are required.
SC-2 DX Semiconductor System Includes:
Ultem Sample Probe
2 PTFE Sample Probes
Standards Rack (10 positions)
4 Large Racks (21, 40, 60, 90 positions)
Micro Rack (21 positions)
High purity PFA dual rinse kit
Pk (10 ea) 50 mL Standards Vials
Pk (60 ea) 15 mL Sample Vials
Pk (30 ea) 2 mL PFA Sample Vials
Part Number
Description
2DX-SEMI
SC-2 DX Semiconductor autosampler with dual flowing rinse
PFA and PVDF vials recommended (see page 72-74)
Autosampler Capacity
Autosampler
SC-2 DX (Super rack)
50 mL
15 mL
8 mL
Microtiter-96 (2 mL)
52 (64)
120 (160)
180
384
SC-4 DX
94
240
360
576
SC-8 DX
208
480
720
N/A
SC-14 DX
304
840
1260
2880*
*Special version SC-14 for microtiter plates
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Page 13
optiFAST System Upgrades
optiFAST System Upgrades
The optiFAST System Upgrades allow any existing SC-FAST system to achieve the performance of the
optiFAST (see page 9). Also included is a convertible sapphire injector, allowing Optima 8000 series
injectors to be used with pre-8000 series Optima instruments.
optiFAST Upgrade (For Non-DXi FAST Systems)
This optiFAST System Upgrade is for labs
that have a FAST system, but do not have a
DXi integrated micro peristaltic pump.
optiFAST System Upgrade Includes:
P7 FAST Valve
Integrated MP2 Precision Micro
Peristaltic Pump
Quartz C2 Spray Chamber
PFA-ST3 MicroFlow Nebulizer
Convertible Sapphire Injector
Part Number
Description
OPT-UP-A-57C optiFAST upgrade for non-DXi
FAST systems
optiFAST Upgrade (For Existing FAST DXi system)
This optiFAST System Upgrade is for labs that
are currently using a FAST DXi in their sample
introduction setup.
optiFAST System Upgrade Includes:
P7 FAST Valve
Quartz C2 Spray Chamber
PFA-ST3 MicroFlow Nebulizer
Convertible Sapphire Injector
Part Number
Description
OPT-UP-B-57C optiFAST upgrade for DXi FAST systems
Page 14
Elemental Scientific
2013
oneFAST Systems
oneFAST
The oneFAST brings the field-proven capabilities of the SC-FAST to non-ESI autosamplers. The oneFAST
hardware and software has been optimized and integrated with the Optima to immediately increase
throughput by speeding stabilization time and rinse-out. The oneFAST reduces instrument maintenance and
matrix exposure while improving long-term performance.
oneFAST Basic
The oneFAST increases throughput with non-ESI
autosamplers.
Includes: FAST Valve
PFA-ST Nebulizer
oneFAST Controller
All Required Tubing
2 Probes-PFA/Carbon Fiber
Part Number
Description
SC-0400
oneFAST basic system
oneFAST Complete Optima
The oneFAST Complete includes an injector and spray
chamber, making any non-ESI autosampler ready for
increased throughput needs.
Includes:
FAST Valve
Quartz Cyclonic Spray Chamber
oneFAST Controller Convertible Sapphire Injector
PFA-ST Nebulizer
All Required Tubing
2 Probes - PFA/Carbon Fiber
Part Number
Description
SC-0457
oneFAST complete system for Optima
oneFAST DXi Complete Optima
The oneFAST DXi Complete includes a FAST DXi,
injector and spray chamber, making any non-ESI
autosampler ready for increased throughput needs.
Includes:
FAST DXi Peripump & Valve
2 Probes - PFA/Carbon Fiber
Quartz Cyclonic Spray Chamber
Convertible Sapphire Injector
oneFAST Controller
PFA-ST3 Nebulizer
All Required Tubing
Part Number
Description
SC-0457-DXi
oneFAST DXi complete system for Optima
www.icpms.com
Page 15
AUTOMATION
Universal, High-Throughput Sample Introduction System
Enclosures and ULPA Filtered Environments
Autosampler Enclosures and ULPA Filtered Environments
Autosampler Enclosures
SC-1807-DX Enclosure with
SC-8 DX autosampler
Enclosures protect samples and standards
from airborne contamination. An exhaust port
(100 mm, included) may be connected to the
laboratory ventilation system to exhaust acid
fumes and protect the laboratory environment
and equipment. Enclosures can be purchased
with or without an ULPA filter.
Enclosure
Only
Autosampler Model
SC-1207-DX-1000
Enclosure with SC-2 DX
autosampler
Enclosure with
ULPA Filter
Enclosure for SC-Micro DX
SC-1607-DX
N/A
Enclosure for SC-2 DX
SC-1207-DX
SC-1207-DX-1000
Enclosure for SC-4 DX
SC-1407-DX
SC-1407-DX-1000
Enclosure for SC-8 DX
SC-1807-DX
SC-1807-DX-1000
Enclosure for SC-14 DX
SC-1107-DX
SC-1107-DX-1030
Ultra-Low Particulate Arrester Air Filter and Mounting Plate
The ULPA (Ultra-Low Particle Arrester) filter creates a clean, positive
pressure environment for samples and standards and prevents
airborne contamination. The ULPA filter removes 99.999% of 0.12
micron particles.
(SC-0602)
ULPA Filter
ULPA Filter Specifications
Air Volume
Noise level
Power
1 m /min
56 dBA
25W
3
Part Number
Description
SC-0602
ULPA filter for ESI enclosures
SC-1107-0026
ULPA filter mounting plate for
SC-2 DX or SC-4 DX
The ULPA filter mounting plate fits the SC-2 DX
and SC-4 DX on either the right or left side of
the enclosure.
Page 16
OR
Elemental Scientific
2013
Autosampler Stands
Mobile Stands for SC-2 DX and SC-4 DX Autosampler
SC-2 DX and SC-4 DX Mobile Stands
AUTOMATION
The mobile stand provides a low-footprint platform for the SC-2 DX or SC-4 DX.
Benefits:
• Mobile with locking wheels for flexible positioning
• Convenient location for rinse and waste containers
• Shelf for additional sample introduction equipment, such as prepFAST
SC-1210-DX mobile stand with
SC-2 DX autosampler
SC-1410-DX mobile stand with
SC-4 DX autosampler
Part Number
Description
Part Number
Description
SC-1210-DX
Mobile stand for SC-2 DX
(autosampler not included)
SC-1410-DX
Mobile stand for SC-4 DX
(autosampler not included)
Accessible rinse
bottle can be refilled
in place
Storage space for
racks, solutions
and accessories
www.icpms.com
Page 17
prep FAST
T
TM
Inline Autocalibration,
Variable Autodilution,
and Auto QC Dilution
prepFAST is a dilution system that
automatically performs precise and
accurate inline dilutions for samples and
standards.
Benefits of prepFAST
• Autodilution
• Autocalibration
• Auto QC dilution
• Auto MSA
• FAST
Samples are rapidly (0.5 mL/sec) and reproducibly vacuum loaded into a sample loop. Inside the valve,
sample is mixed with the diluent and internal standard. The system delivers the diluted and mixed
sample to the nebulizer with final dilutions ranging between 1x and 400x.
Central to the system is the S400V syringe pump module. Precise (<± 0.05%), accurate (<± 0.2%),
smooth and balanced delivery of solution over a wide range of flow rates (1 to 1000 μL/min) ensures
rapid and reliable inline dilutions.
Capable of up to 400x dilution, the prepFAST is the fastest, simplest way to ensure high quality data in
every run.
P7+ Load
To ICP / ICP-MS Nebulizer
Sample
Internal Standard
Carrier
Diluent
Vacuum
P7+ Inject/Dilute
To ICP / ICP-MS Nebulizer
Rinse
Internal Standard
Carrier
Diluent
Vacuum
The prepFAST uses FAST vacuum loading to rapidly fill a sample loop. After sample injection, variable
syringe-driven carrier, diluent, and internal standard flows are mixed using the custom P7+ inline mixing
valve. The result is variable, inline dilution with FAST stabilization and washout.
Pa
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Autodilution in Seconds
Tedious manual preparation steps are
automatically handled by the prepFAST system,
making better use of time and resources.
Automated dilution is used for both calibration
and sample dilution. Dilutions are performed by
accurately controlling the sample and diluent
flow rates. Desired dilution factors are achieved
in seconds by using in-valve mixing capabilities.
Mixing inline eliminates the need to premix/dilute
samples in discrete tubes prior to analysis and
greatly improves sample throughput. Combined
with FAST technology, rapid sample uptake
and FAST washout times are independent of
dilution factor, allowing rapid injection of the next
sample.
• Rapid vacuum loading
• Inline dilution as sample is injected
• Rapid uptake and stabilization of sample
Autocalibration
Manual Dilution vs. prepFAST Autodilution
100x
2x
A 20 ppm standard was determined with various dilution
factors by manual dilution and prepFAST autodilution.
prepFAST inline autodilution is accurate and saves time.
Manual Calibration vs. prepFAST Autocalibration
User predefined dilution factors for a single
multi-element standard are used to build
calibration curves. Accuracy of dilution is
illustrated by excellent linearity of the calibration
curve (R2 = 0.9999).
• Automatically calibrates the instrument from a
single standard solution
• Improved linearity vs. calibrations prepared in
separate tubes
• Prepare calibration from a single multi-element
standard
• Easily create calibration curves with more
points (weighted curves)
• One bottle or two bottles per method—leaves
space in standards rack for more calibration
curves and QC
• Eliminate manual dilution errors
10x
Manual
Calibration
Autocalibration
prepFAST autocalibration from a single multi-element
standard saves time and improves accuracy.
2500x fold washout of Ag in seconds
< 2.5% RSD over 14 hours
FAST washout even for memory prone elements
Long-term stability
www.
ww
www.icpms.com
w icpms.com
Page 19
Page
19
prep FAST
T
TM
Automated QC Dilutions
Optima Winlab 5.3 software automatically
detects QC, internal standard, and sample
limit failures and directs the prepFAST to
automatically and immediately dilute and
reanalyze samples.
QC based automated dilution
of over range samples
Procedure:
• Optima software detects QC, internal
standard, or sample limit failure.
• prepFAST automatically dilutes the
sample inline using a user-defined
dilution factor (DF).
• If the diluted sample passes, the
sequence continues.
• If the diluted sample fails again, the
sample is automatically diluted by
DF2 up to DF = 400.
Sample limits and QC checks
can be defined for each analyte
in the Optima method.
Internal standard recovery can be monitored, and low or high
recoveries trigger autodilution and reanalysis.
Pa
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2013
Automated MSA
prepFAST automatically performs method of
standard additions to compensate for matrix
effects in high matrix samples.
Ba in 10% Brine
Procedure:
• Sample is introduced at the same flow
rate for each point on the standard
additions curve
• Different amounts of standard is added
from a single stock solution
• Diluent flow keeps the total solution flow
rate constant
Benefits:
• Best way to correct for matrix effects
• Completely automated, no manual
dilutions
Method of Standard Additions
curves in 10% Brine
Zn in 10% Brine
SC-2 DX prepFAST
(2ADFi-57C)
www.
ww
www.icpms.com
w icpms.com
Page 21
Page
21
prep FAST
T
TM
prepFAST Upgrade Path For
prepFAST
PerkinElmer Optima
Step 1. Select a prepFAST complete system
prepFAST System
P/N
prepFAST SC-2 DXi complete
2ADFi-57C
prepFAST SC-4 DXi complete
4ADFi-57C
prepFAST SC-8 DXi complete
8ADFi-57C
prepFAST SC-14 DXi complete
14ADFi-57C
Step 1. To upgrade an existing FAST,
FAST DXi or optiFAST system, select a
prepFAST S400V module (one required)
or
prepFAST
P/N
prepFAST module
PF-S400V
*HF resistant prepFAST module
PF-S400V-HF
*ESI suggests the (M157-5470) PFA HF-resistant spray
chamber with endcap
prepFAST Complete
System includes:
• SC-DX FAST autosampler
• 4 Syringe pump dilution module (S400V)
Step 2. Verify that you have one of the
following FAST systems (one required)
• Quartz C2 spray chamber
• FAST DXi micro peripump
FAST Systems
P/N
• Integrated P7+ FAST valve
SC-2 DX OptiFAST
2OPTF-87C
• Sapphire injector
SC-2 FAST DXi
2DXFi-57C
• PFA nebulizer
SC-2 DX FAST
2DXF-57C
• prepFAST cart
SC-4 DX OptiFAST
4OPTF-87C
SC-4 FAST DXi
4DXFi-57C
SC-4 DX FAST
4DXF-57C
SC-8 DX OptiFAST
8OPTF-87C
SC-8 FAST DXi
8DXFi-57C
SC-8 DX FAST
8DXF-57C
PerkinElmer Optima
8300 ICP
SC-14 DX OptiFAST
14OPTF-87C
SC-14 FAST DXi
14DXFi-57C
SC-14 DX FAST
14DXF-57C
optiFAST recommended
Step 3. (Optional) Select a prepFAST cart
to match the SC-DX FAST autosampler
Page 22
Elemental Scientific
Cart
P/N
SC-2 DX prepFAST Cart
SC-1210-DX-PF
SC-4 DX prepFAST Cart
SC-1410-DX-PF
SC-8 DX prepFAST Shelf
SC-1103-DX-PF
SC-14 DX prepFAST Shelf
SC-1103-DX-PF
2013
PC
3x
PC 3x Peltier Controlled
Cyclonic Chamber
Thermally stabilized
inlet system for the
PerkinElmer Optima
• Temperature control from
-10°C to +80°C
• Thermal stabilization of spray
chamber improves long-term stability
biility
• Last set temperature saved for stand
ta
and
alone operation
• USB or Bluetooth connectivity
• Remote monitoring and control
PC3x Peltier Heated or
Cooled Inlet System
See page 64 for more information.
Heating Function
Increases Sensitivity!
www.icpms.com
Elemental
Scientific
Page 23
hydrideICP
TM
A New, Compact Hydride
Generation System for ICP
with Improved Stability and
Performance
The new hydrideICP, a standalone hydride
generation system with precision micro peristaltic
pump, provides sub-ppb detection limits for
hydride-forming elements such as As, Se, Sb
and Hg.
Benefits:
• Increased sensitivity, up to 100x for hydrideforming elements
• Improved detection limits for As, Hg, Se, Sb and
other hydride-forming elements
• Improved stability
- MP2 micro peripump precisely mixes sample
and reagents, producing a stable formation of
H2 gas and hydrides
• Compact
- hydrideICP is the smallest system of its kind
on the market (95 mm x 118 mm x 140 mm)
hydrideICP generation system for
PerkinElmer ICP
• Chemically resistant construction
- MP2 micro peripump with ceramic pins, a PFA
mixing block and quartz GLS
• Convenient
- hydrideICP includes a PFA mixing block, which
is completely integrated into the MP2 pump
Universal spray chamber adapter
Universal spray chamber adapter replaces
the nebulizer on a cyclonic spray chamber
The universal spray chamber adapter is used to
connect the hydride gas/liquid separator to any spray
chamber.
Page 24
Hg Calibration Curve – 0, 0.5, 1, 5, and
10 ppb (Normal Resolution)
Elemental Scientific
2013
y
Sample
in
Hydrides
out to ICP
HCl NaBH4
in
in
Hydride
Generation
Ar
in
Sample In (As3+, Se4+)
Reagents (HCl, NaBH4)
Sweep Gas (Ar)
Matrix (Na+, Cl-, B[OH]3)
Analytes (AsH3, SeH2)
ESI has developed the smallest,
highest-performing and most
stable gas liquid separator
on the market. The design
promotes rapid mixing of sample
and reagents, resulting in an
efficient reaction and separation
of hydride gases from sample
liquids in a small volume.
