Freeze Dry Systems and Accessories

Freeze Dry Systems and Accessories
Freeze Dry Systems and Accessories
FreeZone Freeze Dry Systems
®
an
Table of Contents:
Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1
Selection Guide . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
FreeZone Freeze Dry Systems
1 Liter Benchtop . . . . . . . . . . . . . . . . . . . . . . . . . 6
2.5 Liter Benchtop . . . . . . . . . . . . . . . . . . . . . . . . 8
2.5 Liter Cascade Benchtop . . . . . . . . . . . . . . . . 10
2.5 Liter Cascade Console . . . . . . . . . . . . . . . . . 12
4.5 Liter Benchtop . . . . . . . . . . . . . . . . . . . . . . . 14
4.5 Liter Console . . . . . . . . . . . . . . . . . . . . . . . . 16
4.5 Liter Cascade Benchtop . . . . . . . . . . . . . . . . 18
4.5 Liter Cascade Console . . . . . . . . . . . . . . . . . 20
4.5 Liter -105° C Cascade Benchtop . . . . . . . . . 22
6 Liter Benchtop . . . . . . . . . . . . . . . . . . . . . . . . 24
6, 12 & 18 Liter Console . . . . . . . . . . . . . . . . . . 26
6 & 12 Liter Cascade Console . . . . . . . . . . . . . . 30
Ordering Information . . . . . . . . . . . . . . . . . . . . 33
overview
L
Labconco has been designing and manufacturing laboratory freeze drying equipment since 1974. Since the beginning,
Labconco has strived to incorporate features that enhance
environmental safety, ease-of-use and durability.
Environmental safety. All refrigeration systems found in
FreeZone Freeze Dry Systems, FreeZone Plus Cascade Freeze
Dry Systems and FreeZone Stoppering Tray Dryers use environmentally-friendly HCFC/CFC-free refrigerants.
Ease of use. FreeZone Freeze Dry Systems were designed
to provide simplicity of use and convenience.
•With automatic start up, pressing one button initiates
collector refrigeration and vacuum. Vacuum pull down is
delayed to allow sufficient time for the collector to cool
ensuring that moisture is trapped by the collector to protect
the pump from contamination.
•Lighted “wave” graphs are visible from a distance, display
amber then green, to indicate when temperature and vacuum levels are right for adding samples.*
Dry Ice Freeze Dry System . . . . . . . . . . . . . . . . . . . . 41
FreeZone Triad Cascade Freeze Dry Systems . . . . . . 42
FreeZone Stoppering Tray Dryers . . . . . . . . . . . . . . . 46
FreeZone Bulk Tray Dryers . . . . . . . . . . . . . . . . . . . . 49
FreeZone Triad, Stoppering Tray Dryers &
Bulk Tray Dryers Accessories . . . . . . . . . . . . . . . . . . 51
Drying Accessories . . . . . . . . . . . . . . . . . . . . . . . . . . .52
Secondary Traps . . . . . . . . . . . . . . . . . . . . . . . . . . . . 55
Rotary Vane Vacuum Pumps & Accessories . . . . . . . 56
FreeZone Benchtop Shell Freezers . . . . . . . . . . . . . . 59
Fast-Freeze Flasks . . . . . . . . . . . . . . . . . . . . . . . . . . 60
®
Lyph-Lock Flasks . . . . . . . . . . . . . . . . . . . . . . . . . . . 61
®
Serum Bottles & Vials . . . . . . . . . . . . . . . . . . . . . . . . 62
Ampules & Miscellaneous Accessories . . . . . . . . . . . 63
FreeZone Freeze Dry Systems in console models are available in 2.5, 4.5, 6, 12 and
18 liter collector capacities.
* Not included on FreeZone 1 Liter Systems
FreeZone Freeze Dry Systems
®
an
overview
Durability. FreeZone Systems have several features designed
to protect the system and vacuum pump.
•The patented moisture sensor protects the vacuum pump
by preventing refrigeration or vacuum start-up when moisture is detected in the collector chamber.*
•The vacuum break valve protects the system from oil backstreaming during power outages.*
•Models are available that include a Teflon**-coated
collector chamber and coil for processes involving corrosive
compounds.
•The purge valve, available on FreeZone 6, 12 and 18 Liter
Console Systems, allows the vacuum pump to be run after
freeze drying is complete so that contaminants may be
purged from the oil.
FreeZone 1 Liter Benchtop Freeze Dry Systems offer an economical solution for
processing light sample loads or dedicated use by one researcher.
•The LCD provides easy-to-read digital readouts of vacuum
in mBar, Pa or Torr and temperature in ° F or ° C. It also
displays service information such as total number of hours
of refrigeration and vacuum pump operation and total
number of hours since the refrigeration and vacuum pump
were serviced.
•The vacuum control valve helps to speed evaporation of
solvent samples by maintaining the vacuum level.*
•The audible/visual alarm alerts the user to abnormal
system events. Alarm messages are displayed on the LCD.*
•The upright collector chamber makes defrosting easy. All
models may be manually defrosted by pouring water into
the upright chamber to melt the collected ice. Some models
include a built-in hot gas defrost that melts the collected ice.
When the defrost function is selected, hot gas from the compressor is circulated through the collector coil. The defrost
feature automatically shuts off when the refrigerant leaving
the collector coil reaches +65° C (+149° F). A collector drain
hose allows convenient emptying of the melted ice.
•The rear-mounted RS-232 port simplifies connection to
a personal computer for operation verification. The time
between data transmissions may be set to occur at 10, 30,
60, 300 or 600 second intervals.*
FreeZone Plus 2.5 Liter Cascade Freeze Dry Systems reach -84° C for processing
samples with low eutectic points. Dual refrigeration cascade models also come in
6 and 12 liter collector capacities.
* Not included on FreeZone 1 Liter Systems
** Teflon® is a registered trademark of E.I. duPont de Nemours
1
FreeZone Freeze Dry Systems
®
an
overview
Left: A built-in shell freezer may be ordered
with selected models of FreeZone 6 Liter Freeze
Dry Systems.
Right: A built-in mini vacuum drying chamber
holds small samples and heats to +60° C (+140° F).
The drying chamber may be ordered with selected
models of FreeZone 6, 12 and 18 Liter Freeze
Dry Systems.
Digital Control Panel Displays System Status
FreeZone 1 Liter Freeze Dry Systems
®
MENU switch. Changes the
display from operating system
parameters to set-up parameters.
SELECT switch. Press to select
between manual or automatic
vacuum pump start-up, desired
vacuum or temperature unit
of measure.
VACUUM MANUAL ON/OFF
switch. Press to start the vacuum
pump manually or to stop the
vacuum pump when operating
in either the auto or manual
start-up mode.
2
LCD. Displays system set-up
and operating parameters. The
user may configure the display
to show vacuum in mBar, Pa or
Torr and temperature in ° F or
° C. Other displays include: total
duration of refrigeration operation, total duration since the
refrigeration system was last serviced, total duration of vacuum
operation and total duration since
the vacuum pump was last
serviced (in hours).
FreeZone Freeze Dry Systems
®
an
overview
FreeZone 2.5–18 Liter Freeze Dry Systems
MENU switch. Press to change
screen display.
®
DEFROST switch with LED
indicator light. Controls the hot
gas chamber defrost function
found on all FreeZone 6, 12
and 18 Liter Console Systems.
VACUUM switch with LED
indicator light. Starts or stops
the vacuum pump.
LCD. Displays system set-up
and operating parameters and
alarm messages. The user may
configure the display to show
vacuum in mBar, Pa or Torr
and temperature in ° F or ° C.
Other displays include: total
duration of refrigeration operation and total duration since
the refrigeration system was
last serviced (in hours); total
duration of vacuum operation
and total duration since the
vacuum pump was last serviced (in hours); time between
RS-232 transmissions (10, 30,
60, 300 or 600 second intervals); and alarm messages:
power failure, improper line
voltage supply, collector temperature rise above -40° C,
service vacuum pump (after
1000 hours of vacuum use)
and moisture in collector.
PURGE switch with LED
indicator light. Controls the
optional purge valve available
on FreeZone 6, 12 and 18 Liter
Console Systems. The green
LED illuminates when the
purge valve is closed, isolating
the pump from the collector
chamber.
SELECT switch. Press to
select desired vacuum or temperature unit of measure or
set-up parameters.
SHELL FREEZER switch
with LED indicator light.
Controls the optional shell
freezer rollers and refrigeration module available on
FreeZone 6 Liter Console
Freeze Dry Systems.
MANUAL refrigeration switch
with LED indicator light. Press
to start the refrigeration only.
AUTO mode switch with
LED indicator light. Controls
refrigeration and the automatic
mode process. In the automatic
mode, the system activates
the vacuum pump when the
collector temperature reaches
-40° C.
VACUUM CHAMBER
switch with LED indicator
light. Controls the optional
mini vacuum drying chamber
available on FreeZone 6, 12
and 18 Liter Console Freeze
Dry Systems.
3
TEMPERATURE GRAPH
DISPLAY. Provides at-a-glance
monitoring of the collector temperature. The highest LED illuminates amber to indicate that
the temperature is warmer than
+10° C. The indicators sequence
down when the temperature
reaches +10, 0, -10, -20, -30
and -40° C. When the collector temperature reaches -40° C,
the lowest LED illuminates
green, indicating temperature
is right to add samples.
ALARM light. LED flashes
red to indicate that a system
alarm event has occurred.
Events that trigger the audible/
visual alarm are: power failure,
improper line voltage supply,
collector temperature rise above
-40° C, service vacuum pump
(after 1000 hours of vacuum
use), and moisture in collector. Pressing the Menu Switch
displays the alarm message on
the LCD.
VACUUM GRAPH DISPLAY.
Provides at-a-glance monitoring of relative system vacuum
level. The highest LED illuminates amber to indicate that the
vacuum level is above 2.0 mBar.
The indicators sequence down
when the vacuum level reaches
2.0, 1.0, 0.8, 0.6, 0.45 and 0.12
mBar. When the vacuum level
is between 0.45 and 0.12, the
lowest LED flashes green. Below
0.12 mBar, the lowest LED illuminates green steadily, indicating samples may be attached to
the freeze dry system.
FreeZone Freeze Dry Systems
®
Selection Guide
System
Style
Application -50° C (-58°F)
-84° C (-119° F)
Capacity
Requirements and Collector/
Cascade Collector/
User Preferences
Refrigeration
Refrigeration
For aqueous samples
For samples with low eutectic points,
including acetonitrile
Optional Teflon-coated
collector available
Optional Teflon-coated collector
available on some models
1 LiterBenchtop
•Light sample loads
•1/3 hp refrigeration system
See pages 6-7
•Removes 1 liter of
•Limited floor space
•Economical water in 24 hours*
2.5 LitersBenchtop
•Light sample loads
•1/3 hp refrigeration system
•Two 1/3 hp refrigeration See pages 8-11
systems
•Removes 2 liters of
•Removes 2.2 liters of
•Limited floor space
water in 24 hours* water in 24 hours*
2.5 LitersConsole
•Light sample loads •Two 1/3 hp refrigeration See pages 12-13
systems
•Low eutectic point samples
•Removes 2.2 liters of
water in 24 hours*
2.5 LitersBenchtop
•Light sample loads •Two 1/3 hp refrigeration systems
™
See pages 30-33
Triad •Low eutectic point samples
•Removes 1.8 liters of
water in 24 hours*
•Stoppers samples in bottles
or vials under vacuum
LitersBenchtop
•Light to moderate sample loads •1/3 hp refrigeration system
•Two 1/3 hp refrigeration systems
See4.5
pages 14-15,
•Removes over 2 liters of
•Removes 4 liters of water
•Limited floor space
18-19 and 22-23
water in 24 hours* in 24 hours*
4.5 LitersConsole
•Light to moderate sample loads •1/3 hp refrigeration system
•Two 1/3 hp refrigeration systems
See pages 16-17
•Removes
over
2
liters
of
•Removes 4 liters of water
and 20-21
water in 24 hours* in 24 hours*
6 LitersBenchtop
•Moderate sample loads
•3/4 hp refrigeration system
See pages 24-25
•Limited floor space
•Removes 4 liters of water •Available with Stoppering in 24 hours*
Tray Dryer
•Moderate sample loads
•3/4 hp refrigeration system
•Two 1/3 hp refrigeration systems
6 LitersConsole
See pages 26-27
•Broadest
range
of
options
•Removes
4
liters
of
water
•Removes
4 liters of water and 30-31
in 24 hours*
•Available with Stoppering in 24 hours*
Tray Dryer
12 LitersConsole
•Sample loads of varying volumes •1 hp refrigeration system
•Two 3/4 hp refrigeration systems
See pages 26, 28,
•Available
with
Stoppering
•Removes 8 liters of
•Removes up to 4 liters of
30 and 32
Tray Dryer water in 24 hours*
water in 24 hours*
18 LitersConsole
•Large volumes of material or
numerous sample batches
See pages 26 and 29
•1-1/2 hp refrigeration system
•Removes 10 liters of
water in 24 hours*
* Freeze drying capacity rating will be lower for samples other than plain water.
4
FreeZone Freeze Dry Systems
®
B U I L T - I N O P T I O N S
-105° C (-157°F)
Purge Valve, Drying Vacuum Glassware
Cascade Collector/
Mini Vacuum Drying Chamber & Accessory
Pump
Refrigeration
Shell Freezer
Tray Dryers, Drying
See pages 57-58
See pages 60-63
Chambers and Manifolds
For samples with very low eutectic
Available on some models
that accommodate samples
in containers or in bulk
points including acetonitrile and
dilute methanol and ethanol
•REQUIRED—
•REQUIRED—
•REQUIRED—
See drying accessories 86 liters/minute unless bulk
on pages 52-54. or larger displacement drying
•REQUIRED—
•REQUIRED—
•REQUIRED—
See drying accessories 86 liters/minute unless bulk
on pages 52-54. or larger displacement drying
•REQUIRED—
•REQUIRED—
•REQUIRED—
See drying accessories 86 liters/minute unless bulk
on pages 52-54. or larger displacement drying
•Permanently installed •REQUIRED—
•REQUIRED—
•One stoppering shelf 98 liters/minute unless bulk
•4 ports or larger displacement† drying
•Two 1/3 hp refrigeration
•Permanently
•REQUIRED—
•REQUIRED—
systemsinstalled or included**86 liters/minuteunless bulk
•10 ports or 12 ports** or larger displacementdrying
•Removes 2.5 liters of
water in 24 hours •Permanently
•REQUIRED—
•REQUIRED—
installed or included**86 liters/minuteunless bulk
•10 ports or 12 ports** or larger displacementdrying
•REQUIRED—
•REQUIRED—
•REQUIRED—
See drying accessories 98 liters/minute unless bulk
†
on pages 46-54. or larger displacement drying
•Purge Valve available
•REQUIRED—
•REQUIRED—
•REQUIRED—
•Mini Vacuum Drying Chamber available See drying accessories 98 liters/minute unless bulk
•Shell Freezer available with -50° C models on pages 46-54. or larger displacement†drying
•Purge Valve available
•REQUIRED—
•REQUIRED—
•REQUIRED—
•Mini Vacuum Drying Chamber available See drying accessories 98 liters/minute unless bulk
†
on pages 46-54. or larger displacement drying
•Purge Valve available
•REQUIRED—
•REQUIRED—
•REQUIRED—
•Mini Vacuum Drying Chamber available See drying accessories 98 liters/minute unless bulk
†
on pages 46-54. or larger displacement drying * Freeze drying capacity rating will be lower for samples other than plain water.
** FreeZone 4.5 Liter Freeze Dry Systems include a permanently-installed 10-port drying
chamber. FreeZone Plus 4.5 Liter Cascade Freeze Dry Systems and FreeZone -105° C 4.5 Liter
Freeze Dry Systems include a 12-Port Drying Chamber 7522800, which requires attachment.
† 144 liters/minute displacement is recommended.
5
FreeZone 1 Liter Benchtop Freeze Dry Systems
®
Features
Rear-mounted 3/4" vacuum
connection extends vertically,
requiring less space.
HCFC/CFC-free refrigeration
system ensures rapid, environmentally-safe cooling. The
condensing module cools the
collector coil to -50° C (-58° F),
ideal for freeze drying aqueous samples. The system uses a
non-flammable refrigerant that
contains no ozone-damaging
hydrochlorofluorocarbons
(HCFCs) or chlorofluorocarbons (CFCs).
&
Benchtop cabinet has small
footprint. Compact cabinet of
durable epoxy-coated steel with
brushed stainless steel front
panel and four rubber feet fits
easily atop a countertop or
laboratory cart.
benefits
Attachment lid makes
connection of accessories easy.
Select from accessory drying
chambers and manifolds (sold
separately).
Upright, stainless steel collector
chamber speeds and simplifies defrost. Hot water may be
poured into the chamber, or
collected ice may be allowed
to melt overnight. Models are
available with Teflon-coated
collector coil and chamber for
additional corrosion resistance.
Factory wired. All models
include a 3-wire cord with
20 amp NEMA plug.
Automatic start-up is quick
and easy to use. Turning on
the main power switch, located
on the right-hand side, initiates
the collector cool-down and
vacuum pull-down sequence if
automatic mode is selected. If
manual mode is selected, turning on the main power switch
initiates collector cool-down,
but the vacuum pump must
be turned on by pressing the
vacuum switch.
LCD displays system set-up and
operating parameters.
Easy-to-follow operating
instructions are printed on the
right-hand side.
Collector drain hose is accessible from the left-hand side for
convenient disposal of defrosted
material. It extends about nine
inches and retracts within the
cabinet when not in use.
Rear-mounted electrical
receptacle allows connection of
the vacuum pump (pump sold
separately).
CE marking. All 230 volt,
50 Hz models conform to the
CE (European Community)
directives.
ETL listed. Models for operation on 115 volts, 60 Hz or 230
volts, 60 Hz carry the ETL mark
signifying they are certified to
UL and CAN/CSA standards for
laboratory equipment.
Exclusive feature
6
FreeZone 1 Liter Benchtop Freeze Dry Systems
®
specifications
All models feature:
• Upright stainless steel collector coil capable of removing 1 liter of
water in 24 hours and holding 1 liter of ice before defrosting.*
• 1/3 hp HCFC/CFC-free refrigeration system to cool collector to
-50° C (-58° F). For aqueous samples. Not for use with samples
containing acetonitrile, methanol or ethanol.
Compact benchtop design with a small footprint.
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
LCD for display of set-up and operating parameters. It may be userconfigured to select either automatic or manual mode operation and
to display vacuum in mBar, Pa or Torr and temperature in ° F or ° C.
It also displays total duration of refrigeration system operation and
time since the refrigeration system was serviced, and the duration
of vacuum pump operation and time since the vacuum pump was
serviced (in hours).
• Automatic start-up for collector cool-down and vacuum pull-down
when programmed for automatic mode.
FreeZone 1 Liter Benchtop Freeze Dry System 7740020, 12-Port Drying Chamber 7522800,
Portable Table 8025000 and miscellaneous glassware.
• Side-mounted, retractable, 9" collector drain hose.
• Clear acrylic lid, 3/4" thick, with 3" diameter attachment port for connection of drying accessories (sold separately).
See ordering information on page 33.
• Side-mounted power switch, rear-mounted electrical receptacle (for
vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3/4" OD vacuum connector, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 12.6" w x 17.9" d x 16.9" h (32.0 cm x 45.4 cm x 42.9 cm).
Models conform to the following standards:
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
Options include:
• Teflon-coated collector coil and chamber for processes involving
corrosive compounds.
• Domestic or international electrical configuration.
All models require (not included):
• Vacuum pump with a displacement of at least 86 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Drying accessory. See pages 52-54.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
* Freeze drying capacity rating will be lower for samples other than plain water.
Exclusive feature
7
FreeZone 2.5 Liter Benchtop Freeze Dry Systems
®
Features
HCFC/CFC-free refrigeration
system ensures rapid, environmentally-safe cooling. The
condensing module cools the
collector coil to -50° C (-58° F),
ideal for freeze drying aqueous
samples. The system uses a nonflammable refrigerant that contains no ozone-damaging hydrochlorofluorocarbons (HCFCs) or
chlorofluorocarbons (CFCs).
&
Rear-mounted 3/4" vacuum
connection extends vertically,
requiring less space.
benefits
Attachment lid makes
connection of accessories easy.
Select from accessory drying
chambers and manifolds (sold
separately).
Vacuum and temperature
graphs display relative system
vacuum and collector temperature. Amber LED “waves”
illuminate when vacuum and
temperature levels are out of
range for adding samples. Green
LED lights indicate that conditions are right to add samples.
LCD displays system set-up
and operating parameters and
alarm messages.
Easy-to-follow operating
instructions are printed on the
right-hand side.
Red alarm light flashes and
beeper sounds to indicate that
an abnormal system event has
occurred. Pressing the Menu
Switch displays the alarm
message on the LCD.
Rear-mounted electrical
receptacle allows connection of
the vacuum pump (pump sold
separately).
Automatic start-up is quick
and easy to use. Pressing one
button initiates the collector
cool-down and vacuum pulldown sequence. Or, manually override this feature at
any time using the separate
switches for manual refrigeration and vacuum.
Collector drain hose is accessible from the left-hand side
for convenient defrost. It
extends about nine inches
and retracts within the cabinet
when not in use.
ETL listed. Models for operation on 115 volts, 60 Hz or 230
volts, 60 Hz carry the ETL mark
signifying they are certified to
UL and CAN/CSA standards for
laboratory equipment.
Upright, stainless steel collector
chamber speeds and simplifies defrost. Hot water may be
poured into the chamber, or
collected ice may be allowed
to melt overnight. Models are
available with Teflon-coated
collector coil and chamber for
additional corrosion resistance.
Vacuum control valve maintains setpoint vacuum level to
speed the freeze dry process.
Moisture sensor protects the
vacuum pump by preventing
refrigeration or vacuum startup when moisture is detected
in the collector chamber area.
Rear-mounted RS-232 port
may be used to transmit data
to a user-supplied computer.
The time between data transmissions may be set to occur at
10, 30, 60, 300 or 600 second
intervals.
Vacuum break valve protects
the system from oil backstreaming by bleeding air into the
system when power to the
freeze dryer or vacuum pump
is shut off. If a brief power
outage occurs (approximately
5 minutes), the freeze dryer
will restart and the refrigeration and vacuum system will
resume operation once power is
restored. If the power failure is
long (approximately 5 minutes)
and the collector warms above
safe limits, the freeze dryer will
not automatically restart, which
prevents melted sample from
being drawn into the collector
and liquid from harming the
vacuum pump.
Factory wired. All models
include a 3-wire cord with
20 amp NEMA plug.
Exclusive feature
8
Benchtop cabinet has small
footprint. Compact cabinet of
durable epoxy-coated steel with
brushed stainless steel front
panel and four rubber feet fits
easily atop a countertop or
laboratory cart.
CE marking. All 230 volt,
50 Hz models conform to the
CE (European Community)
directives.
FreeZone 2.5 Liter Benchtop Freeze Dry Systems
®
specifications
All models feature:
• Upright stainless steel collector coil capable of removing 2 liters of
water in 24 hours and holding 2.5 liters of ice before defrosting.*
• 1/3 hp HCFC/CFC-free refrigeration system to cool collector to
-50° C (-58° F). For aqueous samples. Not for use with samples
containing acetonitrile, methanol or ethanol.
Compact benchtop design with a small footprint.
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
LCD that displays system operating parameters, set-up parameters and
alarm messages. It may be user-configured to display vacuum in mBar,
Pa or Torr and temperature in ° F or ° C. It also displays total number of
hours of refrigeration system operation and time since the refrigeration
system was serviced and the total number of hours of vacuum pump
operation and time since the vacuum pump was serviced (in hours).
Red alarm light that flashes and beeper that sounds to indicate that an
abnormal system event has occurred, including: power failure, improper line voltage supply, collector temperature rise above -40° C, service
vacuum pump (after 1000 hours of vacuum use), and moisture in collector. Pressing the Menu Switch displays the alarm message on the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of relative system vacuum and collector temperature.
Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off. If a power outage less
than approximately 5 minutes occurs, the freeze dryer will restart
and the refrigeration and vacuum system will resume operation once
power is restored. If the power failure is more than approximately
5 minutes and the collector warms above safe limits, the freeze dryer
will not automatically restart.
• Rear-mounted RS-232 port to transmit data to a user-supplied computer. Transmission intervals may be user-configured for 10, 30, 60, 300
or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Side-mounted, retractable, 9" collector drain hose.
• Clear acrylic lid, 3/4" thick, with 3" diameter port for connection of
drying accessories (sold separately).
• Side-mounted power switch, rear-mounted electrical receptacle (for
vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3/4" OD vacuum connection, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 12.6" w x 17.9" d x 16.9" h (32.0 cm x 45.4 cm x 42.9 cm).
FreeZone 2.5 Liter Benchtop Freeze Dry System 7670520, Clear Chamber with Valves
7443500, Portable Table 8025000 and miscellaneous glassware.
All models require (not included):
• Vacuum pump with a displacement of at least 86 liters per minute, 0.002 mBar ultimate pressure and fitting suitable for 3/4" ID
vacuum hose. See pages 56-58.
• Drying accessory. See pages 52-54.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
See ordering information on page 33.
Models conform to the following standards:
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
Options include:
• Teflon-coated collector coil and chamber for processes involving
corrosive compounds.
• Domestic or international electrical configuration.
*Freeze drying capacity rating will be lower for samples other than plain water.
Exclusive feature
9
FreeZone Plus 2.5 Liter Cascade Benchtop Freeze Dry Systems
®
™
Features
HCFC/CFC-free refrigeration
system ensures rapid,
environmentally-safe cooling.
