DFS High Resolution GC/MS - Thermo Fisher Scientific

DFS High Resolution GC/MS - Thermo Fisher Scientific
MASS SPECTROMETRY
Product Sp e ci f i ca t i ons
DFS High Resolution GC/MS
High Performance Magnetic Sector GC/MS
The Thermo Scientific DFS high
resolution GC/MS is the highest
performance, most efficient and simple
to operate magnetic sector mass
spectrometer ever built.
• Performance - Modern innovations in
ion optics, magnet and electric sector
design, provide industry leading specificity for trace target compound analysis;
whilst delivering unrivalled signal to noise
characteristics for reliable peak integration
and quantification.
• Simplicity - The DFS mass spectrometer
is simple to operate and feels like a
benchtop GC/MS. Automated tune and
mass calibration ease adoption of the
technology into the laboratory, whilst
freeing the analyst for other tasks.
• Efficiency - Lowest in class running
costs, combined with high throughput
capabilities of dual GC configurations,
significantly increase laboratory sample
capacity whilst reducing cost per sample.
DFS Mass Spectrometer
The DFS is a high resolution magnetic sector
mass spectrometer like none before. It has
been designed from the ground up to benefit
from new innovations and modern production
techniques. Cumulative advances in modern
component design and manufacture,
combine to provide the most powerful
high resolution GC/MS ever for the most
demanding confirmatory POPs analyses.
2
Hardware Specifications
Ion Source
The ion source has been designed with
special emphasis on sensitivity and durability
for increased productivity, low maintenance
and increased uptime.
Vacuum Interlock
The DFS mass spectrometer is equipped
with a vacuum interlock for quick exchange
of ionization volumes and filaments without
venting.
• Plug-in ion source with optimized box
design for quick exchange including
built in ion extraction lens for ease of
maintenance
• Pneumatically actuated by system control
• Exchange of ion volume and filament
without venting
• Optimized long lifetime filaments for EI
and CI
• Independent source temperature control
• Simple source design - clean quickly
• Inert composition - clean less frequently
Reference Inlet
An independent reference calibrant system
that is continuously flow adjustable and can
be individually evacuated. It allows syringe
introduction of liquid or gaseous samples.
By separating the reference inlet from the
GC interface, maintainance is reduced and
uptime maximized.
• Eliminates improper manual operation
Tuning
The DFS system uses the same Thermo
Scientific tuning software found on other
Thermo Scientific GC/MS & LC/MS
instruments; TunePlus™. Designed with
automation and simplicity in mind; the
tuning process, experiment and sequence
set-up is intuitive and rapid. The DFS mass
spectro-meter enables the reliable, routine
use of AUTOTUNE in all ionization modes
without restrictions, including slit control and
automated resolution settings.
Mass Calibration
Thermo Fisher Scientific invented the field
calibration method of scanning magnetic
mass spectrometers. The DFS system offers
full data system control of field calibration
scanning.
The mass scale needs to be calibrated
only once. The operator can change mass
range and scan speed without the need for
recalibration. It is the same approach and
handling as known from benchtop GC/MS
systems.
• Constant mass calibration based on
magnetic field measurement
• Calibration independent of mass range,
scan speed, scan mode (including linked
scan MS/MS), ion polarity and ionization
technique
• No recalibration required after change of
ion volume or ionization technique
3
Analyzer
The newly designed DFS analyzer has
virtually no image aberrations. It is perfectly
double focusing; employing an ultra high
precision toroidal electrostatic analyzer
and a carefully refined magnetic analyzer. This directly translates into stability and
ruggedness.
• Novel ion optics design is based on the
proven reverse Nier-Johnson geometry
• Mass independent focus with uniform
resolution throughout the mass range
• Ion optics optimized for an acceleration
voltage of 5 kV
• All ionization techniques operational with
full acceleration voltage
• High precision, data system controlled,
continuously variable Tantalum entrance
and exit slits for fast response and long
lifetime
• Low hysteresis, radially laminated H-type
magnet of special metal alloy with mass
independent focal length, deflection radius
350 mm, deflection angle 65°
Performance Characteristics
• Sensitivity (EI GC/MS):
>200:1 for 20 fg 2378TCDD
at m/z 322, R = 10,000, S/N=PtP 4SD.