Drain
1
OPTIMA
Sample
Sample
Gas +
Hydrides
2
Internal
Standard
PE Optima
3
Hydride
Gas/Liquid
Separator
HCl
4
Sample
Gas
NaBH4
5
Waste
6
Waste
ESI MP2 Peripump
6 channels
© 2012 Elemental Scientific
hydrideICP with internal standard system diagram
www.icpms.com
Part Number
Description
HG-MP2-6-A
Hydride ICP Generation System. HydrideICP Generator Kit (Hydride
quartz gas-liquid separator, four way tee, MP2 precision micro
peristaltic pump, universal spray chamber adapter and mounting plate).
Page 25
TM
Simple, Accurate, and FAST
Hydride Generation for ICP
The hydrideFAST 1 is a compact, inline,
easy-to-use device that generates hydrides
for ICP detection with high sensitivity and low
detection limits. The combination of the MP2
precision micro peripump and the patentpending hydrideFAST gas liquid separator
provides high sensitivity and excellent
detection limits.
SC-4 DX hydrideFAST 1 system for
the PerkinElmer Optima
hydrideFAST 1 System For PerkinElmer Optima
SC-DX FAST A/S
8 Channel FAST DXi
Peripump & Valve
Gas Liquid
Separator
Quartz Cyclonic
Spray Chamber






System
hydrideFAST 1
hydrideFAST 1
upgrade from
FAST
hydrideFAST 1 for the PE Optima
Detection limits (3s) for hydride-forming
elements in hydrideFAST mode
Analyte
LOD (ppb)
As
0.05
Se
0.08
Hg
0.02
Sb
0.1
Calibration curve for Se.
Calibration points at 0, 0.5, 1, 5, and 10 ppb.
Page 26
The hydrideFAST 1 system
has one mode of operation:
Mode 1 (hydride generation only)
Calibration curve for As.
Calibration points at 0, 0.5, 1, 5, and 10 ppb.
Elemental Scientific
2013
4
ICP Torch
Sapphire Injector
3
5
Vacuum
6
2
Universal Spray
Chamber Adapter
Cyclonic
Spray
Chamber
1
1
Carrier
Hydride
Gas/Liquid
Separator
2
SC DX FAST
Autosampler
Sample
Gas
HCl
3
NaBH4
4
5
Waste
ESI Micro Peripump
4 channels
© 2011 Elemental Scientific
hydrideFAST 1 system diagram including autosampler and FAST valve
hydrideFAST 1
Hydride-forming elements analyzed
hydrideFAST 1 Systems
hydrideFAST Spares
Part Number
Description
Part Number
Description
2HYF-1-57C
hydrideFAST 1 system SC-2 DXi
HG-USCA-01
4HYF-1-57C
hydrideFAST 1 system SC-4 DXi
Universal spray chamber adapter
for hydrideFAST 1
HG-GLS-001
Quartz hydride gas-liquid separator
HYF-UP1-A-57
hydrideFAST 1 upgrade from FAST
HG-MK-1
Hydride generator mounting kit
www.icpms.com
Page 27
hydride FAST 2
TM
Simultaneous hydride generation
and direct nebulization
The hydrideFAST 2 is an inline sample
introduction system that combines hydride
generation and direct nebulization for
simultaneous determination of all analytes.
This system improves sensitivity for hydrideforming elements while maintaining the multielement capabilities of direct nebulization.
The combination of the MP2 precision micro
peripump, the hydrideFAST gas liquid
separator and the C2 dual cyclonic spray
chamber are key to the excellent performance
of the hydrideFAST 2.
SC-4 DX hydrideFAST 2 system
for the PerkinElmer Optima
hydrideFAST 2 System For PerkinElmer Optima
SC-DX
FAST A/S
System
hydrideFAST 2
hydrideFAST 2
upgrade from
FAST

8 Channel FAST
DXi Peripump
& Valve
Gas Liquid
Separator
Quartz Hydride
C2 Chamber
PFA-ST
Nebulizer
Convertible
Sapphire
Injector










hydrideFAST 2
Hydride-forming elements analyzed in
modes 1 and 2
Elements analyzed in nebulization
modes 2 and 3
Page 28
Elemental Scientific
2013
,&37RUFK
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hydrideFAST 2 system diagram including autosampler and FAST valve
hydrideFAST 2 for the PE Optima
Detection limits (3s) for
hydride-forming and non-hydride
elements in hydrideFAST mode
Analyte
LOD (ppb)
As
0.08
Se
0.1
Hg
0.1
Sb
0.3
Ti
0.1
Mn
0.1
www.icpms.com
The hydrideFAST 2 system has three
modes of operation:
Mode 1 (hydride generation only)
Mode 2 (Simultaneous hydride generation
and FAST nebulization)
Mode 3 (FAST nebulization only)
hydrideFAST 2 Systems
Part Number
Description
2HYF-2-57C
hydrideFAST 2 system SC-2 DXi
4HYF-2-57C
hydrideFAST 2 system SC-4 DXi
HYF-UP2-A-57
hydrideFAST 2 upgrade from FAST
Page 29
brine FAST S4
T
TM
The brineFAST S4 is the all-new sample
introduction system for the determination of trace
impurities in brines and other high matrix samples
by ICPOES. Early detection of low and sub-ppb
alkaline earth and transition metals in high purity
brines improves chlor-alkali plant process control
and prevents costly damage to fluoropolymer
membrane cells. Undiluted 30% brines may be
sampled and analyzed directly, eliminating sample
preparation and reducing contamination.
Features:
• Fully automated, inline preconcentration and
matrix removal
• Direct mode with up to 50x fixed inline dilution
• Complete flexibility for preconcentration and
direct analysis
- Preconcentration
- Direct
- Preconcentration and Direct
• Eliminate peristaltic pump tubing
• Reduce carryover
• No daily maintenance
• Faster than the original brineFAST
• Detection limits in brine up to 400x better than
traditional sample introduction
Intensity
SC-2 DX brineFAST S4 system
Applications:
• Preconcentration mode for determination of low
and sub-ppb Ca, Mg, and other metals in 30%
brine
• Chlor-alkali plant product monitoring for caustic
soda and bleach
• Determination of alkali earth metals and many
transition metals in any high salt matrix sample
• High throughput FAST analysis with inline
dilution in Direct mode
Typical calibration curve for ultra-pure brine, <10 ppb.
Page 30
Time
Simultaneous elution profiles for
preconcentration elements allows simple
quantification after matrix removal.
Typical calibration curve for 50% Caustic Soda
(10x diluted) demonstrating linearity at higher
concentrations. If needed, higher level calibrations
at the ppm level are also linear.
Elemental Scientific
2013
All brineFAST S4 Systems
Include:
brineFAST
Ŷ Preconcentration
Ŷ Direct mode
• SC-DX FAST autosampler
• S400V syringe pump and
valve module
• FAST DXi dual valve module
and all connections
• brineFAST S4 concentrator
column
• brineFAST S4 cleanup
column
• Quartz C2 spray chamber
• Convertible sapphire injector
Spike recovery in 50%
caustic soda (10x diluted)
Analyte
% Recovery
Fe
99
Ni
99
Cu
99
Pb
101
Brine + 5 ppb
5 ppb
(1% HCl)
Calibration
blank (1% HCl)
Spike recoveries in 50%
Caustic soda (10x diluted)
show excellent recovery
against a calibration curve
prepared in diluted nitric
acid. Spike level is 50 ppb
(500 ppb for Fe).
Undiluted brine
Spectral data shows equal response for a Mg spike
in a 1% HCl standard and 30% brine.
Percent Spike Recovery Comparison in 30% Brine
Method Detection Limits Comparison in 30% Brine
Analyte
Traditional
(ppb)
brineFAST S4
(ppb)
Improvement
Factor
Ca
8.0
0.02
410
Mg
1.7
0.01
190
Fe
6.3
0.2
28
Traditional Introduction
(spiked at 100 ppb)
brineFAST S4
(spiked at 5 ppb)
Ca
132
103
Ba
1.4
0.2
7
Mg
64
96
Sr
1.1
0.01
150
Fe
104
95
Mn
1.2
0.02
57
Ba
106
99
Sr
75
99
Mn
111
99
Analyte
Comparison of spike recoveries for traditional
analysis and the brineFAST S4 preconcentration
technique. Note that the spike levels are 20x
lower with the brineFAST S4 than with the original
introduction system.
www.icpms.com
Part Number
Description
2BF-S4-57C
brineFAST S4 system SC-2 DXi
4BF-S4-57C
brineFAST S4 system SC-4 DXi
Page 31
oil FAST
TM
The oilFAST is the fastest sample introduction
system for the determination of wear metals
in lubricating oils, with sample-to-sample time
less than 20 seconds. When configured for
inline mixing, the oilFAST can analyze up to 140
samples per hour.
Benefits:
• Fastest sample throughput
• Fastest rinse-out
• Lowest carryover
• Reliable long-term performance with fewest
moving parts
• Simple conversion from undiluted mixing
• Large channels for rapid sample loading
• Integrated sample mixing (oilFAST 2)
• The valve and pump module integrates to the
ICP instrument
SC-4 DX oilFAST 2 system
oilFAST SYSTEMS FOR PERKINELMER OPTIMA
Screen Tip
Probe
FAST
Injection
 


 


System
Description
SC-DX
oilFAST 1
SC-DX autosampler,
integrated MP2 precision
micro peristaltic pump with
FAST valve, Gem Cone oil
nebulizer and screen tip
probe
SC-DX autosampler,
integrated MP2 precision
micro peristaltic pump with
dual FAST valves, Gem
Cone oil nebulizer and
screen tip probe
oilFAST 2
Unmixed
Gem Cone
Oil Nebulizer
Mixed
Sample
Pre-mixing

Analysis Time Per Sample
80
70
60
Time (s)
50
40
30
20
10
0
SC-FAST With Mixing
Diesel engine oil sample with
kerosene diluent, before and after
3-second mixing, using the oilFAST 2.
Page 32
SC-FAST Without Mixing
Conventional Oil
Autosampler
Compared to conventional autosamplers, the
oilFAST improves sample-to-sample analysis time by
a factor of 3.5 (< 17 seconds per sample).
Elemental Scientific
2013
Gemcone
Oil
Nebulizer
FAST
Valve
ICP Torch with
Sapphire Injector
SC DX FAST
Autosampler
Waste
Ar
Regulator
0.25bar
or
Kerosene
Carrier
N2
PE Optima
Argon
Vacuum
Kerosene
Rinse
OPTIMA
Waste
Dual Valve DXi with
4 channel micro peripump
© 2011Elemental Scientific
oilFAST 2 High-Speed ICP sample introduction system diagram, with sample pre-mixing.
Integrated sample mixing, through the ESI screen-tip mixing
probe, is a low-maintenance, effective solution for mixing. The
oilFAST 2 system can mix sample and diluent using inert gas
probes. After 3 seconds bubble mixing is complete, the FAST
vacuum loads the sample onto a loop for introduction.
Screen Tip Oil Probe
oilFAST Analysis: 100 ppm Co internal standard recovery
120
% recovery
100
80
60
40
20
0
0
25
50
75
sample #
100
125
150
1.6E+07
100000
1.2E+07
75000
8.0E+06
50000
4.0E+06
25000
0
0.0E+00
0
20
40
60
80
Sample #
100
120
Signal Intensity: Fe259
Signal Intensity: Ca315
oilFAST Analysis: 140 samples in 1 hour
140
Repeated analysis of a pooled oil sample containing
Co internal standard and 21 analytes, including Ca at 4300 ppm
and Fe at 8 ppm, showing stability over one hour.
www.icpms.com
60 position metal sample rack
(See page 78 for more information)
Part
Number
Description
4OF1-57A
oilFAST 1 system SC-4 DXi
8OF1-57A
oilFAST 1 system SC-8 DXi
4OF2-57A
oilFAST 2 system SC-4 DXi
8OF2-57A
oilFAST 2 system SC-8 DXi
Page 33
soil FAST
T
TM
The soilFAST combines a high-speed
autosampler with fluoropolymer injection
valve for robust, high-throughput sample
analysis. Samples are vacuum loaded into a
fluoropolymer loop in less than one second
and injected into the nebulizer and micro spray
chamber. Ninety Mehlich-3 soil extract samples
may be determined in less than 11 minutes only 7 seconds, sample-to-sample.
All soilFAST Systems Include:
• SC-DX autosampler
• FAST DXi valve module and all connections
• Quartz micro cyclonic spray chamber
• Convertible sapphire injector
SC-2 DX soilFAST system
Concentration (ppm)
Element
1 mm 6 port FAST valve and micro quartz
cyclonic spray chamber
Spike
Determined
% Recovered
Mg
600
590
98
Ca
6000
5934
99
K
1000
968
97
Na
150
153
102
Fe
200
197
98
Mn
100
99
99
Cu
20
19.8
99
B
5
5.0
100
P
200
200
100
S
100
99
99
Zn
10
9.8
98
Typical soilFAST recoveries
Quartz
Micro Cyclonic
Spray Chamber
Sample
Gas In
OPTIMA
4
5
Vacuum
3
V1
2
6
PFA-ST
Nebulizer
PE Optima
ICP Torch with
Sapphire Injector
SC-2/4DX FAST Autosampler
Carrier
Waste
ESI DXi Module with
FAST Valve &
4ch Micro Peripump
© 2011 Elemental Scientific
soilFAST system diagram
Page 34
Elemental Scientific
2013
Calibration of SC-FAST, Optima 5300, 7 seconds sample-to-sample
Boron Reproducibility
Calcium Reproducibility
244 boron spectral overlays. The blank, 1.25 ppm,
2.5 ppm, and 5 ppm boron standards are each
analyzed 61 times.
244 calcium spectral overlays. The blank, 1000 ppm,
3000 ppm, and 6000 ppm calcium standards are
each analyzed 61 times.
Operating Parameters
Part Number
Description
Sample Loop
0.1 mL
2SLF-57C
soilFAST system SC-2 DXi
Fill Time
0.5 sec
4SLF-57C
soilFAST system SC-4 DXi
ICP Read Delay
1 sec
8SLF-57C
soilFAST system SC-8 DXi
Integration Parameters
Manual, 2 ms,100 reps
soilFAST system SC-14 DXi
1500 W
14SLF-57C
ICP Power
Nebulizer Gas Flow Rate
0.5 L/min
www.icpms.com
Page 35
micro FAST OSP
The microFAST OSP uses prepFAST
technology to determine low ppb
concentrations of metals in undiluted, volatile
solvents such as methylbutane, hexane,
octane, benzene, toluene, gasoline, and
naphtha. One dedicated syringe loads a
sample or standard onto a custom, inert
injection valve. When the sample is injected
into the ICP, three additional high-purity
syringes, flowing at micro flow rates, perform
the desired dilution and addition of internal
standard.
Benefits:
• All liquid flows are syringe driven
• Syringe loading of micro samples
• Autocalibration
• Automated addition of internal standard
• Inline dilution
• Analyze undiluted volatile solvents
• Micro flow rates from 5 to 40 μL/min
• High sensitivity
• Minimize or eliminate sensitivity differences
due to speciation of Si and other elements
SC-2 DX microFAST OSP system
All microFAST OSP Systems Include:
• SC-DX FAST autosampler
• FAST DXi valve module and all connections
• S400V syringe pump module
• Sapphire injector
• PC3x Peltier controlled quartz drainless o-ring-free
cyclonic spray chamber
Load
Internal Standard
Sample
Nebulizer
To ICP / ICP-MS
Diluent
Carrier
Sample
Inject/Dilute
Internal Standard
Rinse
Nebulizer
To ICP / ICP-MS
Diluent
Carrier
Vacuum
Page 36
Elemental Scientific
2013
Autocalibration
microFAST OSP calibration curves prepared from a single stock standard in undiluted toluene, 10 ppb to 100 ppb.
Spike Recoveries in High TDS
Organometallic Samples
Calibration of Silicone Oil in Undiluted MIBK
)
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Trimethylaluminum (TMA) is a pyrophoric liquid used
in semiconductor manufacturing processes. Elemental
impurities in TMA can be determined by diluting it in
toluene and measuring it directly with the microFAST
OSP. Spike recoveries at 0.1 and 0.5 ppm for various
common contaminants are shown.
www.icpms.com
Determination of silicone oil extracted in MIBK is of
interest for quality control processes in the medical
industry. The microFAST OSP can automatically build
the calibration from a single stock standard of silicone
oil in MIBK for trace detection and determination of
silicone oil in undiluted MIBK extractions.