Two condensing modules, used
in series, cool the collector coil
to -84° C (-119° F), ideal for
freeze drying samples with low
eutectic points including acetonitrile. The systems use a nonflammable refrigerant that contains no ozone-damaging hydrochlorofluorocarbons (HCFCs) or
chlorofluorocarbons (CFCs).
&
Rear-mounted 3/4" vacuum
connection extends vertically,
requiring less space.
benefits
Attachment lid makes
connection of accessories easy.
Select from accessory drying
chambers and manifolds (sold
separately).
Vacuum and temperature
graphs display relative system
vacuum and collector temperature. Amber LED “waves”
illuminate when vacuum and
temperature levels are out of
range for adding samples. Green
LED lights indicate that conditions are right to add samples.
LCD displays system set-up
and operating parameters and
alarm messages.
Easy-to-follow operating
instructions are printed on the
right-hand side.
Red alarm light flashes and
beeper sounds to indicate that
an abnormal system event has
occurred. Pressing the Menu
Switch displays the alarm
message on the LCD.
Rear-mounted electrical
receptacle allows connection of
the vacuum pump (pump sold
separately).
Automatic start-up is quick and
easy to use. Pressing one button
initiates the collector cool-down
and vacuum pull-down
sequence. Or, manually override
this feature at any time using the
separate switches for manual
refrigeration and vacuum.
Collector drain hose is accessible
from the left-hand side for convenient disposal of defrosted
material. It extends about nine
inches and retracts within the
cabinet when not in use.
ETL listed. Models for operation on 115 volts, 60 Hz or 230
volts, 60 Hz carry the ETL mark
signifying they are certified to
UL and CAN/CSA standards for
laboratory equipment.
Upright, stainless steel collector
chamber speeds and simplifies
defrost. A baffle maximizes ice
loading capabilities by evenly
distributing collected ice over
the entire collector coil. Hot
water may be poured into the
chamber, or collected ice may
be allowed to melt overnight.
Models are available with
Teflon-coated collector coil and
chamber for additional corrosion resistance.
Vacuum control valve maintains setpoint vacuum level to
speed the freeze dry process.
Rear-mounted RS-232 port
may be used to transmit data
to a user-supplied computer.
The time between data transmissions may be set to occur at
10, 30, 60, 300 or 600 second
intervals.
Vacuum break valve protects
the system from oil backstreaming by bleeding air into the
system when power to the
freeze dryer or vacuum pump
is shut off. If a brief power
outage occurs (approximately
5 minutes), the freeze dryer
will restart and the refrigeration and vacuum system will
resume operation once power is
restored. If the power failure is
long (approximately 5 minutes)
and the collector warms above
safe limits, the freeze dryer will
not automatically restart, which
prevents melted sample from
being drawn into the collector
and liquid from harming the
vacuum pump.
CE marking. All 230 volt,
50 Hz models conform to the
CE (European Community)
directives.
10
Moisture sensor protects the
vacuum pump by preventing
refrigeration or vacuum startup when moisture is detected
in the collector chamber area.
Benchtop cabinet has small
footprint. Compact cabinet of
durable epoxy-coated steel with
brushed stainless steel front
panel and four rubber feet fits
easily atop a countertop or
laboratory cart.
Factory wired. All models
include a 3-wire cord with
20 amp NEMA plug.
Exclusive feature
FreeZone Plus 2.5 Liter Cascade Benchtop Freeze Dry Systems
®
™
specifications
All models feature:
• Upright stainless steel collector coil capable of removing 2.2 liters of
water in 24 hours and holding 2.5 liters of ice before defrosting.*
• Dual 1/3 HCFC/CFC-free refrigeration systems to cool collector to
-84° C (-119° F). For samples containing water or acetonitrile. Not for
use with samples containing methanol or ethanol.
Compact benchtop cabinet with small footprint.
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
LCD that displays system operating parameters, set-up parameters
and alarm messages. It may be user-configured to display vacuum in
mBar, Pa or Torr and temperature in ° F or ° C. It also displays total
number of hours of refrigeration system operation and time since
the refrigeration system was serviced, and the total number of hours
of vacuum pump operation and time since the vacuum pump was
serviced (in hours).
Red alarm light that flashes and beeper that sounds to indicate that an
abnormal system event has occurred, including: power failure, improper
line voltage supply, collector temperature rise above -40° C, service
vacuum pump (after 1000 hours of vacuum use), and moisture in collector. Pressing the Menu Switch displays the alarm message on the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of relative system vacuum and collector temperature.
Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off. If a power outage less
than approximately 5 minutes occurs, the freeze dryer will restart
and the refrigeration and vacuum system will resume operation once
power is restored. If the power failure is more than approximately
5 minutes and the collector warms above safe limits, the freeze dryer
will not automatically restart.
• Rear-mounted RS-232 port to transmit data to a user-supplied
computer. Transmission intervals may be user-configured for 10, 30,
60, 300 or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Side-mounted, retractable, 9" collector drain hose.
• Clear acrylic lid, 3/4" thick, with 3" diameter port for connection of
drying accessories (sold separately).
• Side-mounted power switch, rear-mounted electrical receptacle (for
vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3/4" OD vacuum connector, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 15.1" w x 23.2" d x 16.9" h (38.3 cm x 59.0 cm x 42.9 cm).
FreeZone Plus 2.5 Liter Cascade Benchtop Freeze Dry System 7670020, 20-Port Manifold
7522300, Rotary Vane Vacuum Pump 1472100, Variable Height Bench 8075000 and
miscellaneous glassware.
All models require (not included):
• Vacuum pump with a displacement of at least 86 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Drying accessory. See pages 52-54.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
See ordering information on page 34.
Models conform to the following standards:
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
Options include:
• Teflon-coated collector coil and chamber for processes involving corrosive compounds.
• Domestic or international electrical configuration.
*Freeze drying capacity rating will be lower for samples other than plain water.
Exclusive feature
11
FreeZone Plus 2.5 Liter Cascade Freeze Dry Systems
®
™
Features
Moisture sensor protects the
vacuum pump by preventing
refrigeration or vacuum startup when moisture is detected
in the collector chamber area.
Rear-mounted 3/4" vacuum
connection extends vertically,
requiring less space.
&
benefits
Attachment lid makes
connection of accessories easy.
Select from accessory drying
chambers and manifolds (sold
separately).
Automatic start-up is quick and
easy to use. Pressing one button
initiates the collector cool-down
and vacuum pull-down sequence.
Or, manually override this feature
at any time using the separate
switches for manual refrigeration
and vacuum.
LCD displays system set-up
and operating parameters and
alarm messages.
Vacuum and temperature
graphs display relative system
vacuum and collector temperature. Amber LED “waves”
illuminate when vacuum and
temperature levels are out of
range for adding samples. Green
LED lights indicate that conditions are right to add samples.
Collector drain hose is accessible from the left-hand side for
convenient disposal of defrosted
material. It extends about nine
inches and retracts within the
cabinet when not in use.
Rear-mounted electrical
receptacle allows connection of
the vacuum pump (pump sold
separately).
Red alarm light flashes and
beeper sounds to indicate that
an abnormal system event has
occurred. Pressing the Menu
Switch displays the alarm
message on the LCD.
Compact console cabinet.
Cabinet, mounted on 3”
diameter casters, is epoxycoated steel with removable
brushed stainless steel front
panel. The interior accommodates a vacuum pump (pump
sold separately.)
HCFC/CFC-free refrigeration
system ensures rapid, environmentally-safe cooling. Two
condensing modules, used in
series, cool the collector coil to
-84° C (-119° F), ideal for freeze
drying samples with low eutectic
points including acetonitrile. The
systems use a non-flammable
refrigerant that contains no
ozone-damaging hydrochlorofluorocarbons (HCFCs) or
chlorofluorocarbons (CFCs).
Easy-to-follow operating
instructions are printed on the
right hand side.
Vacuum break valve protects
the system from oil backstreaming by bleeding air into
the system when power to the
freeze dryer or vacuum pump
is shut off. If a brief power
outage occurs (approximately
5 minutes), the freeze dryer
will restart and the refrigeration and vacuum system will
resume operation once power
is restored. If the power failure
is long (approximately 5 minutes) and the collector warms
above safe limits, the freeze
dryer will not automatically
restart, which prevents melted
sample from being drawn into
the collector and liquid from
harming the vacuum pump.
Upright, stainless steel collector
chamber speeds and simplifies
defrost. A baffle maximizes ice
loading capabilities by evenly
distributing collected ice over
the entire collector coil. Hot
water may be poured into the
chamber, or collected ice may
be allowed to melt overnight.
Models are available with
Teflon-coated collector chamber and coils for additional
corrosion resistance.
Factory wired. All models
include a 3-wire cord with
20 amp NEMA plug.
ETL listed. Models for operation on 115 volts, 60 Hz or 230
volts, 60 Hz carry the ETL mark
signifying they are certified to
UL and CAN/CSA standards for
laboratory equipment.
CE marking. All 230 volt,
50 Hz models conform to the
CE (European Community)
directives.
Rear-mounted RS-232 port
may be used to transmit data
to a user-supplied computer.
The time between data transmissions may be set to occur at
10, 30, 60, 300 or 600 second
intervals.
Vacuum control valve maintains setpoint vacuum level to
speed the freeze dry process.
Exclusive feature
12
FreeZone Plus 2.5 Liter Cascade Freeze Dry Systems
®
™
specifications
All models feature:
• Upright stainless steel collector coil capable of removing 2.2 liters of
water in 24 hours and holding 2.5 liters of ice before defrosting.*
• Dual 1/3 hp HCFC/CFC-free refrigeration systems to cool collector to
-84° C (-119° F). For samples containing water or acetonitrile. Not for
use with samples containing methanol or ethanol.
Compact console cabinet with 3" diameter casters.
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
LCD that displays system operating parameters, set-up parameters
and alarm messages. It may be user-configured to display vacuum in
mBar, Pa or Torr and temperature in ° F or ° C. It also displays total
number of hours of refrigeration system operation and time since
the refrigeration system was serviced, and the total number of hours
of vacuum pump operation and time since the vacuum pump was
serviced (in hours).
Red alarm light that flashes and beeper that sounds to indicate that
an abnormal system event has occurred, including: power failure,
improper line voltage supply, collector temperature rise above -40° C,
service vacuum pump (after 1000 hours of vacuum use), and moisture
in collector. Pressing the Menu Switch displays the alarm message on
the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of
relative system vacuum and collector temperature.
Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off. If a power outage less
than approximately 5 minutes occurs, the freeze dryer will restart
and the refrigeration and vacuum system will resume operation once
power is restored. If the power failure is more than approximately
5 minutes and the collector warms above safe limits, the freeze dryer
will not automatically restart.
• Rear-mounted RS-232 port to transmit data to a user-supplied
computer. Transmission intervals may be user-configured for 10, 30,
60, 300 or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Side-mounted, retractable, 9" collector drain hose.
• Clear acrylic lid, 3/4" thick, with 3" diameter port for connection of
drying accessories (sold separately).
• Side-mounted power switch, rear-mounted electrical receptacle (for
vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3/4" OD vacuum connector, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 18.6" w x 23.2" d x 37.4" h
(47.2 cm x 59.0 cm x 95.0 cm).
• Usable interior space: 14.0" w x 18.5" d x 16.0" h
(35.6 cm x 47.0 cm x 40.6 cm).
FreeZone Plus 2.5 Liter Cascade Freeze Dry System 7420020, Clear Chamber with
Valves 7443500, Product Shelves 7442100 and miscellaneous glassware.
All models require (not included):
• Vacuum pump with a displacement of at least 86 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Drying accessory. See pages 52-54.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
See ordering information on page 34.
Models conform to the following standards:
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
Options include:
• Teflon-coated collector coil and chamber for processes involving
corrosive compounds.
• Domestic or international electrical configuration.
*Freeze drying capacity rating will be lower for samples other than plain water.
Exclusive feature
13
FreeZone 4.5 Liter Benchtop Freeze Dry Systems
®
features
Permanently-installed drying
chamber facilitates sample
connection. The stainless steel
chamber includes ten valves
to allow connection of serum
bottles, ampules or freeze dry
flasks with 1/2" or 3/4" adapters. Each valve has a beveled
edge to provide at-a-glance indication of whether the valve is
open or closed. The clear acrylic
lid permits easy monitoring of
ice build-up on the collector.
&
benefits
Upright, stainless steel collector
chamber speeds and simplifies defrost. Hot water may be
poured into the chamber, or
collected ice may be allowed
to melt overnight. Models are
available with Teflon-coated
collector coil and chamber for
additional corrosion resistance.
Rear-mounted 3/4" vacuum
connection extends vertically,
requiring less space.
Easy-to-follow operating
instructions are printed on the
right-hand side.
Vacuum control valve maintains setpoint vacuum level to
speed the freeze dry process.
Vacuum and temperature
graphs display relative system
vacuum and collector temperature. Amber LED “waves” illuminate when vacuum and temperature levels are out of range
for adding samples. Green LED
lights indicate that conditions
are right to add samples.
LCD displays system set-up
and operating parameters and
alarm messages.
Rear-mounted electrical
receptacle allows connection of
the vacuum pump (pump sold
separately).
Red alarm light flashes and
beeper sounds to indicate that
an abnormal system event has
occurred. Pressing the Menu
Switch displays the alarm
message on the LCD.
Automatic start-up is quick
and easy to use. Pressing one
button initiates the collector
cool-down and vacuum pulldown sequence. Or, manually override this feature at
any time using the separate
switches for manual refrigeration and vacuum.
Collector drain hose is accessible
from the left-hand side for convenient defrost. It extends about
nine inches and retracts within
the cabinet when not in use.
Rear-mounted RS-232 port
may be used to transmit data
to a user-supplied computer.
The time between data transmissions may be set to occur at
10, 30, 60, 300 or 600 second
intervals.
Vacuum break valve protects
the system from oil backstreaming by bleeding air into the
system when power to the
freeze dryer or vacuum pump
is shut off. If a brief power outage occurs (approximately 5
minutes), the freeze dryer will
restart and the refrigeration
and vacuum system will
resume operation once power
is restored. If the power failure
is long (approximately 5 minutes) and the collector warms
above safe limits, the freeze
dryer will not automatically
restart, which prevents melted
sample from being drawn into
the collector and liquid from
harming the vacuum pump.
Factory wired. All models
include a 3-wire cord with
20 amp NEMA plug.
ETL listed. Models for operation on 115 volts, 60 Hz or 230
volts, 60 Hz carry the ETL mark
signifying they are certified to
UL and CAN/CSA standards for
laboratory equipment.
HCFC/CFC-free refrigeration
system ensures rapid, environmentally-safe cooling. The
condensing module cools the
collector coil to -50° C (-58° F),
ideal for freeze drying aqueous
samples. The system uses a non-flammable refrigerant that
contains no ozone-damaging
hydrochlorofluorocarbons
(HCFCs) or chlorofluorocarbons
(CFCs).
Exclusive feature
14
Moisture sensor protects the
vacuum pump by preventing
refrigeration or vacuum startup when moisture is detected
in the collector chamber area.
Benchtop cabinet has small
footprint. Compact cabinet
of durable epoxy-coated steel
with brushed stainless steel
front panel and four rubber
feet fits easily atop a countertop or laboratory cart.
CE marking. All 230 volt,
50 Hz models conform to the
CE (European Community)
directives.
FreeZone 4.5 Liter Benchtop Freeze Dry Systems
®
specifications
All models feature:
• Upright stainless steel collector coil capable of removing 2 liters of
water in 24 hours and holding 4.5 liters of ice before defrosting.*
• 1/3 hp HCFC/CFC-free refrigeration system to cool collector to -50° C (-58° F). For aqueous samples. Not for use with samples containing acetonitrile, methanol or ethanol.
• Permanently-installed 10-port stainless steel drying chamber with
1/2" thick, clear acrylic lid with neoprene gasket.
• Compact benchtop design with a small footprint.
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• LCD that displays system operating parameters, set-up parameters and
alarm messages. It may be user-configured to display vacuum in mBar,
Pa or Torr and temperature in ° F or ° C. It also displays total number of
hours of refrigeration system operation and time since the refrigeration
system was serviced and the total number of hours of vacuum pump
operation and time since the vacuum pump was serviced (in hours).
• Red alarm light that flashes and beeper that sounds to indicate that an
abnormal system event has occurred, including: power failure, improper
line voltage supply, collector temperature rise above -40° C, service vacuum pump (after 1000 hours of vacuum use), and moisture in collector.
Pressing the Menu Switch displays the alarm message on the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of
relative system vacuum and collector temperature.
• Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
• Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off. If a power outage less
than approximately 5 minutes occurs, the freeze dryer will restart
and the refrigeration and vacuum system will resume operation once
power is restored. If the power failure is more than approximately
5 minutes and the collector warms above safe limits, the freeze dryer
will not automatically restart.
• Rear-mounted RS-232 port to transmit data to a user-supplied computer. Transmission intervals may be user-configured for 10, 30, 60,
300 or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Side-mounted, retractable, 9" collector drain hose.
• Side-mounted power switch, rear-mounted electrical receptacle (for
vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3/4" OD vacuum connection, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 18.6" w x 18.5" d x 22.5" h (47.2 cm x 47 cm x 57.2 cm).
FreeZone 4.5 Liter Benchtop Freeze Dry System 7750020, Utility Cart 8007000 and
Chemical-Resistant Rotary Vane Vacuum Pump 7769600.
All models require (not included):
• Vacuum pump with a displacement of at least 86 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
See ordering information on page 34.
Models conform to the following standards:
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
Options include:
• Teflon-coated collector coil and chamber for processes involving
corrosive compounds.
• Domestic or international electrical configuration.
*Freeze drying capacity rating will be lower for samples other than plain water.
Exclusive feature
15
FreeZone 4.5 Liter Freeze Dry Systems
®
Features
Automatic start-up is quick
and easy to use. Pressing one
button initiates the collector
cool-down and vacuum pulldown sequence. Or, manually
override this feature at any time
using the separate switches for
manual refrigeration and vacuum.
&
benefits
HCFC/CFC-free refrigeration
system ensures rapid,
environmentally-safe cooling.
The condensing module cools
the collector coil to -50° C
(-58° F), ideal for freeze drying
aqueous samples. The system
uses a non-flammable refrigerant
that contains no ozone-damaging
hydrochlorofluorocarbons
(HCFCs) or chlorofluorocarbons (CFCs).
Upright, stainless steel collector
chamber speeds and simplifies defrost. Hot water may be
poured into the chamber, or
collected ice may be allowed
to melt overnight. Models are
available with Teflon-coated
collector chamber and coils for
additional corrosion resistance.
Moisture sensor protects the
vacuum pump by preventing
refrigeration or vacuum startup when moisture is detected
in the collector chamber area.
Permanently-installed drying
chamber facilitates sample
connection. The stainless steel
chamber includes ten valves
to allow connection of serum
bottles, ampules or freeze dry
flasks with 1/2" or 3/4" adapters.
Each valve has a beveled edge
to provide at-a-glance indication
of whether the valve is open or
closed. The clear acrylic lid permits easy monitoring of ice
build-up on the collector.
LCD displays system set-up and
operating parameters and alarm
messages.
Vacuum and temperature
graphs display relative system
vacuum and collector temperature. Amber LED “waves”
illuminate when vacuum and
temperature levels are out of
range for adding samples. Green
LED lights indicate that conditions are right to add samples.
Collector drain hose is accessible
from the left-hand side for convenient defrost. It extends about
nine inches and retracts within
the cabinet when not in use.
Red alarm light flashes and
beeper sounds to indicate that
an abnormal system event has
occurred. Pressing the Menu
Switch displays the alarm
message on the LCD.
Rear-mounted 3/4" vacuum
connection extends vertically,
requiring less space.
Vacuum control valve maintains setpoint vacuum level to
speed the freeze dry process.
Rear-mounted electrical
receptacle allows connection of
the vacuum pump (pump sold
separately).
Rear-mounted RS-232 port
may be used to transmit data
to a user-supplied computer.
The time between data transmissions may be set to occur at
10, 30, 60, 300 or 600 second
intervals.
Compact console cabinet.
Cabinet, mounted on 3"
diameter casters, is epoxycoated steel with a removable
brushed stainless steel front
panel. The interior accommodates a vacuum pump (sold
separately).
Easy-to-follow operating
instructions are printed on the
right-hand side.
Factory wired. All models
include a 3-wire cord with
20 amp NEMA plug.
ETL listed. Models for operation on 115 volts, 60 Hz or 230
volts, 60 Hz carry the ETL mark
signifying they are certified to
UL and CAN/CSA standards for
laboratory equipment.
CE marking. All 230 volt,
50 Hz models conform to the
CE (European Community)
directives.
Exclusive feature
16
Vacuum break valve protects
the system from oil backstreaming by bleeding air into
the system when power to the
freeze dryer or vacuum pump
is shut off. If a brief power
outage occurs (approximately
5 minutes), the freeze dryer
will restart and the refrigeration and vacuum system will
resume operation once power
is restored. If the power failure
is long (approximately 5 minutes) and the collector warms
above safe limits, the freeze
dryer will not automatically
restart, which prevents melted
sample from being drawn into
the collector and liquid from
harming the vacuum pump.
FreeZone 4.5 Liter Freeze Dry Systems
®
specifications
All models feature:
• Upright stainless steel collector coil capable of removing 2 liters of
water in 24 hours and holding 4.5 liters of ice before defrosting.*
• 1/3 hp HCFC/CFC-free refrigeration system to cool collector to
-50° C (-58° F). For aqueous samples. Not for use with samples containing acetonitrile, methanol or ethanol.
• Permanently-installed 10-port stainless steel drying chamber with
1/2" thick, clear acrylic lid with neoprene gasket.
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• LCD that displays system operating parameters, set-up parameters
and alarm messages. It may be user-configured to display vacuum in
mBar, Pa or Torr and temperature in ° F or ° C. It also displays total
number of hours of refrigeration system operation and time since the
refrigeration system was serviced and the total number of hours of
vacuum pump operation and time since the vacuum pump was serviced (in hours).
• Red alarm light that flashes and beeper that sounds to indicate that an
abnormal system event has occurred, including: power failure, improper
line voltage supply, collector temperature rise above -40° C, service vacuum pump (after 1000 hours of vacuum use), and moisture in collector.
Pressing the Menu Switch displays the alarm message on the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of
relative system vacuum and collector temperature.
• Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
• Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off. If a power outage less
than approximately 5 minutes occurs, the freeze dryer will restart
and the refrigeration and vacuum system will resume operation once
power is restored. If the power failure is more than approximately
5 minutes and the collector warms above safe limits, the freeze dryer
will not automatically restart.
• Rear-mounted RS-232 port to transmit data to a user-supplied computer. Transmission intervals may be user-configured for 10, 30, 60,
300 or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Side-mounted, retractable, 9" collector drain hose.
• Side-mounted power switch, rear-mounted electrical receptacle
(for vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3" diameter casters.
• 3/4" OD vacuum connection, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 18.6" w x 24.0" d x 48.1" h (47.2 cm x 61.0 cm x 122.2 cm).
• Usable interior space: 14.0" w x 18.5" d x 21.0" h (35.6 cm x 47.0 cm x 53.3 cm).
FreeZone 4.5 Liter Freeze Dry System 7751020.
All models require (not included):
• Vacuum pump with a displacement of at least 86 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
See ordering information on page 34.
Models conform to the following standards:
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
Options include:
• Teflon-coated collector coil and chamber for processes involving
corrosive compounds.
• Domestic or international electrical configuration.
*Freeze drying capacity rating will be lower for samples other than plain water.
Exclusive feature
17
FreeZone Plus 4.5 Liter Cascade Benchtop Freeze Dry Systems
®
™
features
Moisture sensor protects the
vacuum pump by preventing
refrigeration or vacuum startup when moisture is detected
in the collector chamber area.
Rear-mounted 3/4" vacuum
connection extends vertically,
requiring less space.
&
benefits
12-Port Drying Chamber
7522800 is included. No
additional drying accessory
is required. Alternate drying
accessories may be purchased
separately.
Automatic start-up is quick and
easy to use. Pressing one button
initiates the collector cool-down
and vacuum pull-down sequence.
Or, manually override this feature
at any time using the separate
switches for manual refrigeration
and vacuum.
Rear-mounted RS-232 port
may be used to transmit data
to a user-supplied computer.
The time between data transmissions may be set to occur at
10, 30, 60, 300 or 600 second
intervals.
LCD displays system set-up
and operating parameters and
alarm messages.
Easy-to-follow operating
instructions are printed on the
right hand side.
Vacuum and temperature
graphs display relative system
vacuum and collector temperature. Amber LED “waves”
illuminate when vacuum and
temperature levels are out of
range for adding samples. Green
LED lights indicate that conditions are right to add samples.
Rear-mounted electrical
receptacle allows connection of
the vacuum pump (pump sold
separately).
Collector drain hose is accessible from the right-hand side for
convenient disposal of defrosted
material. It extends about nine
inches and retracts within the
cabinet when not in use.
Red alarm light flashes and
beeper sounds to indicate that
an abnormal system event
has occurred. Pressing the
Menu Switch displays the
alarm message on the LCD.
Benchtop cabinet has small
footprint. Compact cabinet
of durable epoxy-coated steel
with brushed stainless steel
front panel and four rubber
feet fits easily atop a countertop or laboratory cart.
Vacuum break valve protects
the system from oil backstreaming by bleeding air into
the system when power to the
freeze dryer or vacuum pump
is shut off. If a brief power
outage occurs (approximately
5 minutes), the freeze dryer
will restart and the refrigeration and vacuum system will
resume operation once power
is restored. If the power failure
is long (approximately 5 minutes) and the collector warms
above safe limits, the freeze
dryer will not automatically
restart, which prevents melted
sample from being drawn into
the collector and liquid from
harming the vacuum pump.
Upright, stainless steel collector
chamber speeds and simplifies defrost. Hot water may be
poured into the chamber, or
collected ice may be allowed
to melt overnight. Models are
available with Teflon-coated
collector chamber and coils for
additional corrosion resistance.