• Mass accuracy < 2 ppm
• Resolution (static) > 60,000 (10% valley)
• Scan rates 0.1 to 10,000 seconds/decade
(continuously variable)
• Mass range 2 - 6000 Da;
2 - 1200 Da at full accelerating voltage
Detection System
The long lifetime secondary electron
multiplier of the DFS analyzer always
provides optimal signal amplification for all
ionization modes including negative CI.
Vacuum System
The clean high vacuum background
produced by turbomolecular pumps enables
the DFS system to achieve lower detection
limits routinely.
• Ultra fast pump down times; reduces
installation and maintainence time maximizing productivity
• Oil-free high vacuum turbo molecular
pumps reduce the high chemical
background observed with other pumping
technologies
• Directly coupled high speed differential
pumping system with three turbo
molecular pumps
• Long lifetime off axis secondary electron
multiplier detection system
• Push-button control
• Post-acceleration/conversion dynode,
variable to ± 20 kV
Electronics Cabinet
Integrated electronics cabinet for low
space requirements. Optimized air flow for
efficient cooling of magnet power supply.
Effective potential decoupling between digital
electronics and mass spectrometer high
voltage and power supplies.
• Quick change mount on an individual
flange
• Innovative Rogowsky magnet entrance
pole pieces for optimum sensitivity
regardless of ionization method
• Automated protection system
• Universal input/output for Ready/Start
communication with external devices
using programmable signal logic
• Novel electrostatic analyzer (ESA) using
a computer optimized toroidal design
for highest mass precision and ion
transmission with virtually no image errors
• Analog in
• Digital in/out
• All focusing and detection elements
housed in a single monoblock vacuum
chamber
• Entire DFS analyzer assembled on an
integrated shock mounted platform for
isolation from floor vibration
Direct Inlet Options
Direct Probe Base Unit (optional)
• Port for direct insertion probe
• Required to attach any of the following
probe options
• Contains exchange lock and probe
electronics
Water Cooled DI Probe (DI / DIP)
(optional)
• Direct insertion probe
DCI Probe (optional)
• Direct chemical ionization probe
• Data system controlled, liquid cooled
• Using reusable filaments
• Using disposable aluminum crucibles
• Ultra fast heating rates of > 500 °C/s
• Heating rates: 20 °C to 200 °C in 30 s,
• Maximum temperature 1600 °C
200 °C to 300 °C in 30 s
• High temperature tip for DCI probe
(optional)
• Temperature range from 10 °C above
ambient
• Maximum temperature 350 °C
• Full data system control
• Using reusable quartz crucibles
• Maximum temperature 800 °C
4
Software Specifications
Thermo Scientific Xcalibur Data System
Xcalibur™ is the uniform software platform
for system control of the Thermo Scientific
GC/MS and LC/MS systems.
The DFS mass spectrometer uses the
Xcalibur instrument control software for
high and low resolution operation, multiple
ion detection MID, selection of positive or
negative ions, linked scans, peak matching,
and full control of analyzer and inlet systems
supporting the following capabilities:
• INTENSITY AUTOTUNE: automated
optimization of tune peak for maximum
senstivity
• RESOLUTION AUTOTUNE: computer
controlled slit settings for maximum
selectivity
• Control of standard and optional inlet
systems
• Instrument diagnostics: full advanced
suite of instrument diagnostics including
integrated parameter logging
Data System
Thermo Scientific TargetQuan
Software Suite (optional)
The special Xcalibur DFS software package
for automated data evaluation on target
compounds including:
• Dioxin method setup
• Support of instrument and quantitation
• Response file and reporting programs
• Data evaluation for isotope dilution
methods as well as relative response
factors
• Compliant with the published EPA
methods for dioxin measurements and
data evaluation according e.g. EPA 1613,
EPA 8280, EPA 8290, EPA 23, EPA 513,
EN 1948 and equivalent JIS methods
• Compliant with the requirement for TEQ
low-med-upper bound reporting
• Standardized output to LIMS systems
Library Options
• NIST Library
• Xcalibur application software,
incorporating all mass spectrometry
processing tasks such as chromatogram
and spectrum display, integrated NIST
library search, CMASS for accurate mass
conversion and averaging, elemental
composition and isotopic pattern
calculation.
• Wiley Library
• QuanBrowser: quantification package
New instrument software releases are
supplied free of charge within 12 month after
delivery.