Page 37
micro FAST OSP
TM
Introduction of silanes and siloxanes in organic solvents
Instrument response from 10 ppm Si standards made from various silanes and siloxanes ranging in MW
from 108 to 793. The microFAST OSP dramatically reduces species-related intensity differences and
allows more accurate determination of Si. Standard sample introduction: sample was diluted in kerosene
and introduced at 0.8 mL/min with a PFA nebulizer and baffled quartz cyclonic spray chamber.
Detection Limits (ppb)
(Sample flow rate, 10 μL/min)
MW
Si-containing
Compound
108.64
chlorotrimethylsilane
144.33
tetraethylsilane
162.38
hexamethyldisiloxane
186.40
divinyltetramethyldisiloxane
Analyte
Heptane
Gasoline
Toluene
Ag 328.068
1.5
25
1.4
Al 308.215
7.8
6.0
9.9
B 249.677
5.4
9.4
0.8
Ba 233.527
0.5
0.9
0.6
Ca 317.933
2.4
3.6
3.9
Cd 228.802
1.1
1.1
1.2
Cr 267.716
1
0.3
0.5
222.47
hexamethylcyclotrisiloxane
Cu 327.393
1.4
0.6
1.0
296.61
Fe 238.204
0.6
1.0
0.5
octamethylcyclotetrasiloxane
K 766.490
1.7
14
36
793.19
octaphenylcyclotetrasiloxane
Mg 285.213
1.1
0.8
0.9
Mn 257.610
0.3
0.4
0.8
Mo 202.031
2.6
1.9
2.1
Ni 221.648
10
0.4
0.5
Pb 220.353
14
1.6
3.6
Sb 206.836
10
2.6
5
Si 251.611
2
1.1
0.5
Sn 189.927
4
1.5
1.6
Ti 334.940
1.3
0.7
0.6
V 290.880
0.8
0.7
0.4
Zn 206.200
1.2
1.4
0.6
Page 38
Part Number
Description
2MFP-57C
microFAST OSP system SC-2 DXi
4MFP-57C
microFAST OSP system SC-4 DXi
Elemental Scientific
2013
brine FAST S4
TM
TM
Improved Detection Limits For Alkaline Earth
And Transition Metals In High Purity Brines
The brineFAST is a fully-automated, online preconcentration
and matrix removal system that improves detection limits for
Ca, Mg, Fe, Ba, Sr, Mn and other elements in undiluted brines
by more than an order of magnitude.
See page 30 for more information.
Elemental
Scientific
PFA and Polypropylene ST-Nebulizers
PFA and Polypropylene
High-Efficiency MicroFlow Nebulizers
MicroFlow nebulizers are resistant to clogging, reliably self-aspirated or pumped to produce a fine aerosol
for high transport efficiency and high sensitivity.
PFA-ST Nebulizers
The PFA-ST MicroFlow nebulizer is made from high purity, HF
resistant PFA. It has an exchangeable external sample uptake
capillary. The sample uptake rate is controlled by the diameter of
the external capillary or probe.
Benefits:
• All PFA construction
• Exchangeable uptake capillaries allow one nebulizer to be used
at different self-aspiration rates from 20 μL/min to 700 μL/min
• Chemically resistant—ideal for strong acids, alkalis and
organics
• Can be pumped from < 0.1 mL/min to 3.0 mL/min
• Direct analysis of volatile and non-volatile organic solvents
• Longer lifetime than glass or quartz nebulizers
Part Number
Description
Part Number
Description
ES-2040-57
PFA-ST self-aspirating nebulizer with
external 1/4-28 threaded connector.
ST3-57
PFA-ST3 MicroFlow nebulizer
with external 1/4-28 threaded
connector. Designed for superior
clog resistance and higher sensitivity
compared to the standard PFA
nebulizer.
Part Number
Description
ES-2030-57
PFA MicroFlow high solids large
bore nebulizer with external 1/4-28
threaded connector. Ideal for strong
acids, high solids, alkalis, organic
solvents, soils and high salt solutions.
Page 40
Elemental Scientific
2013
PolyPro-ST Nebulizer
The PolyPro-ST nebulizer is a low cost HF resistant
alternative to the PFA nebulizer. The PolyPro nebulizer
has a lower chemical resistance than the PFA nebulizer,
but has the same high-efficiency aerosol generation.
It is a robust nebulizer that can self-aspirate with an
exchangeable external sample uptake capillary or can be
used with a peristaltic pump.
Part Number
Description
ES-4040-57
Poly-pro self-aspirating nebulizer with
external 1/4-28 threaded connector
apex MicroFlow PFA Self-Aspirating Nebulizers
Part Number
Description
ES-2040-7000
High temperature apex-ST PFA
MicroFlow nebulizer with external
1/4-28 threaded connector
ES-2002-7000
High temperature apex-100 PFA
nebulizer with integrated 90-150 μL/min
self-aspiration capillary.
SAMPLE INTRODUCTION
These nebulizers allow self-aspiration at low sample
consumption rates with the apex high sensitivity
desolvation system.
ES-2002-7205-080 High temperature apex-100 PFA
nebulizer with Ultem manual sampling
probe, 90-150 μL/min, 80 cm capillary
Syringe Flush Kit
Use syringe and white adapter to back-flush the carrier
line or tee-line. Use syringe and red adapter to forward
flush the carrier line, the side port of the tee-line, and to
forward flush the PFA nebulizer.
Part Number
Description
SC-0599-0109
Syringe flush kit. Includes 3 mL syringe, two
luer to 1/4-28 adapters.
Nebulizer Obstruction Removal Kit
While naturally resistant to obstructions, PFA
nebulizers may occasionally require maintenance.
Use this kit to safely remove obstructions in all
PFA-ST nebulizers for long-term high performance.
Never back-flush a PFA-ST nebulizer.
Part Number
Description
ES-2046-0001
Fused silica obstruction removal kit for
ST-type nebulizers. Includes one guide,
10 pieces of fused silica and instructions.
www.icpms.com
Page 41
Probes and Capillaries for ST-Nebulizers
Sample Capillaries / Probes
PFA Sample Capillaries for ST Nebulizers
Part
Number
I.D.
Self-aspiration rate
(@1L/m Ar)
ES-2045
0.15 mm 20 μL/min
■ (red)
■ (purple)
ES-2043
0.20 mm 50 μL/min
ES-2042
0.25 mm 100 μL/min ■ (green)
ES-2047
0.30 mm 200 μL/min ■ (yellow)
ES-2041
0.50 mm 400 μL/min ■ (orange)
ES-2044
0.80 mm 700 μL/min ■ (blue)
ES-2049
1.00 mm 1 mL/min
■ (gray)
Carbon Fiber Supported Autosampler Probes for ST Nebulizers
ST nebulizer probes connect directly to any ST-type nebulizer.
The 1/4-28 threaded fitting provides a secure, zero-deadvolume connection with no additional fittings required.
Probes for ESI SC Autosamplers
Part Number
Probe i.d.
ES-5037-3250-080 0.25 mm
Capillary Self-aspiration
Length rate (@1L/m Ar)
80 cm
100 μL/min
ES-5037-3500-080 0.50 mm
80 cm
400 μL/min
ES-5037-3250-100 0.25 mm
100 cm
100 μL/min
ES-5037-3500-100 0.50 mm
100 cm
400 μL/min
Also available with Ultem support.
Probes for PE S10 Autosamplers
Part Number
Probe i.d.
Capillary Self-aspiration
Length rate (@1L/m Ar)
ES-5037-9250-100
0.25 mm
100 cm
100 μL/min
ES-5037-9500-100
0.50 mm
100 cm
400 μL/min
Also available with Ultem support.
Probes can be custom-made to specific
lengths and materials at no extra charge.
Page 42
Elemental Scientific
2013
PFA Integrated Capillary Nebulizers
PFA Nebulizers with Integrated Capillaries
PFA Nebulizers with Integrated Capillaries
Self-aspirating PFA MicroFlow nebulizers are
constructed entirely from chemically resistant
fluoropolymers ideal for strong acids, alkalis,
organics and high salt solutions. They are
resistant to clogging, and produce a fine
aerosol for high transport efficiency and high
sensitivity.
Benefits:
• Integrated capillary for self-aspiration, ideal
for low flow, clean applications
• Chemically resistant—ideal for strong acids,
alkalis, organics
• Low, spike-free background for important
elements such as Fe and Ca
• Produces a fine aerosol for high transport
efficiency and high sensitivity
• Direct analysis of volatile and non-volatile
organic solvents
PFA Nebulizers with
Integrated Fluoropolymer Capillaries
Model
Part Number
Measured self-aspiration
rate (@1L/m Ar)
PFA-20
ES-2020
20 μL/min
PFA-50
ES-2000
50 μL/min
PFA-100
ES-2002
100 μL/min
PFA-200
ES-2003
200 μL/min
PFA-400
ES-2005
400 μL/min
Other flow rates made to order
www.icpms.com
Page 43
SAMPLE INTRODUCTION
• All PFA construction
PFA Integrated Probe Nebulizers
PFA Nebulizers with Integrated Probes
Self-Aspirating PFA Nebulizers with Integrated Probes
These nebulizers self-aspirate at lowflow rates with any autosampler and
provide the same benefits of the PFA
MicroFlow nebulizer. The integrated
sampling probe is constructed by
encapsulating a rigid support material
between layers of PFA to provide
a chemically-resistant probe that is
mechanically stable and resilient.
Probes can be custom made to
specific lengths and materials at
no extra charge.
PFA MicroFlow Nebulizer with Integrated
Autosampler Probe (Carbon Fiber support)
for Environmental/Clinical Applications
PFA MicroFlow Nebulizer with Integrated
Autosampler Probe (Ultem support) for
High Purity Semiconductor Applications
Model
Part Number
Self-aspiration
rate (@1L/m Ar)
Length
Model
Part Number
Self-aspiration
rate (@1L/m Ar)
Length
PFA-20
ES-2020-3503-100
20 μL/min
100 cm
PFA-20
ES-2020-3505-100
20 μL/min
100 cm
PFA-50
ES-2000-3503-100
50 μL/min
100 cm
PFA-50
ES-2000-3505-100
50 μL/min
100 cm
PFA-100
ES-2002-3503-100
100 μL/min
100 cm
PFA-100 ES-2002-3505-100
100 μL/min
100 cm
PFA-200
ES-2003-3503-100
200 μL/min
100 cm
PFA-200 ES-2003-3505-100
200 μL/min
100 cm
PFA-400
ES-2005-3503-100
400 μL/min
100 cm
PFA-400 ES-2005-3505-100
400 μL/min
100 cm
Also available with PEEK support and for S10 Autosampler
Page 44
Elemental Scientific
2013
MEINHARD
®
NEW PLUS NEBULIZERS
with PFA FitKit Quick Connects
MEINHARD® SilQ+ high purity nebulizer
with PFA FitKit
NEW
EW
W Quartz and Glass
Nebulizers
ebullizers with PFA FitKit
• SilQ+
lQ+ High
H
Purity Quartz Nebulizer
• TQ+
Q+ Qua
Quartz
artz Nebulizer
• TR+ Glass
ss Nebulizer
See page 46 for more information.
Enhance Your Detection Limits,
Reduce Sample Contamination
www.icpms.com
Elemental
Scientific
Page 45
MEINHARD® Quartz and Glass Nebulizers
MEINHARD ®
Concentric Nebulizers for ICPOES
MEINHARD® Plus Nebulizers have the lowest dead volume of any glass or quartz nebulizer. The low dead
volume and high sensitivity provide excellent detection limits and washout.
Each MEINHARD® Plus nebulizer comes with the FitKit+ gas and sample quick connect fittings. The
connections are made with high-purity PFA, minimizing the chance of contamination during backflow events.
The gas connection fits snugly over the maria on the sidearm of the nebulizer.
Features for all MEINHARD® Plus Nebulizers:
• Self aspiration rate 0.5 mL/min with argon flow 1 L/min at 50 PSI (3.4 bar/345 kPa).
• Peristaltic pumped rate 0.1 mL/min to 3.0 mL/min.
• Includes FG Gas Quick Connect (PFA) and F2 Quick Connect with 0.5 mm i.d. ■ (orange marker) capillary,
70 cm.
Quartz Nebulizers
NEW SilQ+ Ultra-high Purity
Quartz Nebulizer
• Highest purity quartz
• Lowest contamination, especially for Al, Fe, K
Part Number
Application
SILQ-50
For use with all
standard non-HF
applications
Part Number
Application
TQP-50
TQP
For use with all
standard non-HF
applications
Part Number
Application
TRP-50
For use with all
standard non-HF
applications
NEW TQ+ Quartz Nebulizer
• Quartz
ers
• Low blank levels compared to glass nebulizers
Glass Nebulizer
NEW TR+ Glass Nebulizer
• Borosilicate glass
• Economical
Page 46
Elemental Scientific
2013
Quartz and Glass High Purity Nebulizers
NEW SilQ+ High Purity Quartz Nebulizer
SilQ+ comes equipped with PFA FitKit gas and
sample quick connect fittings that eliminate
contaminants from the conventional connectors
commonly used with other nebulizers. The
fittings can be rapidly attached and removed.
The gas quick connect creates a snug seal
around the maria on the SilQ+ sidearm.
MEINHARD® SilQ+ high purity nebulizer
with PFA FitKit+
Each nebulizer is manufactured and tested to
exacting specifications. The standard SilQ+
nebulizer requires 50 psi for 1 L/min of argon
carrier and 0.5 mL/min solution uptake. Other
versions are available.
Potential Blank from Nebulizer
Comparison of metal impurity in SilQ+ and TQ+
Quartz nebulizers. SilQ+ impurities on average
are 60 times lower than standard quartz nebulizers.
Aluminum impurities in SilQ+ nebulizers are more
than 400,000 times lower than glass.
Comparison of metal impurity in Glass and TQ+
Quartz nebulizers. Glass nebulizers have high levels
of impurity for elements such as Al, Fe, K, Mg.
www.icpms.com
Page 47
SAMPLE INTRODUCTION
The SilQ+ nebulizer by MEINHARD® is perfect
for applications requiring high sensitivity. Made
from the highest purity synthetic quartz, the
SilQ+ nebulizer has low levels of trace elemental
impurities, reducing the risk of sample
contamination. SilQ+ nebulizers improve
wash-out rates and generate low, stable blanks
that can enhance ICP detection limits.
PFA FitKit MEINHARD® Nebulizer Connectors
NEW Plus Nebulizer PFA FitKit Quick Connects
FG Gas Quick Connect for MEINHARD® Nebulizers
FG Gas Quick Connect for MEINHARD® Nebulizers with
maria for both small bore and standard bore nebulizers.
Part Number
Application
FG
For use with all MEINHARD® nebulizers
FG Gas Quick Connect with
connector for PFA tubing
Elemental Scientific introduces the PFA FitKit Quick Connects, a revolutionary new gas and sample fitting
system for MEINHARD® Plus nebulizers. The kit includes a gas connection (FG), standard integrated
capillary sample connection (F2) and two other sample connection (F1 and F0) options to choose from.
FG gas connection forms a tight seal over the maria on the sidearm of the MEINHARD® nebulizers.
FG offers the benefits of an easy-to-use quick connect while maintaining high purity for sensitive
ICP applications. In a test that simulated a backflow event, FG produced
concentrations of elements like Fe and Cr that were four orders of magnitude
lower than concentrations leached from a conventional fitting (Figure 1).
Benefits:
• High purity PFA fluoropolymer construction
maria
• Easy to connect and disconnect
• One connection fits any MEINHARD® nebulizer
Conventional gas
line connector
PFA FG quick
connect gas line
Figure 1. Leach test of a conventional gas line connector and PFA FG
Page 48
Elemental Scientific
2013
Convenient PFA Connectors
The sample connector is a low dead-volume quick connect for MEINHARD® Plus nebulizers. It offers a fast
stabilization time and a reliable seal with chemically resistant PFA. Three versions are available in a variety
of flow rates for different ICP applications.