HCFC/CFC-free refrigeration
system ensures rapid,
environmentally-safe cooling.
Two condensing modules, used
in series, cool the collector coil
to -84° C (-119° F), ideal for
freeze drying samples with low
eutectic points including acetonitrile. The systems use a
non-flammable refrigerant that
contains no ozone-damaging
hydrochlorofluorocarbon (HCFCs)
or chlorofluorocarbons (CFCs).
ETL listed. Models for operation on 115 volts, 60 Hz or 230
volts, 60 Hz carry the ETL mark
signifying they are certified to
UL and CAN/CSA standards for
laboratory equipment.
CE marking. All 230 volt,
50 Hz models conform to the
CE (European Community)
directives.
Factory wired. All models
include a 3-wire cord with
20 amp NEMA plug.
Vacuum control valve maintains setpoint vacuum level to
speed the freeze dry process.
Exclusive feature
18
FreeZone Plus 4.5 Liter Cascade Benchtop Freeze Dry Systems
®
™
specifications
All models feature:
• Upright stainless steel collector coil capable of removing 4 liters of
water in 24 hours and holding 4.5 liters of ice before defrosting.*
•Dual 1/3 hp HCFC/CFC-free refrigeration systems to cool collector
to -84° C (-119° F). For samples containing water or acetonitrile.
Not for use with samples containing methanol or ethanol.
• 12-Port Drying Chamber 7522800 included (requires attachment).
• Compact benchtop design with a small footprint.
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• LCD that displays system operating parameters, set-up parameters
and alarm messages. It may be user-configured to display vacuum in
mBar, Pa or Torr and temperature in ° F or ° C. It also displays total
number of hours of refrigeration system operation and time since
the refrigeration system was serviced and the total number of hours
of vacuum pump operation and time since the vacuum pump was
serviced (in hours).
• Red alarm light that flashes and beeper that sounds to indicate that
an abnormal system event has occurred, including: power failure,
improper line voltage supply, collector temperature rise above -40° C,
service vacuum pump (after 1000 hours of vacuum use), and moisture
in collector. Pressing the Menu Switch displays the alarm message on
the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of
relative system vacuum and collector temperature.
• Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
• Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off.
• Rear-mounted RS-232 port to transmit data to a user-supplied
computer. Transmission intervals may be user-configured for 10, 30,
60, 300 or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Side-mounted, retractable, 9" collector drain hose.
• Clear acrylic lid, 3/4" thick, with 3" diameter port for connection of
drying chamber (included).
• Side-mounted power switch, rear-mounted electrical receptacle (for
vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3/4" OD vacuum connection, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 22.5" w x 24.2" d x 15.0" h (without drying
chamber) (57.2 cm x 61.5 cm x 38.1 cm).
• Overall dimensions: 22.5" w x 24.2" d x 25.4" h (with drying
chamber) (57.2 cm x 61.5 cm x 64.5 cm).
FreeZone Plus 4.5 Liter Cascade Benchtop Freeze Dry System 7386020.
All models require (not included):
• Vacuum pump with a displacement of at least 86 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
See ordering information on page 35.
Models conform to the following standards:
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
Options include:
• Teflon-coated collector coil and chamber for processes involving
corrosive compounds.
• Domestic or international electrical configuration.
*Freeze drying capacity rating will be lower for samples other than plain water.
Exclusive feature
19
FreeZone Plus 4.5 Liter Cascade Freeze Dry Systems
®
™
features
Moisture sensor protects the
vacuum pump by preventing
refrigeration or vacuum start-up
when moisture is detected in
the collector chamber area.
Rear-mounted 3/4" vacuum
connection extends vertically,
requiring less space.
&
benefits
12-Port Drying Chamber
7522800 is included. No
additional drying accessory
is required. Alternate drying
accessories may be purchased
separately.
Automatic start-up is quick and
easy to use. Pressing one button
initiates the collector cool-down
and vacuum pull-down sequence.
Or, manually override this feature
at any time using the separate
switches for manual refrigeration
and vacuum.
Upright, stainless steel collector
chamber speeds and simplifies defrost. Hot water may be
poured into the chamber, or
collected ice may be allowed
to melt overnight. Models are
available with Teflon-coated
collector chamber and coils for
additional corrosion resistance.
Rear-mounted electrical
receptacle allows connection of
the vacuum pump (pump sold
separately).
Vacuum and temperature
graphs display relative system
vacuum and collector temperature. Amber LED “waves”
illuminate when vacuum and
temperature levels are out of
range for adding samples. Green
LED lights indicate that conditions are right to add samples.
Collector drain hose is accessible from the right-hand side for
convenient disposal of defrosted
material. It extends about nine
inches and retracts within the
cabinet when not in use.
Red alarm light flashes and
beeper sounds to indicate that
an abnormal system event
has occurred. Pressing the
Menu Switch displays the
alarm message on the LCD.
Compact console cabinet.
Cabinet, mounted on 3"
diameter casters, is epoxycoated steel with removable
brushed stainless steel front
panel. The interior accommodates a vacuum pump (pump
sold separately.)
HCFC/CFC-free refrigeration
system ensures rapid,
environmentally-safe cooling.
Two condensing modules, used
in series, cool the collector coil
to -84° C (-119° F), ideal for
freeze drying samples with low
eutectic points including acetonitrile. The systems use a
non-flammable refrigerant that
contains no ozone-damaging
hydrochlorofluorocarbon (HCFCs)
or chlorofluorocarbons (CFCs).
LCD displays system set-up
and operating parameters and
alarm messages.
Easy-to-follow operating
instructions are printed on the
right hand side.
Vacuum break valve protects
the system from oil backstreaming by bleeding air into
the system when power to the
freeze dryer or vacuum pump
is shut off. If a brief power
outage occurs (approximately
5 minutes), the freeze dryer
will restart and the refrigeration and vacuum system will
resume operation once power
is restored. If the power failure
is long (approximately 5 minutes) and the collector warms
above safe limits, the freeze
dryer will not automatically
restart, which prevents melted
sample from being drawn into
the collector and liquid from
harming the vacuum pump.
Rear-mounted RS-232 port
may be used to transmit data
to a user-supplied computer.
The time between data transmissions may be set to occur at
10, 30, 60, 300 or 600 second
intervals.
ETL listed. Models for operation on 115 volts, 60 Hz or 230
volts, 60 Hz carry the ETL mark
signifying they are certified to
UL and CAN/CSA standards for
laboratory equipment.
CE marking. All 230 volt,
50 Hz models conform to the
CE (European Community)
directives.
Factory wired. All models
include a 3-wire cord with
20 amp NEMA plug.
Vacuum control valve maintains setpoint vacuum level to
speed the freeze dry process.
Exclusive feature
20
FreeZone Plus 4.5 Liter Cascade Freeze Dry Systems
®
™
specifications
All models feature:
• Upright stainless steel collector capable of removing 4 liters of water in
24 hours and holding 4.5 liters of ice before defrosting.*
•Dual 1/3 hp CFC-free refrigeration systems to cool collector
to -84° C (-119° F). For samples containing water or acetonitrile.
Not for use with samples containing methanol or ethanol.
• 12-Port Drying Chamber 7522800 included (requires attachment).
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• LCD that displays system operating parameters, set-up parameters
and alarm messages. It may be user-configured to display vacuum in
mBar, Pa or Torr and temperature in ° F or ° C. It also displays total
number of hours of refrigeration system operation and time since
the refrigeration system was serviced and the total number of hours
of vacuum pump operation and time since the vacuum pump was
serviced (in hours).
• Red alarm light that flashes and beeper that sounds to indicate that an
abnormal system event has occurred, including: power failure, improper
line voltage supply, collector temperature rise above -40° C, service vacuum pump (after 1000 hours of vacuum use), and moisture in collector.
Pressing the Menu Switch displays the alarm message on the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of
relative system vacuum and collector temperature.
• Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
• Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off. If a power outage less
than approximately 5 minutes occurs, the freeze dryer will restart
and the refrigeration and vacuum system will resume operation once
power is restored. If the power failure is more than approximately
5 minutes and the collector warms above safe limits, the freeze dryer
will not automatically restart.
• Rear-mounted RS-232 port to transmit data to a user-supplied
computer. Transmission intervals may be user-configured for 10, 30,
60, 300 or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Side-mounted, retractable, 9" collector drain hose.
• Clear acrylic lid, 3/4" thick, with 3" diameter port for connection of
drying chamber (included).
• Side-mounted power switch, rear-mounted electrical receptacle
(for vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3" diameter casters.
• 3/4" OD vacuum connection, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 22.5" w x 24.2" d x 36.5" h (without drying
chamber) (57.2 cm x 61.5 cm x 92.7 cm).
• Overall dimensions: 22.5" w x 24.2" d x 46.9" h (with drying chamber) (57.2 cm x 61.5 cm x 119.1 cm).
FreeZone Plus 4.5 Liter Cascade Freeze Dry System 7387020.
Options include:
• Teflon-coated collector coil and chamber for processes involving
corrosive compounds.
• Domestic or international electrical configuration.
All models require (not included):
• Vacuum pump with a displacement of at least 86 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
See ordering information on page 35.
Models conform to the following standards:
• UL Standard 61010A-1 (60 Hz models).
• CAN/CSA C22.2 No. 1010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
*Freeze drying capacity rating will be lower for samples other than plain water.
Exclusive feature
21
FreeZone -105° C 4.5 Liter Benchtop Freeze Dry Systems
®
features
Moisture sensor protects the
vacuum pump by preventing
refrigeration or vacuum startup when moisture is detected
in the collector chamber area.
Rear-mounted 3/4" vacuum
connection extends vertically,
requiring less space.
&
benefits
12-Port Drying Chamber
7522800 is included. No
additional drying accessory
is required. Alternate drying
accessories may be purchased
separately.
Automatic start-up is quick and
easy to use. Pressing one button
initiates the collector cool-down
and vacuum pull-down sequence.
Or, manually override this feature
at any time using the separate
switches for manual refrigeration
and vacuum.
Rear-mounted RS-232 port
may be used to transmit data
to a user-supplied computer.
The time between data transmissions may be set to occur at
10, 30, 60, 300 or 600 second
intervals.
LCD displays system set-up
and operating parameters and
alarm messages.
Easy-to-follow operating
instructions are printed on the
right hand side.
Vacuum and temperature
graphs display relative system
vacuum and collector temperature. Amber LED “waves”
illuminate when vacuum and
temperature levels are out of
range for adding samples. Green
LED lights indicate that conditions are right to add samples.
Rear-mounted electrical
receptacle allows connection of
the vacuum pump (pump sold
separately).
Collector drain hose is accessible from the right-hand side for
convenient disposal of defrosted
material. It extends about nine
inches and retracts within the
cabinet when not in use.
Red alarm light flashes and
beeper sounds to indicate that
an abnormal system event
has occurred. Pressing the
Menu Switch displays the
alarm message on the LCD.
Benchtop cabinet has small
footprint. Compact cabinet
of durable epoxy-coated steel
with brushed stainless steel
front panel and four rubber
feet fits easily atop a countertop or laboratory cart.
Vacuum break valve protects
the system from oil backstreaming by bleeding air into
the system when power to the
freeze dryer or vacuum pump
is shut off. If a brief power
outage occurs (approximately
5 minutes), the freeze dryer
will restart and the refrigeration and vacuum system will
resume operation once power
is restored. If the power failure
is long (approximately 5 minutes) and the collector warms
above safe limits, the freeze
dryer will not automatically
restart, which prevents melted
sample from being drawn into
the collector and liquid from
harming the vacuum pump.
Upright, stainless steel collector
chamber speeds and simplifies defrost. Hot water may be
poured into the chamber, or
collected ice may be allowed
to melt overnight. Models are
available with Teflon-coated
collector chamber and coils for
additional corrosion resistance.
HCFC/CFC-free refrigeration
system ensures rapid,
environmentally-safe cooling.
Two condensing modules, used
in series, cool the collector coil
to -105° C (-157° F), ideal for
freeze drying samples with very
low eutectic points, including
ones containing dilute methanol
or ethanol. The systems use
a refrigerant that contains no
ozone-damaging hydrochlorofluorocarbons (HCFCs) or
chlorofluorocarbons (CFCs).
ETL listed. Models for operation on 115 volts, 60 Hz or 230
volts, 60 Hz carry the ETL mark
signifying they are certified to
UL and CAN/CSA standards for
laboratory equipment.
CE marking. All 230 volt,
50 Hz models conform to the
CE (European Community)
directives.
Vacuum control valve maintains setpoint vacuum level to
speed the freeze dry process.
22
Factory wired. All models
include a 3-wire cord with
20 amp NEMA plug.
Exclusive feature
FreeZone -105° C 4.5 Liter Cascade Benchtop Freeze Dry Systems
®
specifications
All models feature:
• Upright stainless steel collector coil capable of removing 2.5 liters of
water in 24 hours and holding 4.5 liters of ice before defrosting.*
•Dual 1/3 hp HCFC/CFC-free refrigeration systems to cool collector
to -105° C (-157° F). For samples containing water, acetonitrile or
dilute methanol or ethanol.
• 12-Port Drying Chamber 7522800 included (requires attachment).
• Compact benchtop design with a small footprint.
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• LCD that displays system operating parameters, set-up parameters
and alarm messages. It may be user-configured to display vacuum in
mBar, Pa or Torr and temperature in ° F or ° C. It also displays total
number of hours of refrigeration system operation and time since
the refrigeration system was serviced and the total number of hours
of vacuum pump operation and time since the vacuum pump was
serviced (in hours).
• Red alarm light that flashes and beeper that sounds to indicate that
an abnormal system event has occurred, including: power failure,
improper line voltage supply, collector temperature rise above -40° C,
service vacuum pump (after 1000 hours of vacuum use), and moisture
in collector. Pressing the Menu Switch displays the alarm message on
the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of
relative system vacuum and collector temperature.
• Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
• Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off.
• Rear-mounted RS-232 port to transmit data to a user-supplied
computer. Transmission intervals may be user-configured for 10, 30,
60, 300 or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Side-mounted, retractable, 9" collector drain hose.
• Clear acrylic lid, 3/4" thick, with 3" diameter port for connection of
drying chamber (included).
• Side-mounted power switch, rear-mounted electrical receptacle
(for vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3/4" OD vacuum connection, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 23.2" w x 25.2" d x 16.0" h (without drying
chamber) (58.7 cm x 64.0 cm x 40.6 cm).
• Overall dimensions: 23.2" w x 25.2" d x 26.4" h (with drying chamber) (58.7 cm x 64.0 cm x 67.1 cm).
FreeZone -105° C 4.5 Liter Cascade Benchtop Freeze Dry System 7382020.
All models require (not included):
• Vacuum pump with a displacement of at least 86 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63
See ordering information on page 35.
Models conform to the following standards:
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
Options include:
• Teflon-coated collector coil and chamber for processes involving
corrosive compounds.
• Domestic or international electrical configuration.
*Freeze drying capacity rating will be lower for samples other than plain water.
Exclusive feature
23
FreeZone 6 Liter Benchtop Freeze Dry Systems
®
Features
Durable benchtop cabinet.
Cabinet is epoxy-coated steel
with a brushed stainless steel
front panel and four rubber
feet and fits easily atop a countertop or laboratory cart.
Automatic start-up is quick and
easy to use. Pressing one button
initiates the collector cool-down
and vacuum pull-down sequence.
Or, manually override this
feature at any time using the
separate switches for manual
refrigeration and vacuum.
&
benefits
Upright, stainless steel collector
chamber speeds and simplifies defrost. Hot water may be
poured into the chamber, or
collected ice may be allowed
to melt overnight. Models are
available with Teflon-coated
collector coil and chamber for
additional corrosion resistance.
Rear-mounted 3/4" vacuum
connection extends parallel to
the back requiring less space.
Attachment port makes
connection of accessories easy.
Select from accessory drying chambers and manifolds
(sold separately).
HCFC/CFC-free refrigeration
system ensures rapid,
environmentally-safe cooling.
The condensing module cools
the collector coil to -50° C
(-58° F), ideal for freeze drying
aqueous samples. The system
uses a non-flammable refrigerant
that contains no ozone-damaging
hydrochlorofluorocarbon (HCFCs)
or chlorofluorocarbons (CFCs).
Easy-to-follow operating
instructions are printed on the
right-hand side.
Moisture sensor protects the
vacuum pump by preventing
refrigeration or vacuum startup when moisture is detected
in the collector chamber area.
Vacuum and temperature
graphs display relative system
vacuum and collector temperature. Amber LED “waves”
illuminate when vacuum and
temperature levels are out of
range for adding samples. Green
LED lights indicate that conditions are right to add samples.
Collector drain hose is accessible
from the right-hand side for convenient defrost. It extends about
nine inches and retracts within
the cabinet when not in use.
Vacuum control valve maintains setpoint vacuum level to
speed the freeze drying process.
ETL listed. Models for operation on 115 volts, 60 Hz or 230
volts, 60 Hz carry the ETL mark
signifying they are certified to
UL and CAN/CSA standards for
laboratory equipment.
Vacuum break valve protects
the system from oil backstreaming by bleeding air into
the system when power to the
freeze dryer or vacuum pump
is shut off. If a brief power
outage occurs (approximately
5 minutes), the freeze dryer
will restart and the refrigeration and vacuum system will
resume operation once power
is restored. If the power failure
is long (approximately 5 minutes) and the collector warms
above safe limits, the freeze
dryer will not automatically
restart, which prevents melted
sample from being drawn into
the collector and liquid from
harming the vacuum pump.
LCD displays system set-up
and operating parameters and
alarm messages.
Rear-mounted RS-232 port
may be used to transmit data
to a user-supplied computer.
The time between data transmissions may be set to occur at
10, 30, 60 300 or 600 second
intervals.
CE marking. All 230 volt,
50 Hz models conform to the
CE (European Community)
directives.
Red alarm light flashes and
beeper sounds to indicate that
an abnormal system event has
occurred. Pressing the Menu
Switch displays the alarm
message on the LCD.
Factory wired. All models
include a 3-wire cord with
20 amp NEMA plug.
Rear-mounted electrical
receptacle allows connection
of the vacuum pump (pump
sold separately).
Exclusive feature
24
FreeZone 6 Liter Benchtop Freeze Dry Systems
®
specifications
All models feature:
• Upright stainless steel collector coil capable of removing 4 liters of
water in 24 hours and holding 6 liters of ice before defrosting.*
• 3/4 hp HCFC/CFC-free refrigeration system to cool collector to -50° C (-58° F). For aqueous samples. Not for use with samples containing acetonitrile, methanol or ethanol.
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• LCD that displays system operating parameters, set-up parameters
and alarm messages. It may be user-configured to display vacuum in
mBar, Pa or Torr and temperature in ° F or ° C. It also displays total
number of hours of refrigeration system operation and time since the
refrigeration system was serviced and the total number of hours of
vacuum pump operation and time since the vacuum pump was serviced (in hours).
• Red alarm light that flashes and beeper that sounds to indicate that an
abnormal system event has occurred, including: power failure, improper
line voltage supply, collector temperature rise above -40° C, service vacuum pump (after 1000 hours of vacuum use), and moisture in collector.
Pressing the Menu Switch displays the alarm message on the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of
relative system vacuum and collector temperature.
• Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
• Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off. If a power outage less
than approximately 5 minutes occurs, the freeze dryer will restart
and the refrigeration and vacuum system will resume operation once
power is restored. If the power failure is more than approximately
5 minutes and the collector warms above safe limits, the freeze dryer
will not automatically restart.
• Rear-mounted RS-232 port to transmit data to a user-supplied
computer. Transmission intervals may be user-configured for 10, 30,
60, 300 or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Side-mounted, retractable, 9" collector drain hose.
• 3" diameter port for connection of drying accessories (sold separately).
• Side-mounted power switch, rear-mounted electrical receptacle (for
vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3/4" OD vacuum connection, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 31.8" w x 28.1" d x 14.5" h (80.8 cm x 71.4 cm x 36.8 cm).
FreeZone 6 Liter Benchtop Freeze Dry System 7752020, Variable Height Bench 8075000,
20-Port Manifold with Support Shelves 7522500 and miscellaneous glassware.
All models require (not included):
• Vacuum pump with a displacement of at least 98 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Drying accessory (except models with Stoppering Tray Dryer).
See pages 46-54.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
See ordering information on page 36.
Models conform to the following standards:
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
Options include:
• Teflon-coated collector coil and chamber for processes involving
corrosive compounds.
• Stoppering Tray Dryer, 32.0" w x 24.6" d x 27.1" h (81.3 cm x 62.4
cm x 68.8 cm). Overall dimensions with Stoppering Tray Dryer: 32.0"
w x 31.1" d x 40.6" h (81.3 cm x 79.0 cm x 103.1 cm). See specifications on pages 38-40.
• Domestic or international electrical configuration.
*Freeze drying capacity rating will be lower for samples other than plain water.
Exclusive feature
25
FreeZone 6, 12 & 18 Liter Freeze Dry Systems
®
Features
Optional built-in mini vacuum
drying chamber holds small
samples, either in bulk or in
small containers such as vials.
It is used in conjunction with
other drying accessories
mounted on the attachment
port. A separate drying accessory is required (sold separately).
Its 50-watt heater is microprocessor-controlled from the front
panel to +60° C (+140° F). (The
chamber is not cooled. The only
cooling is from the frozen sample.)
&
Rear-mounted electrical
receptacle allows connection
of the vacuum pump (pump
sold separately).
benefits
Attachment port makes
connection of accessories easy.
Select from accessory drying
chambers and manifolds
(sold separately).
Vacuum and temperature
graphs display relative system
vacuum and collector temperature. Amber LED “waves”
illuminate when vacuum and
temperature levels are out of
range for adding samples. Green
LED lights indicate that conditions are right to add samples.
LCD displays system set-up
and operating parameters and
alarm messages.
Red alarm light flashes and
beeper sounds to indicate that
an abnormal system event has
occurred. Pressing the Menu
Switch displays the alarm
message on the LCD.
Easy-to-follow operating
instructions are printed on the
left-hand side.
Automatic start-up is quick
and easy to use. Pressing one
button initiates the collector
cool-down and vacuum pulldown sequence. Or, manually
override this feature at any time
using the separate switches
for manual refrigeration
and vacuum.
Collector drain hose is accessible
from the front for convenient
defrost. It extends about nine
inches and retracts within the
cabinet when not in use.
CE marking. All 230 volt,
50 Hz models conform to the
CE (European Community)
directives.
Moisture sensor protects the
vacuum pump by preventing
refrigeration or vacuum startup when moisture is detected
in the collector chamber area.
HCFC/CFC-free refrigeration
system ensures rapid,
environmentally-safe cooling.
The condensing module cools the
collector coil to -50° C (-58° F),
ideal for freeze drying aqueous
samples. The system uses a
non-flammable refrigerant that
contains no ozone-damaging
hydrochlorofluorocarbons (HCFCs)
or chlorofluorocarbons (CFCs).
Optional built-in shell freezer
(6 liter models only) permits
sample preparation while other
samples lyophilize. The bath has
two rollers to rotate flasks up to
1200 ml in size in heat transfer
solution. The bath’s separate
CFC-free refrigeration system
ensures rapid pre-freezing.
A drain hose is accessible from
the front for easy disposal of the
heat transfer solution.
Factory wired. All models
include a 3-wire cord with
20 amp NEMA plug.
ETL listed. Models for operation on 115 volts, 60 Hz or 230
volts, 60 Hz carry the ETL mark
signifying they are certified to
UL and CAN/CSA standards for
laboratory equipment.
Exclusive feature
Upright, stainless steel collector
chamber speeds and simplifies
defrost. Models are available
with Teflon-coated collector
coil and chamber for additional
corrosion resistance.
Rear-mounted RS-232 port
may be used to transmit data
to a user-supplied computer.
The time between data transmissions may be set to occur at
10, 30, 60, 300 or 600 second
intervals.
Optional purge valve isolates
the vacuum pump from the
freeze dry system. The pump
starts and warms the oil, while
the collector cools, before pulling vacuum on the system.
Pump life may be extended
by purging small amounts of
contaminants from the vacuum
pump oil. Green indicator lights
when the purge valve is closed.
Hot gas defrost. Hot gas from the
compressor is circulated through
the collector coil and automatically shuts off when the refrigerant reaches +65° C (+149° F).
26
Durable console cabinet. Cabinet,
mounted on 3" diameter casters,
is epoxy-coated steel with a
removable brushed stainless steel
front panel. The roomy interior
accommodates a vacuum pump
(pump sold separately).
Vacuum control valve maintains setpoint vacuum level to
speed the freeze drying process.
Vacuum break valve protects
the system from oil backstreaming by bleeding air into the
system when power to the
freeze dryer or vacuum pump
is shut off. If a brief power
outage occurs (approximately
5 minutes), the freeze dryer
will restart and the refrigeration and vacuum system will
resume operation once power is
restored. If the power failure is
long (approximately 5 minutes)
and the collector warms above
safe limits, the freeze dryer will
not automatically restart, which
prevents melted sample from
being drawn into the collector
and liquid from harming the
vacuum pump.
FreeZone 6 Liter Freeze Dry Systems
®
specifications
All models feature:
• Upright stainless steel collector coil capable of removing 4 liters of
water in 24 hours and holding 6 liters of ice before defrosting.*
• 3/4 hp HCFC/CFC-free refrigeration system to cool collector to -50° C (-58° F). For aqueous samples. Not for use with samples containing acetonitrile, methanol or ethanol.
• Clear acrylic chamber lid, 3/4" thick, with neoprene gasket.
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• LCD that displays system operating parameters, set-up parameters and
alarm messages. It may be user-configured to display vacuum in mBar,
Pa or Torr and temperature in ° F or ° C. It also displays total number of
hours of refrigeration system operation and time since the refrigeration
system was serviced and the total number of hours of vacuum pump
operation and time since the vacuum pump was serviced (in hours).