• MS data import and export using the
ANDI/netCDF formats, conversion from
Finnigan MassLab data file formats, ASCII
text export
• Standardized output to LIMS systems
• Pfleger-Maurer-Weber Library
• Thermo Scientific Pesticide Library
Software Licenses
The DFS Xcalibur software licenses are
supplied for instrument control as well as
reprocessing.
Personal Computer in the following
minimum configuration*: Dell Optiplex 990
MT Core i3-2100
• 3.1 GHz Processor
• Mini Tower case
• 4096 MB 800 MHz DDR2 RAM
• 1TB SATA II hard disk
• DVD-RW drive
• DVI Add-in card
• Network card 10/100
• 2 PCI and 1 PCI-Express slot space
• 1 parallel port
• 2 serial ports
• 12 USB 2.0
• Graphics chip on board, up to 128 MB of
memory
• 10/100/1000 Ethernet chip on board
• U.S. keyboard black
• Dell USB 6-Button Optical Mouse Black
• Microsoft Windows 7 Professional
Operating system (32Bit OS)
• Microsoft Office 2010 Professional
• Mouse and Keyboard
• High resolution 22 inch TFT color monitor
• Optional laser printer, BW,
1200 x 1200 dpi, up to 25 pages/min
* Minimum data system specifications
may change without prior notice in case of
technological improvement. Call for latest
configuration.
Gas Chromatography Options
IEC (Integrated Electronic Control)
Gas Specification
Detectors
Thermo Scientific TRACE 1310
Gas Chromatograph
The TRACE™ 1300 Series GC consists of
two models designed to meet the specific
needs of all laboratories. The TRACE
1310 GC features a complete icon-driven
touch-screen user interface ideal for direct
instrument control in larger routine and
method development laboratories. The
TRACE 1300 GC is the budget-conscious
investment for the basic routine laboratory
looking for an intuitive single-button system,
that provides ease of use with minimal
instrument interaction. Both instruments
offer the same user-exchangeable, instant
connect injector and detector modules and
fast oven performance with exceptional
retention time stability to reach an incredibly
high lab productivity at reduced cost of
ownership.
• Up to 18 channels of integrated electronic
gas control
• Detectors Available: Flame Ionization
Detector, Thermal Conductivity Detector,
Electron Capture Detector, Nitrogen
Phosphorus Detector, full range of Thermo
Scientific mass spectrometers
Optional Instant Connect Auxiliary Gas
Module
• Allows for the control of three additional
gas channels
• Flameout detection and automatic reignition
Performance Specifications
Injectors
• Linear Dynamic Range: >107 (±10%)
• Maximum Number Injectors Installed: 2
• Maximum Temperature: 450 °C in steps
of 0.1 °C
• Typical Retention Time Repeatability:
<0.0008 min
• Typical Peak Area Repeatability: <0.5 %
RSD
Oven Specifications
• Column Oven (H × W × D): 27 × 27 ×
17.7 cm; 12.9 L
• Operating Temperature Range: ambient
+3 °C to 450 °C
• Cryogenic Option Minimum Temperature:
-100 °C with liquid Nitrogen; -50 with
liquid CO2
• Temperature Set Point Resolution: 0.1 °C
• Number of Ramps/Plateaus: 32/33
• Maximum Heating Rate: 125 °C/min
T Range °C
H
eating Rate °C/min
Model: 220 Volts Model: 110 Volts
50 to 70 125
90
70 to 115 100 65
115 to 175 80 50
175 to 300 50 30
300 to 450 35 20
• Oven Cool-Down (22 °C ambient): 450 °C
to 50 °C in <4 minutes
• Ambient Rejection: <0.01 °C per 1 °C
• Pressure Set Points Minimum Increments:
0.01 kPa-0.001 psi in all ranges
Carrier Gas Control Common to all
Injectors
• Split Ratio: Up to 12500:1
• Available as Instant Connect, userexchangeable modules
• Pressure Range: 0–1000 kPa (0–145 PSI)
• Maximum number Installed: 3 including a
mass spectrometers on the same oven
• Modes: Constant and programmed
pressures and flows
• Fast Data Acquisition Rate: up to 300 Hz
for FID, TCD, ECD, and NPD
• Total Flow Setting:
– Control of split flow in 1 mL/min from 0 to 1250 mL/min
– Purge flow from 0 to 50 mL/min
• Available as Instant Connect, userexchangeable modules
Instant Connect Split/Splitless
• Suitable for all capillary columns
(50 μm to530 μm i.d.)