Benefits:
• Fast stabilization time and ultra-low dead-volume
• High purity PFA fluoropolymer construction
• Easy to connect and disconnect
Sample connectors available:
F2: Standard integrated capillary for self-aspiration or pumping. Standard with all nebulizers.
F0: Encapsulated micro tubing for microflow rates with the lowest internal volume of any nebulizer.
F1: Detachable capillary for a wide range of applications.
F2 Standard Integrated Capillary
Part Number
Application
F2-50
Compatible with all
MEINHARD® Plus nebulizers.
SAMPLE INTRODUCTION
F2 Standard integrated capillary for self-aspiration or pumping.
Includes 0.5 mm i.d. ■ (orange marker) 70 cm long capillary.
F0 Encapsulated Micro Tubing
F0 Encapsulated micro tubing for low uptake rates from
0.1 to 0.5 mL/min and the lowest internal volume of any
nebulizer. Includes 0.25 mm i.d. ■ (green marker) 70 cm
long micro capillary.
Part Number
Application
F0-25
Compatible with all
MEINHARD® Plus nebulizers.
F1 Detachable Capillary
F1 Detachable capillary for a wide range of applications.
Includes 0.80 mm i.d. ■ (blue marker) 70 cm long capillary.
Part Number
Application
F1-80
Compatible with all
MEINHARD® Plus nebulizers.
www.icpms.com
Page 49
pergo Nebulizer Gas Humidifier
pergo High Solids Accessory
The pergo improves performance of all
MEINHARD® nebulizers for the routine
analysis of brines, fusion digests and
other high TDS samples.
PRG-01-MAPlus pergo high
solids accessory with TQ+
MEINHARD® nebulizer
A high-pressure membrane positioned
inside a temperature-controlled
water reservoir perfuses water vapor
into the ICP nebulizer gas stream.
By increasing humidity in the argon
nebulizer gas, the pergo prevents salt
deposits at the nebulizer tip, improving
short and long-term signal stability.
Benefits:
• Improved RSDs
• Improved short and long-term stability
• Improved detection limits
• Faster washout
• Ability to use high sensitivity
nebulizers for high TDS samples
TQP-50
TQ+ Quartz
Nebulizer
• Reduce long-term drift
• Extends the length of analytical runs
pergo
Ar nebulizer gas is humidified using a tube-shaped membrane placed in a PFA water
reservoir at atmospheric pressure. The water vapor condenses inside the nebulizer tip,
preventing salt build-up.
Page 50
Elemental Scientific
Water microdroplets
continuously clean the
inside of the nebulizer
and prevent salt deposits.
2013
with pergo
SAMPLE INTRODUCTION
RSDs for seawater samples
improve with the pergo.
without pergo
The unique pergo design offers
many advantages over other types
of argon humidifiers.
Advantages:
• Higher, more consistent humidity
• Superior long-term stability for
high TDS samples
• Safe and easy to use
- Atmospheric pressure water
reservoir
• Optional USB communication for
programmable humidity levels
with pergo
without pergo
Long-term stability is improved with the pergo, reducing drift and extending
the length of the analytical run when salty samples are analyzed.
www.icpms.com
Part Number
Description
PRG-01
pergo argon high solids accessory. Includes nebulizer gas line
connector kit.
PRG-01-MAPlus
pergo argon high solids accessory. Includes a MEINHARD®
Type A Plus high performance nebulizer.
Page 51
Cyclonic Spray Chambers
Spray Chambers
NEW!
C2 Dual Cyclonic Spray Chambers
The C2 dual cyclonic spray chamber improves both sensitivity and precision
with its unique dual cyclonic aerosol flow path, improving detection limits.
Even at very high sample flow rates, the C2 chamber significantly reduces
droplet buildup in the injector that can cause plasma instability or outages.
The C2 chamber reduces the chance of accidental torch flooding events,
preventing costly damage to the torchbox components.
Part Number
Description
ES-3D57-1111-19 Quartz C2 dual cyclonic spray chamber,
threaded drain port, connection for ESI
injector, drain line assembly included
(ES-2044-0006)
Application
Used for improved
precision and low blanks.
C2 quartz chamber
Part Number
Description
ES-3H57-1111-19 Quartz hydride C2 dual cyclonic
spray chamber, threaded drain port,
connection for ESI injector, hydride gas
port, drain line assembly included
(ES-2044-0006)
Application
Used for improved
precision and low blanks.
Hydride gas port for use
with hydrideFAST or with
any additional gas.
C2 quartz hydride chamber
with additional gas port
C2 Chamber
Unbaffled Cyclonic Chamber
The C2 chamber improves sensitivity and precision compared to the standard unbaffled cyclonic chamber, which
improves detection limits and analytical quality.
Page 52
Elemental Scientific
2013
Spray Chambers / PFA Elbow Adapters
Description
Application
ES-3157-1401-21 O-ring-free quartz cyclonic spray
chamber, hydride gas port, drain line
included (ES-2044-0002)
Chamber for hydrideFAST,
or additional gas. Provides
low blanks.
Part Number
Application
Description
ES-3157-1001-21 Quartz (unbaffled) cyclonic spray
chamber, drain line included
(ES-2044-0002)
ES-3157-1011-21 Quartz (7 mm baffle) cyclonic spray
chamber, drain line included
(ES-2044-0002)
Part Number
Description
All-purpose for non-HF
samples. Provides excellent
sensitivity, stability and low
blanks.
Application
ES-3157-3011-21 PFA (7 mm baffle) cyclonic spray
chamber, drain line included
(ES-2044-0002)
All-purpose, offers
resistance to hydrofluoric
acid while maintaining the
benefits of cyclonic spray
chambers.
Part Number
Description
Application
ES-5103-4090
PFA elbow adapter for PerkinElmer
Optima injector
Connects ESI cyclonic
spray chambers to
standard Optima injector
Part Number
Description
Application
ES-5103-4070
PFA elbow adapter for ESI injector
Connects ESI cyclonic
spray chambers to
standard ESI injector
Part Number
Description
Application
M157-5470
PFA 47mm M100 spray chamber with
o-ring-free PFA endcap, drain line
included (ES-2044-0002)
All-purpose, offers
resistance to hydrofluoric
acid.
www.icpms.com
SAMPLE INTRODUCTION
Part Number
Page 53
Cyclonic Spray Chambers
Spray Chambers
Spray Chambers
ESI cyclonic spray chambers feature secure, leak-free threaded drain port,
o-ring-free connections to the nebulizer and torch injector, internal baffle
and threaded auxiliary port for addition gas.
Part Number
Description
Application
ES-3457-1011-19 Quartz (7 mm baffle) micro cyclonic
spray chamber, drain line included
(ES-2044-0002)
Used with soilFAST and
other aqueous applications
Part Number
Application
Description
ES-3457-1021-19 Quartz (5 mm baffle) micro cyclonic
spray chamber with additional gas port,
drain line included (ES-2044-0002)
Used with oilFAST
and organic solvent
applications, optional
oxygen addition, not for use
with aqueous solutions
G1 Cyclonic Spray Chambers for Optima
The new G1 o-ring-free cyclonic spray chamber connects to the
standard Optima injector base, offering the advantages of sensitivity,
washout, and solvent and chemical resistance.
Part Number
Material
Description
Application
G1-57-Q
Quartz
G1-57-P
Pyrex
G1 o-ring-free unbaffled
cyclonic spray chamber
For a wide range of non-HF
applications. Quartz offers
low blanks, while glass is
more economical for many
applications.
G1-57-BQ
Quartz
G1-57-BP
Pyrex
G1 o-ring-free baffled
cyclonic spray chamber
Drain line included (ES-2044-0002)
ES-3157-1009-13 quartz
cylonic spray chamber
mounted to the Optima
PerkinElmer standard ceramic injector
Page 54
Elemental Scientific
2013
Torches and Injectors
Convertible Injectors for Optima
Convertible Sapphire Injector and Adapter
Sapphire injectors are used for environmental, geochemistry,
and HF applications. This injector includes the black
PEEK adapter (ES-5787) to convert for use with Optima
4000/5000/7000 series instruments.
Part Number
Size
ES-1503-8157
1.5 mm
Description
Convertible sapphire injector. HF-resistant.
ES-1503-8187
1.8 mm
Convertible sapphire injector. HF-resistant.
Supplied with most FAST systems for the
Optima
Convertible Quartz Injector and Adapter
Part Number
Size
ES-1524-8107
1.0 mm
ES-1524-8157
1.5 mm
SAMPLE INTRODUCTION
Quartz injectors are recommended for non-HF applications.
This injector includes the black PEEK adapter (ES-5787)
to convert for use with Optima 4000/5000/7000 series
instruments.
Description
Convertible quartz injector for organic
solvents.
Threaded Adapter for ESI Convertible Injectors
Part Number
Description
ES-5787
Replacement black PEEK threaded adapter for ESI
convertible injectors
www.icpms.com
Page 55
Torches and Injectors
Injectors for Optima 8x00 Series Standard Torches
Optima 8x00 Series Quartz Torches
Part Number
Description
ES-1402-8000 Demountable quartz torch, no slot, short for organic
solvents
ES-1402-8001 Demountable quartz torch, one slot, copper strip
ES-1402-8003 Demountable quartz torch, three slots
Sapphire Injectors
Sapphire injectors are used for environmental, geochemistry,
and HF applications on the Optima 8x00 series instruments.
Part Number
Size
Description
ES-1503-8150 1.5 mm Sapphire injector. HF-resistant.
ES-1503-8180 1.8 mm
ES-1503-8250 2.5 mm
Quartz Injectors
Optima 8x00 series quartz injectors are used for volatile
organic solvent introduction and recommended for a wide
range of non-HF applications.
Part Number
Size
Description
ES-1524-8100 1.0 mm Quartz injector for organic solvents.
ES-1524-8150 1.5 mm Quartz injector
ES-1524-8200 2.0 mm Quartz injector
ES-1524-8250 2.5 mm Quartz injector. Improved stability for high
matrix/high TDS environmental samples.
Platinum Injectors
Platinum injectors are used for introducing volatile organic
solvents and HF-containing semiconductor-grade chemicals.
Part Number
Size
ES-1513-8100
1.0
ES-1513-8150
1.5
ES-1513-8200
2.0
Page 56
Description
Platinum injector
Elemental Scientific
2013
Injectors for Optima 4x00, 5x00 and 7x00 Series Standard Torches
Optima 4x00, 5x00 and 7x00 Quartz Torches
Part Number
Description
ES-1402-4001 Demountable quartz torch, no slot, short for organic
solvents
ES-1402-4000 Demountable quartz torch, one slot, copper strip
ES-1402-4004 Demountable quartz torch, three slots
Sapphire Injectors
Sapphire injectors are used for environmental, geochemistry,
and HF applications on the Optima 4x00, 5x00 and 7x00 series
instruments.
Part Number
Size
Description
SAMPLE INTRODUCTION
ES-1503-4150 1.5 mm Sapphire injector. HF-resistant.
ES-1503-4180 1.8 mm
ES-1503-4250 2.5 mm
Quartz Injectors
Quartz injectors for the Optima 4x00, 5x00 and 7x00 series
instruments are recommended for a wide range of non-HF
applications.
Part Number
Size
Description
ES-1524-4100 1.0 mm Quartz injector for organic solvents.
ES-1524-4150 1.5 mm Quartz injector
ES-1524-4200 2.0 mm Quartz injector
ES-1524-4250 2.5 mm Quartz injector. Improved stability for high matrix/
high TDS environmental samples.
Platinum Injectors
Platinum injectors are used for introducing volatile organic
solvents and HF-containing semiconductor-grade chemicals.
Part Number
Size
ES-1513-4100
1.0
ES-1513-4150
1.5
ES-1513-4200
2.0
www.icpms.com
Description
Platinum injector
Page 57
Peristaltic Pumps
Integrated MP2 Precision
Micro Peristaltic Pumps for the
PerkinElmer Optima
The MP2 (Micro Peristaltic Pump) provides better
stability than standard peristaltic pumps. Roller
configuration and precision machining minimizes
gaps between rollers, resulting in even pressure
points along the pump tubing. Reduced pump
pulsation improves signal stability, data quality
and detection limits.
Benefits:
• Pump design extends tubing lifetime
MP2-4-57
integrated precision
micro peristaltic pump
• Stand alone and integrated versions
• Chemically resistant
- Ceramic pins and PTFE-coated
metal components are resistant to
acids and organic solvents
• Pump network software control
• Precision
• Low pulsation
- 12 closely-spaced rollers improve
signal stability
• Optimized for all flow rates
- Accurate pumping across a wide range
of rates from low 0.20 μL/min to 10 mL/min
• 1, 2, 3, 4, 6 and 8 channels (stand alone MP2)
• 3, 4 and 6 channels (integrated MP2)
MP2 Optima Specifications:
MP2 shows improved low flow stability compared
to a standard peripump
Channels:
1-6 channels
Flow Rates:
0.20 μL/min to 10 mL/min per channel
Part Number Description
Tubing:
0.13 mm i.d. to 3.17 mm i.d.
Page 58
MP2-3-57
MP2 integrated 3 channel precision micro peristaltic pump
MP2-4-57
MP2 integrated 4 channel precision micro peristaltic pump
MP2-6-57
MP2 integrated 6 channel precision micro peristaltic pump
Elemental Scientific
2013
Stand Alone MP2 Precision Micro Peristaltic Pumps
MP2 Precision Micro Peristaltic Pumps
The MP2 is a compact precise stand alone micro peripump
with a flow rate range from 0.20 μL/min to 10 mL/min and is
available with one to eight channels. Optimized for low-flow
rates, the MP2 uses either MPP tubing or standard 3-stop
pump tubing.
CONTROLLED BY THE INSTRUMENT PC USB PORT
Number of Channels
MP2-1-PC
1 channel MP2 precision micro peristaltic pump
MP2-2-PC
2 channel MP2 precision micro peristaltic pump
MP2-3-PC
3 channel MP2 precision micro peristaltic pump
MP2-4-PC
4 channel MP2 precision micro peristaltic pump
MP2-6-PC
6 channel MP2 precision micro peristaltic pump
MP2-8-PC
8 channel MP2 precision micro peristaltic pump
Includes: Cable to control with DX Autosampler
CTFE PERIPUMP FITTINGS (Non-barbed)
Used in Low Pressure Applications
Part Number
Qty
Size
ES-2501-PPF1
1 ea.
ES-2501-PPM1
1 ea.
MP2-4-PC
stand alone precision
micro peristaltic pump
CTFE PERIPUMP FITTINGS (Barbed)
Used in High Pressure Applications
Part Number
Qty
Size
Female
(small)
ES-2501-PPF2
1 ea.
Female
(small)
Male
(small)
ES-2501-PPM2
1 ea.
Male
(small)
BLK WHT
ORG BLK
1200
1.2
1000
1
y = .633x
R =1
800
0.8
600
0.6
400
0.4
200
0.2
0
0
0
0.5
1
1.5
2
Pump Speed (RPM)
MP2 pump linearity < 1 μL/min
www.icpms.com
2.5
10000
Flow Rate ( L/min)
1.4
Flow Rate ( L/min)
Flow Rate (nL/min)
12000
1400
8000
y = 69.606x
R = 0.99999
6000
4000
2000
0
0
25
50
75
100
125
150
Pump Speed (RPM)
MP2 pump linearity up to 10 mL/min
Page 59
175
SAMPLE INTRODUCTION
Part Number
MP2 Peristaltic Pump Tubing
MP2 Pump Tubing
Tubing for MP2 Micro Peristaltic Pumps (Packs of 12)
Non-Flared
i.d.