• Red alarm light that flashes and beeper that sounds to indicate that
an abnormal system event has occurred, including: power failure,
improper line voltage supply, collector temperature rise above -40° C,
service vacuum pump (after 1000 hours of vacuum use), and moisture in collector. Pressing the Menu Switch displays the alarm message
on the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of
relative system vacuum and collector temperature.
• Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
• Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off. If a power outage less
than approximately 5 minutes occurs, the freeze dryer will restart
and the refrigeration and vacuum system will resume operation once
power is restored. If the power failure is more than approximately
5 minutes and the collector warms above safe limits, the freeze dryer
will not automatically restart.
• Rear-mounted RS-232 port to transmit data to a user-supplied computer. Transmission intervals may be user-configured for 10, 30, 60,
300 or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Hot gas defrost and switch.
• Front-mounted, retractable, 9" collector drain hose.
• 3" diameter stainless steel port for connection of drying accessories
(sold separately).
• Side-mounted power switch, rear-mounted electrical receptacle (for
vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3” diameter casters.
• 3/4" OD vacuum connection, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 32.2" w x 28.0” d x 36.3" h
(81.8 cm x 71.1 cm x 92.1 cm).
• Usable interior space: 15.0" w x 24.5" d x 22.0" h (38.1 cm x 62.2
cm x 55.9 cm). Usable interior space on models with built-in shell
freezer: 11.5” w x 24.5” d x 12.0” h (29.2 cm x 62.2 cm x 30.5 cm).
FreeZone 6 Liter Freeze Dry System with built-in shell freezer 7753522, 16-Port Drying
Chamber 7522900 and miscellaneous glassware.
Options include:
• Teflon-coated collector coil and chamber for processes involving
corrosive compounds.
• Purge valve with switch for isolating the vacuum pump from the
freeze dry system.
• Built-in stainless steel mini vacuum drying chamber, 5.1" w x 13.0" d x
2.5" h (12.9 cm x 33.0 cm x 6.4 cm), that includes 50-watt heater with
microprocessor control to +60° C (+140° F), 3/4" thick clear acrylic lid
and neoprene gasket. (Chamber is not cooled. The only cooling is from
the frozen sample.)
• Built-in shell freezer with stainless steel bath, 5.5" w x 12.5" d x 7.5"
h (30.5 cm x 14.0 cm x 19.0 cm), that includes 1/3 hp CFC-free refrigeration system with microprocessor control to -40° C (-40° F), 3/4"
thick high-density polyethylene lid, neoprene gasket and drain hose.
• Stoppering Tray Dryer, 32.0" w x 24.6" d x 27.1" h (81.3 cm x
62.4 cm x 68.8 cm). Overall dimensions with Stoppering Tray Dryer:
32.0" w x 31.0" d x 63.4" h (81.3 cm x 78.7 cm x 160.9 cm). See
specifications on pages 46-48.
• Domestic or international electrical configuration.
All models require (not included):
• Vacuum pump with a displacement of at least 98 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Drying accessory (except for models with Stoppering Tray Dryer).
See pages 46-54.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
Models conform to the following standards:
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
See ordering information on pages 37-38.
Exclusive feature
*Freeze drying capacity rating will be lower for samples other than plain water.
27
FreeZone 12 Liter Freeze Dry Systems
®
specifications
All models feature:
• Upright stainless steel collector coil capable of removing 8 liters of
water in 24 hours and holding 12 liters of ice before defrosting.*
• 1 hp HCFC/CFC-free refrigeration system to cool collector to -50° C (-58° F). For aqueous samples. Not for use with samples
containing acetonitrile, methanol or ethanol.
• Clear acrylic chamber lid, 3/4" thick, with neoprene gasket.
• Brushed stainless steel and glacier white epoxy-coated steel exterior
with blue accents.
• LCD that displays system operating parameters, set-up parameters
and alarm messages. It may be user-configured to display vacuum in
mBar, Pa or Torr and temperature in ° F or ° C. It also displays total
number of hours of refrigeration system operation and time since
the refrigeration system was serviced and the total number of hours
of vacuum pump operation and time since the vacuum pump was
serviced (in hours).
• Red alarm light that flashes and beeper that sounds to indicate that
an abnormal system event has occurred, including: power failure,
improper line voltage supply, collector temperature rise above -40° C,
service vacuum pump (after 1000 hours of vacuum use), and moisture in collector. Pressing the Menu Switch displays the alarm message
on the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of
relative system vacuum and collector temperature.
• Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
• Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off. If a power outage less
than approximately 5 minutes occurs, the freeze dryer will restart
and the refrigeration and vacuum system will resume operation once
power is restored. If the power failure is more than approximately
5 minutes and the collector warms above safe limits, the freeze dryer
will not automatically restart.
• Rear-mounted RS-232 port to transmit data to a user-supplied computer. Transmission intervals may be user-configured for 10, 30, 60,
300 or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Hot gas defrost and switch.
• Front-mounted, retractable, 9" collector drain hose.
• 3" diameter stainless steel port for connection of drying accessories
(sold separately).
• Side-mounted power switch, rear-mounted electrical receptacle (for
vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3" diameter casters.
• 3/4" OD vacuum connection, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 32.2" w x 28.0" d x 36.3" h
(84.8 cm x 71.1 cm x 92.1 cm).
• Usable interior space: 14.0" w x 24.5" d x 22.0" h
(35.6 cm x 62.2 cm x 55.9 cm).
FreeZone 12 Liter Freeze Dry System with Stoppering Tray Dryer 7759040 and
Serum Bottles 7573210.
Options include:
• Teflon-coated collector coil and chamber for processes involving
corrosive compounds.
• Purge valve with switch for isolating the vacuum pump from the
freeze dry system.
• Built-in stainless steel mini vacuum drying chamber, 5.1" w x 13.0" d
x 2.5" h (12.9 cm x 33.0 cm x 6.4 cm), that includes 50-watt heater
with microprocessor control to +60° C (+140° F), 3/4" thick clear
acrylic lid and neoprene gasket. (Chamber is not cooled. The only
cooling is from the frozen sample.)
• Stoppering Tray Dryer, 32.0" w x 24.6" d x 27.1" h (81.3 cm x 62.4 cm
x 68.8 cm). Overall dimensions with Stoppering Tray Dryer: 32.0" w x
31.0" d x 63.4" h (81.3 cm x 78.7 cm x 160.9 cm). See specifications on
pages 46-48.
• Domestic or international electrical configuration.
All models require (not included):
• Vacuum pump with a displacement of at least 98 liters per minute,
0.002 mBar ultimate pressure, reverse IEC plug and fitting suitable for
3/4" ID vacuum hose. See pages 56-58.
• Drying accessory (except models with Stoppering Tray Dryer).
See pages 46-54.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
Models conform to the following standards:
• UL Standard 61010-1 (230 volts, 60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (230 volts, 60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
See ordering information on pages 39-40.
Exclusive feature
*Freeze drying capacity rating will be lower for samples other than plain water.
28
FreeZone 18 Liter Freeze Dry Systems
®
specifications
All models feature:
• Upright stainless steel collector coil capable of removing 10 liters of
water in 24 hours and holding 18 liters of ice before defrosting.*
• 1-1/2 hp HCFC/CFC-free refrigeration system to cool collector to -50° C (-58° F). For aqueous samples. Not for use with samples
containing acetonitrile, methanol or ethanol.
• Clear acrylic chamber lid, 3/4" thick, with neoprene gasket.
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• LCD that displays system operating parameters, set-up parameters
and alarm messages. It may be user-configured to display vacuum in
mBar, Pa or Torr and temperature in ° F or ° C. It also displays total
number of hours of refrigeration system operation and time since
the refrigeration system was serviced and the total number of hours
of vacuum pump operation and time since the vacuum pump was
serviced (in hours).
• Red alarm light that flashes and beeper that sounds to indicate that
an abnormal system event has occurred, including: power failure,
improper line voltage supply, collector temperature rise above -40° C,
service vacuum pump (after 1000 hours of vacuum use), and moisture
in collector. Pressing the Menu Switch displays the alarm message
on the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of
relative system vacuum and collector temperature.
• Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
• Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off. If a power outage less
than approximately 5 minutes occurs, the freeze dryer will restart
and the refrigeration and vacuum system will resume operation once
power is restored. If the power failure is more than approximately
5 minutes and the collector warms above safe limits, the freeze dryer
will not automatically restart.
• Rear-mounted RS-232 port to transmit data to a user-supplied computer. Transmission intervals may be user-configured for 10, 30, 60,
300 or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Hot gas defrost and switch.
• Front-mounted, retractable, 9" collector drain hose.
• 3" diameter stainless steel port for connection of drying accessories
(sold separately).
• Side-mounted power switch, rear-mounted electrical receptacle (for
vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3" diameter casters.
• 3/4" OD vacuum connection, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 32.2" w x 28.0" d x 36.3" h
(84.8 cm x 71.1 cm x 92.1 cm).
• Usable interior space: 14.0" w x 24.5" d x 22.0" h
(35.6 cm x 62.2 cm x 55.9 cm).
FreeZone 18 Liter Freeze Dry System 7755040, 48-Port Manifold 7868500 and
miscellaneous glassware.
Options include:
• Teflon-coated collector coil and chamber for processes involving
corrosive compounds.
• Purge valve with switch for isolating the vacuum pump from the
freeze dry system.
• Built-in stainless steel mini vacuum drying chamber, 5.1" w x
13.0" d x 2.5" h (12.9 cm x 33.0 cm x 6.4 cm), that includes 50-watt
heater with microprocessor control to +60° C (+140° F), 3/4" thick
clear acrylic lid and neoprene gasket. (Chamber is not cooled. The
only cooling is from the frozen sample.)
• Domestic or international electrical configuration.
All models require (not included):
• Vacuum pump with a displacement of at least 98 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Drying accessory. See pages 46-54.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
Models conform to the following standards:
See ordering information on page 41.
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
*Freeze drying capacity rating will be lower for samples other than plain water.
Exclusive feature
29
FreeZone Plus 6 & 12 Liter Cascade Freeze Dry Systems
®
™
Features
Optional built-in mini vacuum
drying chamber holds small samples, either in bulk or in small
containers such as vials. It is used
in conjunction with other drying
accessories mounted on the
attachment port. A separate drying accessory is required (sold
separately). Its 50-watt heater is
microprocessor- controlled from
the front panel to +60° C
(+140° F). (The chamber is not
cooled. The only cooling is from
the frozen sample.)
&
benefits
Attachment port makes
connection of accessories easy.
Select from accessory drying
chambers and manifolds
(sold separately).
LCD displays system set-up
and operating parameters and
alarm messages.
Vacuum and temperature
graphs display relative system
vacuum and collector temperature. Amber LED “waves”
illuminate when vacuum and
temperature levels are out of
range for adding samples. Green
LED lights indicate that conditions are right to add samples.
Easy-to-follow operating
instructions are printed on
the left-hand side.
Red alarm light flashes and
beeper sounds to indicate that
an abnormal system event has
occurred. Pressing the Menu
Switch displays the alarm
message on the LCD.
Automatic start-up is quick and
easy to use. Pressing one button
initiates the collector cool-down
and vacuum pull-down sequence.
Or, manually override this feature
at any time using the separate
switches for manual refrigeration
and vacuum.
Moisture sensor protects the
vacuum pump by preventing
refrigeration or vacuum startup when moisture is detected
in the collector chamber area.
Collector drain hose is accessible
from the front for convenient
defrost. It extends about 9 inches
and retracts within the cabinet
when not in use.
Factory wired. All models
require a 3-wire cord with
20 amp NEMA plug.
CE marking. All 230 volt,
50 Hz models conform to the
CE (European Community)
directives.
ETL listed. Models for operation on 115 volts, 60 Hz or 230
volts, 60 Hz carry the ETL mark
signifying they are certified to
UL and CAN/CSA standards for
laboratory equipment.
Upright, stainless steel collector
chamber speeds and simplifies
defrost. Models are available
with Teflon-coated collector
coil and chamber for additional
corrosion resistance.
Vacuum control valve maintains setpoint vacuum level to
speed the freeze drying process.
HCFC/CFC-free refrigeration
systems ensure rapid,
environmentally-safe cooling.
Two refrigeration systems, used
in series, cool the stainless steel
collector to -84° C (-119° F)
making this system ideal for
freeze drying samples with low
eutectic points including acetonitrile. The systems use a
non-flammable refrigerant that
contains no ozone-damaging
hydrochlorofluorocarbon (HCFCs)
or chlorofluorocarbons (CFCs).
Optional purge valve isolates
the vacuum pump from the
freeze dry system. The pump
starts and warms the oil, while
the collector cools, before pulling vacuum on the system.
Pump life may be extended
by purging small amounts of
contaminants from the vacuum
pump oil. Green indicator lights
when the purge valve is closed.
Durable console cabinet.
Cabinet, mounted on 3"
diameter casters, is epoxycoated steel with a removable
brushed stainless steel front
panel. The roomy interior
accommodates a vacuum pump
(pump sold separately).
Rear-mounted RS-232 port may
be used to transmit data to a
user-supplied computer. The
time between data transmissions
may be set to occur at 10, 30,
60, 300 or 600 second intervals.
Hot gas defrost. Hot gas from the
compressor is circulated through
the collector coil and automatically shuts off when the refrigerant reaches +65° C (+149° F).
Rear-mounted electrical
receptacle allows connection
of the vacuum pump
(pump sold separately).
Exclusive feature
30
Vacuum break valve protects the
system from oil backstreaming
by bleeding air into the system
when power to the freeze dryer
or vacuum pump is shut off.
If a brief power outage occurs
(approximately 5 minutes), the
freeze dryer will restart and the
refrigeration and vacuum system
will resume operation once
power is restored. If the power
failure is long (approximately 5
minutes) and the collector
warms above safe limits, the
freeze dryer will not automatically restart, which prevents
melted sample from being drawn
into the collector and liquid from
harming the vacuum pump.
Stainless steel baffle maximizes ice loading capabilities by
evenly distributing collected ice
over the entire collector coil.
FreeZone Plus 6 Liter Cascade Freeze Dry Systems
®
™
specifications
All models feature:
• Upright stainless steel collector coil and chamber with stainless steel
baffle capable of removing 4 liters of water in 24 hours and holding
6 liters of ice before defrosting.*
• Two 1/3 hp HCFC/CFC-free refrigeration systems, used in series, to
cool collector to -84° C (-119° F). For samples containing water or
acetonitrile. Not for use with samples containing methanol or ethanol.
• Clear acrylic chamber lid, 3/4" thick, with neoprene gasket.
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• LCD that displays system operating parameters, set-up parameters
and alarm messages. It may be user-configured to display vacuum in
mBar, Pa or Torr and temperature in ° F or ° C. It also displays total
number of hours of refrigeration system operation and time since the
refrigeration was serviced and the total number of hours of vacuum
pump operation and time since the vacuum pump was serviced (in
hours).
• Red alarm light that flashes and beeper that sounds to indicate that an
abnormal system event has occurred, including: power failure, improper
line voltage supply, collector temperature rise above -40° C, service vacuum pump (after 1000 hours of vacuum use), and moisture in collector.
Pressing the Menu Switch displays the alarm message on the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of
relative system vacuum and collector temperature.
• Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
• Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off. If a power outage less
than approximately 5 minutes occurs, the freeze dryer will restart
and the refrigeration and vacuum system will resume operation once
power is restored. If the power failure is more than approximately
5 minutes and the collector warms above safe limits, the freeze dryer
will not automatically restart.
• Rear-mounted RS-232 port to transmit data to a user-supplied computer. Transmission intervals may be user-configured for 10, 30, 60,
300 or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Hot gas defrost and switch.
• Front-mounted, retractable, 9" collector drain hose.
• 3" diameter stainless steel port for connection of drying accessories
(sold separately).
• Side-mounted power switch, rear-mounted electrical receptacle (for
vacuum pump connection) and 3-wire cord with plug.
• 3" diameter casters.
• 3/4" OD vacuum connection, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 32.2" w x 28.0" d x 36.3" h
(84.8 cm x 71.1 cm x 92.1 cm).
• Usable interior space: 14.0" w x 24.5" d x 22.0" h (35.6 cm x 62.2 cm x 55.9 cm)
FreeZone Plus 6 Liter Cascade Freeze Dry System 7934020, FreeZone Stoppering Tray
Dryer 7948020, 6-Port Tray Dryer Manifold 7726500 and miscellaneous glassware.
Options include:
• Teflon-coated collector coil and chamber for processes involving corrosive compounds.
• Purge valve with switch for isolating the vacuum pump from the
freeze dry system.
• Built-in stainless steel mini vacuum drying chamber, 5.1" w x 13.0" d x
2.5" h (12.9 cm x 33.0 cm x 6.4 cm), that includes 50-watt heater with
microprocessor control to +60° C (+140° F), 3/4" thick clear acrylic
lid and neoprene gasket. (Chamber is not cooled. The only cooling is
from the frozen sample.)
• Domestic or international electrical configuration.
All models require (not included):
• Vacuum pump with a displacement of at least 98 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Drying accessory. See pages 46-54.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
See ordering information on page 39.
Models conform to the following standards:
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
* Freeze drying capacity rating will be lower for samples other than plain water.
Exclusive feature
31
FreeZone Plus 12 Liter Cascade Freeze Dry Systems
®
™
specifications
All models feature:
• Upright stainless steel collector coil and chamber with stainless steel
baffle capable of removing 4 liters of water in 24 hours and holding
12 liters of ice before defrosting.*
• Two 3/4 hp HCFC/CFC-free refrigeration systems, used in series, to
cool collector to -84° C (-119° F). For samples containing water or
acetonitrile. Not for use with samples containing methanol or ethanol.
• Clear acrylic chamber lid, 3/4" thick, with neoprene gasket.
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• LCD that displays system operating parameters, set-up parameters
and alarm messages. It may be user-configured to display vacuum in
mBar, Pa or Torr and temperature in ° F or ° C. It also displays total
number of hours of refrigeration system operation and time since the
refrigeration was serviced and the total number of hours of vacuum
pump operation and time since the vacuum pump was serviced (in
hours).
• Red alarm light that flashes and beeper that sounds to indicate that
an abnormal system event has occurred, including: power failure,
improper line voltage supply, collector temperature rise above -40° C,
service vacuum pump (after 1000 hours of vacuum use), and moisture
in collector. Pressing the Menu Switch displays the alarm message on
the LCD.
• LED vacuum and temperature “waves” for at-a-glance display of
relative system vacuum and collector temperature.
• Moisture sensor that prevents refrigeration or vacuum start-up when
moisture is detected in the collector chamber area.
• Vacuum control valve that maintains setpoint vacuum level.
• Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off. If a power outage less
than approximately 5 minutes occurs, the freeze dryer will restart
and the refrigeration and vacuum system will resume operation once
power is restored. If the power failure is more than approximately 5
minutes and the collector warms above safe limits, the freeze dryer
will not automatically restart.
• Rear-mounted RS-232 port to transmit data to a user-supplied computer. Transmission intervals may be user-configured for 10, 30, 60,
300 or 600 seconds.
• Automatic start-up switch for collector cool-down and vacuum
pull-down with manual override switches.
• Hot gas defrost and switch.
• Front-mounted, retractable, 9" collector drain hose.
• 3" diameter stainless steel port for connection of drying accessories
(sold separately).
• Side-mounted power switch, rear-mounted electrical receptacle (for
vacuum pump connection) and 3-wire cord with 20 amp plug.
• 3" diameter casters.
• 3/4" OD vacuum connection, three feet of 3/4" ID vacuum hose and
two clamps.
• Overall dimensions: 32.2" w x 28.0" d x 36.3" h
(84.8 cm x 71.1 cm x 92.1 cm).
• Usable interior space: 11.5" w x 24.5" d x 16.5" h
(29.2 cm x 62.2 cm x 41.9 cm)
FreeZone Plus 12 Liter Cascade Freeze Dry System with built-in vacuum drying chamber
7960046, 12-Port Drying Chamber 7522800 and miscellaneous glassware.
Options include:
• Teflon-coated collector coil and chamber for processes involving
corrosive compounds.
• Purge valve with switch for isolating the vacuum pump from the
freeze dry system.
• Built-in stainless steel mini vacuum drying chamber, 5.1" w x 13.0" d x
2.5" h (12.9 cm x 33.0 cm x 6.4 cm), that includes 50-watt heater with
microprocessor control to +60° C (+140° F), 3/4" thick clear acrylic lid
and neoprene gasket. (Chamber is not cooled. The only cooling is from
the frozen sample.)
• Domestic or international electrical configuration.
All models require (not included):
• Vacuum pump with a displacement of at least 98 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Drying accessory. See pages 46-54.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
See ordering information on page 40.
Models conform to the following standards:
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
*Freeze drying capacity rating will be lower for samples other than plain water.
Exclusive feature
32
FreeZone Freeze Dry Systems
®
Ordering
Information
FreeZone 1 Liter Benchtop Freeze Dry Systems. See specifications on page 7.
®
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
Teflon-Coated
Shipping
Collector
Weight
Coil & Chamber
7740020
115 volts, 60 Hz, 14.0 A**
115 volts, 20 amps
85 lbs. (39 kg)
7740021
115 volts, 60 Hz, 14.0 A**
115 volts, 20 amps
•
85 lbs. (39 kg)
7740040
230 volts, 60 Hz, 7.0 A†
North America, 230 volts
7740041
230 volts, 60 Hz, 7.0 A†
North America, 230 volts
7740030*
230 volts, 50 Hz, 7.0 A†
7740031*
230 volts, 50 Hz, 7.0 A†Schuko
7740060*
230 volts, 50 Hz, 7.0 A†
British (UK)
7740061*
230 volts, 50 Hz, 7.0 A†
British (UK)
7740070*
230 volts, 50 Hz, 7.0 A†
7740071*
230 volts, 50 Hz, 7.0 A†China/Australia
85 lbs. (39 kg)
•
85 lbs. (39 kg)
Schuko
85 lbs. (39 kg)
•
85 lbs. (39 kg)
85 lbs. (39 kg)
•
85 lbs. (39 kg)
China/Australia
85 lbs. (39 kg)
•
85 lbs. (39 kg)
FreeZone 2.5 Liter Benchtop Freeze Dry Systems. See specifications on page 9.
®
Catalog
Number
115 volt, 15 amp
Electrical
Requirements
115 volt, 20 amp
Receptacle &
Plug Type
Teflon-Coated
Shipping
Collector
Weight
Coil & Chamber
7670520
115 volts, 60 Hz, 14.0 A**
7670521
115 volts, 60 Hz, 14.0 A**
7670540
230 volts, 60 Hz, 7.0 A†
7670541
230 volts, 60 Hz, 7.0 A†
7670530*
230 volts, 50 Hz, 7.0 A†
115 volts, 20 amps
85 lbs. (39 kg)
•
85 lbs. (39 kg)
115 volts, 20 amps
North America, 230 volts
British (UK)
•
North America, 230 volts
85 lbs. (39 kg)
Schuko
7670531*
230 volts, 50 Hz, 7.0 A Schuko
7670560*
230 volts, 50 Hz, 7.0 A†
7670561*
230 volts, 50 Hz, 7.0 A 7670570*
230 volts, 50 Hz, 7.0 A†
7670571*
230 volts, 50 Hz, 7.0 A China/Australia
†
†
Schuko
85 lbs. (39 kg)
•
British (UK)
115 volt, 15 amp
85 lbs. (39 kg)
85 lbs. (39 kg)
115 volt, 20 amp
•
British (UK)
85 lbs. (39 kg)
•
85 lbs. (39 kg)
115 volt,
115 volt, 15 amp
British (UK)
Schuko
Electrical Receptacle & Plug ConfigurationsChina/Australia
North America, 230 volts
115 volts, 20 amps
115 volt, 15 amp
115 volt, 20 amp
Schuko
British (UK)
China/Australia
British (UK)
North America 230 volt
British (UK)
85 lbs. (39 kg)
China/Australia
†
115 volt, 15 a
85 lbs. (39 kg)
Schuko
China/Austra
North America
China/Australia
British (UK)
Schuko
North America 230 volt
China/Australia
Schuko
* International electrical configuration.
** System amperage shown includes 8 amp maximum vacuum pump rating.
†
System amperage shown includes 4.5 amp maximum vacuum pump rating.
33
North America 230 volt
FreeZone Freeze Dry Systems
®
ordering
Information
FreeZone Plus 2.5 Liter Cascade Benchtop Freeze Dry Systems. See specifications on page 11.
®
™
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
Teflon-Coated
Shipping
Collector
Weight
Coil & Chamber
7670020
7670021
7670040
7670041
7670030*
7670031*
7670060*
7670061*
7670070*
7670071*
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
•
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
•
230 volts, 50 Hz, 10.0 A†
Schuko
230 volts, 50 Hz, 10.0 A†Schuko
•
230 volts, 50 Hz, 10.0 A†
British (UK)
230 volts, 50 Hz, 10.0 A†
British (UK)
•
230 volts, 50 Hz, 10.0 A†
China/Australia
230 volts, 50 Hz, 10.0 A†China/Australia
•
129 lbs. (59 kg)
129 lbs. (59 kg)
129 lbs. (59 kg)
129 lbs. (59 kg)
129 lbs. (59 kg)
129 lbs. (59 kg)
129 lbs. (59 kg)
129 lbs. (59 kg)
129 lbs. (59 kg)
129 lbs. (59 kg)
FreeZone Plus 2.5 Liter Cascade Console Freeze Dry Systems. See specifications on page 13.