• Compatible with 1/8” and 1/16” packed
column using adapters. Supports P&T/TD/
HS by special adapter. Compatible Merlin
Microseal™ septum.
• Dedicated split/splitless injector with
integrated backflush capabilities
• Maximum Temperature: 400 °C
Instant Connect Programmable
Temperature Vaporizer
• Supports hot/cold split and splitless
modes as well as large volume injections
(solvent split) and On Column (TPOC).
Compatible Merlin Microseal septum.
• Dedicated PTV injector with integrated
backflush capabilities
• Temperature Range: Air forced cooling to
ambient +5 °C up to 450 °C
• Cryogenic Option Minimum Temperature:
-100 °C with liquid nitrogen; -50 °C with
CO2
• Temperature programming of up to 3
ramps at up to 870 °C/min
Instant Connect Flame Ionization
Detector
• Capillary column optimized compatible
with 1/8” and 1/16” packed column
• MDL: <1.8 pg C/s
• Sensitivity: >0.03 Coulombs/gC
• IEC:
– Air: 0–500 mL/min in 0.1 steps
– H2: 0–100 mL/min in 0.1 steps
– Makeup gas (N2 or He) 0–50 mL/min in 0.1 steps
Instant Connect Thermal Conductivity
Detector
• Capillary column optimized (micro TCD)
compatible with 1/8” and 1/16” packed
column
• Maximum Temperature: 400 °C in steps
of 0.1 °C
• MDL: <400 pg tridecane/mL with He
carrier or <20 pg tridecane/s with a total
flow through the cell of 3 mL/min
• Linear Dynamic Range: 105
5
6
Instant Connect Electron Capture
Detector
• Radioactive Source: 370 MBq equal to 10
mCi, 63Ni
• MDL: <6 fg/s lindane
• Linear Dynamic Range: >104 with lindane
• Maximum Temperature: 400 °C in 0.1 °C
steps
• IEC: 0 to 500 mL/min makeup in 0.1
steps
• Make-up Gas: Nitrogen or 95% argon/5%
methane
Thermo Scientific
TriPlus RSH Autosampler
Seamless Operation
The Thermo Scientific TriPlus RSH
Autosampler offers exceptional precision,
flexibility, and productivity in robotic,
sample-handling solutions. Compatible with
Thermo Scientific GC and GC/MS systems,
the autosampler sets new standards in
automation and provides advanced liquidhandling cycles that enable automated
functionality beyond traditional liquid,
headspace, and solid-phase microextraction
(SPME*) injections.
Accurate automation of a multitude of
traditionally manual tasks is enabled by a
new and innovative ATC (Automatic Tool
Change) capability. The ATC feature enables
the user to set up a sequence using up to
six different syringes, automatically loaded
by the autosampler to accurately perform
dilutions, calibrations, and sample injections.
The ability to exchange syringes for different
tasks enables high-precision sample
handling in a single, unattended sequence
prior to automated sample injection.
Integrated Sampling System
• MDL: <20 fg P/s and <100 fg N/s with
standard ceramic bead
The TriPlus™ RSH autosampler expands
automated capabilities beyond sample
injections to advanced sample-handling
cycles. Automating the whole workflow, from
sample preparation to injection, increases
precision and reproducibility and enables
unprecedented flexibility and productivity in
GC and GC-MS sampling.
• Selectivity: gP/gC = 200000; gN/gC =
80000
Ultimate Productivity
Instant Connect Nitrogen Phosphorus
Detector
• NPD available with ceramic beads and
compatible with element-specific sources
• Linear Dynamic Range: 104
• Maximum Temperature: 450 °C in steps
of 0.1 °C
• IEC:
– Air: 0–500 mL/min in 0.1 steps
– H2: 0–10 mL/min in 0.1 steps
– Makeup gas (Nitrogen): 0–50 mL/min in 0.1 steps
General Specifications
• Heated Zones: Up to 7
• Time Events: 63. Support up to 8 valves
• Operating Altitude: Up to 3500 m above
sea level
• Dimensions (H × W × D): 45 × 44 × 67
cm
• Weight (Kg): 35 Kg main unit plus
0.8 Kg each module
Certifications
Conforms to the following safety standards:
– International Electrotechnical Commission
(IEC):
61010-1:2001 - 61010-2-010:2003 61010-2-081:2001 + A1:(2003)
– CAN/CSA C22.2 No. 61010-1 and UL
61010-1
– EuroNorm (EN): 61010-1:2001 - 61010-2010:2004 - 61010-2-081:2002
Conforms to the following regulations on
Electromagnetic Compatibility (EMC) and
Radio Frequency Interference (RFI):
– CISPR 11/EN 55011: Group 1 Class A
– IEC/EN 61326-1:2006
Designed for expanded productivity, this
integrated sampling system accommodates
large sample capacities supporting full,
unattended 24/7 operation. As an example,
a maximum of 972, 2 mL vials combined
with multiple 100 mL wash/waste bottles
enable week-end long unattended operations
– a goal not attainable with most other
sampling systems currently on the market.