Stop Colors
Calibration Slope
(μL/min per RPM)
PVC
2-stop
Santoprene
2-stop
Flared*
Solva
2-stop
PVC
2-stop
Solva
2-stop
0.13 mm Orange
Black
0.6
MPP-013-PVC
MPP-013-F-PVC MPP-013-F-S
0.19 mm Orange
Red
1.3
MPP-019-PVC
MPP-019-F-PVC MPP-019-F-S
0.27 mm Orange
Blue
2.7
MPP-027-PVC
MPP-027-F-PVC MPP-027-F-S
0.38 mm Orange
Green
4.7
MPP-038-PVC MPP-038-PHR
MPP-038-F-PVC MPP-038-F-S
0.44 mm
Green
Yellow
7.6
MPP-044-PVC
MPP-044-F-PVC MPP-044-F-S
0.51 mm Orange
Yellow
9.5
MPP-051-PVC
MPP-051-F-PVC MPP-051-F-S
0.57 mm
Yellow
11
MPP-057-PVC
MPP-057-F-PVC MPP-057-F-S
White
14
MPP-064-PVC
MPP-064-F-PVC MPP-064-F-S
White
0.64 mm Orange
0.76 mm
Black
Black
0.89 mm Orange Orange
19
MPP-076-PVC MPP-076-PHR MPP-076-S MPP-076-F-PVC MPP-076-F-S
24
MPP-089-PVC
MPP-089-S MPP-089-F-PVC MPP-089-F-S
0.95 mm
White
Black
28
MPP-095-PVC
MPP-095-S MPP-095-F-PVC MPP-095-F-S
1.02 mm
White
White
31
MPP-102-PVC
MPP-102-S MPP-102-F-PVC MPP-102-F-S
1.09 mm
White
Red
33
MPP-109-PVC
MPP-109-S MPP-109-F-PVC MPP-109-F-S
1.14 mm
Red
Red
35
MPP-114-PVC
MPP-114-S MPP-114-F-PVC
1.22 mm
Red
Grey
46
MPP-122-PVC
MPP-122-S
1.30 mm
Grey
Grey
47
MPP-130-PVC MPP-130-PHR MPP-130-S
1.42 mm
Yellow
Yellow
50
MPP-142-PVC
1.52 mm
Yellow
Blue
51
MPP-152-PVC MPP-152-PHR MPP-152-S
1.65 mm
Blue
Blue
55
MPP-165-PVC
MPP-165-S
1.75 mm
Blue
Green
58
MPP-175-PVC
MPP-175-S
1.85 mm
Green
Green
61
MPP-185-PVC
MPP-185-S
2.06 mm
Purple
Purple
64
MPP-206-PVC
MPP-206-S
2.20 mm
Purple
Black
65
MPP-220-PVC
MPP-220-S
2.54 mm
Purple
Orange
67
MPP-254-PVC
MPP-254-S
2.79 mm
Purple
White
69
MPP-279-PVC
MPP-279-S
3.17 mm
Black
White
70
MPP-317-PVC MPP-317-PHR MPP-317-S
72 mm
Bridge Length
*For easy insertion of PFA capillaries
MPP-142-S
72 mm
72 mm
72 mm
72 mm
i.d. = internal diameter
Non-Flared
Flared
PP2'
)ODUHGWRPP,'
/HQJWKPP
%RWK(QGV
PVC
Santoprene
SOLVA
MP2 PUMP TUBING STARTER KIT
Part Number Description
MPP-K-1
MP2 Pump Tubing Starter Kit comprised of 34 packs of 12 tubes, one package of each light-purple
highlighted part number in the table above. Includes: 26 packs of PVC tubing (0.13 to 3.17 mm i.d.) 3 packs
of Santoprene tubing and 5 packs of Solva tubing. Kit also includes: 30 CTFE Fluoropolymer Peripump
Fittings: 5 small female (ES-2501-PPF1), 5 small male (ES-2501-PPM1), 5 medium female (ES-2501-PPF3),
5 medium male (ES-2501-PPM3), 5 large female (ES-2501-PPF5) and 5 large male (ES-2501-PPM5).
Page 60
Elemental Scientific
2013
Syringe Pumps
SYRIX Syringe Pumps
SYRIX features an innovative drive mechanism for
the precise control of liquid samples and reagents.
Wetted parts are o-ring-free and offer high chemical
resistance.
SYRIX is highly configurable for a wide range of
applications such as micro sample loading and
remote monitoring.
Features:
• Wide flow rate range
- < 10 μL/min to > 40 mL/min
• A variety of syringe sizes
- 0.3 mL to 3 mL
• O-ring-free
• Syringe material
- PTFE/Quartz
- Fluoropolymer
• Optional integrated switching valve
• Convenient software control interface
• Connects directly to SC-DX autosampler
SYRIX syringe pump with valve
(PF-6503-1030-DX)
SYRIX SYRINGE PUMPS
3.0 mL quartz syringe
(PF-0599-1030)
Part Number
Description
Application
PF-6500-1030-DX
SYRIX precision o-ring-free
programmable syringe pump
system without integrated
3-port valve.
Precise, controlled delivery of
sample to the Optima. Useful for
volatile / viscous samples and for
accurate online continuous dilution.
PF-6503-1030-DX
SYRIX precision o-ring-free
programmable syringe pump
system with integrated 3-port
valve.
Accurately delivers micro-volume
samples to the FAST loop.
SYRIX SYRINGE PUMP SPARES
Part Number
Description
PF-0599-1003
0.3 mL quartz syringe
PF-0599-1030
3.0 mL quartz syringe
PF-0599-3003
0.3 mL HF resistant syringe
PF-0599-3030
3.0 mL HF resistant syringe
0.3 mL quartz syringe
(PF-0599-1003)
www.icpms.com
Page 61
SAMPLE INTRODUCTION
SYRIX syringe pump
(PF-6500-1030-DX)
apex Systems
apex High Sensitivity
Desolvating Systems
Sample transport efficiency is
enhanced by nebulizing liquid samples
into a heated cyclonic spray chamber
using a special version of the PFA-ST
nebulizer. A low-volume three-stage
Peltier-cooled desolvation system is
incorporated for online removal of
solvent vapor. Self aspiration or an
MP2 precision micro peristaltic pump is
recommended for the apex.
apex E - Inlet System. Features
an o-ring-free pyrex flow path for
high sensitivity and low background
for samples that do not contain
hydrofluoric acid. The apex E sample
path design ensures rapid rinse-out of
any high sensitivity ICP introduction
system.
apex E Advantages:
• Increases sensitivity 3 to 10 fold.
• One switch operation.
• Pumped or self-aspirated nebulizer.
• Consumes less sample than standard
introduction systems.
• Fast-rinsing.
• Small size—fits into even cramped
laboratories.
• Integrated 4 channel peristaltic pump for
waste removal.
• Designed for easy cleaning and low
maintenance.
Preset dual temperature settings for
heater and cooler. Patented flow path
design ensures rapid wash-in / washout.
Calibration curves for Mn and Pb from 0.5 ppb to 10 ppb show
sensitivity better than 4M counts/ppm Mn and 32k counts/ppm Pb.
Page 62
Elemental Scientific
2013
apex FAST High Sensitivity Desolvating Systems
The apex FAST is a compact, high
performance sample introduction system
for the Optima. The apex FAST is available
in E and HF options. It can be controlled
via any SC-Autosampler or oneFAST unit,
making it fully automated and integrated to
the Optima.
An MP2 precision micro perstaltic pump or
the FAST DXi is recommended for sample
introduction with the apex FAST.
Combination of apex inlet
system with FAST injection valve
Model
Part Number
apex E
ES-4857-1000-21
apex E FAST
ES-48FH-24-57
Integrated
FAST Valve
High
Sensitivity
O-ring-free
Single Switch
Operation
Optima Mounting Shelf
The mounting shelf for Optima is a multi-component
shelf to position the nebulizer close to the injector.
These components may include: FAST valves, apex,
apex FAST, PC3, PC3 FAST, PC3x and PC3-LT.
Part Number
Description
ES-2999-5621 Two piece mounting shelf for PE
Optima. For use with apex / PC3-LT.
www.icpms.com
Page 63
SAMPLE INTRODUCTION
Requires FAST-enabled autosampler.
PC3 Peltier Coolers and Heaters
PC3 Peltier Cooled Cyclonic Spray Chambers
The PC3 is a small, robust Peltier cooled cyclonic spray
chamber. The PC3 offers the advantages of low memory
effects, constant temperature, fast rinse-out and high sample
transport efficiency. The cooled outer walls of the PC3 spray
chamber enhance long-term signal stability, reduce polyatomic
interferences such as oxides, and reduce solvent loading
when volatile organic solvents are analyzed.
PC3 / PC3-LT
The PC3 has 2 preset temperatures +2°C / -5°C and is ideal for
analysis of aqueous or aqueous/organic mixtures.
The PC3-LT operates at -20°C to reduce the solvent load on the
plasma for analysis of 100% volatile organic solvents.
ES-4190-57-29
PC3
PC3 / PC3-LT Kits Include:
HF PC3 / PC3-LT Kits Include:
Quartz Injector (DV only)
Sapphire Injector (DV only)
PFA-ST MicroFlow Nebulizer
PFA-ST MicroFlow Nebulizer
Quartz Cyclonic Spray Chamber
PFA Cyclonic Spray Chamber
Part Number
Injector
Size
Description
Temperature
Additional
Gas Port
ES-4190-57-29 (DV)
1.5 mm
PC3 organic sample
introduction kit Peltier cooler
ES-4190-57V-29 (V)
N/A
+2°C / -5°C
Yes
ES-4190-57-29-PFA
(DV)
1.5 mm
HF PC3 organic
sample introduction
kit - Peltier cooler
+2°C / -5°C
Yes
ES-9190-57-29 (DV)
1.0 mm
+2°C / -20°C
Yes
ES-9190-57V-29 (V)
N/A
PC3-LT organic
sample introduction
kit - Peltier cooler
ES-9190-57-29
PC3 -LT
All PC3 kits include a PFA-ST nebulizer (ES-2040-57)
NEW!
PC3x Peltier Controlled Heated or Cooled Cyclonic Chamber
The PC3x is a compact Peltier heated and cooled inlet system which
incorporates the ESI cyclonic spray chamber. The PC3x heats or
cools the outer walls of the cyclonic spray chamber, reducing the
water or solvent vapor loading on the plasma, resulting in enhanced
stability and performance. The PC3x can be connected to any ICP.
• Temperature control from -10°C to +80°C
• Thermal stabilization of spray chamber improves long-term stability
• Last set temperature saved for stand alone operation
• USB or Bluetooth connectivity
• Remote monitoring and control
PC3x Kit Includes:
PFA-ST MicroFlow Nebulizer
Quartz Cyclonic Spray Chamber
Page 64
Part Number Description
Quartz Injector
PC3X-57-29
PC3x thermally stabilized inlet system
All PC3 kits include a PFA-ST nebulizer (ES-2040-57)
Elemental Scientific
2013
HF Resistant Sample Introduction Kit
HF-Resistant Sample Introduction Kit / Pipette Tips
PFA Sample Introduction Kit for PE Optima
The PFA kit is an ultra-pure, HF-resistant introduction
system for the Optima. All wetted surfaces are PFA
and sapphire. It is used by a majority of semiconductor
labs worldwide for the analysis of semiconductor-grade
chemicals and other high purity chemicals.
• Easy installation
• Clean PFA components for lower
background equivalent concentration (BEC)
and detection limits
• O-ring-free connections—ensures lowest
BEC’s, highest chemical resistance and easy
cleaning
• Chemically resistant—suitable for nearly all
samples, including strong acids, alkalis and
organic solvents
• Low sample consumption—ideal for VPD
and preconcentrated samples
• Fast washout
M257-DV Series HF-Resistant PFA Sapphire
Sample Introduction Kit for PE Optima
Part Number
Description
M257-DV
Complete HF-resistant sample
introduction kit. Includes PFA-ST
nebulizer, PureCap PFA endcap, 47
mm PFA spray chamber, 1.8 mm
convertible sapphire injector and
quartz torch. For the Optima DV (Axial)
M157-5470
PFA 47mm M100 spray chamber with
o-ring-free PFA endcap
M157-5470 PFA spray chamber on
the PerkinElmer Optima
High Purity PFA Pipette Tips
High purity PFA pipette tips are used to minimize
contamination of semiconductor and biological samples.
Part Number
Volume
Qty
ES-7000-0101
100-200 μL
10 pk
Pre-cleaned PFA Pure
Tip pipette tips
ES-7000-0111
100-200 μL
96 pk
Pre-cleaned PFA Pure
Tip pipette tips
ES-7000-1001
1000 μL
10 pk
Pre-cleaned PFA Pure
Tip pipette tips
www.icpms.com
Description
Page 65
SAMPLE INTRODUCTION
Benefits:
FAST Valves, Stators and Rotors
High Purity Valves
High purity valve stators and rotors provide a liquid path with low contamination and low carryover for the
best ICP results. PFA rotors are durable, clean and chemically-resistant. CTFE stators offer high impact
strength and chemical and corrosion resistance over a wide temperature range.
FAST Sample Injection Valves
4
Port Valve
P/N: SC-0599-1015
Description: CTFE high-flow 4 port valve head for SC-FAST
Specifications: CTFE stator, PTFE rotor, 0.8 mm
Applications: microFAST selection valve, oilFAST
6
Port Valve
P/N: SC-0599-1010 (PTFE Rotor)
SC-0599-1011 (PEEK Composite Rotor)
Description: CTFE high-flow 6 port valve head for SC-FAST
Specifications: CTFE stator, PTFE or composite rotor, 0.8 mm
Applications: Standard FAST, seaFAST, TRUFAST, chromFAST, apex FAST
6
Port Valve - P6
P/N: PF-P6
Description: P6 CTFE high-flow 6 port valve head for SC-FAST
Specifications: CTFE stator, PFA rotor, 1 mm, low maintenance
Applications: Standard FAST
7
Port Valve
NEW!