®
™
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
Teflon-Coated
Shipping
Collector
Weight
Coil & Chamber
7420020
7420021
7420040
7420041
7420030*
7420031*
7420060*
7420061*
7420070*
7420071*
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
•
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
•
230 volts, 50 Hz, 10.0 A†Schuko
230 volts, 50 Hz, 10.0 A†Schuko
•
230 volts, 50 Hz, 10.0 A†
British (UK)
230 volts, 50 Hz, 10.0 A†
British (UK)
•
230 volts, 50 Hz, 10.0 A†China/Australia
115 volt, 20 amp
115 volt, 15 amp
230 volts, 50 Hz, 10.0 A†China/Australia
•
171 lbs. (78 kg)
171 lbs. (78 kg)
171 lbs. (78 kg)
171 lbs. (78 kg)
171 lbs. (78 kg)
171 lbs. (78 kg)
171 lbs. (78 kg)
171 lbs. (78 kg)
171 lbs. (78 kg)
171 lbs. (78 kg)
FreeZone Plus 4.5 Liter Benchtop Freeze Dry Systems. See specifications on page 15.
®
™
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
Teflon-Coated
Shipping
Collector
Weight
Coil & Chamber
7750020
7750021
7750040
7750041
7750030*
7750031*
7750060*
7750061*
7750070*
7750071*
115 volts, 60 Hz, 14.0 A**
115 volts, 20 amps
102 lbs. (46 kg)
115 volts, 60 Hz, 14.0 A**
115 volts, 20 amps
102 lbs. (46 kg)
•
230 volts, 60 Hz, 7.0 A†
North America, 230 volts
102 lbs. (46 kg)
230 volts, 60 Hz, 7.0 A†
North America, 230 volts
102 lbs. (46 kg)
•
102 lbs. (46 kg)
230 volts, 50 Hz, 7.0 A†Schuko
115 volt, 20 amp
115 volt, 15 amp
230 volts, 50 Hz, 7.0 A†Schuko
102 lbs. (46 kg)
•
Schuko
230 volts, 50 Hz, 7.0 A†
British (UK)
102 lbs. (46 kg)
230 volts, 50 Hz, 7.0 A†
British (UK)
102 lbs. (46 kg)
•
230 volts, 50 Hz, 7.0 A†China/Australia
102 lbs. (46 kg)
230 volts, 50 Hz, 7.0 A†China/Australia
102 lbs. (46 kg)
•
Schuko
Electrical Receptacle & Plug ConfigurationsChina/Australia
North America, 230 volts
115 volts, 20 amps
115 volt, 20 amp
* International electrical configuration.
Schuko
British (UK)
China/Australia
British (UK)
North America 230 volt
Schuko
** System amperage shown includes 8 amp maximum vacuum pump rating.
†
British (UK)
115 volt, 20
115 volt, 15 amp
British (UK)
115 volt, 15 amp
115 volt, 15 amp
British (UK)
China/Australia
System amperage shown includes 4.5 amp maximum vacuum pump rating. .
North America 23
British (UK)
China/Australia
34
Schuko
FreeZone Freeze Dry Systems
®
ordering
Information
FreeZone 4.5 Liter Console Freeze Dry Systems. See specifications on page 17.
®
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
Teflon-Coated
Shipping
Collector
Weight
Coil & Chamber
7751020
7751021
7751040
7751041
7751030*
7751031*
7751060*
7751061*
7751070*
7751071*
115 volts, 60 Hz, 14.0 A**
115 volts, 20 amps
115 volts, 60 Hz, 14.0 A**
115 volts, 20 amps
•
230 volts, 60 Hz, 7.0 A†
North America, 230 volts
230 volts, 60 Hz, 7.0 A†
North America, 230 volts
•
230 volts, 50 Hz, 7.0 A†
Schuko
230 volts, 50 Hz, 7.0 A†Schuko
•
230 volts, 50 Hz, 7.0 A†
British (UK)
230 volts, 50 Hz, 7.0 A†
British (UK)
•
230 volts, 50 Hz, 7.0 A†
China/Australia
230 volts, 50 Hz, 7.0 A†China/Australia
•
162 lbs. (73 kg)
162 lbs. (73 kg)
162 lbs. (73 kg)
162 lbs. (73 kg)
162 lbs. (73 kg)
162 lbs. (73 kg)
162 lbs. (73 kg)
162 lbs. (73 kg)
162 lbs. (73 kg)
162 lbs. (73 kg)
FreeZone Plus 4.5 Liter Cascade Benchtop Freeze Dry Systems. See specifications on page 19.
®
™
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
Teflon-Coated
Shipping
Collector
Weight
Coil & Chamber
7386020
7386021
7386040
7386041
7386030*
7386031*
7386060*
7386061*
7386070*
7386071*
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
•
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
•
230 volts, 50 Hz, 10.0 A†Schuko
230 volts, 50 Hz, 10.0 A†Schuko
•
230 volts, 50 Hz, 10.0 A†
British (UK)
230 volts, 50 Hz, 10.0 A†
British (UK)
•
230 volts, 50 Hz, 10.0 A†China/Australia
230 volts, 50 Hz, 10.0 A†China/Australia
•
131 lbs. (59 kg)
131 lbs. (59 kg)
131 lbs. (59 kg)
131 lbs. (59 kg)
131 lbs. (59 kg)
131 lbs. (59 kg)
131 lbs. (59 kg)
131 lbs. (59 kg)
131 lbs. (59 kg)
131 lbs. (59 kg)
FreeZone Plus 4.5 Liter Cascade Console Freeze Dry Systems. See specifications on page 21.
®
™
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
Teflon-Coated
Shipping
Collector
Weight
Coil & Chamber
7387020
7387021
7387040
7387041
7387030*
7387031*
7387060*
7387061*
7387070*
7387071*
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
•
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
•
230 volts, 50 Hz, 10.0 A†Schuko
230 volts, 50 Hz, 10.0 A†Schuko
•
230 volts, 50 Hz, 10.0 A†
British (UK)
230 volts, 50 Hz, 10.0 A†
British (UK)
•
230 volts, 50 Hz, 10.0 A†China/Australia
230 volts, 50 Hz, 10.0 A†China/Australia
•
181 lbs. (82 kg)
181 lbs. (82 kg)
181 lbs. (82 kg)
181 lbs. (82 kg)
181 lbs. (82 kg)
181 lbs. (82 kg)
181 lbs. (82 kg)
181 lbs. (82 kg)
181 lbs. (82 kg)
181 lbs. (82 kg)
FreeZone -105° C 4.5 Liter Cascade Benchtop Freeze Dry Systems. See specifications on page 23.
®
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
Teflon-Coated
Shipping
Collector
Weight
Coil & Chamber
7382020
7382021
7382040
7382041
7382030*
7382031*
7382032*
7382033*
7382034*
7382035*
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
•
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
•
230 volts, 50 Hz, 10.0 A†Schuko
230 volts, 50 Hz, 10.0 A†Schuko
•
230 volts, 50 Hz, 10.0 A†
British (UK)
230 volts, 50 Hz, 10.0 A†
British (UK)
•
230 volts, 50 Hz, 10.0 A†China/Australia
230 volts, 50 Hz, 10.0 A†China/Australia
•
* International electrical configuration.
** System amperage shown includes 8 amp maximum vacuum pump rating.
35
†
180 lbs. (82 kg)
180 lbs. (82 kg)
180 lbs. (82 kg)
180 lbs. (82 kg)
180 lbs. (82 kg)
180 lbs. (82 kg)
180 lbs. (82 kg)
180 lbs. (82 kg)
180 lbs. (82 kg)
180 lbs. (82 kg)
System amperage shown includes 4.5 amp maximum vacuum pump rating.
FreeZone Freeze Dry Systems
®
ordering
Information
FreeZone 6 Liter Benchtop Freeze Dry Systems. See specifications on page 25.
®
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
Teflon-Coated
Shipping
Collector
Weight
Coil & Chamber
7752020
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
150 lbs. (68 kg)
7752021
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
•
150 lbs. (68 kg)
7752040
230 volts, 60 Hz, 8.0 A†
North America, 230 volts
7752041
230 volts, 60 Hz, 8.0 A†
North America, 230 volts
7752030*
230 volts, 50 Hz, 8.0 A†
7752031*
230 volts, 50 Hz, 8.0 A†Schuko
150 lbs. (68 kg)
•
150 lbs. (68 kg)
Schuko
150 lbs. (68 kg)
•
7752060*
230 volts, 50 Hz, 8.0 A†
British (UK)
7752061*
230 volts, 50 Hz, 8.0 A†
British (UK)
7752070*
230 volts, 50 Hz, 8.0 A†
7752071*
230 volts, 50 Hz, 8.0 A†China/Australia
150 lbs. (68 kg)
150 lbs. (68 kg)
•
150 lbs. (68 kg)
China/Australia
150 lbs. (68 kg)
•
150 lbs. (68 kg)
FreeZone 6 Liter Benchtop Freeze Dry Systems with Stoppering Tray Dryers. See specifications on page 25.
®
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
Teflon-Coated
Stoppering
Collector
Tray
Coil & Chamber
Shipping
Weight
7758020
115 volts, 60 Hz, 16.0 A**
115 volts, 60 Hz, 16.0 A† †
115 volts, 20 amps
•
115 volts, 20 amps
Shipped in two cartons
7758021
115 volts, 60 Hz, 16.0 A**
115 volts, 60 Hz, 16.0 A† †
115 volts, 20 amps
•
•
115 volts, 20 amps
Shipped in two cartons
7758040
230 volts, 60 Hz, 8.0 A†
230 volts, 60 Hz, 8.0 A† †
North America, 230 volts
•
North America, 230 volts
115 volt, 20 amp
7758041
230 volts, 60 Hz, 8.0 A†
230 volts, 60 Hz, 9.0 A† †
North America, 230 volts
•
•
North America, 230 volts
7758030*
230 volts, 50 Hz, 8.0 A†Schuko •
572 lbs. (259 kg)
230 volts, 50 Hz, 9.0 A† †Schuko
Shipped in two cartons
7758031*
115 volts, 50 Hz, 8.0 A**
Schuko
572 lbs. (259 kg)
•
•
British (UK)
115 volts, 60 Hz, 9.0 A† †Schuko
Shipped in two cartons
7758060*
230 volts, 50 Hz, 8.0 A†
230 volts, 60 Hz, 9.0 A† †
British (UK)
•
British (UK)
Shipped in two cartons
7758061*
115 volts, 50 Hz, 8.0 A**
115 volts, 60 Hz, 9.0 A† †
British (UK)
•
•
British (UK)
Shipped in two cartons
115 volt, 20 amp
7758070*
230 volts, 50 Hz, 8.0 A†China/Australia
572 lbs. (259 kg)
•
Schuko
230 volts, 60 Hz, 9.0 A† †China/Australia Shipped in two cartons
7758071*
230 volts, 50 Hz, 8.0 A†China/Australia
572 lbs. (259 kg)
•
•
230 volts, 60 Hz, 9.0 A† †China/Australia Shipped in two cartons
572 lbs. (259 kg)
572 lbs. (259 kg)
572 lbs. (259 kg)
Shipped in two cartons
115 volt, 15 amp
115 volt, 15 amp
572 lbs. (259 kg)
Shipped in two cartons
572 lbs. (259 kg)
572 lbs. (259 kg)
Schuko
Electrical Receptacle & Plug ConfigurationsChina/Australia
115 volts, 20 amps
115 volt, 15 amp
North America, 230 volts
115 volt, 20 amp
Schuko
British (UK)
China/Australia
British (UK)
North America 230 volt
Schuko
* International electrical configuration. ** System amperage shown includes 8 amp maximum vacuum pump rating.
††
Electrical requirements of the Stoppering Tray Dryer.
British (UK)
36
†
System amperage shown includes 4.5 amp maximum vacuum pump rating.
China/Australia
British (UK)
115 volt, 20
115 volt, 15 amp
British (UK)
115 volt, 15 amp
Schuko
China/Australia
North America 23
FreeZone Freeze Dry Systems
®
ordering
Information
FreeZone 6 Liter Console Freeze Dry Systems. See specifications on page 27.
®
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
7753020
7753021
7753022
7753024
7753026
7753027
7753040
7753041
7753042
7753044
7753046
7753047
7753030*
7753031*
7753032*
7753034*
7753036*
7753037*
7753060*
7753061*
7753062*
7753064*
7753066*
7753067*
7753070*
7753071*
7753072*
7753074*
7753076*
7753077*
115 volts, 60 Hz, 16.0 A**
115 volts, 60 Hz, 16.0 A**
115 volts, 60 Hz, 16.0 A**
115 volts, 60 Hz, 16.0 A**
115 volts, 60 Hz, 16.0 A**
115 volts, 60 Hz, 16.0 A**
Teflon-Coated
Purge
Collector
Valve
Coil & Chamber
Mini
Chamber
115 volts, 20 amps
115 volts, 20 amps
•
115 volts, 20 amps
•
115 volts, 20 amps
•
•
115 volts, 20 amps
•
•
115 volts, 20 amps
•
•
•
230 volts, 60 Hz, 8.0 A†
North America, 230 volts
230 volts, 60 Hz, 8.0 A††
North America, 230 volts
•
230 volts, 60 Hz, 8.0 A†
North America, 230 volts
•
230 volts, 60 Hz, 8.0 A†
North America, 230 volts
•
•
230 volts, 60 Hz, 8.0 A†
North America, 230 volts
•
•
230 volts, 60 Hz, 8.0 A†
North America, 230 volts
•
•
•
230 volts, 50 Hz, 8.0 A†
Schuko
230 volts, 50 Hz, 8.0 A†Schuko •
230 volts, 50 Hz, 8.0 A†Schuko •
230 volts, 50 Hz, 8.0 A†Schuko •
•
230 volts, 50 Hz, 8.0 A†Schuko •
•
230 volts, 50 Hz, 8.0 A†Schuko •
•
•
230 volts, 50 Hz, 8.0 A†
British (UK)
230 volts, 50 Hz, 8.0 A†
British (UK)
•
230 volts, 50 Hz, 8.0 A†
British (UK)
•
230 volts, 50 Hz, 8.0 A†
British (UK)
•
•
230 volts, 50 Hz, 8.0 A†
British (UK)
•
•
230 volts, 50 Hz, 8.0 A†
British (UK)
•
•
•
230 volts, 50 Hz, 8.0 A†
China/Australia
230 volts, 50 Hz, 8.0 A†China/Australia •
230 volts, 50 Hz, 8.0 A†China/Australia
•
230 volts, 50 Hz, 8.0 A†China/Australia •
•
230 volts, 50 Hz, 8.0 A†China/Australia
•
•
230 volts, 50 Hz, 8.0 A†China/Australia •
•
•
Shipping
Weight
254 lbs. (115 kg)
254 lbs. (115 kg)
257 lbs. (117 kg)
257 lbs. (117 kg)
272 lbs. (123 kg)
272 lbs. (123 kg)
254 lbs. (115 kg)
254 lbs. (115 kg)
257 lbs. (117 kg)
257 lbs. (117 kg)
272 lbs. (123 kg)
272 lbs. (123 kg)
254 lbs. (115 kg)
254 lbs. (115 kg)
257 lbs. (117 kg)
257 lbs. (117 kg)
272 lbs. (123 kg)
272 lbs. (123 kg)
254 lbs. (115 kg)
254 lbs. (115 kg)
257 lbs. (117 kg)
257 lbs. (117 kg)
272 lbs. (123 kg)
272 lbs. (123 kg)
254 lbs. (115 kg)
254 lbs. (115 kg)
257 lbs. (117 kg)
257 lbs. (117 kg)
272 lbs. (123 kg)
272 lbs. (123 kg)
FreeZone 6 Liter Console Freeze Dry Systems with Purge Valves and Shell Freezers. See specifications on page 27.
®
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
7753522
7753524
7753542
7753544
7753532*
7753534*
7753562*
7753564*
7753572*
7753574*
Teflon-Coated
Purge
Collector
Valve
Coil & Chamber
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
•
230 volts, 60 Hz, 10.0 A**
North America, 230 volts
230 volts, 60 Hz, 10.0 A**
North America, 230 volts
•
230 volts, 50 Hz, 10.0 A†Schuko
230 volts, 50 Hz, 10.0 A†Schuko •
230 volts, 50 Hz, 10.0 A†
British (UK)
230 volts, 50 Hz, 10.0 A†
British (UK)
•
230 volts, 50 Hz, 10.0 A†China/Australia
230 volts, 50 Hz, 10.0 A†China/Australia •
* International electrical configuration.
** System amperage shown includes 8 amp maximum vacuum pump rating.
37
†
•
•
•
•
•
•
•
•
•
•
Shell
Freezer
Shipping
Weight
•
•
•
•
•
•
•
•
•
•
324 lbs. (147 kg)
324 lbs. (147 kg)
324 lbs. (147 kg)
324 lbs. (147 kg)
324 lbs. (147 kg)
324 lbs. (147 kg)
324 lbs. (147 kg)
324 lbs. (147 kg)
324 lbs. (147 kg)
324 lbs. (147 kg)
System amperage shown includes 4.5 amp maximum vacuum pump rating.
FreeZone Freeze Dry Systems
®
ordering
Information
FreeZone 6 Liter Console Freeze Dry Systems with Stoppering Tray Dryers. See specifications on page 27.
®
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
Teflon-Coated
Purge
Collector
Valve
Coil & Chamber
Stoppering
Tray Dryer Shipping
Weight
7758520
115 volts, 60 Hz, 16.0 A**
115 volts, 60 Hz, 16.0 A††
115 volts, 20 amps
•
115 volts, 20 amps
Shipped in two cartons
7758521
115 volts, 60 Hz, 16.0 A**
115 volts, 60 Hz, 16.0 A††
115 volts, 20 amps
•
•
115 volts, 20 amps
Shipped in two cartons
7758522
115 volts, 60 Hz, 16.0 A**
115 volts, 60 Hz, 16.0 A††
115 volts, 20 amps
•
•
115 volts, 20 amps
Shipped in two cartons
7758524
115 volts, 60 Hz, 16.0 A**
115 volts, 60 Hz, 16.0 A††
115 volts, 20 amps
•
•
•
115 volts, 20 amps
Shipped in two cartons
7758540
230 volts, 60 Hz, 8.0 A†
230 volts, 60 Hz, 9.0 A††
North America, 230 volts
•
North America, 230 volts
Shipped in two cartons
7758541
230 volts, 60 Hz, 8.0 A††
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
•
•
North America, 230 volts
Shipped in two cartons
7758542
230 volts, 50 Hz, 8.0 A††
230 volts, 50 Hz, 9.0 A†
North America, 230 volts
•
•
North America, 230 volts
Shipped in two cartons
7758544
230 volts, 50 Hz, 8.0 A††
230 volts, 50 Hz, 9.0 A†
North America, 230 volts
•
•
•
North America, 230 volts
Shipped in two cartons
7758530*
230 volts, 50 Hz, 8.0 A†Schuko•
676 lbs. (307 kg)
230 volts, 50 Hz, 9.0 A††Schuko
Shipped in two cartons
7758531*
230 volts, 50 Hz, 8.0 A†Schuko •
676 lbs. (307 kg)
•
230 volts, 50 Hz, 9.0 A††Schuko
Shipped in two cartons
7758532*
230 volts, 50 Hz, 8.0 A†Schuko •
679 lbs. (308 kg)
•
230 volts, 60 Hz, 9.0 A††Schuko
Shipped in two cartons
7758534*
230 volts, 60 Hz, 8.0 A†Schuko •
679 lbs. (308 kg)
•
•
230 volts, 60 Hz, 9.0 A††Schuko
Shipped in two cartons
115 volt, 20 amp
7758560*
230 volts, 50 Hz, 8.0 A†
230 volts, 60 Hz, 9.0 A††
British (UK)
•
British (UK)
Shipped in two cartons
7758561*
230 volts, 60 Hz, 8.0 A†
230 volts, 60 Hz, 9.0 A††
British (UK)
•
•
British (UK)
Shipped in two cartons
7758562*
230 volts, 60 Hz, 8.0 A†
230 volts, 60 Hz, 9.0 A††
British (UK)
•
•
British (UK)
Shipped in two cartons
7758564*
230 volts, 60 Hz, 8.0 A†
230 volts, 60 Hz, 9.0 A††
British (UK)
•
•
•
British (UK)
7758570*
230 volts, 50 Hz, 8.0 A†China/Australia •
676 lbs. (307 kg)
230 volts, 60 Hz, 9.0 A††China/Australia
Shipped in two cartons
7758571*
230 volts, 50 Hz, 8.0 A†China/Australia •
676 lbs. (307 kg)
• 115 volt, 20 amp
115 volt, 15 amp
230 volts, 60 Hz, 9.0 A††China/Australia
Shipped in two cartons
7758572*
Schuko
230 volts, 60 Hz, 8.0 A†China/Australia
679 lbs. (308 kg)
•
•
230 volts, 60 Hz, 9.0 A††China/Australia
Shipped in two cartons
7758574*
230 volts, 60 Hz, 8.0 A†China/Australia •
679 lbs. (308 kg)
•
•
230 volts, 60 Hz, 9.0 A††China/Australia
Shipped in two cartons
676 lbs. (307 kg)
676 lbs. (307 kg)
679 lbs. (308 kg)
679 lbs. (308 kg)
676 lbs. (307 kg)
676 lbs. (307 kg)
679 lbs. (308 kg)
679 lbs. (308 kg)
115 volt, 15 amp
676 lbs. (307 kg)
676 lbs. (307 kg)
679 lbs. (308 kg)
British (UK)
Shipped in two cartons
Schuko
Electrical Receptacle & Plug ConfigurationsChina/Australia
115 volts, 20 amps
115 volt, 15 amp
North America, 230 volts
115 volt, 20 amp
Schuko
British (UK)
China/Australia
British (UK)
North America 230 volt
Schuko
* International electrical configuration. ** System amperage shown includes 8 amp maximum vacuum pump rating.
††
Electrical requirements of the Stoppering Tray Dryer.
British (UK)
38
†
System amperage shown includes 4.5 amp maximum vacuum pump rating.
China/Australia
British (UK)
115 volt, 20
115 volt, 15 amp
British (UK)
115 volt, 15 amp
679 lbs. (308 kg)
Schuko
China/Australia
North America 23
FreeZone Freeze Dry Systems
®
ordering
Information
FreeZone Plus 6 Liter Cascade Console Freeze Dry Systems. See specifications on page 31.
®
Catalog
Number
™
Electrical
Requirements
Receptacle &
Plug Type
7934020
7934021
7934022
7934024
7934026
7934027
7934040
7934041
7934042
7934044
7934046
7934047
7934030*
7934031*
7934032*
7934034*
7934036*
7934037*
7934060*
7934061*
7934062*
7934064*
7934066*
7934067*
7934070*
7934071*
7934072*
7934074*
7934076*
7934077*
Teflon-Coated
Purge
Collector
Valve
Coil & Chamber
Mini
Chamber
Shipping
Weight
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
270 lbs. (122 kg)
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
270 lbs. (122 kg)
•
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
273 lbs. (124 kg)
•
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
273 lbs. (124 kg)
•
•
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
288 lbs. (131 kg)
•
•
115 volts, 60 Hz, 16.0 A**
115 volts, 20 amps
288 lbs. (131 kg)
•
•
•
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
270 lbs. (122 kg)
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
270 lbs. (122 kg)
•
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
273 lbs. (124 kg)
•
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
273 lbs. (124 kg)
•
•
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
288 lbs. (131 kg)
•
•
230 volts, 60 Hz, 10.0 A†
North America, 230 volts
288 lbs. (131 kg)
•
•
•
230 volts, 50 Hz, 10.0 A†Schuko
270 lbs. (122 kg)
230 volts, 50 Hz, 10.0 A†Schuko •
270 lbs. (122 kg)
230 volts, 50 Hz, 10.0 A†Schuko •
273 lbs. (124 kg)
230 volts, 50 Hz, 10.0 A†Schuko •
273 lbs. (124 kg)
•
230 volts, 50 Hz, 10.0 A†Schuko •
288 lbs. (131 kg)
•
230 volts, 50 Hz, 10.0 A†Schuko •
288 lbs. (131 kg)
•
•
230 volts, 50 Hz, 10.0 A†
British (UK)
270 lbs. (122 kg)
230 volts, 50 Hz, 10.0 A†
British (UK)
270 lbs. (122 kg)
•
230 volts, 50 Hz, 10.0 A†
British (UK)
273 lbs. (124 kg)
•
230 volts, 50 Hz, 10.0 A†
British (UK)
273 lbs. (124 kg)
•
•
230 volts, 50 Hz, 10.0 A†
British (UK)
288 lbs. (131 kg)
•
•
230 volts, 50 Hz, 10.0 A†
British (UK)
288 lbs. (131 kg)
•
•
•
230 volts, 50 Hz, 10.0 A†China/Australia270 lbs. (122 kg)
230 volts, 50 Hz, 10.0 A†China/Australia •
270 lbs. (122 kg)
230 volts, 50 Hz, 10.0 A†China/Australia
273 lbs. (124 kg)
•
230 volts, 50 Hz, 10.0 A†China/Australia •
273 lbs. (124 kg)
•
230 volts, 50 Hz, 10.0 A†China/Australia
288 lbs. (131 kg)
•
•
230 volts, 50 Hz, 10.0 A†China/Australia •
288 lbs. (131 kg)
•
•
FreeZone 12 Liter Console Freeze Dry Systems. See specifications on page 28.