Unmatched Flexibility
The TriPlus RSH robotic sample-handling
system offers liquid, headspace, and
solid phase microextraction – capabilities
you expect as being a standard part of a
multi-axis autosampler. In these modes, the
sampling system delivers the precision you
demand for achieving exceptional results.
Scalable capabilities enable expanded GC
and GC-MS application ranges, accurate
micro-sample injections, and the matching of
techniques to sample types.
* Sold under license from Supelco®
TriPlus RSH Configurations
The TriPlus RSH Autosampler is available in
the following configurations:
• TriPlus RSH for automated liquid sampling
• TriPlus RSH for static headspace
automation
• TriPlus RSH for automated liquid and
headspace sampling and injection
Additional upgrade kits are available
to transform existing versions into
multitechnique platforms.
Description l XYZ robotic sample handling
apparatus with automatic syringe switch
concept. When the optional accessories
are installed, the system is capable of
automating sample preparation steps
like standard dilution, standard addition,
sequential dilution, derivatization and
vortexing.
Communication l Two independent LAN
Local User Interface l LED status
indicators. Optional control panel with
4 keys, round knob, and graphical LCD
display.
Instrument Control l Thermo Scientific
chromatography data systems integrated
with Virtual Terminal software to
completely mimic the physical controller
Teaching Functions l Manual without using
tools or external devices
Injector Compatibility l Compatible with
on-column, programmable temperature
vaporizing, packed, purged packed, splitsplitless injectors
High Throughput Configuration
Dual GC set-up with Double Pro and
Confirmation modes: Single TriPlus RSH
serving two independent GC or GC/MS
systems, for liquid, HS or SPME sample
injection or for sample preparation,
using the same or two different software
systems. Two different methods can be
used. Rapid Mode starts the syringe
7
washing cycle during the current GC
cooling phase.
Barcode Reader l Two active laser
scanners for all standard vials using
1-dimension barcodes in a horizontal
orientation.
Vortexer l Intensive mixing of 0.5, 0.7, 2, 5,
10, or 20 mL vials with an agitation speed
up to 2000 rpm
Vial Trays l Heated and cooled trays expand
the range of available applications from
sample injection to sample/standard
preparation
GC Mounting Kits l Thermo Scientific
TRACE 1300 GC, TRACE 1310 GC,
TRACE GC Ultra and FOCUS GC
Configuration for Liquid Sampling
Vial Volumes l 300 μL fixed insert vials,
0.5, 0.7, 2, 2.5, 10, and 20 mL. 96/384
Microtiter or Deep Well plates with
Automatic Foil Cutter to pierce alumina or
plastic foils prior the needle penetration
Syringe Cleaning l Wash stations for up to
4 different solvents for a total of 40 mL
(standard). Optional large washing stations
for up to 3 × 100 mL solvent bottles.
Waste: 1 × 10 mL or drain to external
waste bottle. Possibility to install multiple
solvent stations to expand solvent and
waste volumes.
Options
• Upgrade to headspace option and its own
accessories
Incubation Oven Temperature Range
40 to 200 °C in 1 °C steps, with agitation
Incubation Time l 0.1 to 600.0 min in 0.1
min increments
Syringe Flush Capability l With inert gas
Solvent Syringe Cleaning l Optional
washing stations (4 × 10 mL or 2 × 100
mL vials)
Multiple Headspace Extraction
Yes (optional accessory)
• Upgrade to SPME option (with or without
headspace option)
Enrichment Sampling l Yes with optional
kit for cold trap
• Peltier-controlled drawer for well plates,
300 μL fixed insert vials, 2 and 10 mL
vials. Temperature selectable between 0
and 40 °C
Injection Speed l 1 to 100 mL/min, in 1
mL/min increments
• Cooled trayholders for well plates, 300 μL
fixed insert vials, 2, 10 and 20 mL vials.