P -S eries Valve
s
P/N: PF-P7 (CTFE stator)
PF-P7-8 (PPS stator)
Description: P7 CTFE high-flow 7 port valve head for SC-FAST
Specifications: CTFE stator, PFA rotor, 1 mm, 0.5 mm
Applications: Standard FAST, inline internal standard addition
8
Port Valve - P7+ P/N: PF-P7X
Description: P7+ CTFE high-flow 8 port valve head for prepFAST
Specifications: CTFE stator, PFA rotor, 1 mm, 0.5 mm
Applications: prepFAST, inline dilution and internal standard addition
8
Port Valve
P/N: SC-0599-1013
Description: CTFE high-flow 8 port valve head for SC-FAST
Specifications: CTFE stator, PTFE rotor, 0.8 mm
Applications: DINFAST, sample pre-loading, dual loop single carrier
10
Port Valve
P/N: SC-0599-1012
Description: CTFE high-flow 10 port valve head for SC-FAST
Specifications: CTFE stator, PTFE rotor, 0.8 mm
Applications: Dual loop/dual carrier injection
Page 66
Elemental Scientific
2013
V-Series Syringe Loading Valves
6
Port Valve
P/N: PF-V6
Description: 6 port syringe loading valve
Specifications: CTFE stator, PFA rotor, 1.0 mm
Applications: S200V syringe valve (not for sample injection)
9
Port Valve
P/N: PF-V9
Description: 9 port syringe loading valve
Specifications: CTFE stator, PFA rotor, 1.0 mm
Applications: S400V syringe valve
12
Port Valve
P/N: PF-V12
Description: 12 port syringe loading valve
Specifications: CTFE stator, PFA rotor, 1.0 mm
Applications: S400V, brineFAST syringe valve
Examples of Materials
Description
Description
Description
CTFE replacement
stator for high-flow
valve
1 mm PFA rotor
PTFE rotor for
high-flow valve
FAST Valves with Spare Rotors and Stators
Rotor Material
P/N Complete Valve
P/N Stator
P/N Rotor
4
0.8 mm
CTFE
PTFE
SC-0599-1015
SC-0599-1015-01
SC-0599-1015-02
6
0.8 mm
CTFE
PTFE
SC-0599-1010
SC-0599-1010-01
SC-0599-1010-02
6
1.0 mm
CTFE
PTFE
SC-0599-1028
SC-0599-1026-01
SC-0599-1026-02
6
0.8 mm
CTFE
Composite (PEEK/PTFE)
SC-0599-1011
SC-0599-1010-01
SC-0599-1010-05
6
1.0 mm
CTFE
Composite (PEEK/PTFE)
SC-0599-1026
SC-0599-1026-01
SC-0599-1026-05
6
1.6 mm
PPS
Composite (PEEK/PTFE)
SC-0599-1032
SC-0599-1032-01
SC-0599-1032-05
6 - P6
P6
CTFE
PFA
PF-P6
PF-P6S
PF-P6R
7 - P7
P7
CTFE
PFA
PF-P7
PF-P7S
PF-P6R
7 - P7
P7
PPS
PFA
PF-P7-8
PF-P7S-8
PF-P6R
8 - P7+
P7
CTFE
PFA
PF-P7X
PF-P7XS
PF-P6R
8
0.8 mm
CTFE
PTFE
SC-0599-1013
SC-0599-1013-01
SC-0599-1013-02
8
1.0 mm
CTFE
Composite (PEEK/PTFE)
SC-0599-1027
SC-0599-1027-01
SC-0599-1027-05
9 - F9
0.8 mm
CTFE
PTFE
SC-0599-1029
SC-0599-1029-01
SC-0599-1013-02
10
0.8 mm
CTFE
PTFE
SC-0599-1012
SC-0599-1012-01
SC-0599-1012-02
11-A11b
A11b
CTFE
PFA
PF-A11b
PF-A11bS
PF-A11bR
11-P11
1.0 mm
CTFE
PFA
PF-P11
PF-P11S
PF-P10R
V-SERIES VALVES WITH REPLACEMENT STATORS AND ROTORS
# of Ports Bore Size Stator Material
Rotor Material
P/N Complete Valve
P/N Stator
P/N Rotor
6
1.0 mm
CTFE
PFA
PF-V6
PF-V6S
PF-V6R
9
1.0 mm
CTFE
PFA
PF-V9
PF-V9S
PF-V9R
12
1.0 mm
CTFE
PFA
PF-V12
PF-V12S
PF-V12R
13
1.0 mm
CTFE
PFA
PF-V13
PF-V13S
PF-V12R
www.icpms.com
Page 67
CONSUMABLES
HIGH-FLOW VALVES WITH REPLACEMENT STATORS AND ROTORS
# of Ports Bore Size Stator Material
Autosampler Probes and Connectors
FAST Probes / Tees / SC-FAST Connecting Lines
FAST Probes
FAST probes offer high chemical resistance for applications
involving strong acids, alkalis and organics. A contoured design
reduces carryover, while an all PFA wetted sample flow path
reduces contamination.
Part Number
Size
Description
Part Number
SC-5037-3501 0.50 mm i.d.
PFA carrier /
■ (orange), 150 cm internal standard
probe for
SC-FAST valve
Size
Description
SC-5037-3755-150 0.80 mm i.d. ■
(blue), 150 cm
SC-5037-3995-150 1.00 mm i.d. ■
(gray), 150 cm
PFA FAST sample
probe for high-flow
SC-FAST valve,
carbon fiber supported
Internal Standard Addition Tee for ESI ST-Nebulizer
Specially designed mixing tee is perfect for online addition of
internal standard or online dilution. Achieves excellent mixing
with minimal dead volume. 0.5 mm i.d. capillary is recommended
for applications with flow rates > 0.3 mL/min.
ES-2040
Part Number
(14 cm)
DXi Part Number
(25 cm)
Description
SC-0317-1250 SC-0317-1250-25 0.25 mm i.d. ■ (green) Attaches to port #3
SC-0317-1500 SC-0317-1500-25 0.50 mm i.d. ■ (orange) Attaches to port #3
ESI PFA-ST Nebulizer
FAST Valve Connecting Line for ESI ST-Nebulizer
Connects the FAST valve to an ESI ST-nebulizer to achieve
fast signal stabilization time and short wash times.
Part Number
(14 cm)
DXi Part Number
(25 cm)
Description
ES-2040
SC-0317-0250 SC-0317-0250-25 0.25 mm i.d. ■ (green) Attaches to
port #3 of the FAST valve.
SC-0317-0500 SC-0317-0500-25 0.50 mm i.d. ■ (orange) Attaches to
port #3 of the FAST valve.
Page 68
Elemental Scientific
ESI PFA-ST Nebulizer
2013
Elemental Scientific recommends using its PFA-ST or MEINHARD® nebulizer with the SC-FAST system for
optimum throughput and performance. ESI offers connecting lines for most nebulizers that laboratories may
already have.
FAST Valve Connecting Line for F7, P7 or P7+ FAST Valves
FAST valve line that connects the F7, P7 or P7+ FAST valve
(port #7) to an ESI ST-nebulizer.
Part Number
(14 cm)
DXi Part Number
(25 cm)
Description
ES-2040
SC-0317-025X SC-0317-025X-25 0.25 mm i.d. ■ (green) Attaches to
port #3 of the FAST valve.
SC-0317-050X SC-0317-050X-25 0.50 mm i.d. ■ (orange) Attaches to
port #3 of the FAST valve.
FAST Valve Connecting Line for MEINHARD® Nebulizers
ESI PFA-ST Nebulizer
F0
F2
PTFE FAST valve line that connects the FAST valve (port #3) to
a MEINHARD® nebulizer to achieve fast signal stabilization time
and short wash times.
Part Number
(14 cm)
DXi Part Number
(25 cm)
Fitting
Type
F0-25-14
F0-25-25
F0
F2-25-14
F2-25-25
F2
F0-50-14
F0-50-25
F0
F2-50-14
F2-50-25
F2
Description
0.25 mm i.d. ■ (green),
14 cm Attaches to port
#3 of the FAST valve.
0.50 mm i.d. ■ (orange),
14 cm Attaches to port
#3 of the FAST valve.
TQ-30-A3
SILQ-50
MEINHARD® glass and quartz nebulizers
FAST Valve Connecting Line for PerkinElmer Gem Cone Nebulizer
PTFE FAST valve line that connects the FAST valve (port #3)
to a PerkinElmer Gem Cone nebulizer to achieve fast signal
stabilization time and short wash times.
Part Number
Description
SC-0317-0500-25GC 0.50 mm i.d. ■ (orange), 25 cm.
Attaches to port #3 of the FAST valve.
SC-0317-0990-25GC 1.00 mm i.d. ■ (gray), 25 cm. Attaches
to port #3 of the FAST valve.
N0770358
PerkinElmer Gem Cone Low-flow Nebulizer
FAST Valve Connecting Line for MIRA MIST Nebulizer
Part Number
Description
SC-0317-0500-BG
0.50 mm i.d. ■ (orange), 17 cm.
Attaches to port #3 of the FAST valve.
SC-0317-0990-BG
1.00 mm i.d. ■ (gray), 17 cm. Attaches
to port #3 of the FAST valve.
CONSUMABLES
PTFE FAST valve line that connects the FAST valve (port #3)
to a MIRA MIST nebulizer to achieve fast signal stabilization
time and short wash times.
PMM4000
TMM3500
MIRA MIST PEEK and PTFE Nebulizers
www.icpms.com
Page 69
Fittings, Tubing and Loops
Fittings / PFA Tubing / Spares Kits
Easy to use, ultra-clean fittings and PFA tubing are ideal for all trace metal analysis applications. Ferrules
install quickly and easily for high-flow applications. Low-flow valve fittings have low dead volume, leak-free
integrated ferrule connections.
Part Number
Description
Quantity
Suggested Use
SC-0599-0116-K
Black, high-flow nut (1/4-28)
for FAST valve and 1/16”
(1.6 mm) ferrule
10
Use with 1/16” (1.6 mm)
o.d. PFA tubing for low
and moderate flow rates
(0.1 mL/min - 2 mL/min)
SC-0599-0108-W
White, high-flow nut (1/4-28)
for FAST valve and 1/8” (3.2
mm) ferrule
10
Use with 1/8” (3.2 mm)
o.d. PFA tubing for highflow rates and vacuum
applications (> 2 mL/min)
SC-0599-F16
1/16” (1.6 mm) Ferrule for
high-flow fitting (1/4-28)
10
Use with 1/16” (1.6 mm)
o.d. PFA tubing
SC-0599-F08
1/8” (3.2 mm) Ferrule for
high-flow fitting (1/4-28)
10
Use with 1/8” (3.2 mm)
o.d. PFA tubing
SC-0599-0001
Black, low-flow nut (M5/
10-32) for FAST valve
10
Use with 1/16” (1.6 mm)
o.d. PFA tubing for lowflow rates (<0.1 mL/min)
High Purity Fluoropolymer Tubing (5 m coil)
Part Number
I.D.
O.D.
Color Code
5MT-015
0.006” (0.15 mm)
1/16” (1.6 mm)
■ (red)
5MT-02
0.008” (0.20 mm)
1/16” (1.6 mm)
■ (purple)
5MT-025
0.010” (0.25 mm)
1/16” (1.6 mm)
■ (green)
5MT-03
0.014” (0.30 mm)
1/16” (1.6 mm)
■ (yellow)
5MT-05
0.019” (0.50 mm)
1/16” (1.6 mm)
■ (orange)
5MT-08
0.031” (0.80 mm)
1/16” (1.6 mm)
■ (blue)
5MT-1
0.039” (1.00 mm)
1/16” (1.6 mm)
■ (gray)
5MT-16
0.063” (1.60 mm)
1/8” (3.2 mm)
SC-FAST Standard Spares Kit
Part Number
Description
SC-0380
Assorted fittings and tubing for FAST systems.
Part Number
Description
SC-0370
Includes all of the assorted fittings and tubing in the
Standard Spares Kit with the addition of a PFA-ST
nebulizer, spare FAST valve and internal standard tee.
SC-FAST Deluxe Spares Kit
Page 70
Elemental Scientific
2013
Sample Loops
PFA crimp free SC-FAST loops provide low resistance for fast loading and rinse out.
0.8 mm i.d. SC-FAST High-Flow Sample Loops
Part Number
Size
Description
SC-0319-01
100 μL loop
SC-0319-02
200 μL loop
SC-0319-03
300 μL loop
Multipurpose PFA FAST loops for
high-flow valves. Recommended
for use with 0.8 mm i.d. ■ (blue)
probe. 1.6 mm o.d., 1/4-28 fittings.
SC-0319-05
500 μL loop
SC-0319-10
1.0 mL loop
SC-0319-15
1.5 mL loop
SC-0319-20
2.0 mL loop
SC-0319-25
2.5 mL loop
SC-0319-30
3.0 mL loop
SC-0319-40
4.0 mL loop
SC-0319-10 1mL sample loop
Standard for FAST Systems
1 mm i.d. SC-FAST High-Flow Sample Loops
Size
Description
SC-0318-03
Part Number
300 μL loop
SC-0318-05
500 μL loop
SC-0318-10
1.0 mL loop
Multipurpose PFA FAST loops for
high-flow valves. Recommended
for use with 1.0 mm i.d. ■ (gray)
probe. 1.6 mm o.d., 1/4-28 fittings.
SC-0318-15
1.5 mL loop
SC-0318-20
2.0 mL loop
SC-0318-25
2.5 mL loop
SC-0318-30
3.0 mL loop
SC-0318-40
4.0 mL loop
SC-0318-25 2.5mL sample loop
1.6 mm i.d. SC-FAST High-Flow Sample Loops
Part Number
Size
Description
SC-0315-025
250 μL loop
SC-0315-05
500 μL loop
SC-0319-10
1.0 mL loop
SC-0315-20
2.0 mL loop
SC-0315-30
3.0 mL loop
SC-0315-40
4.0 mL loop
High volume, fast-loading PFA
FAST loops for high-flow valves.
Recommended for use with 1.0
mm i.d. ■ (gray) probes and
applications requiring larger
sample volumes or high flow rates.
3.2 mm o.d., 1/4-28 fittings.
SC-0312-06
6.0 mL loop
SC-0312-08
8.0 mL loop
CONSUMABLES
SC-0315-30 3mL sample loop
0.8 mm i.d. SC-FAST Low-Flow Sample Loops
Part Number
Size
SC-0312-01
100 μL loop
SC-0312-02
200 μL loop
SC-0312-03
300 μL loop
SC-0312-05
500 μL loop
SC-0312-10
1.0 mL loop
SC-0312-20
2.0 mL loop
www.icpms.com
Description
Low volume, low-flow PFA
FAST loops for low-flow valves.
Recommended for use with 0.8
mm i.d. ■ (blue) or smaller probe.
1.6 mm o.d., M5/10-32 fittings.
SC-0312-10 1mL sample loop
Page 71
High Purity HF-Resistant Sample Vials and Bottles
PFA Sample Vessels
PFA Vials
PFA vials are ideal for applications that require the highest sensitivity. Made of ultra-pure, ultra-chemically
resistant material, these vials are an excellent choice for high purity, semiconductor and micro samples.
• Non-contaminating • Graduated
• Temperature range of -200 °C to 260 °C
• HF-resistant
• Conical bottom • Self-standing
Vials
Fits Racks
V-14-0311-CG
V-14-0312-CG
MR-21-14 (pg 77), MR-40-14 (pg 77), SR4-60-14 (pg 79)
V-14-0314-CG
Part Number
Qty
Part Number
Qty
V-14-0311CG-X
10
V-14-0309-X
10
Description
Volume
14 mm o.d.
graduated PFA
micro vial
1 mL
Brim full
2 mL
Part Number
Qty
Part Number
Qty
V-14-0312CG-X
10
V-14-0300-X
10
Description
Volume
14 mm o.d.
graduated PFA
micro vial
Brim full
3 mL
Part Number
Qty
V-14-0314CG-X
10
Description
Volume
14 mm o.d.
graduated PFA
micro vial
Description
PFA cap for
14 mm micro vials
Description
2 mL
PFA snap-on cap for 14 mm
graduated PFA micro vials
Part Number
Qty
V-14-0301-X
10
Description
PFA cap with knob
for 14 mm graduated
PFA micro vials.
4 mL
Brim full
4.5 mL
PFA cap with knob allows
for precise removal with
the ETFE tweezers
Part Number
Qty
ES-7225-0001
1
Description
ETFE tweezers for removal
of PFA cap with knob
Page 72
Elemental Scientific
2013
PFA Bottles and Vials
Bottles / Vials
Fits Racks
V-31-15
SR2-21-30 (pg 78), MR-10-30 (pg 77)
V-31-30
SR2-27-31 (pg 78), MR-10-30 (pg 77), ST10-31 (pg 80)
V-31-60
LR-21-30 (pg 76), LMR-21-30-R (pg 76), SR2-27-31 (pg 78), HR-21-30 (pg 77), ST10-31 (pg 80)
V-28-0360
SR2-27-28 (pg 78), ST10-28 (pg 80)
V-50-0360
SR2-12-50 (pg 78), ST2-9-50 (pg 81), ST4-9-50 (pg 80), SR4-20-50 (pg 79)
Part Number
Qty
V-28-0360-V
5
Description
Volume
28 mm o.d. PFA
bottle and cap
20 mL
Part Number
Qty
V-50-0360
1
Description
Volume
50 mm o.d. PFA
bottle and cap
with TFM insert
125 mL
• Semiconductor, high purity, and aggressive
chemical applications
• The most translucent PFA vials available
• Low absorption of biological materials for
many research applications
Part Number
Qty
V-31-15-X
10
Description
Volume
30 mm o.d.
graduated
PFA vial
15 mL
Part Number
Qty
V-31-30-X
10
Description
Volume
30 mm o.d.
graduated
PFA vial
30 mL
Part Number
Qty
V-31-60-X
10
Description
Volume
30 mm o.d.
graduated
PFA vial
60 mL
Part Number
Qty
V-31-SC-X
10
Description
Screw cap for
30 mm o.d. vials
www.icpms.com
Page 73
CONSUMABLES
PFA bottles and vials are ideal for a wide range of demanding fluid handling and storage applications in
general laboratory, semiconductor and environmental industries.
High Purity HF-Resistant Sample Vials and Bottles
!