®
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
7754040
7754041
7754042
7754044
7754046
7754047
7754030*
7754031*
7754032*
7754034*
7754036*
7754037*
7754060*
7754061*
7754062*
7754064*
7754066*
7754067*
7754070*
7754071*
7754072*
7754074*
7754076*
7754077*
Teflon-Coated
Purge
Collector
Valve
Coil & Chamber
Mini
Chamber
Shipping
Weight
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
275 lbs. (125 kg)
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
275 lbs. (125 kg)
•
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
278 lbs. (126 kg)
•
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
278 lbs. (126 kg)
•
•
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
293 lbs. (133 kg)
•
•
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
293 lbs. (133 kg)
•
•
•
230 volts, 50 Hz, 9.0 A†Schuko
275 lbs. (125 kg)
230 volts, 50 Hz, 9.0 A†Schuko •
275 lbs. (125 kg)
230 volts, 50 Hz, 9.0 A†Schuko •
278 lbs. (126 kg)
230 volts, 50 Hz, 9.0 A†Schuko •
278 lbs. (126 kg)
•
230 volts, 50 Hz, 9.0 A†Schuko •
293 lbs. (133 kg)
•
230 volts, 50 Hz, 9.0 A†Schuko •
293 lbs. (133 kg)
•
•
230 volts, 50 Hz, 9.0 A†
British (UK)
275 lbs. (125 kg)
230 volts, 50 Hz, 9.0 A†
British (UK)
275 lbs. (125 kg)
•
230 volts, 50 Hz, 9.0 A†
British (UK)
278 lbs. (126 kg)
•
230 volts, 50 Hz, 9.0 A†
British (UK)
278 lbs. (126 kg)
•
•
230 volts, 50 Hz, 9.0 A†
British (UK)
293 lbs. (133 kg)
•
•
230 volts, 50 Hz, 9.0 A†
British (UK)
293 lbs. (133 kg)
•
•
•
230 volts, 50 Hz, 9.0 A†China/Australia
275 lbs. (125 kg)
230 volts, 50 Hz, 9.0 A†China/Australia •
275 lbs. (125 kg)
230 volts, 50 Hz, 9.0 A†China/Australia
278 lbs. (126 kg)
•
230 volts, 50 Hz, 9.0 A†China/Australia •
278 lbs. (126 kg)
•
230 volts, 50 Hz, 9.0 A†China/Australia
293 lbs. (133 kg)
•
•
230 volts, 50 Hz, 9.0 A†China/Australia •
293 lbs. (133 kg)
•
•
* International electrical configuration.
†
System amperage shown includes 4.5 amp maximum vacuum pump rating.
39
FreeZone Freeze Dry Systems
®
ordering
Information
FreeZone 12 Liter Console Freeze Dry Systems with Stoppering Tray Dryers. See specifications on page 28.
®
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
Teflon-Coated
Purge
Collector
Valve
Coil & Chamber
Stoppering
Tray Dryer Shipping
Weight
230 volts, 60 Hz, 8.0 A†
North America, 230 volts
697 lbs. (316 kg)
•
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
Shipped in two cartons
230 volts, 60 Hz, 8.0 A†
North America, 230 volts
697 lbs. (316 kg)
•
•
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
Shipped in two cartons
230 volts, 50 Hz, 8.0 A††
North America, 230 volts
700 lbs. (318 kg)
•
•
230 volts, 50 Hz, 9.0 A†
North America, 230 volts
Shipped in two cartons
230 volts, 50 Hz, 8.0 A†
North America, 230 volts
700 lbs. (318 kg)
•
•
•
230 volts, 50 Hz, 9.0 A†
North America, 230 volts
Shipped in two cartons
230 volts, 50 Hz, 8.0 A†Schuko•
697 lbs. (316 kg)
230 volts, 50 Hz, 9.0 A† Schuko
Shipped in two cartons
230 volts, 50 Hz, 8.0 A†Schuko •
697 lbs. (316 kg)
•
230 volts, 50 Hz, 9.0 A††Schuko
Shipped in two cartons
230 volts, 50 Hz, 8.0 A†Schuko •
700 lbs. (318 kg)
•
230 volts, 60 Hz, 9.0 A† Schuko
Shipped in two cartons
230 volts, 60 Hz, 8.0 A†Schuko •
700 lbs. (318 kg)
•
•
230 volts, 60 Hz, 9.0 A††Schuko
Shipped in two cartons
230 volts, 50 Hz, 8.0 A†
British (UK)
697 lbs. (316 kg)
•
230 volts, 60 Hz, 9.0 A†
British (UK)
Shipped in two cartons
230 volts, 60 Hz, 8.0 A†
British (UK)
697 lbs. (316 kg)
•
•
230 volts, 60 Hz, 9.0 A††
British (UK)
Shipped in two cartons
230 volts, 60 Hz, 8.0 A†
British (UK)
700 lbs. (318 kg)
•
•
230 volts, 60 Hz, 9.0 A†
British (UK)
Shipped in two cartons
230 volts, 60 Hz, 8.0 A†
British (UK)
700 lbs. (318 kg)
•
•
•
230 volts, 60 Hz, 9.0 A††
British (UK)
Shipped in two cartons
230 volts, 50 Hz, 8.0 A†China/Australia •
697 lbs. (316 kg)
230 volts, 60 Hz, 9.0 A†China/Australia
Shipped in two cartons
230 volts, 50 Hz, 8.0 A†China/Australia •
697 lbs. (316 kg)
•
230 volts, 60 Hz, 9.0 A†China/Australia
Shipped in two cartons
230 volts, 60 Hz, 8.0 A†China/Australia
700 lbs. (318 kg)
•
•
230 volts, 60 Hz, 9.0 A†China/Australia
Shipped in two cartons
230 volts, 60 Hz, 8.0 A†China/Australia •
700 lbs. (318 kg)
•
•
230 volts, 60 Hz, 9.0 A†China/Australia
Shipped in two cartons
7759040
7759041
7759042
7759044
7759030*
7759031*
7759032*
7759034*
7759060*
7759061*
7759062*
7759064*
7759070*
7759071*
7759072*
7759074*
FreeZone Plus 12 Liter Cascade Freeze Dry Systems. See specifications on page 32.
®
Catalog
Number
™
Electrical
Requirements
Receptacle &
Plug Type
7960040
7960041
7960042
7960044
7960046
7960047
7960030*
7960031*
7960032*
7960034*
7960036*
7960037*
7960060*
7960061*
7960062*
7960064*
7960066*
7960067*
7960070*
7960071*
7960072*
7960074*
7960076*
7960077*
Teflon-Coated
Purge
Collector
Valve
Coil & Chamber
Mini
Chamber
Shipping
Weight
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
319 lbs. (145 kg)
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
319 lbs. (145 kg)
•
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
322 lbs. (146 kg)
•
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
322 lbs. (146 kg)
•
•
†
230 volts, 60 Hz, 9.0 A North America, 230 volts
337 lbs. (153 kg)
•
•
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
337 lbs. (153 kg)
•
•
•
230 volts, 50 Hz, 9.0 A†Schuko
319 lbs. (145 kg)
230 volts, 50 Hz, 9.0 A†Schuko •
319 lbs. (145 kg)
†
230 volts, 50 Hz, 9.0 A Schuko •
322 lbs. (146 kg)
230 volts, 50 Hz, 9.0 A†Schuko •
322 lbs. (146 kg)
•
230 volts, 50 Hz, 9.0 A†Schuko •
337 lbs. (153 kg)
•
230 volts, 50 Hz, 9.0 A†Schuko •
337 lbs. (153 kg)
•
•
230 volts, 50 Hz, 9.0 A†
British (UK)
319 lbs. (145 kg)
†
230 volts, 50 Hz, 9.0 A British (UK)
319 lbs. (145 kg)
•
230 volts, 50 Hz, 9.0 A†
British (UK)
322 lbs. (146 kg)
•
230 volts, 50 Hz, 9.0 A†
British (UK)
322 lbs. (146 kg)
•
•
230 volts, 50 Hz, 9.0 A†
British (UK)
337 lbs. (153 kg)
•
•
†
230 volts, 50 Hz, 9.0 A British (UK)
337 lbs. (153 kg)
•
•
•
230 volts, 50 Hz, 9.0 A†China/Australia
319 lbs. (145 kg)
230 volts, 50 Hz, 9.0 A†China/Australia •
319 lbs. (145 kg)
230 volts, 50 Hz, 9.0 A†China/Australia •
322 lbs. (146 kg))
•
230 volts, 50 Hz, 9.0 A†China/Australia •
322 lbs. (146 kg))
•
†
230 volts, 50 Hz, 9.0 A China/Australia
337 lbs. (153 kg)
•
•
230 volts, 50 Hz, 9.0 A†China/Australia •
337 lbs. (153 kg)
•
•
* International electrical configuration. ** System amperage shown includes 8 amp maximum vacuum pump rating.
††
Electrical requirements of the Stoppering Tray Dryer.
40
†
System amperage shown includes 4.5 amp maximum vacuum pump rating.
FreeZone Freeze Dry Systems
®
ordering
Information
FreeZone 18 Liter Console Freeze Dry Systems. See specifications on page 29.
®
Catalog
Number
Electrical
Requirements
Receptacle &
Plug Type
7755040
7755041
7755042
7755044
7755046
7755047
7755030*
7755031*
7755032*
7755034*
7755036*
7755037*
7755060*
7755061*
7755062*
7755064*
7755066*
7755067*
7755070*
7755071*
7755072*
7755074*
7755076*
7755077*
Teflon-Coated
Purge
Collector
Valve
Coil & Chamber
Mini
Chamber
Shipping
Weight
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
285 lbs. (129 kg)
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
285 lbs. (129 kg)
•
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
288 lbs. (131 kg)
•
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
288 lbs. (131 kg)
•
•
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
303 lbs. (137 kg)
•
•
230 volts, 60 Hz, 9.0 A†
North America, 230 volts
303 lbs. (137 kg)
•
•
•
115 volt, 20 amp
230 volts, 50 Hz, 9.0 A†Schuko
285 lbs. (129 kg)
115 volt, 15 amp
†
230 volts, 50 Hz, 9.0 A Schuko •
285 lbs. (129 kg)
230 volts, 50 Hz, 9.0 A†Schuko •
288 lbs. (131 kg)
230 volts, 50 Hz, 9.0 A†Schuko •
288 lbs. (131 kg)
•
230 volts, 50 Hz, 9.0 A†Schuko •
303 lbs. (137 kg)
•
230 volts, 50 Hz, 9.0 A†Schuko •
303 lbs. (137 kg)
•
•
230 volts, 50 Hz, 9.0 A†
British (UK)
285 lbs. (129 kg)
230 volts, 50 Hz, 9.0 A†
British (UK)
285 lbs. (129 kg)
•
British(UK)
(UK)
230 volts, 50 Hz, 9.0 A†
British
288 lbs. (131 kg)
•
230 volts, 50 Hz, 9.0 A†
British (UK)
288 lbs. (131 kg)
•
•
†
230 volts, 50 Hz, 9.0 A British (UK)
303 lbs. (137 kg)
•
•
230 volts, 50 Hz, 9.0 A†
British (UK)
303 lbs. (137 kg)
•
•
•
230 volts, 50 Hz, 9.0 A†China/Australia
285 lbs. (129 kg)
230 volts, 50 Hz, 9.0 A†China/Australia •
285 lbs. (129 kg)
115 volt, 20 amp
230 volts, 50 Hz, 9.0 A†China/Australia •
288 lbs. (131 kg)
•
115 volt, 15 amp
230 volts, 50 Hz, 9.0 A†China/Australia •
288 lbs. (131 kg)
•
Schuko
230 volts, 50 Hz, 9.0 A†China/Australia
303 lbs. (137 kg)
•
•
230 volts, 50 Hz, 9.0 A†China/Australia •
303 lbs. (137 kg)
•
•
* International electrical configuration.
†
115 volt,
115 volt, 15 amp
Schuko
Electrical Receptacle & Plug ConfigurationsChina/Australia
115 volt, 15 amp
British (UK)
North America, 230 volts
115 volt, 20 amp
China/Australia
Schuko
British (UK)
Schuko
Dry Ice Benchtop Freeze Dry System
China/Australia
&
China/Australia
British (UK)
North America 230 volt
specifications
Schuko
British (UK)
System amperage shown includes 4.5 amp maximum vacuum pump rating.
British (UK)
115 volts, 20 amps
115 volt, 15 a
Ordering
North America
Schuko
Information
For the laboratory with occasional lyophilization requirements, the Dry Ice Benchtop Freeze Dry
North America
230 volt drying. Since dry ice cools alcohol or other heat
System provides a simple, economical means
of freeze
China/Australia
transfer solutions to approximately -75° C (-103° F), the Dry Ice Benchtop Freeze Dry System is ideal
for processing materials with low eutectic points.
The Dry Ice Benchtop Freeze Dry System is equipped with a center well for dry ice and solvent that
serves as a water vapor collector and doubles as a convenient pre-freezing bath. Flasks, serum bottles
and ampules may be frozen by dipping and rotating them in the well.
North
America 230 (24.8
volt
7522700 Dry Ice Benchtop Freeze Dry System. Chamber, 9.8" h x 8.8"
diameter
cm x
22.2 cm), type 304 stainless steel with twelve valves and single run capacity of 1 liter. Valves accommodate either 1/2" or 3/4" flask adapters. Includes dry ice/solvent center well with 1.92 liter capacity and cover, 1/2" OD port for connection to vacuum pump and 3/8" OD port for connection to
vacuum gauge. Dry ice, vacuum pump, vacuum gauge, tubing and glassware are required
(not included). See pages 56-58 for vacuum pumps and accessories. See pages 60-63 for glassware.
Shipping weight 11 lbs. (5 kg)
North America 230 volt
41
China/Austra
FreeZone Triad Freeze Dry Systems
®
™
features
&
benefits
FreeZone Triad is an all-in-one benchtop cascade
lyophilizer and stoppering tray dryer. Just add a vacuum
pump and glassware and begin pre-freezing, freeze drying
and stoppering under vacuum.
One large processing shelf may be used to pre-freeze
samples in containers or bulk to -75° C. Dual refrigeration
systems cool to -85° C to freeze dry low eutectic point samples
on the shelf or on four sample valves mounted to the lefthand side. After freeze drying, vials or serum bottles on the
processing shelf may be stoppering under vacuum using a
pneumatic mechanism that does not require compressed gas.
Four sample valves increase
the capacity and flexibility of
the freeze dryer. Four valves
allow connection of flasks
and other freeze dry glassware. Samples in the flasks
and in the tray dryer may be
lyophilized simultaneously.
Large clear acrylic door
provides complete visibility of
the processing shelf.
Hot gas defrost. Hot gas from
the compressor is circulated
through the collector coil and
automatically shuts off when
the refrigerant reaches +60° C
(+140° F) or after 3 hours.
Automatic control of temperature enhances consistency
and convenience of repetitive
protocols. A microprocessorbased controller permits up
to five different temperature
programs to be stored and
repeated, each using a timed
pre-freezing segment plus as
many as five different ramping and holding segments.
Rear-mounted RS-232 port
may be used to transmit data
to a user-supplied computer.
Vacuum control/break valve
maintains set point vacuum
level to speed the freeze dry
process. At the same time,
it protects the system from
oil backstreaming by bleeding air into the system when
power to the freeze dryer or
vacuum pump is shut off. If a
brief power outage occurs, the
freeze dryer will restart and
the refrigeration and vacuum
system will resume operation
once power is restored. If the
power failure is longer and
the collector warms above
safe limits, the freeze dryer
will not automatically restart,
which prevents melted sample from being drawn into the
vacuum pump.
Rear-mounted electrical
receptacle allows connection of the vacuum
pump (pump sold
separately).
Durable exterior of brushed
stainless steel and glacier white
epoxy-coated steel with blue
accents.
Stoppering control regulates
the stoppering mechanism
when the chamber is under
vacuum.
ETL listed. The 230 volt, 60
Hz model carries the ETL mark
signifying it is certified to UL
and CAN/CSA standards for
laboratory equipment.
CE marking. The 230 volt,
50 Hz model conforms to the
CE (European Community)
directives.
1/8" OD backfill port introduces
sterile air or inert gas from an
outside source to the chamber,
protecting samples from
atmospheric moisture and
contaminants.
Exclusive feature
42
FreeZone Triad Freeze Dry Systems
®
™
features
&
benefits
Built-in pneumatic mechanism stoppers containers on processing shelf.
Containers are stoppered while the chamber is under vacuum and
without the use of compressed gas.
Collector drain pan and hose. A stainless steel drain pan (above) catches
defrosted condensate, which may be conveniently emptied through the
attached drain hose (above, right). The pan is removable for cleaning.
HCFC/CFC-free refrigeration system ensures environmentally-safe cooling.
Two refrigeration modules, used in series, cool the collector coil to -85° C
(-121° F), ideal for freeze drying samples with low eutectic points
including acetonitrile. The same refrigeration system and a 1000-watt
heater efficiently cool and heat the shelf. Temperature of the fluid circulating through channels in the shelf may be set to a pre-freeze temperature of -75° C (-103° F) or between -55° C to +50° C (-67 to +122° F) for
freeze drying and is maintained within 1° C of set point. The system uses
a non-flammable refrigerant that contains no ozone-damaging hydrochlorofluorocarbons (HCFCs) or chlorofluorocarbons (CFCs).
The shelf may be loaded with unstoppered
vials or bottles. Stoppers should be inserted
in container openings in the raised position.
One sensor probe monitors sample temperature, which is digitally
displayed on the LCD.
When the stoppering control is activated,
atmospheric pressure causes the diaphragm
to expand. Pressure from the expanding
diaphragm forces the stoppering platen
downward until it makes contact with the
stoppers, forcing them into the containers.
Serum Bottle Capacity of the FreeZone Triad System
Chamber pre-freezes samples to save money and time. Samples may
be frozen on the shelf, eliminating the need for a separate freezer and
product transfer.
Size
2 ml
3 ml
5 ml
10 ml
20 ml
30 ml
50 ml
100 ml
125 ml
Exclusive feature
43
Catalog Number
Shelf Capacity
7575010400
7575210441
7573010
233
7573210196
7573410121
757361086
757381064
757401042
757421036
FreeZone Triad Freeze Dry Systems
®
™
features
&
benefits
User-Friendly Control Panel
Green RUN/STOP indicator
illuminates steadily while freeze
drying is in progress and turns
off when the RUN/STOP switch
terminates a run. If a power
failure occurs during processing, the indicator flashes when
power is restored.
LCD prompts the user to set
programming parameters and
displays shelf, sample and collector temperatures in ° C or
° F; vacuum in mBar, Pa or
Torr. When the automatic
mode is selected, the display
also indicates the program
number selected, which
segment of the program is
in progress and the time
remaining for that segment.
DISPLAY switch changes
the screen format from SET
UP to AUTO to MONITOR to
MANUAL.
Green display indicators
glow to signify which display
format is shown.
Red LED Alarm indicator
flashes and beeper sounds
to indicate that an abnormal
system event has occurred.
Alarm messages are displayed
on the LCD. The beeper
mutes after one minute.
DEFROST switch with
LED indicator light controls
the hot gas defrost function.
RUN/STOP switch initiates
the start or stop of the lyophilization process.
MODE switch selects
either manual or automatic
operation.
“Up” and “down” arrows
are used in programming to
change a parameter set point
or scroll through programs or
choices.
ENTER switch is used in programming to enter a selected
set point or program into
memory.
Exclusive feature
44
VACUUM switch with
LED indicator light manually
starts or stops the vacuum
pump.
FreeZone Triad Freeze Dry Systems
®
specifications
™
&
ordering
information
Specifications:
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• Large acrylic door, 1" thick, with neoprene gasket.
• Processing shelf, 12.4" w x 14.5" d (31.5 cm x 36.8 cm). Spacing
between the shelf and top of the chamber accommodates containers
with stoppers up to a maximum height of 148 mm and minimum
height of 31 mm.
• Pneumatic stoppering mechanism that inflates the diaphragm and
lowers the stoppering platen above the shelf. No compressed gas
is required.
• One probe for monitoring sample temperature.
• Stainless steel collector coil capable of removing 1.84 liters of water
in 24 hours and holding 2.5 liters of ice before defrosting.*
• Two 1/3 hp HCFC/CFC-free refrigeration systems, used in series,
to cool the collector to -85° C (-121° F) and work in concert with a
1000-watt heater to cool and heat fluid medium circulating through
channels in the shelf. Fluid temperature may be set from -55° C to
+50° C (-67° to +122° F) or to pre-freeze shelf temperature of -75°
C (-103° F). Microprocessor controls circulating fluid temperature to
±1° C of set point. For samples containing water or acetonitrile. Not
for use with samples containing methanol or ethanol.
• Four left-side mounted neoprene valve ports.
• LCD that displays shelf, sample and collector temperature in ° C or
° F, vacuum in mBar, Pa or Torr. When in Automatic mode, LCD also
displays the program selected, the present segment that is ramping or
holding, time remaining in present segment, and end of program.
• Microprocessor-controlled temperature programming from -55°
C to +50° C (-67° to +122° F) during ramping and holding and
-75° C (-103° F) during pre-freezing; and memory to store five programs, each with a pre-freeze segment plus five additional segments,
for repetition of identical protocols.
• Control panel that includes Run/Stop, Mode, Enter, “Up” arrow,
“Down” arrow, Vacuum, Defrost, and Display switches; green indicator lights for Run/Stop, Automatic and Manual mode, and Set Up,
Automatic, Monitor and Manual display; red LED Alarm indicator;
Stoppering control knob; Vacuum Release valve control knob; and
1/8" OD Back Fill port.
• Red LED Alarm indicator that flashes and beeper sounds to indicate
that an abnormal system event has occurred, including: shelf temperature variation more than ±2° C as measured by the shelf temperature
sensor, collector temperature above -40° C, vacuum pressure changes
more than 0.500 mBar, shelf temperature outside of set point during
ramping, power failure, unevenly loaded shelf during stoppering, and
service vacuum pump (after 1000 hours of vacuum use). Alarm messages are displayed on the LCD. The beeper mutes after one minute.
• Vacuum control valve that maintains set point vacuum level.
• Vacuum break valve that bleeds air into the system when power to
the freeze dryer or vacuum pump is shut off. If a brief power outage
occurs, the freeze dryer will restart and the refrigeration and vacuum
system will resume operation once power is restored. If the power
failure is longer and the collector warms above safe limits, the freeze
dryer will not automatically restart.
FreeZone Triad Freeze Dry System 7400040 and miscellaneous glassware.
• Rear-mounted RS-232 port to transmit data to a user-supplied computer. Transmission intervals may be user-configured for 10, 30, 60,
300 or 600 seconds.
• Hot gas defrost with switch and automatic shut off when refrigerant
reaches +65° C (+149° F) or after 3 hours.
• Stainless steel condensate pan with drain hose.
• Left side-mounted power switch and rear-mounted electrical receptacle for vacuum pump connection.
• Overall dimensions: 28.5" w x 29.5" d x 28.0" h (72.4 cm x 74.9 cm x 71.1 cm).
Models conform to the following standards:
• UL Standard 61010A-1 (230 volt, 60 Hz model).
• CAN/CSA C22.2 No. 1010.1 (230 volt, 60 Hz model).
• CE Conformity marking (230 volt, 50 Hz model).
Option includes:
• Domestic or international electrical configuration.
All models require (not included):
• Vacuum pump with a displacement of at least 98 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Freeze dry glassware if not bulk freeze drying. See pages 60-63.
See page 51 for FreeZone Triad accessories.
Catalog
Electrical
Receptacle & Plug
Shipping
7400040 208/230 volts, 60 Hz, 9.0 A North America, 230 volts 450 lbs. (204 kg)
7400030*
230 volts, 50 Hz, 9.0 A
7400060*
230 volts, 50 Hz, 9.0 A
British (UK)
450 lbs. (204 kg)
7400070*
230 volts, 50 Hz, 9.0 A
China/Australia
450 lbs. (204 kg)
Schuko
*Freeze drying capacity rating will be lower for samples other than plain water.
** International electrical configuration
Exclusive feature
45
450 lbs. (204 kg)
FreeZone Stoppering Tray Dryers
®
Features
Power switch turns all power
to the Tray Dryer on or off.
&
benefits
Three sensor probes monitor
sample temperature, which is
digitally displayed on the LCD.
Stoppering control regulates the
up and down movement of the
shelves while the chamber is
under vacuum. See description
on page 39.
Clear acrylic viewing door
provides complete visibility
of the three process shelves.
Three large shelves, each with
196 square inches of space,
accommodate bulk trays or
batches of serum bottles, vials
or ampules. Samples may be lyophilized and then stoppered, if
desired, on three large adjustable
shelves. See the chart on page 39
for serum bottle capacities.
Chamber pre-freezes samples to
save money and time. Samples
may be frozen on the shelves,
eliminating the need for a separate freezer and product transfer.
1/8" OD backfill port introduces sterile air or inert gas
from an outside source to the
chamber, protecting samples
from atmospheric moisture
and contaminants.
Optional Isolation Valve
7761500 isolates the Stoppering
Tray Dryer from the Freeze Dry
System to shorten time necessary to reestablish working
vacuum levels and to provide a
means for checking end point.
While the researcher loads and
pre-freezes samples on the
shelves, the Isolation Valve may
be closed allowing the Freeze
Dry System’s vacuum and collector to reach working levels.
At the end of lyophilization,
the valve may be closed to test
the rate of vacuum decay in the
Tray Dryer. Rapid decay indicates end point has not been
reached. See page 40 for
ordering information.
RS-232 cable connection port,
located on the back, allows communication of the Stoppering
Tray Dryer with the microprocessor of the Freeze Dry
System when connected via the
interconnect Cable 7353403
included. This communication
permits 1) automatic start up of
the vacuum pump to occur after
time has elapsed in Segment 1
when the Stoppering Tray Dryer
is used in the AUTO mode; 2)
use of one computer to accept
data from both the Stoppering
Tray Dryer and the Freeze
Dry System.
Support stand simplifies connection to FreeZone 6, 12 or
18 Liter Freeze Dry System.
Support stand completes the
connection between the Tray
Dryer attachment port and
the Freeze Dry System of your
choice. The stand elevates the
Tray Dryer above the work surface of the Freeze Dry System
to allow unobstructed access to
the collector compartment or
optional built-in vacuum drying
chamber or shell freezer.