Temperature selectable between 4 and 70
°C. Requires external circulator bath.
Needle Lengths l 65 mm, compatible with
every injector port
• Solvent/reagent reservoir
Typical Performance l ≤0.7 RSD % under
Thermo Scientific standard conditions
Options
• Upgrade to Liquid option
• Upgrade to SPME option
Bottom-Sensing Vials l Capable of liquid
injection starting from small-volume
samples. Capability to inject from samples
as low as 5 µL into a vial. Possibility of
performing up to three 1 µL injections
from a 5 µL sample, depending on vial
type.
• Large Volume Wash Station
Height from Vial Bottom l User selectable
between 0.1 and 32 mm in 0.1 mm steps
• Basic enrichment
• Cooled trayholders for 300 μL fixed insert
vials, 2, 10 and 20 mL vials; requires
external circulator bath; temperature
selectable between 4 °C and 70 °C
• Enrichment needle solvent wash
Injection Speed for Liquid Samples
Selectable from 0.1 μL/sec up to 2000
μL/sec and fully programmable
• SPME Fiber Cleaning Station
• Internal standard double
• Solvent/reagent reservoir
• Internal standard post
• Large Volume Wash Station
Sample Capacity (Depending
on autosampler, GC and MS
configurations)
• Up to 4608 well plates or 6912 well plates
with extended X-arm
• Up to 840 0.5/0.7 mL vials or 1260
0.5/0.7 mL vials with the extended X-arm
Injection Volume l Range from 0.1 to
10,000 μL in 0.1 μL steps to 100 μL and
1 μL steps between 100 μL and 10 mL.
Needle lengths: 57 mm or 85 mm Liquid
Injection Modes – 8 fully customizable
method-specific preset menus available:
• Needle solvent wash
• Solvent flush double
• Solvent flush post
Typical Performance – ≤0.3 RSD %
obtained under Thermo Scientific standard
conditions
Configuration for Headspace
• Up to 648 2 mL sample vials or 972 2 mL
vials with the extended X-arm
Vial Volumes l 2, 10 and 20 mL
• Up to 240 10 mL or 20 mL vials or 360
10 mL or 20 mL vials with the extended
X-arm
Sample Capacity (Depending
on autosampler, GC and MS
configurations) l Up to 180 10 or 20 mL
vials or 300 10 or 20 mL vials with the
extended X-arm
Syringes (Capable of handling liquid
volumes in the range 0.1 μL – 10 mL)
Capable of using 0.5 μL, 1.0 μL, 5 μL, 10
μL (standard), 25 μL, 50 μL, 100 μL, 250
μL, 500 μL, 1000 μL, 10000 μL syringes
for sample injection and/or volume
transfer
Syringe Sizes l 1, 2.5, and 5 mL
Injection Volume Range l 0.1 to 5 mL in
0.1 mL steps depending on syringe
Syringe Temperature l OFF or 40 °C to
150 °C in 1 °C steps
Incubation Oven Capacity l 6 vials
• Peltier-cooled trayholder for 300 μL
fixed insert vials, 2 and 10 mL vials;
temperature selectable between 0 °C and
40 °C
Solid Phase Micro Extraction Option
Vial Volumes l 2, 10 and 20 mL
Sample Capacity l Depending on
Autosampler, GC and MS configurations:
• Up to 840 0.5/0.7 mL vials or 1260
0.5/0.7 mL vials with the extended X-arm
• Up to 648 2 mL sample vials or 972 2 mL
vials with the extended X-arm
• Up to 180 10 or 20 mL vials or 300 10 or
20 mL vials with the extended X-arm
Incubation Oven Capacity l 6 vials
Incubation Oven Temperature Range
40 °C to 200 °C in 1 °C steps, with
agitation
Vial Penetration Depth l Standard or
custom between 5 mm and 20 mm,
suitable for liquid or headspace extraction
Fiber Conditioning Station l Optional,
2-ports and a needle guide, 40-350 °C,
inert gas purged. Fiber: 23 gauge. One
fiber holder to automate all fibers.