W
E
N
2 mL PVDF Autosampler Vial
A low cost alternative to PFA for many ultra-trace metal analyses
Elemental Scientific introduces new PVDF sample vials, a low-cost
complement to our high-performance PFA vials. These high tensile
strength, fluoropolymer vials can replace more expensive PFA vials
in many applications.
• Semiconductor grade PVDF fluoropolymer
• High dielectric and mechanical strength, flexible
• Excellent for the analysis of Nitric Acid, Hydrochloric Acid,
Hydrofluoric Acid, or Ammonium Hydroxide
• Resistant to most mineral and organic acids, as well as aliphatic
and aromatic hydrocarbons, alcohols, halogenated solvents, and
oxidizing agents
• Self-standing
• Conical internal bottom for micro sample analysis
• Suitable for most semiconductor pure chemicals
• Not recommended for ketones, acetone,
ethyl acetate, and MIBK
• Optional PFA enclosures
• Available standard or pre-cleaned
V-14-0712
2 mL PVDF
autosampler vial
PVDF Vials and PFA Caps
P/N
Qty Description
V-14-0712-X 10 PVDF vial, 2 mL
V-14-0712-C 100 PVDF vial, 2 mL
V-14-0712-M 1000 PVDF vial, 2 mL
V-14-0309-X 10 PFA cap for V-14 vial
V-14-0309-C 100 PFA cap for V-14 vial
Pre-cleaned PVDF Vials and Caps
P/N
Qty Description
Pre-cleaned PVDF
vial, 2 mL
Pre-cleaned PFA
VPC-14-0309-C 100
cap for V-14 vial
VPC-14-0712-C 100
Bottles / Vials Fits Racks
V-14-0712
V-14-0712
2 mL PVDF autosampler
vial with PFA cap
MR-21-14 (pg 79), MR-40-14
(pg 79), SR4-60-14 (pg 81)
Page 74
Elemental Scientific
2013
Sample Vessels
Non-PFA Sample Vessels
Non-PFA Vials, Tubes and Bottles
Non-PFA sample vessels manufactured from plastics, such as polypropylene, polyethylene and polystyrene,
are a sensible alternative to consider when breakage, surface inertness, and/or disposal costs are a concern.
Vials
Fits Racks
V-8-0505
MR-60-08 (pg 77), MR-90-08 (pg 77)
V-13-0200-R
LR-90-13-R (pg 76), LMR-90-13-R (pg 76), LMR-90-13-R-3T (pg 76), ST-PR-5 (pg 81)
V-20-0290
LR-40-20 (pg 76)
V-16-0225
HR-60-16 (pg 77), LR-60-16 (pg 76), LMR-60-16-R (pg 76), SR2-80-16 (pg 78), ST-PR-5 (pg 81)
V-28-0260
HR-21-30 (pg 77), ST10-28 (pg 80), LR-21-30 (pg 76), LMR-21-30-R (pg 76), SR2-27-28 (pg 78), ST-PR-5
(pg 81), ST-EX-5 (pg 81)
V-50-0460
SR4-20-50 (pg 79), SR2-12-50 (pg 78), ST-PR-5 (pg 81), ST2-9-50 (pg 81), ST4-9-50 (pg 80)
V-61-0661
SR4-15-60 (pg 79), ST7-60 (pg 80), ST-PR-5 (pg 81), ST-EX-5 (pg 81)
www.icpms.com
Qty
Part Number
Qty
V-8-0505-C
100
V-13-0200R-XC
90
V-13-0200R-D
500
Description
Volume
13 mm o.d.
polystyrene
tube with
rounded bottom
8 mL
V-8-0505-D
500
Description
Volume
8 mm o.d.
centrifuge tube
0.5 mL
Part Number
Qty
Part Number
Qty
V-20-0290-L
50
V-16-0225-LX
60
V-20-0290-D
500
V-16-0225-D
500
Description
Volume
Description
Volume
20 mm o.d.
polypropylene tube
with screw cap
20 mL
16 mm o.d.
polypropylene tube
with screw cap
15 mL
Part Number
Qty
Part Number
Qty
V-28-0260-L
50
V-50-0460-XII
12
V-28-0260-D
500
V-50-0460-XXIV
24
Description
Volume
Description
Volume
28 mm o.d.
polypropylene
tube with
screw cap
50 mL
50 mm o.d.
polyethylene
bottle with
screw cap
50 mL
Part Number
Qty
V-61-0661-XII
12
V-61-0661-C
100
Description
Volume
61 mm o.d.
polyethylene wide
mouth bottle
250 mL
Page 75
CONSUMABLES
Part Number
Microtiter Plates
Microtiter Plates / Covers
Microtiter Plates
Microtiter plates are ideal for micro volume applications such as storage and sample transfer.
All microtiter plates can be used on the following Elemental Scientific autosamplers:
SC-2, SC-4, SC-2 DX, SC-4 DX, SC-Micro DX
Part Number
Part Number
Description
MT-24-10mL-02 1 Pk (5 ea) 24 well, 10 mL microtiter
plate, square well, pyramid bottom
Description
MT-48-5mL-02
1 Pk (5 ea) 48 well, 5 mL microtiter
plate, square well, pyramid bottom
Part Number
Part Number
Description
MT-96-2mL-02
1 Pk (5 ea) 96 well, 2 mL microtiter
plate, square well, pyramid bottom
MT-96-500-05-V
1 Pk (5 ea) 96-well, 500μL
microtiter plate, polystyrene
Description
MT-48-7.5mL-02 1 Pk (3 ea) 48 well, 7.5 mL microtiter
plate, square well, pyramid bottom
Microtiter Plate Cover
This rigid plastic microtiter plate cover is primarily used to
protect against environmental contamination.
Part Number
Qty
Description
MT-00-02
5
Polypropylene cover for
microtiter plates
Page 76
Elemental Scientific
2013
X-Piercing Film Cover / XP Probe Arm
X-Piercing Microtiter Plate Cover
The X-piercing cover minimizes evaporation of micro
samples awaiting analysis and protects against
environmental contamination.
MT-96-500-05
Remove X-Piercing cover
from it’s backing and place
on the microtiter plate
MT-96-XP
Part Number
Qty
Description
MT-96-XP
25
X-Piercing film cover for
96 well microtiter plate
X-Piercing cover helps
prevent contamination
during sampling
CONSUMABLES
XP Probe Arm
The XP probe arm must be used in place of
the reset probe arm when an X-Piercing cover
has been applied to a 96 well microtiter plate.
Part Number
Qty Description
SC-0105-DX-XP 1
www.icpms.com
XP Probe arm for SC-2 DX /
SC-4 DX Autosampler
Page 77
Large Autosampler Racks
SC-Autosampler Racks (LR Size)
Description
LR-90-13-R
13 mm 90 position large sample rack
for 8 mL tubes
Part #
Diam.
LR-40-20
20 mm 40 position large sample rack
for 20 mL tubes
Part #
Diam.
Description
Description
LR-60-16
16 mm 60 position large sample rack
for 15 mL tubes
Part #
Diam.
LR-21-30
30 mm 21 position large sample rack
for 50 mL and 60 mL tubes
V-31-60
V-28-0260
Diam.
V-20-0290
Part #
V-16-0225
V-13-0200-R
Plastic large racks are recommended for aqueous samples.
All LR racks can be used on the following ESI autosamplers:
SC-2, SC-4, SC-8, SC-14, SC-2 DX, SC-4 DX, SC-8 DX, SC-14 DX
Description
SC-Autosampler Coated Metal Racks (LR Size)
Metal racks are coated with an epoxy paint that forms a protective barrier over the rack material.
13 mm 90 position metal large
sample rack for 8 mL tubes
Description
Part #
Part #
Diam.
LMR-60-16-R
16 mm 60 position metal large
sample rack for 15 mL tubes
Diam.
Page 78
Description
Description
LMR-90-13-R-3T 13 mm 90 position 3 tier metal large
sample rack for 8 mL tubes
V-31-60
V-28-0260
Diam.
LMR-90-13-R
V-16-0225
Part #
V-13-0200-R
V-13-0200-R
All coated metal racks can be used on the following ESI autosamplers:
SC-2, SC-4, SC-8, SC-14, SC-2 DX, SC-4 DX, SC-8 DX, SC-14 DX
Part #
Diam.
LMR-21-30-R
30 mm 21 position metal large sample
rack for 50 mL and 60 mL tubes
Elemental Scientific
Description
2013
Heated and Micro Autosampler Racks
SC-Autosampler Heated Racks (LR Size)
V-28-0260
V-31-60
V-16-0225
All heated racks can be used on the following Elemental Scientific autosamplers:
SC-2, SC-4, SC-8, SC-14, SC-2 DX, SC-4 DX, SC-8 DX, SC-14 DX
Part #
Diam.
Description
HR-60-16
16 mm 60 position heated large sample
rack for 15 mL tubes
Part #
Diam.
Description
HR-21-30
30 mm 21 position heated large sample
rack for 50 mL and 60 mL tubes
SC-Autosampler Racks (MR Size)
V-8-0505
V-8-0505
All MR racks can be used on the following Elemental Scientific autosamplers: SC-2, SC-4, SC-2 DX,
SC-4 DX, SC-Micro DX
MR-90-08
8 mm
90 position CPVC micro sample
rack for 0.5 mL tubes
MR-60-08
8 mm
60 position CPVC micro sample
rack for 0.5 mL tubes
14 mm 40 position micro sample rack
for 1 mL, 2 mL and 4 mL tubes
Part #
Diam.
MR-10-30
30 mm 10 position micro sample rack
for 15 mL and 30 mL tubes
www.icpms.com
Diam.
Description
MR-21-14
14 mm 21 position micro sample rack
for 1 mL, 2 mL and 4 mL tubes
CONSUMABLES
MR-40-14
Part #
V-31-30
Description
V-31-15
Diam.
V-14-0712
V-14-0712
Part #
Description
V-14-0314CG
Description
V-14-0312CG
Diam.
V-14-0311CG
Part #
V-14-0314CG
Description
V-14-0312CG
Diam.
V-14-0311CG
Part #
Part #
Description
MR-00-01
Cover for SC-micro racks
Page 79
Super Autosampler Racks
Large-volume samples can be analyzed using ESI super racks without transferring the sample to a smaller
tube, reducing prep time and chance of contamination.
SC-Autosampler Racks (SR2 Size)
SR2-80-16
16 mm 80 position super sample rack
for 15 mL tubes
Part #
Diam.
Description
Description
SR2-27-28
28 mm 27 position super sample rack
for 20 mL and 50 mL tubes
Diam.
Description
SR2-21-30 30 mm 21 position super sample rack for 15
mL tubes
V-50-0460
V-50-0360
Diam.
Part #
SR2-27-31 31 mm 27 position super sample rack for 30
mL and 60 mL tubes
Part #
Diam.
Description
SR2-12-50
50 mm
12 position super sample rack
for 125 mL bottles
Page 80
Part #
V-31-15
Description
V-31-60
Diam.
V-31-30
Part #
V-28-0260
V-28-0360
V-16-0225
All SR2 racks can be used on the following ESI autosamplers:
SC-2, SC-2 DX
Elemental Scientific
2013
SC-Autosampler Racks (SR4 Size, Type 1)
V-14-0314CG
V-14-0312CG
V-14-0311CG
V-14-0712
All SR4 racks can be used on the following ESI autosamplers:
SC-2, SC-4, SC-2 DX, SC-4 DX
Part #
Diam.
Description
SR4-60-14
14 mm 60 position super sample rack
for 1 mL, 2 mL and 4 mL tubes
Part #
Description
SR4-00-01
Cover for 60 position SR-4
super rack
SC-Autosampler Racks (SR4 Size, Type 2)
Diam.
Description
SR4-15-60
60 mm 15 position super sample rack for
250 mL bottles
V-50-0460
Part #
Diam.
Description
SR4-20-50
50 mm
20 position super sample rack
for 125 mL bottles
CONSUMABLES
Part #
V-50-0360
V-61-0661
All ST type 1 racks can be used on the following ESI autosamplers:
SC-4, SC-4 DX
The SR4-15-60 super rack will
hold fifteen 100 mL volumetric
flasks or 250 mL bottles
SR4-15-60 super
rack with 100 mL
volumetric flasks
www.icpms.com
Page 81
Standards Autosampler Racks
SC-Autosampler Racks (ST Size, Type 1)
Part #
Diam.
ST10-28
28 mm 10 position standards rack for 20
mL and 50 mL tubes
Description
V-31-60
V-31-30
V-28-0260
V-28-0360
All ST type 1 racks can be used on the following ESI autosamplers: SC-2, SC-4, SC-8, SC-14, SC-2
DX, SC-4 DX, SC-8 DX, SC-14 DX
Part #
Diam.
Description
ST10-31
31 mm
10 position standards rack for
30 mL and 60 mL tubes
SC-Autosampler Racks (ST Size, Type 2)
V-50-0460
V-50-0360
All ST type 2 racks can be used on the following ESI autosamplers:
SC-2, SC-2 DX
Part #
Diam.
ST2-9-50
50 mm 9 position standards rack for 125 mL bottles.
Recommended for prepFAST with SC-DX
Page 82
Description
Elemental Scientific
2013
SC-Autosampler Racks (ST Size, Type 3)
V-50-0460
V-50-0360
V-61-0661
The ST type 3 rack can be used on the following ESI autosamplers:
SC-4 DX, SC-14, SC-14 DX
Part #
Diam.
Description
ST7-60
60 mm 7 position standards rack for
250 mL bottles
Part #
Diam.
Description
ST4-9-50
50 mm
9 position standards rack for
125 mL bottles. Recommended
for prepFAST.
SC-Autosampler Racks (ST Size, Type 4)
V-61-0661
V-28-0260
V-61-0661
V-50-0460
V-28-0260
V-16-0225
V-13-0200-R
The ST type 4 rack can be used on the following ESI autosamplers:
SC-2 DX, SC-4 DX
Diam.
Description
Part #
Diam.
Description
ST-PR-5
60 mm
5 position priority samples rack for 8 mL,
15 mL, 50 mL, 125 mL and 250 mL bottles.
Fits over SC-DX rinse station.
ST-EX-5
60 mm
5 position extra standards
rack for 50 mL and 250 mL
bottles. Fits over SC-DX
rinse station.
CONSUMABLES
Part #
www.icpms.com
Page 83
Installation and Training
Silver Level ESI Installation & Training
The silver level installation and training
package is a 1 day on-site installation
and method development for SC-FAST
or oneFAST on ICP in US, Canada, or
Western Europe.
Includes: Hardware installation
Software methods
Basic system familiarization
Travel time & expenses for
ESI employee or contractor
SC-FAST standard spares
kit (SC-0380)
Part Number
Description
FI-SC-01
On-site 1 day installation
for SC-FAST high
throughput system
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3KRQH_)D[_(PDLOHVL#LFSPVFRP_:HEZZZLFSPVFRP
Gold Level ESI Installation & Training
The gold level installation and training package is a 2½ day
on-site installation and method development for the SC-FAST,
prepFAST or oneFAST on ICP in US, Canada, or Western Europe.
Includes: Hardware installation
Software methods
Basic system familiarization
Necessary method validation
User Training
Travel time & expenses for
ESI employee or contractor
SC-FAST deluxe spares
kit (SC-0370)
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Part Number
Description
FI-SC-02
On-site 2½ day installation
for SC-FAST or prepFAST
high throughput systems
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The SC-FAST & oneFAST
Consumables/Spares Kit is a great
value at no extra expense with the
Gold Installation & Training.