Vacuum release valve control
vents the chamber so the
chamber door may be opened.
This control may also be used
to introduce inert gas into the
chamber when the gas line is
connected to the backfill port.
CE marking. The 230 volt,
50 Hz model conforms to the
CE (European Community)
directives.
46
Separate 1 hp HCFC/CFC-free
refrigeration system and 1000watt heater ensure efficient
cooling and heating of the
shelves. Temperature of fluid
circulating through channels in
the shelves may be set between
-40° C and +40° C (-40° F and
+104° F). A microprocessor
maintains system temperature
within 1° C of set point. The
system uses a non-flammable
refrigerant that contains no
ozone-damaging hydrochlorofluorocarbons (HCFCs) or
chlorofluorocarbons (CFCs).
Automatic control of temperature enhances consistency and
convenience of repetitive protocols. A microprocessor-based
controller permits up to five
different temperature programs
to be stored and repeated, each
using as many as five different
segments. For each segment,
the length of time the temperature should hold and rate at
which the temperature should
be increased or decreased may
be programmed.
ETL listed. Models for operation
on 115 volts, 60 Hz or 230 volts,
60 Hz carry the ETL mark signifying they are certified to UL and
CAN/CSA standards for laboratory equipment.
FreeZone Stoppering Tray Dryers
®
Features
&
benefits
User-Friendly Control Panel
Green RUN/STOP indicator
illuminates steadily while freeze
drying is in progress and turns
off when the programmed cycle
is completed or if the process is
terminated in mid-cycle.
RUN/STOP switch
initiates the start or stop of
the lyophilization process.
LCD prompts the user to set
programming parameters and
displays system and probe
temperatures in ° C or ° F and
vacuum in mBar, Pa or Torr.
When the automatic mode is
selected, the display also indicates which segment of the
program is in progress.
Red LED Alarm indicator flashes and beeper sounds to indicate
that an abnormal system event has occurred, including: system temperature variation more than ±2° C as measured by the system temperature
sensor, vacuum pressure changes more than 0.500 mBar, system temperature outside of set point during ramping, power failure, improper
line voltage supply, and faulty temperature probe. Alarm messages are
displayed on the LCD. The beeper mutes after one minute.
ENTER is used in programming to enter a selected set
point or program into memory.
“Up” arrow is used in
programming to increase a
parameter set point or scroll
through programs or choices.
DISPLAY changes the screen
format from SET UP to AUTO
to MONITOR to MANUAL.
MODE switch selects either
manual or automatic operation.
“Down” arrow is used in
programming to decrease a
parameter set point or scroll
through programs or choices.
Built-in pneumatic mechanism stoppers containers on all three shelves.
The Stoppering Tray Dryer may be
loaded with unstoppered vials or
bottles on all three shelves. Stoppers
should be inserted in vial or bottle
openings in the raised position.
When the stoppering control is activated, atmospheric pressure causes
the diaphragm to expand. Pressure
from the expanding diaphragm
causes the bottom shelf to rise until
the loaded tray makes contact with
the shelf above it.
The diaphragm continues to expand
until all three shelves have made
contact with each other allowing all
vials or bottles to be stoppered under
vacuum.
47
Green display indicators
glow to signify which display
format is shown. If a power
failure occurs during processing, the indicator flashes when
power is restored.
Serum Bottle & Vial Capacity of the
Stoppering Tray Dryer
Size
Catalog
Shelf
No. of
Total
Number Capacity ShelvesCapacity
2 ml
3 ml
5 ml
5 ml
10 ml
10 ml
20 ml
30 ml
50 ml
100 ml
125 ml
7575010430
7575210483
7573010255
7762300255
7573210195
7762600255
7573410132
757361086
757381072
757401042
757421036
3
3
3
3
3
3
3
3
2
2
1
1290
1449
765
765
585
765
396
258
144
84
36
FreeZone Stoppering Tray Dryers
®
specifications
&
ordering
Information
Specifications:
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• Acrylic door, 1" thick.
• Three processing shelves, each 16.5" w x 12" d (41.9 cm x 30.5 cm)
with 196 square inches of area. Spacing between the shelves accommodates containers with stoppers up to a maximum height of 75 mm
and minimum height of 38 mm when three shelves are used, a maximum height of 107 mm and minimum height of 56 mm when two
shelves are used, and a maximum height of 196 mm and minimum
height of 114 mm when one shelf is used.
• Three probes for monitoring sample or shelf temperature.
• 3" diameter outlet, located on the bottom of the tray dryer cabinet,
for connection to a FreeZone 6, 12 or 18 Liter Freeze Dry System
(freeze dryer is required and not included).
• 1 hp HCFC/CFC-free refrigeration system and 1000-watt electric
heater for cooling and heating fluid medium circulating through channels in the shelves from -40° C to +40° C (-40° to +104° F). Microprocessor controls circulating fluid temperature to ±1° C of set point.
• LCD that displays system and probe temperatures in ° C or ° F,
vacuum in mBar, Pa or Torr, when in Monitor mode; and additionally, when in Auto mode, the segment of the program that is in progress, time remaining in present segment, and end of program.
• Microprocessor-controlled temperature ramp and hold programming
from -40° C to +40° C (-40° to +104° F) and memory to store five
programs and repetition of identical protocols.
• Control panel that includes Run/Stop, Mode, “Up” arrow, “Down”
arrow, Enter and Display switches; green indicator lights for Run/Stop,
Automatic and Manual mode, and Set Up, Automatic, Monitor and
Manual display; red LED Alarm indicator; Stoppering control knob;
Vacuum Release valve control knob; and 1/8" OD Back Fill port.
• Red LED Alarm indicator that flashes to indicate that an abnormal
system event has occurred, including: system temperature variation
more than ±2° C as measured by the system temperature sensor,
vacuum pressure changes more than 0.500 mBar, system temperature outside of set point during ramping, power failure, improper line
voltage supply, and faulty temperature probe. Alarm messages are
displayed on the LCD. The beeper mutes after one minute.
• Rear-mounted RS-232 cable connection port and interconnect cable
for communication of the Tray Dryer with the Freeze Dry System.
• Side-mounted power switch.
• Overall dimensions: 33.3" w x 24.6" d x 27.1"47p7.409 h
(82.0 cm x 62.4 cm x 68.8 cm).
FreeZone Stoppering Tray Dryer 7948020, 6-Port Tray Dryer Manifold 7726500 and
FreeZone 12 Liter Freeze Dry System 7754040.
All models require (not included):
• FreeZone 6, 12 or 18 Liter Freeze Dry System. The FreeZone
Stoppering Tray Dryer and Freeze Dry System may be ordered as
separate components or together as one catalog number on selected
models of FreeZone 6 Liter Benchtop Freeze Dry Systems or FreeZone
6 or 12 Liter Freeze Dry Systems. See pages 24-32.
• Vacuum pump with a displacement of at least 98 liters per minute,
0.002 mBar ultimate pressure and fitting suitable for 3/4" ID vacuum
hose. See pages 56-58.
• Freeze dry glassware if not bulk freeze drying. See pages 62-63.
Catalog
Number
Models conform to the following standards:
• UL Standard 61010-1 (60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (60 Hz models).
• CE Conformity marking (230 volts, 50 Hz models).
Option includes:
Electrical
Requirements
Plug
Type
7948020
115 volts, 60 Hz, 16.0 A
115 volts, 20 amps
422 lbs. (191 kg)
7948040
230 volts, 60 Hz, 9.0 A
North America, 230 volts
422 lbs. (191 kg)
7948030*
230 volts, 50 Hz, 9.0 A
Schuko
422 lbs. (191 kg)
7948060*
230 volts, 50 Hz, 9.0 A
British (UK)
422 lbs. (191 kg)
7948070*
230 volts, 50 Hz, 9.0 A
China/Australia
422 lbs. (191 kg)
• Domestic or international electrical configuration.
See page 51 for Stoppering Tray Dryer accessories.
* International electrical configuration
Exclusive feature
48
Shipping
Weight
FreeZone Bulk Tray Dryers
®
Features
Power switch turns all power
to the Tray Dryer on or off.
&
Vacuum release valve control
vents the chamber so the
chamber door may be opened.
benefits
Three shelves, each with a 200watt heater, provide ample room
for bulk samples or samples in
serum bottles or vials. Each shelf
is 12.7" w x 16.6" d (32.2 cm x
42.2 cm) to provide 210 square
inches of area. Each shelf may be
set above sample temperature up
to +60° C (+140° F). A microprocessor maintains system temperature within 3° C of set point.
(Shelves are not cooled. The only
cooling is from the frozen sample.)
The chamber can accommodate
two additional shelves. See page
51 for ordering information.
Clear acrylic viewing door
provides visibility of the
chamber interior.
RS-232 cable connection port,
located on the back, allows
communication of the Bulk
Tray Dryer with an IBMcompatible, user-supplied
computer. Parameters that may
be monitored include shelf set
point temperature, actual temperature of each shelf, run time
and operating status. RS-232
Cable is required (not
included). See page 64.
Support stand simplifies connection to FreeZone 6, 12 or
18 Liter Freeze Dry System.
Support stand completes the
connection between the Tray
Dryer attachment port and
the Freeze Dry System of your
choice. The stand elevates the
Tray Dryer above the work surface of the Freeze Dry System
to allow unobstructed access to
the collector compartment or
optional built-in vacuum drying
chamber or shell freezer.
ETL listed. All 115 volt models
carry the ETL mark signifying
they are certified to UL and
CAN/CSA standards for laboratory equipment.
Three sensor probes monitor
sample temperature, which is
digitally displayed on the LCD.
Connections are provided for
two additional sensor probes
(Additional sensors are sold
separately and as a component
to Heated Shelves with Sensors).
Six-Port Manifold (models 7806021 and 7806031) increases flexibility and
capacity of the FreeZone System. Six valves, which accommodate either
1/2" or 3/4" flask adapters, allow connection of flasks and other freeze dry
glassware so that samples attached to the manifold and in the Tray Dryer
may be lyophilized simultaneously.
LCD displays set point temperature, actual temperatures and
Run (“R”) or Stop (“S”) mode.
CE marking. All 230 volt
models conform to the
CE (European Community)
directives.
2.2”
(55.9 mm)
2.2”
(55.9 mm)
5.1”
(129.5 mm)
13.8”
2.2”
(350.5 mm)
(55.9 mm)
2.2”
(55.9 mm)
5.1”
(129.5 mm)
RUN/STOP switch initiates the
Bulk Tray Dryer to control the
temperature of the shelves at
the set point temperature.
2.2”
“Up” and “down” arrows are
used in programming to change
the set point temperature above
sample temperature to +60° C
(+140° F). The chamber is not
cooled. The only cooling is from
the frozen sample.
(55.9 mm)
49
FreeZone Bulk Tray Dryers
®
specifications
&
ordering
Information
Specifications:
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• Acrylic door, 1" thick.
• Three shelves, each 12.7" w x 16.6" d (32.2 cm x 42.2 cm) to provide
210 square inches of area. Chamber may accommodate two additional
shelves (sold separately).
• 200-watt heater on each shelf for heating to +60° C (+140° F).
A microprocessor maintains system temperature within 3° C of set
point. (Shelves are not cooled by the Bulk Tray Dryer. The only
cooling is from the frozen sample.)
• Three sensor probes for monitoring sample or shelf temperature.
Connections for two additional sensors are provided (additional
sensors sold separately).
• LCD that displays set point and temperature (°C) of each shelf and
“R” for Run mode or “S” for Stop mode.
• Control panel with Run/Stop, “Up” arrow and “Down” arrow switches.
• Vacuum release valve for venting the chamber so the chamber door
may be opened.
• Rear-mounted RS-232 cable connection port for communication
with a user-supplied IBM-compatible computer. Monitored parameters are shelf set point temperature, actual temperature of each shelf,
run time and operating status. RS-232 Cable is required (not
included). See page 64.
• Side-mounted power switch.
• Integral Support Stand completes the connection between the Tray
Dryer attachment port and the FreeZone 6, 12 or 18 Liter Freeze Dry
System of your choice. The stand elevates the Tray Dryer above the
work surface of the Freeze Dry System to allow unobstructed access to
the collector compartment.
• Overall dimensions: 27.1" h x 32.2" w x 21.5" d (69 cm x 82 cm x 55 cm).
FreeZone Bulk Tray Dryer with 6-Port Manifold 7806021 and FreeZone 12 Liter Freeze
Dry System with Teflon-Coated Collector 7754041.
Options include:
• Pre-installed 6-Port Tray Dryer Manifold 7726500.
• Domestic or international electrical configuration.
Models conform to the following standards:
All models require (not included):
• UL Standard 61010-1 (115 volt models).
• CAN/CSA C22.2 No. 61010.1 (115 volt models).
• CE Conformity marking (230 volt models).
Catalog
Number
Electrical
Requirements
• FreeZone 6, 12 or 18 Liter Freeze Dry System. See pages 24-32.
• Vacuum pump with a displacement of at least 98 liters per
minute, 0.002 mBar ultimate pressure, and fitting suitable for
3/4" ID vacuum hose. See pages 56-58.
• Freeze dry glassware if not bulk freeze drying. See pages 62-63.
Plug
Type
6-Port
Manifold
Shipping
Weight
7806020
7806021
115 volts, 60 Hz, 8.0 A
115 volts, 60 Hz, 8.0 A
115 volts, 15 amps
115 volts, 15 amps
•
7806040
230 volts, 60 Hz, 4.0 A
North America, 230 volts
262 lbs.(119 kg)
7806041
230 volts, 60 Hz, 4.0 A
North America, 230 volts
262 lbs. (119 kg)
7806030*
7806031*
7806060*
262 lbs. (119 kg)
262 lbs. (119 kg)
230 volts, 50 Hz, 4.0 A
•
Schuko
262 lbs. (119 kg)
230 volts, 50 Hz, 4.0 A
Schuko
262 lbs. (119 kg)
230 volts, 50 Hz, 4.0 A
•
British (UK)
7806061*
230 volts, 50 Hz, 4.0 A
British (UK)
262 lbs. (119 kg)
7806070*
230 volts, 50 Hz, 4.0 A
•
China/Australia
7806071*
230 volts, 50 Hz, 4.0 A
China/Australia
262 lbs. (119 kg)
See page 51 for Bulk Tray Dryer accessories.
Exclusive feature
50
•
* International electrical configuration
262 lbs. (119 kg)
262 lbs. (119 kg)
FreeZone Triad, Stoppering Tray Dryers & Bulk Tray Dryers
®
™
accessories
7756100 Tray with
Slide-Out Bottom
12.0" w x 14" d (30.5
cm x 35.6 cm). Stainless
steel tray has separate
bottom that slides out to
allow glassware containers
direct contact with shelf.
Shipping weight 5 lbs.
(2.3 kg)
7761500 Isolation Valve
Isolates the Tray Dryer from the
Freeze Dry System to shorten the time
necessary to reestablish working vacuum levels and to provide a means
for determining end point. Consists
of a valve, valve handle, clamps, couplings and installation instructions.
Mounts underneath the support stand
included with the Tray Dryer. May be installed before or after the Tray
Dryer is installed on the Freeze Dry System. For use with Stoppering
Tray Dryers 7806020, 7806040 and 7806030 and Bulk Tray Dryers
7806060 and 7806070. The Isolation Valve and 6-Port Tray Dryer
Manifold 7726500 may not be field installed together.* Shipping weight
5 lbs. (2.3 kg)
7439300 Microcentrifuge Tube Holder.
3.0" w x 2.25" d x 1.0" h (7.6 cm x 5.7 cm
x 2.5 cm), anodized aluminum block with
twelve bore holes that accommodate
1.7 ml microcentrifuge tubes. Holder may
be placed on any flat freeze drying surface
such as inside Clear Chambers or the
built-in vacuum drying chamber of
FreeZone Console Systems; or on FreeZone Stoppering or Bulk Tray
Dryer Shelves, Product Shelves, or Heated Product Shelves. One each.
Microcentrifuge tubes are not included. Shipping weight 0.6 lb. (0.3 kg)
For FreeZone Stoppering Tray Dryers
7756300 Shelf Spacers
9.0" w x 13.0" d x 2.5" h (22.9 cm x 33.0 cm x 6.4 cm). Stainless steel
spacers placed on one or two empty shelves assist stoppering of partial
loads of small vials or bottles. One pair. Shipping weight 3 lbs. (1.4 kg)
7726500 6-Port Tray Dryer Manifold
30.0" w x 16.5" d x 7.0" h (76.2 cm x 41.9 cm x 17.8 cm). Six valves
provide the flexibility to connect flasks and other freeze dry glassware to
the Freeze Dry System with Tray Dryer. Valves accommodate either 1/2"
or 3/4" flask adapters. Mounts to the support stand included with the
FreeZone Stoppering and Bulk Tray Dryer. May be field installed before or
after the Tray Dryer is installed on the Freeze Dry System. The 6-Port Tray
Dryer Manifold and Isolation Valve 7761500 may not be field installed
together.* Included with Bulk Tray Dryer 7806021, 7806041, 7806031,
7806061 and 7806071. Shipping weight 19 lbs. (8.6 kg)
For FreeZone Bulk Tray Dryers
Heated Shelves with Sensors
12.7" w x 16.6" d (32.2
cm x 42.2 cm). Stainless
steel shelves include 200watt heater and sensor
probe. FreeZone Bulk Tray
Dryers include three and
can accommodate two
additional Heated Shelves
with Sensors. The Sensor,
included with the Heated
Shelf or sold separately, may be used to monitor sample or shelf temperature, which is displayed on the LCD of the FreeZone Bulk Tray Dryer.
7516200 Support Grid
7.0" w x 7.0" d (17.8 cm x 17.8 cm),
has stainless steel tray with removable plastic grid to provide support
for Stoppering Ampules and other
small specimen containers. Grid holds
144 containers of 12 mm diameter.
Shipping weight 2.5 lbs. (1.1 kg)
7756200 Bulk Tray
11.5" w x 15.0" d x 0.8" h
(29.2 cm x 38.1 cm x 2.0 cm).
Stainless steel tray contains liquids
for pre-freezing and bulk drying.
Shipping weight 3 lbs. (1.4 kg)
* Contact Labconco for ordering information on models with factory-installed 6-Port
Tray Dryer Manifold and Isolation Valve.
51
Catalog
Description
Number
7760800
Heated Shelf with Sensor for
115 volt, 50/60 Hz operation
7760801
Heated Shelf with Sensor for
230 volt, 50/60 Hz operation
Shipping
Weight
15 lbs. (6.8 kg)
7754100
0.5 lb. (0.2 kg)
Sensor only
15 lbs. (6.8 kg)
Drying Accessories
Use the key below to select the drying chamber or manifold that will fit the FreeZone System you have selected.
1 = Fits any FreeZone 1 Liter Freeze Dry System
2.5 = Fits any FreeZone 2.5 Liter Freeze Dry System
4.5 = Fits any FreeZone 4.5 Liter Freeze Dry System
4.5A= Fits any FreeZone 4.5 Liter Freeze Dry System
with Attachment Port Lid Accessory 7762800 attached (sold separately)
4.5P= Fits any FreeZone Plus 4.5 Liter Cascade Freeze Dry System
6 = Fits any FreeZone 6 Liter Freeze Dry System
12 = Fits any FreeZone 12 Liter Freeze Dry System
18 = Fits any FreeZone 18 Liter Freeze Dry System
7522800 12-Port
Drying Chamber
9.75" h x 8.0" diameter
(24.8 cm x 20.3 cm), type
304 stainless steel, 1/2"
thick acrylic lid with neoprene gasket, complete
with 12 neoprene valves
with molded plastic knobs that accommodate both 1/2" and 3/4" adapters
for connection of flasks. Shipping weight 11 lbs. (5 kg) 1, 2.5, 4.5P, 6, 12, 18
7522900 16-Port
Drying Chamber
13.0" h x 13.0" diameter
(33 cm x 33 cm), type
304 stainless steel, 3/4"
thick acrylic lid with neoprene gasket, complete
with 16 neoprene valves
with molded plastic knobs that accommodate both 1/2" and 3/4" adapters
for connection of flasks. Shipping weight 21 lbs. (9.5 kg) 4.5P, 6, 12, 18
Clear Chambers
with Valves
Provide visibility into the
acrylic chamber during
bulk drying as well as
accommodate connection
of freeze dry glassware to
eight valves. Include clear
acrylic cylinder; anodized aluminum lid; eight neoprene valves with molded plastic knobs for use with both 1/2" and 3/4" adapters; clear acrylic
attachment port lid with 3" diameter opening and neoprene gasket.
Clear Chambers
Provide visibility into the
chamber during bulk
drying. Include clear
acrylic lid with neoprene
gasket, vacuum release
valves and pass-through
for electrical transformer
cords, clear acrylic attachment port lid with 3" diameter opening and
neoprene gasket.
Catalog
Dimensions
Accommodate
For Shipping
use with:
Wt.
Catalog
Dimensions
Accommodate
For Shipping
use with:
Wt.
Cylinder
7443500 9.25" dia. x 9.75" h
(23.5 cm x 24.4 cm)
1, 2.5, 4.5,
6, 12, 18
13.5 lbs.
(5.9 kg)
Cylinder
7442900 9.25" dia. x 9.75" h
(23.5 cm x 24.4 cm)
1, 2.5, 4.5,
6, 12, 18
13.5 lbs.
(5.9 kg)
15 lbs.
(6.8 kg)
Overall
10.3" dia. x 13.1" h
(26.2 cm x 33.3 cm)
Cylinder
7867000 12.0" dia. x 12.6" h
(30.5 cm x 36.6 cm)
Product Shelves 7442100
Heated Product Shelves
7418000, 7418001,
7509200 and 7509201
Product Shelves 7442100
and 7441700
6, 12, 18
15 lbs.
(6.8 kg)
Overall
14.6" dia. x 12.2" h
(37.1 cm x 31.0 cm)
Cylinder
7444000 12.0" dia. x 12.6" h
(30.5 cm x 38.0 cm)
Product Shelves 7442100
Heated Product Shelves
7509200, 7509201,
7418000 and 7418001
Product Shelves 7442100
and 7441700
Heated Product Shelves
Overall
7418000, 7418001, 7509400,
17.3" dia. x 15.0" h 7509401, 7509200 and 7509201
(43.9 cm x 38.1 cm)
6, 12, 18
Overall
Heated Product Shelves
13.6" dia. x 16.3" h 7418000, 7418001, 7509400,
(34.5 cm x 41.4 cm) 7509401, 7509200 and 7509201
52
Drying Accessories
Clear Stoppering Chambers
23.0" h x 13.5" diameter (58.4 cm
x 34.3 cm). Provide an economical
means of stoppering serum bottles
under original vacuum. Consists of
clear acrylic cylinder, stainless steel
top plate, two 10.0" diameter aluminum shelves and low voltage transformer with variable heat control to
+40° C (±104° F) and electrical cord
with plug. Clear, 3/4" thick acrylic
lid has neoprene gasket, vacuum
release valve and stoppering handle.
Also include 3/4" thick, clear acrylic
attachment port lid with 3" diameter opening; neoprene gasket and
pass-through for electrical transformer cord. Serum bottles or vials with
stoppers in the raised position may be loaded on the two shelves. After
freeze drying is complete, the stoppering handle may be turned, slowly
moving the top plate downward until it makes contact with the sample
containers on the top shelf and the sample containers on the bottom shelf
make contact with the top shelf. Pressure from the top plate and shelf
push the stoppers into the containers, stoppering them under vacuum.
Accommodate small containers from 2 to 5 milliliters.
Catalog
Number
Electrical
Requirements
For
use with:
Shipping Weight
7868020
115 volts, 50/60 Hz
6, 12, 18
30 lbs. (13.6 kg)
7868030
230 volts, 50/60 Hz
6, 12, 18
30 lbs. (13.6 kg)
Product Shelves Accommodate bulk samples, microtiter plates, vials or serum bottles.
Heated Product Shelves with Variable Heat Control
Consist of three aluminum shelves with 1/4" rims, three stainless steel support rods, nine clips for shelf height adjustment, low voltage trans-former
with variable heat control to +40° C (+104° F), and three rubber feet.
Product Shelves
Consist of three aluminum shelves with 1/4" rims, three stainless steel
support rods, nine clips for shelf height adjustment, and three rubber feet.