Installation Requirements
Environment
Recirculating Water Chiller
The DFS mass spectrometer can be
configured with the optional Thermo
Scientific NESLAB ThermoFlex TF25
recirculating chiller. The chiller is compact,
quiet and efficient. The ThermoFlex TF25
is available in both air-cooled and water
cooled configurations, for a quiet laboratory
for stable and precise cooling of magnet
and turbo molecular pumps. The cooler is
controlled by a temperature sensor mounted
on the DFS magnet.
Compressed Air
Compressed air with a pressure of 6 bar
(87 psi) is required to operate the pneumatic
valves of the instrument. A suitable
compressor can be ordered from Thermo
Fisher Scientific (Part No. 026 1850).
Room Temperature
Laboratory room temperature must be
maintained between 15 °C and 26 °C
(59 °F and 79 °F). The optimum operation
temperature is between 18 °C and 21 °C
(65 °F and 70 °F).
Space Requirement
Air Conditioning Load
The average power dissipation during
analysis operation for a basic DFS system,
including gas chromatograph and data
system, is approximately 4.7 kW (4.5 BTU/s).
For dual GC configuration, the average air
conditioning load amounts approximately
to 4.9 kW (4.7 BTU/s).
DFS Mass Spectrometer
• HxD 140.6 cm (55.4”) x 156.8 cm (62.5”)
• Width with one GC installed
161.1 cm (63.5”)
• Width with two GCs installed
209.1 cm (82.4”)
• Precise temperature control and
temperature stability of up to ± 0.1 °C
• MS console with analyzer and magnet
900 kg (2000 lb)
• Adjustable high and low temperature
safeties with audible alarm
• Data system 130 kg (< 290 lb)
• Environmentally-friendly CFC-free aircooled refrigeration system ThermoFlex
TF25 - 79.6 Kg. 44 x 67 x 73 cm
TRACE 1310 GC
• Dimensions (H × W × D): 45 × 44 × 67
cm
Supplies
• Weight (Kg): 35 Kg main unit plus 0.8 Kg
each module (78 lb)
Power
The DFS mass spectrometer is designed to
operate at a nominal voltage of 230 V AC,
50/60 Hz. The minimum and maximum
voltage tolerances are in compliance with
IEC 950, Amend 2, 1993. Approximate
consumption values for regular operation are:
• Column Oven (H × W × D): 27 × 27 ×
17.7 cm; 12.9 L
• 0,9 kW for GC operation
• 1,9 kW for MS operation
• 1,6 kW for chiller
Helium
For GC carrier gas: 99.996%, ultra-high
purity. Total hydrocarbons should be less
than 2.0 ppm.
• GC with console 35 kg (78 lb)
Humidity
The relative humidity of the operating
environment must be between 30% and
70%, with no condensation.
Recommended Instrument Clearences
and Weight Distribution
TriPlus RSH Autosampler
Overall dimensions on the GC:
• Length (X axis) 80 cm
The extended extended model length
is 120 cm
• Height approximately 70 cm, dependent
on mounting kit
CPU: 42 x 18 x 44.5 cm (16.5 x 7 x 17”)
Monitor: 42 x 40 x 43 cm (16.5 x 16 x 17”)
Keyboard: 2.5 x 47 x 18 cm (1 x 18 x 7“)
thermoscientific.com/dfs
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Africa-Other +27 11 570 1840
Australia +61 2 8844 9500
Austria +43 1 333 50 34 0
Belgium +32 53 73 42 41
Canada +1 800 530 8447
China +86 10 8419 3588
Denmark +45 70 23 62 60
Europe-Other +43 1 333 50 34 0
PS30096_E 07/12G
Finland /Norway/Sweden
+46 8 556 468 00
France +33 1 60 92 48 00
Germany +49 6103 408 1014
India +91 22 6742 9434
Italy +39 02 950 591
Japan +81 45 453 9100
Latin America +1 608 276 5659
Middle East +43 1 333 50 34 0
Netherlands +31 76 579 55 55
South Africa +27 11 570 1840
Spain +34 914 845 965
Switzerland +41 61 716 77 00
UK +44 1442 233555
USA +1 800 532 4752
Product Sp e ci f i ca t i ons
Detailed installation requirements are
provided in the DFS Preinstallation
Requirements Guide PN/1194630
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