Page 84
Elemental Scientific
2013
Autosampler Dimensions
SC-2 DX Autosampler with Enclosure and ULPA Filter Dimensions
578mm
SC-2 DX Autosampler Enclosure with
ULPA Filter (P/N: SC-1207-1000)
300mm
146mm
542mm
929mm
1079mm
472mm
Optional
ULPA
Filter
[RH or LH]
622mm
150mm
SC-4 DX Autosampler with Enclosure and ULPA Filter Dimensions
SC-4 DX Autosampler Enclosure with
ULPA Filter (P/N: SC-1407-1000)
578mm
300mm
770mm
146mm
935mm
472mm
1085mm
622mm
Optional
ULPA
Filter
[RH or LH]
150mm
www.icpms.com
Page 85
Autosampler Dimensions
SC-8 DXS Autosampler with Enclosure Dimensions
SC-8 DXS Autosampler Enclosure
(P/N: SC-1807-DX)
850mm
548mm
770mm
130mm
1016mm
514mm
1565mm
1063mm
254mm
SC-14 DXS Autosampler with Enclosure and ULPA Filter Dimensions
SC-14 DXS Autosampler Enclosure with
ULPA Filter (P/N: SC-1107-DX-1030)
884mm
615mm
1168mm
130mm
985mm
1586mm
517mm
1115mm
254mm
Page 86
Elemental Scientific
2013
Index
Item # .........Page
Item # .........Page
Item # .........Page
2ADFi-57C ..................22
2BF-S4-57C................31
2DX............................. 11
2DXF-57C............. 11, 22
2DXFi-57C ............ 11, 22
2DX-SEMI...................13
2HYF-1-57C ...............27
2HYF-2-57C ...............29
2MFP-57C ..................38
2OPTF-87C .......... 11, 22
2SLF-57C ...................35
4ADFi-57C ..................22
4BF-S4-57C................31
4DX............................. 11
4DXF-57C............. 11, 22
4DXFi-57C ............ 11, 22
4HYF-1-57C ...............27
4HYF-2-57C ...............29
4MFP-57C ..................38
4OF1-57A ...................33
4OF2-57A ...................33
4OPTF-87C .......... 11, 22
4SLF-57C ...................35
5MT-1 .........................70
5MT-02 .......................70
5MT-03 .......................70
5MT-05 .......................70
5MT-08 .......................70
5MT-015 .....................70
5MT-16 .......................70
5MT-025 .....................70
8ADFi-57C ..................22
8DX.............................12
8DX-BT .......................12
8DXF-57C.............12, 22
8DXF-BT-57C .............12
8DXFi-57C ............12, 22
8DXFi-BT-57C ............12
8OF1-57A ...................33
8OF2-57A ...................33
8OPTF-87C ..........12, 22
8OPTF-BT-87C...........12
8SLF-57C ...................35
14ADFi-57C ................22
14DX...........................12
14DX-BT .....................12
14DXF-57C...........12, 22
14DXF-BT-57C ...........12
14DXFi-57C ..........12, 22
14DXFi-BT-57C ..........12
14OPTF-87C ........12, 22
14OPTF-BT-87C.........12
14SLF-57C .................35
ES-3D57-1111-19 .......52
ES-3H57-1111-19 .......52
ES-48FH-24-57 ..........63
ES-1402-4000 ............57
ES-1402-4001 ............57
ES-1402-4004 ............57
ES-1402-8000 ............56
ES-1402-8001 ............56
ES-1402-8003 ............56
ES-1503-4150 ............57
ES-1503-4180 ............57
ES-1503-4250 ............57
ES-1503-8150 ............56
ES-1503-8157 ............55
ES-1503-8180 ............56
ES-1503-8187 ............55
ES-1503-8250 ............56
ES-1513-4100 ............57
ES-1513-4150 ............57
ES-1513-4200 ............57
ES-1513-8100 ............56
ES-1513-8150 ............56
ES-1513-8200 ............56
ES-1524-4100 ............57
ES-1524-4150 ............57
ES-1524-4200 ............57
ES-1524-4250 ............57
ES-1524-8100 ............56
ES-1524-8107 ............55
ES-1524-8150 ............56
ES-1524-8157 ............55
ES-1524-8200 ............56
ES-1524-8250 ............56
ES-2000......................43
ES-2000-3503-100 .....44
ES-2000-3505-100 .....44
ES-2002......................43
ES-2002-3503-100 .....44
ES-2002-3505-100 .....44
ES-2002-7000 ............41
ES-2002-7205-080 .....41
ES-2003......................43
ES-2003-3503-100 .....44
ES-2003-3505-100 .....44
ES-2005......................43
ES-2005-3503-100 .....44
ES-2005-3505-100 .....44
ES-2020......................43
ES-2020-3503-100 .....44
ES-2020-3505-100 .....44
ES-2030-57 ................40
ES-2040-57 ................40
ES-2040-7000 ............41
ES-2041......................42
ES-2042......................42
ES-2043......................42
ES-2044......................42
ES-2045......................42
ES-2046-0001 ............41
ES-2047......................42
ES-2049......................42
ES-2501-PPF1 ...........59
ES-2501-PPF2 ...........59
ES-2501-PPM1...........59
ES-2501-PPM2...........59
ES-2999-5621 ............63
ES-3157-1001-21 .......53
ES-3157-1011-21 .......53
ES-3157-1401-21 .......53
ES-3157-3011-21 .......53
ES-3457-1011-19 .......54
ES-3457-1021-19 .......54
ES-4040-57 ................41
ES-4190-57-29 ...........64
ES-4190-57-29-PFA ...64
ES-4190-57V-29 .........64
ES-4857-1000-21 .......63
ES-5037-3250-080 .....42
ES-5037-3250-100 .....42
ES-5037-3500-080 .....42
ES-5037-3500-100 .....42
ES-5037-9250-100 .....42
ES-5037-9500-100 .....42
ES-5103-4070 ............53
ES-5103-4090 ............53
ES-5787......................55
ES-7000-0101 ............65
ES-7000-0111 .............65
ES-7000-1001 ............65
ES-7225-0001 ............72
ES-9190-57-29 ...........64
ES-9190-57V-29 .........64
F0-25 ..........................49
F0-25-14 .....................69
F0-25-25 .....................69
F0-50-14 .....................69
F0-50-25 .....................69
F1-80 ..........................49
F2-25-14 .....................69
F2-25-25 .....................69
F2-50 ..........................49
F2-50-14 .....................69
F2-50-25 .....................69
FG...............................48
FI-SC-01 .....................84
FI-SC-02 .....................84
G1-57-BP....................54
G1-57-BQ ...................54
G1-57-P ......................54
G1-57-Q......................54
HG-GLS-001...............27
HG-MP2-4-A ...............27
HG-MP2-6-A ...............25
HG-USCA-01 ..............27
HR-21-30 ....................79
HR-60-16 ....................79
HYF-UP1-A-57 ...........27
HYF-UP2-A-57 ...........29
LMR-21-30-R ..............78
LMR-60-16-R ..............78
LMR-90-13-R ..............78
LMR-90-13-R-3T ........78
LR-21-30.....................78
LR-40-20.....................78
LR-60-16.....................78
LR-90-13-R .................78
M157-5470 ...........53, 65
M257-DV ....................65
m-DX ..........................13
MP2-1-PC ...................59
MP2-2-PC ...................59
MP2-3-57 ....................58
MP2-3-PC ...................59
MP2-4-57 ....................58
MP2-4-PC ...................59
MP2-6-57 ....................58
MP2-6-PC ...................59
MP2-8-PC ...................59
MPP-013-F-PVC.........60
MPP-013-F-S..............60
MPP-013-PVC ............60
MPP-019-F-PVC.........60
MPP-019-F-S..............60
MPP-019-PVC ............60
MPP-027-F-PVC.........60
MPP-027-F-S..............60
MPP-027-PVC ............60
MPP-038-F-PVC.........60
MPP-038-F-S..............60
MPP-038-PHR ............60
MPP-038-PVC ............60
MPP-044-F-PVC.........60
MPP-044-F-S..............60
MPP-044-PVC ............60
MPP-051-F-PVC.........60
MPP-051-F-S..............60
MPP-051-PVC ............60
MPP-057-F-PVC.........60
MPP-057-F-S..............60
MPP-057-PVC ............60
MPP-064-F-PVC.........60
MPP-064-F-S..............60
MPP-064-PVC ............60
MPP-076-F-PVC.........60
MPP-076-F-S..............60
MPP-076-PHR ............60
MPP-076-PVC ............60
MPP-076-S .................60
MPP-089-F-PVC.........60
MPP-089-F-S..............60
MPP-089-PVC ............60
MPP-089-S .................60
MPP-095-F-PVC.........60
MPP-095-F-S..............60
MPP-095-PVC ............60
MPP-095-S .................60
MPP-102-F-PVC.........60
MPP-102-F-S..............60
MPP-102-PVC ............60
MPP-102-S .................60
MPP-109-F-PVC.........60
MPP-109-F-S..............60
MPP-109-PVC ............60
MPP-109-S .................60
MPP-114-F-PVC .........60
MPP-114-PVC ............60
MPP-114-S .................60
www.icpms.com
Item # .........Page
Item # .........Page
Item # .........Page
MPP-122-PVC ............60
MPP-122-S .................60
MPP-130-PHR ............60
MPP-130-PVC ............60
MPP-130-S .................60
MPP-142-PVC ............60
MPP-142-S .................60
MPP-152-PHR ............60
MPP-152-PVC ............60
MPP-152-S .................60
MPP-165-PVC ............60
MPP-165-S .................60
MPP-175-PVC ............60
MPP-175-S .................60
MPP-185-PVC ............60
MPP-185-S .................60
MPP-206-PVC ............60
MPP-206-S .................60
MPP-220-PVC ............60
MPP-220-S .................60
MPP-254-PVC ............60
MPP-254-S .................60
MPP-279-PVC ............60
MPP-279-S .................60
MPP-317-PHR ............60
MPP-317-PVC ............60
MPP-317-S .................60
MPP-K-1 .....................60
MR-00-01....................79
MR-10-30....................79
MR-21-14....................79
MR-40-14....................79
MR-60-08....................79
MR-90-08....................79
MT-00-02 ....................76
MT-24-10mL-02 ..........76
MT-48-5mL-02 ............76
MT-48-7.5mL-02 .........76
MT-96-2mL-02 ............76
MT-96-XP ...................77
OPT-UP-A-57C ...........14
OPT-UP-B-57C ...........14
PC3X-57-29 ................64
PF-0599-1003.............61
PF-0599-1030.............61
PF-0599-3003.............61
PF-0599-3030.............61
PF-6500-1030-DX ......61
PF-6503-1030-DX ......61
PF-A11b......................67
PF-A11bR ...................67
PF-A11bS ...................67
PF-P6 ...................66, 67
PF-P6R .......................67
PF-P6S .......................67
PF-P7 ...................66, 67
PF-P7-8 ................66, 67
PF-P7S .......................67
PF-P7S-8 ....................67
PF-P7X .................66, 67
PF-P7XS.....................67
PF-P10R .....................67
PF-P11........................67
PF-P11S .....................67
PF-S400V ...................22
PF-S400V-HF .............22
PF-V6 .........................67
PF-V6R .......................67
PF-V6S .......................67
PF-V9 .........................67
PF-V9R .......................67
PF-V9S .......................67
PF-V12 .......................67
PF-V12R .....................67
PF-V12S .....................67
PF-V13 .......................67
PF-V13S .....................67
PRG-01.......................51
PRG-01-MAPlus .........51
SC-0105-DX-XP .........77
SC-0312-01 ................71
SC-0312-02 ................71
SC-0312-03 ................71
SC-0312-05 ................71
SC-0312-06 ................71
SC-0312-08 ................71
SC-0312-10 ................71
SC-0312-20 ................71
SC-0315-05 ................71
SC-0315-20 ................71
SC-0315-025 ..............71
SC-0315-30 ................71
SC-0315-40 ................71
SC-0317-025X ............69
SC-0317-025X-25.......69
SC-0317-050X ............69
SC-0317-050X-25.......69
SC-0317-0250 ............68
SC-0317-0250-25 .......68
SC-0317-0500 ............68
SC-0317-0500-25 .......68
SC-0317-0500-25GC..69
SC-0317-0500-BG ......69
SC-0317-0990-25GC..69
SC-0317-0990-BG ......69
SC-0317-1250 ............68
SC-0317-1250-25 .......68
SC-0317-1500 ............68
SC-0317-1500-25 .......68
SC-0318-03 ................71
SC-0318-05 ................71
SC-0318-10 ................71
SC-0318-15 ................71
SC-0318-20 ................71
SC-0318-25 ................71
SC-0318-30 ................71
SC-0318-40 ................71
SC-0319-01 ................71
SC-0319-02 ................71
SC-0319-03 ................71
SC-0319-05 ................71
SC-0319-10 ................71
SC-0319-15 ................71
SC-0319-20 ................71
SC-0319-25 ................71
SC-0319-30 ................71
SC-0319-40 ................71
SC-0370 .....................70
SC-0380 .....................70
SC-0400 .....................15
SC-0457 .....................15
SC-0457-DXi ..............15
SC-0599-0001 ............70
SC-0599-0108-W........70
SC-0599-0109 ............41
SC-0599-0116-K .........70
SC-0599-1010 ......66, 67
SC-0599-1010-01 .......67
SC-0599-1010-02 .......67
SC-0599-1010-05 .......67
SC-0599-1011 ......66, 67
SC-0599-1012 ......66, 67
SC-0599-1012-01 .......67
SC-0599-1012-02 .......67
SC-0599-1013 ......66, 67
SC-0599-1013-01 .......67
SC-0599-1013-02 .......67
SC-0599-1015 ......66, 67
SC-0599-1015-01 .......67
SC-0599-1015-02 .......67
SC-0599-1026 ............67
SC-0599-1026-01 .......67
SC-0599-1026-02 .......67
SC-0599-1026-05 .......67
SC-0599-1027 ............67
SC-0599-1027-01 .......67
SC-0599-1027-05 .......67
SC-0599-1028 ............67
SC-0599-1029 ............67
SC-0599-1029-01 .......67
SC-0599-1032 ............67
SC-0599-1032-01 .......67
SC-0599-1032-05 .......67
SC-0599-F08 ..............70
SC-0599-F16 ..............70
SC-0602 .....................16
SC-1103-DX-PF..........22
SC-1107-0026 ............16
SC-1107-DX ...............16
SC-1107-DX-1030 ......16
SC-1207-DX ...............16
SC-1207-DX-1000 ......16
SC-1210-DX ...............17
SC-1210-DX-PF .........22
SC-1407-DX ...............16
SC-1407-DX-1000 ......16
SC-1410-DX ...............17
SC-1410-DX-PF .........22
SC-1607-DX ...............16
SC-1807-DX ...............16
SC-1807-DX-1000 ......16
SC-5037-3501 ............68
SC-5037-3755-150 .....68
SC-5037-3995-150 .....68
SILQ-50 ......................46
SR2-12-50 ..................80
SR2-21-30 ..................80
SR2-27-28 ..................80
SR2-27-31 ..................80
SR2-80-16 ..................80
SR4-00-01 ..................81
SR4-15-60 ..................81
SR4-20-50 ..................81
SR4-60-14 ..................81
ST2-9-50.....................82
ST3-57 ........................40
ST4-9-50.....................83
ST7-60 ........................83
ST10-28 ......................82
ST10-31 ......................82
ST-EX-5 ......................83
ST-PR-5 ......................83
TQP-50 .......................46
TRP-50 .......................46
V-8-0505-C .................75
V-8-0505-D .................75
V-13-0200R-D.............75
V-13-0200R-XC ..........75
V-14-0300-X ...............72
V-14-0301-X ...............72
V-14-0309-C ...............74
V-14-0309-X .........72, 74
V-14-0311CG-X ..........72
V-14-0312CG-X ..........72
V-14-0314CG-X ..........72
V-14-0712 ...................74
V-14-0712-C ...............74
V-14-0712-M ...............74
V-14-0712-X ...............74
V-16-0225-D ...............75
V-16-0225-LX .............75
V-20-0290-D ...............75
V-20-0290-L ................75
V-28-0260-D ...............75
V-28-0260-L ................75
V-28-0360-V ...............73
V-31-15-X ...................73
V-31-30-X ...................73
V-31-60-X ...................73
V-31-SC-X ..................73
V-50-0360 ...................73
V-50-0460-XII .............75
V-50-0460-XXIV..........75
V-61-0661-C ...............75
V-61-0661-XII .............75
VPC-14-0309-C ..........74
VPC-14-0712-C ..........74
Page 87
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El
Elemental
emen
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ificc
ESI-C-87-2013-B
2013
2013
20
3
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