Product Shelves
Catalog
Number
7442100
7441700
Shelves
For use with: Dimensions
9.4" h. x 6.25" dia. (23.9 cm x 15.9 cm)
12.2" h. x 9.9" dia. (31.0 cm x 25.1 cm)
Chambers 7522900, 7442900, 7443500, 7444000, 7522800 and 7867000
Chambers 7522900, 7444000 and 7867000
Shipping
Weight
1.5 lbs. (0.7 kg)
2.0 lbs. (0.9 kg)
Heated Product Shelves with Variable Heat Control
Catalog
Number
Shelves
Dimensions
Electrical
For use with: Requirements
Shipping
Weight
7509200
6.5" dia. x 9.0" h (15.9 cm x 22.9 cm)
115 volts, 50/60 Hz
Chambers 7522800, 7522900, 7443500, 7444000, 7442900 and 7867000
13 lbs. (5.9 kg)
7418000
7.25" dia. x 9.4" h (18.1 cm x 23.9 cm)
115 volts, 50/60 Hz
Chambers 7522900, 7443500, 7444000, 7442900 and 7867000
14 lbs. (6.4 kg)
7509400
10.0" dia. x 11.75" h (24.5 cm x 29.8 cm)
115 volts, 50/60 Hz
Chambers 7522900, 7444000 and 7867000
15 lbs. (6.8 kg)
7509201*
6.5" dia. x 9.0" h (15.9 cm x 22.9 cm)
230 volts, 50/60 Hz
Chambers 7522800, 7522900, 7443500, 7444000, 7442900 and 7867000
13 lbs. (5.9 kg)
7418001*
7.25" dia. x 9.4" h (18.1 cm x 23.9 cm)
230 volts, 50/60 Hz
Chambers 7522900, 7443500, 7444000, 7442900 and 7867000
14 lbs. (6.4 kg)
7509401*
10.0" dia. x 11.75" h (24.5 cm x 29.8 cm)
230 volts, 50/60 Hz
Chambers 7522900, 7444000 and 7867000
15 lbs. (6.8 kg)
* International electrical configuration
53
Drying Accessories
7522200 4-Port
Manifold
9.0" h x 8.7" w x 8.7"
d (22.9 cm x 22.1 cm x
22.1 cm), type 304 stainless steel, complete with
four neoprene valves with
molded plastic knobs that
accommodate both 1/2"
and 3/4" adapters for connection of flasks. Shipping
weight 2 lbs. (1 kg)
1, 2.5, 4.5A, 4.5P
7522500 20-Port
Manifold with
Support Shelves
10.0" h x 29.6" w x 24.2" d
(25.4 cm x 75.2 cm x
61.5 cm), type 304 stainless steel, complete with
twenty neoprene valves
with molded plastic
knobs that accommodate
both 1/2" and 3/4" adapters and two adjustable aluminum support shelves
with stainless steel rods. Shipping weight 15 lbs. (6.8 kg) 6, 12, 18
7548000 24-Port
Two-Tier Manifold
20.0" h x 26.4" w x 10.6" d
(50.8 cm x 67.1 cm x 26.9 cm),
type 304 stainless steel, complete with 24 neoprene valves
with molded plastic knobs that
accommodate both 1/2" and 3/4"
adapters for connection of flasks.
Shipping weight 20 lbs. (9.1 kg)
6, 12, 18
7868500 48-Port Ampule Manifold
28.6" h x 5.0" w x 5.0" d (72.7 cm x 12.7 cm x
12.7 cm), type 304 stainless steel, tree-type, with
48 each 1/4" OD pipe stems that accommodate
gum rubber or similar tubing to fit over any
Labconco Ampule. Tubing is not included.
Shipping weight 12 lbs. (5.4 kg)
1, 2.5, 4.5P, 6, 12, 18
7522300 20-Port Manifold
11.0" h x 27.4" w x 8.7" d (27.9 cm x 68.5 cm x 22.1 cm), type 304
stainless steel, complete with 20 neoprene valves with molded plastic
knobs that accommodate both 1/2" and 3/4" adapters for connection of
flasks. Shipping weight 15 lbs. (6.8 kg) 1, 2.5, 4.5A, 4.5P, 6, 12, 18
7762800 Attachment Port Lid
10.38" diameter (26.4 cm),
replaces the lid to the drying chamber on FreeZone 4.5
Liter Systems, to permit use of
the 4-Port Manifold 7522200,
20-Port Manifold 7522300,
48-Port Manifold 7868500 or Clear Chamber 7867000. Includes 3/4"
thick, clear acrylic cover with 3" diameter opening and gasket and acrylic
plug with gasket (for periods of non-use). Shipping weight 2.0 lbs. (0.9 kg)
7522400 10-Port Manifold with Support Shelf
10.0" h x 29.6" w x 14.6" d (25.4 cm x 75.2 cm x 37.1 cm), type 304
stainless steel, complete with ten neoprene valves with molded plastic
knobs that accommodate both 1/2" and 3/4" adapters and adjustable
aluminum support shelf with stainless steel rods. Shipping weight 11 lbs.
(5 kg) 6, 12, 18
54
Secondary Traps
7394800
Liquid Nitrogen
Secondary Trap
For processing
samples with ultra
low eutectic points.
Secondary Trap connects in series with
a freeze dry system
and vacuum pump
to prevent contaminants from migrating into the vacuum pump. After pulling a vacuum, liquid nitrogen may
be introduced via the liquid nitrogen port. Liquid nitrogen cools to -196°
C (-321° F) to trap contaminants with low eutectic points. The well
may be defrosted and the liquid drained from the drain hose. Glacier
white epoxy-coated steel construction. Two valves may be opened (trap)
or closed (by-pass). Opened valves allow gaseous contaminants to be
trapped in the liquid nitrogen well. Closed valves allow gaseous contaminants to by-pass the well during defrosting and draining. 3/4" OD inlet
and outlet connections. Includes an insulated filler tube for connection
to a user-supplied liquid nitrogen tank; 20" wire-reinforced PVC tubing,
3/4" ID; and two clamps. Liquid nitrogen is required (not included).
Shipping weight 24 lbs. (10.9 kg)
7772000 Soda Acid Trap
Secondary trap connects in series with freeze dry system and vacuum
pump to prevent migration of corrosive chemicals into pump interior.
Clear acrylonitrile body allows visual check of color indicating media.
Media changes from white to blue when exhausted. 3/4" OD inlet and
outlet connections. Includes 20" wire-reinforced PVC tubing, 3/4" ID,
and one clamp. Shipping weight 12 lbs. (5.4 kg)
7772100 Replacement Cartridge for Soda Acid Trap 7772000
Shipping weight 4 lbs. (1.8 kg)
Dry Ice
Secondary Traps
For processing
samples with low
eutectic points.
Traps connect in
series with a freeze
dry system and
vacuum pump to
prevent contaminants from migrating into the vacuum
pump. An insulated
well, when dry ice and solvent are added, cools to approximately -75° C
(-103° F). When used alone, Dry Ice Secondary Traps may serve as an
inexpensive collector. Simply connect a sample directly to the incoming
port and add a vacuum pump to the outgoing port. Dry ice and solvent, such as alcohol, are required (not included).
7772500 Activated Carbon Solvent Trap
Secondary trap connects in series with freeze dry system and vacuum
pump to prevent migration of organic solvents into pump interior.
Cartridge contains 11 ounces of activated carbon media. 3/4" OD inlet
and outlet connections. Includes 20" wire-reinforced PVC tubing, 3/4"
ID, and one clamp. Shipping weight 12 lbs. (5.4 kg)
7772600 Replacement Cartridge for Activated Carbon Solvent Trap
Shipping weight 4 lbs. (1.8 kg)
Catalog
Number
Dimensions
(h x diameter)
Inlet/Outlet Connections
Well
Volume
Ice Trapping
Capacity
Shipping
Weight
7538000
9.75" x 7.8" (24.8 x 19.8 cm)
3/4" OD
3.10 liters
900 ml
9 lbs. (4.1 kg)
7538200*
7538400*
9.75" x 7.8" (24.8 x 19.8 cm)
7.8" x 6.6" (19.8 x 16.8 cm)
1/2" OD
1/2" OD
3.10 liters
1.92 liters
900 ml
200 ml
9 lbs. (4.1 kg)
5 lbs. (2.3 kg)
* Not for use with FreeZone Systems in this catalog.
55
Rotary Vane Vacuum Pumps
Rotary Vane Vacuum Pumps provide the performance required for good
freeze drying results and fit easily into the cabinets of FreeZone console
models. Belt driven pumps of equivalent performance are also suitable;
however, due to the large size of these pumps, they may not fit into the
FreeZone System’s cabinet.
Use the Selection Guide below to find the recommended Combination
Rotary Vane/Diaphragm Pump or General Purpose Rotary Vane Vacuum
Pump based on your sample type and FreeZone System’s electrical configuration.
Selection Guide
FreeZone
Freeze Dry System
1 Liter Benchtop
7740020, 7740021
7740030, 7740031, 7740040, 7740041,
7740060, 7740061, 7740070, 7740071
Sample
Type
Recommended Vacuum Pump(s)
With 115 volt plug
See
With 230 volt reverse IEC plugPage
Aqueous
147210058
Acids and/or Solvents
758400057
Aqueous 773940258
Acids and/or Solvents
758400257
2.5 Liter Benchtop, Cascade Benchtop & Console
7420020, 7420021, 7670020, 7670021, 7670520, 7670521Aqueous
147210058
Acids and/or Solvents
758400057
7420030, 7420031, 7420040, 7420041, 7420060, 7420061,Aqueous 773940258
7420070, 7420071, 7670030, 7670031, 7670040, 7670041,
Acids and/or Solvents
758400257
7670060, 7670061, 7670070, 7670071, 7670530, 7670531,
7670540, 7670541, 7670560, 7670561, 7670570, 7670571
2.5 Liter Cascade Triad
Aqueous 7739402
58
7400030, 7400040, 7400060, 7400070
Acids and/or Solvents
7584002
59
4.5 Liter Benchtop & Console, Cascade Benchtop &
Console, -105° C Benchtop
7382020, 7382021, 7386020, 7386021, 7387020,Aqueous
147210058
7387021, 7750020, 7750021, 7751020, 7751021
Acids and/or Solvents
758400057
7382030, 7382031, 7382040, 7382041, 7382060, 7382061,Aqueous 773940258
7382070, 7382071, 7386030, 7386031, 7386040, 7386041,
Acids and/or Solvents
758400257
7386060, 7386061, 7386070, 7386071, 7387030, 7387031,
7387040, 7387041, 7387060, 7387061, 7387070, 7387071,
7750030, 7750031, 7750040, 7750041, 7750060, 7750061,
7750070, 7750071, 7751030, 7751031, 7751040, 7751041,
7751060, 7751061, 7751070, 7751071
6 Liter Benchtop & Console
7752020, 7752021, 7753020, 7753021, 7753522, 7753524,Aqueous
146770058
7758020, 7758021, 7758520, 7758521, 7758522, 7758524,
Acids and/or Solvents
758400057
7934020, 7934021, 7934022, 7934024, 7934026, 7934027
7752030, 7753031, 7752040, 7752041, 7752060, 7752061,Aqueous 773940358
7752070, 7752071, 7753030, 7753031, 7753032, 7753034,
Acids and/or Solvents
758400257
7753036, 7753037, 7753040, 7753041, 7753042, 7753044,
7753046, 7753047, 7753060, 7753061, 7753062, 7753064,
7753066, 7753067, 7753070, 7753071, 7753072, 7753074,
7753076, 7753077, 7753532, 7753534, 7753542, 7753544,
7753562, 7753564, 7753572, 7753574, 7758530, 7758531,
7758532, 7758534, 7758540, 7758541, 7758542, 7758544,
7758560, 7758561, 7758562, 7758564, 7758570, 7758571,
7758572, 7758574, 7934030, 7934031, 7934032, 7934034,
7934036, 7934037, 7934040, 7934041, 7934042, 7934044,
7934046, 7934047, 7934060, 7934061, 7934062, 7934064,
7934066, 7934067, 7934070, 7934071, 7934072, 7934074,
7934076, 7934077
12 Liter Console & Cascade Console
7754030, 7754031, 7754032, 7754034, 7754036, 7754037,
7754040, 7754041, 7754042, 7754044, 7754046, 7754047,Aqueous
7754060, 7754061, 7754062, 7754064, 7754066, 7754067,
Acids and/or Solvents
7754070, 7754071, 7754072, 7754074, 7754076, 7754077,
7759030, 7759031, 7759032, 7759034, 7759040, 7759041,
7759042, 7759044, 7759060, 7759061, 7759062, 7759064,
7759070, 7759071, 7759072, 7759074, 7960030, 7960031,
7960032, 7960034, 7960036, 7960037, 7960040, 7960041,
7960042, 7960044, 7960046, 7960047, 7960060, 7960061,
7960062, 7960064, 7960066, 7960067, 7960070, 7960071,
7960072, 7960074, 7960076, 7960077
18 Liter Console
7755030, 7755031, 7755032, 7755034, 7755036, 7755037,Aqueous
7755040, 7755041, 7755042, 7755044, 7755046, 7755047,
Acids and/or Solvents
7755060, 7755061, 7755062, 7755064, 7755066, 7755067,
7755070, 7755071, 7755072, 7755074, 7755076, 7755077
56
7739403
58
758400257
7739403
58
758400257
Combination Rotary Vane/Diaphragm Vacuum Pumps
VACUUBRAND HYBRID* Vacuum Pumps
• Environmentally-friendly. Pump oil lasts up to 10 times longer than in
conventional rotary vane pumps under virtually all conditions. Fewer
oil changes conserves resources.
• Designed for use with acids and other harsh chemicals including TFA,
TFA by-products, acetonitrile, HBe and HNO3 present in samples such
as HPLC-prepared and peptide purified materials.
• Ultimate vacuum (partial pressure) 2 x 10-3 mBar (1.5 micron)
• Compatible with FreeZone Freeze Dry Systems and CentriVap®
Centrifugal Concentrators.
• Pressure control valve compensates for the different volumes displaced
by the two pumps.
• Combination pump system consists of a two-stage rotary vane pump
and two-stage, chemically-resistant diaphragm pump. The rotary vane
pump provides the deep vacuum required for good freeze drying
results and other evaporation needs. These pumps have the vacuum
capabilities of a rotary vane pump combined with the solvent and acid
handling capabilities of a PTFE** diaphragm pump.
• Glass separator captures downstream condensate vapors.
• 3/4" OD inlet adapter.
• Include one liter bottle of vacuum pump oil, power switch, power
cord and plug.
• Low maintenance, longer lasting. The diaphragm pump removes the
condensable vapors in the rotary vane pump before they can contaminate the oil, thus extending the life of the oil and ultimately the life
of the pump.
Catalog
Electrical
Number
Configuration
7584000
7584002
Displacement
At 60 Hz (50 Hz)
liter/minute
115 volts, 60 Hz, 5.1 A
115
Includes 115 volt NEMA 5-15P plug.
230 volts, 50/60 Hz, 2.7 A
Includes 230 volt reverse IEC plug.
*VACUUBRAND HYBRID™ is a trademark of VACUUBRAND GMBH + CO KG.
115
(98)
** Polytetrafluoroethylene
57
Dimensions
w x d x h
inches (cm)
Shipping
Weight
lbs. (kg)
20.0 x 12.0 x 9.1
(51.0 x 30.5 x 23.0)
66 (30 kg)
20.0 x 12.0 x 9.1
(51.0 x 30.5 x 23.0)
66 (30 kg)
Rotary Vane Vacuum Pumps & Vacuum Pump Accessories
• Include four each one liter bottles of vacuum pump oil and one
exhaust filter with oil mist and odor filter elements.
• Retractable lifting handle (Models 1472100, 7739400 and 7739402).
• Lifting bracket (Models 1467700, 7739401 and 7739403).
Vacuum Pump Accessories
1988000 Vacuum Pump Oil. One liter bottle. Replacement oil for
General Purpose Vacuum Pumps 1472100, 7739400, 7739402, 1467700,
7739401 and 7739403. Shipping weight 2 lbs. (1 kg)
1472200 Inlet Filter. For General Purpose Vacuum Pumps 1472100,
7739400, 7739402, 1467700, 7739401 and 7739403. Prevents oil back
streaming from the pump and protects the pump from damage from
submicron particles. Includes filter assembly and one filter cartridge. Life
approximately 1000 hours at 1.33 x 10-2 mBar (10 microns) vacuum.
Shipping weight 1 lb. (0.5 kg)
1472500 Replacement Inlet Filter Cartridge. For 1472200. Shipping
weight 0.5 lb. (0.2 kg)
1473400 Replacement Exhaust Filter. For General Purpose Vacuum
Pumps 1472100, 7739400, 7739402, 1467700, 7739401 and 7739403.
Removes oil mist and odor from pump exhaust. Ducting to outside not
required. Includes filter assembly, one oil mist filter cartridge and one
odor filter cartridge. Oil mist filter cartridge life is approximately one
year and odor filter cartridge life is approximately six months at 1.33 x
10-2 mBar (10 microns) vacuum. Shipping weight 1 lb. (0.5 kg)
General Purpose Rotary Vane Vacuum Pumps
• Designed for use with aqueous samples.
• Compatible with FreeZone Freeze Dry Systems, CentriVap Centrifugal
Concentrators and Protector® Controlled Atmosphere Glove Boxes.
• Ultimate vacuum (total pressure) 2 x 10-3 mBar (1.5 micron).
• On/off switch.
• Two inlet adapters (1/2" and 3/4" OD).
• Mode selector with two positions: High Vacuum and High
Throughput.
• Gas ballast with three positions: Closed, Low Flow and High Flow.
• Single phase direct drive motor, totally enclosed and fan cooled. Should
the motor overheat, the thermal overload device switches off the
pump. When the pump cools down, the motor automatically restarts.
• Isolation valve seals the inlet to prevent oil and air contamination of
the system in the event of power failure.
• Cast aluminum casing and rubber feet.
Catalog
Electrical
Number
Configuration
1472100
7739400*
7739402
1467700
7739401*
7739403
115 volts, 50/60 Hz, 4.6 A
Includes 115 volt NEMA 5-15P plug.
230 volts, 50/60 Hz, 2.4 A
Includes 220 volt NEMA 6-15P plug.
230 volts, 50/60 Hz, 2.4 A
Includes 230 volt reverse IEC plug.
115 volts, 50/60 Hz, 7.8 A
Includes 115 volt NEMA 5-15P plug.
230 volts, 50/60 Hz, 4.0 A
Includes 220 volt NEMA 6-15P plug.
230 volts, 50/60 Hz, 4.0 A
Includes 230 volt reverse IEC plug.
1473200 Replacement Oil Mist Exhaust Filter Cartridge.
For 1473400. Life is approximately one year at 1.33 x 10-2 mBar
(10 microns) vacuum. Shipping weight 0.5 lb. (0.2 kg)
1473300 Replacement Odor Exhaust Filter Cartridge. For 1473400.
Life is approximately one year at 1.33 x 10-2 mBar (10 microns) vacuum.
Package of five. Shipping weight 0.5 lb. (0.2 kg)
7584300 VACUUBRAND† B-Oil. One liter. Replacement oil for
VACUUBRAND HYBRID† Vacuum Pumps 7584000 and 7584002.
Shipping weight 2 lbs. (1 kg)
† VACUUBRAND™ and VACUUBRAND HYBRID™ are trademarks of VACUUBRAND GMBH + CO KG.
Displacement
At 60 Hz (50 Hz)
liter/minute
Dimensions
w x d x h
inches (cm)
117
(98)
117
(98)
117
(98)
195
(163)
195
(163)
195
(163)
6.5 x 17.0 x 10.4
(15.8 x 43.0 x 26.1)
6.5 x 17.0 x 10.4
(15.8 x 43.0 x 26.1)
6.5 x 17.0 x 10.4
(15.8 x 43.0 x 26.1)
6.5 x 18.5 x 10.4
(15.8 x 47.0 x 26.1)
6.5 x 18.5 x 10.4
(15.8 x 47.0 x 26.1)
6.5 x 18.5 x 10.4
(15.8 x 47.0 x 26.1)
* Not for direct electrical connection to FreeZone Systems in this catalog.
58
Shipping
Weight
lbs. (kg)
62 (28)
62 (28)
62 (28)
65 (30)
65 (30)
65 (30)
FreeZone Benchtop Shell Freezers
®
specifications
&
ordering
Information
FreeZone Benchtop Shell Freezers provide a compact system for prefreezing samples for lyophilization. The stainless steel bath has two
rollers that rotate Fast-Freeze Flasks in a low temperature heat transfer
solution, such as methanol or ethanol, so that a uniform thin coating
of sample freezes to the interior surface of the container. Shell freezing
increases the surface area to volume ratio, which facilitates efficient
vapor flow from the sample to the collector during lyophilization.
All models feature:
• Brushed stainless steel and glacier white, epoxy-coated steel exterior
with blue accents.
• 1/2 hp HCFC/CFC-free refrigeration system capable to cool the heat
transfer solution to -40° C (-40° F).
• Stainless steel bath, 5.5" w x 12.0" d x 6.5" h (14.0 cm x 30.5 cm x
16.5 cm), surrounded by urethane foam insulation with white highdensity polyethylene cover. Two chain-driven rollers, powered by a
sparkless induction motor, rotate flasks up to 1200 ml.
Approximately two liters of transfer solution are required
(not included).
• LED temperature “wave” for at-a-glance display of bath temperature from -20 to -42° C. LEDs illuminate amber as the system cools.
When the system reaches operating temperature, the bottom LED
illuminates green.
• Right-side mounted power switch.
• Left-side mounted retractable bath drain hose.
• 8-foot, 3-wire cord with plug.
• Overall dimensions: 15.1" w x 22.1" d x 19.7" h (38.4 cm x 56.1 cm x 50.0 cm).
FreeZone Benchtop Shell Freezer 7949020.
Models conform to the following standards:
• UL Standard 61010-1 (115 and 230 volt, 60 Hz models).
• CAN/CSA C22.2 No. 61010.1 (115 and 230 volt, 60 Hz models).
• CE Conformity marking (230 volt, 50 Hz model).
Catalog
Number
7949020
115 volts, 60 Hz, 6.0 A
Option includes:
7949040
230 volts, 60 Hz, 3.0 A
• Domestic or international electrical configuration.
7949030*
230 volts, 50 Hz, 3.0 A
Schuko
96 lbs. (44 kg)
7949060*
230 volts, 50 Hz, 3.0 A
British (UK)
96 lbs. (44 kg)
7949070*
230 volts, 50 Hz, 3.0 A
China/Australia
96 lbs. (44 kg)
Electrical
Requirements
Fast-Freeze Flask Capacity of
Benchtop Shell Freezer
Flask Size
40 ml
80 ml
120 ml
150 ml
300 ml
600 ml
750 ml
900 ml
1200 ml
* International electrical configuration
59
Quantity
2
2
2
2
1
1
1
1
1
Plug
Type
115 volts, 15 amps
Shipping
Weight
96 lbs. (44 kg)
North America, 230 volts 96 lbs. (44 kg)
Fast-Freeze Flasks
®
Variety of adapters
available. You may
select from glass or
stainless steel adapters, available straight
or with 45° bend.
(Required — order
separately.)
7541200
7541000
Top seals easily.
The flexible silicone
rubber top snaps on
and off easily, yet provides a reliable, high
vacuum seal.
7540900
7541100
7540400
7540000
7540200
7540600
Only two
pieces per flask.
The complete
Fast-Freeze Flask
has only two
components:
•a high strength
borosilicate
glass bottom to withstand
extreme temperatures
and high
vacuum.
•a flexible, noncontaminating
silicone rubber
top.
No vacuum
grease is
necessary.
No threads,
hooks or springs
are needed.
Entire flask may
be autoclaved.
7540800
7540300
Fast-Freeze Flasks
Select Fast-Freeze Flasks based on your sample sizes. Flasks should be
filled to no more than one-third of their volume so that maximum surface
area is achieved and efficient lyophilization is assured. A complete FastFreeze Flask includes a rubber top, glass bottom and a supply of filter paper.
Tops, bottoms and filter paper are available separately as replacement
components. Adapters are required to attach flasks to freeze dry valve ports.
Flask
Complete
Flask
Flask
Size
Flask
Bottom
Top
40 ml
80 ml
120 ml
150 ml
300 ml
600 ml
750 ml
900 ml
1200 ml
2000 ml
7540000
7540200
7540300
7540400
7540600
7540800
7541100
7540900
7541000
7541200
7542000
7542200
7542300
7542400
7542600
7542800
7542700
7542900
7543000
7543200
7544000
7544000
7544200
7544200
7544200
7544400
7544400
7544400
7544400
7544400
Flask Top
Adapter
Diameter*
1/2"
1/2"
3/4"
3/4"
3/4"
3/4"
3/4"
3/4"
3/4"
3/4"
Dimensions/ Flask Bottom
HxD
76 mm x 34 mm
115 mm x 34 mm
68 mm x 59.2 mm
85 mm x 59.2 mm
145 mm x 59.2 mm
135 mm x 90.2 mm
162 mm x 90.2 mm
190 mm x 90.2 mm
240 mm x 90.2 mm
380 mm x 90.2 mm
Compatible with
all major brands of
laboratory freeze
dry apparatus.
No complex filter
retainer is necessary.
For those who use
filters, they are easily
inserted between the
adapter and top of the
flask. One hundred
filters are supplied
with each flask.
Wide mouth
opening loads
fast, cleans easily.
Horizontal shell
freezing. Flask
may be placed in
a horizontal position and rotated
in a bath for shell
freezing.
Available in ten
convenient sizes.
Flat bottom
reduces spills,
provides better
balance.
Adapters
Add the Adapters for connecting the Fast-Freeze
Flasks to the valve ports on your drying chamber
or manifold. Choose borosilicate glass or stainless
steel adapters in 1/2" and 3/4" diameters.
Flask Holders
Help to prevent sample melt back. They allow a
small Fast-Freeze Flask Bottom containing the
sample to be placed inside a larger Fast-Freeze
Flask so that the vacuum surrounding the
sample insulates it from the room atmosphere.
Stainless steel. Flasks not included. Shipping
weight 1 lb. (0.5 kg)
Diameter
Straight 45° Bend
Adapter Adapter
Borosilicate Glass
1/2" flask top to 1/2" valve* 75450007545600
3/4" flask top to 3/4" valve* 75452007545800
1/2" flask top to 3/4" valve* 75454007546000
3/4" flask top to 1/2" valve* 75454007546000
Stainless Steel
1/2" flask top to 1/2" valve* 75470007547400
3/4" flask top to 3/4" valve* 75472007547600
Catalog Description
Number
7543300 Small Flask Holder. Compatible with inner flasks 7542000 (40 ml) 7544810 Replacement Filter Paper
and 7542200 (80 ml) and outer flasks 7541100 (750 ml) and 1000 (10 packages of 100). 1" diameter (28mm).
7540900 (900 ml).
Pore size 17 microns. Shipping weight 0.5 lb. (0.2 kg)
7543400 Large Flask Holder. Compatible with inner flasks 7542300 (120 ml), *Valves on the freeze dry systems, drying chambers and manifolds offered in this catalog fit adapters
7542400 (150 ml) and 7542600 (300 ml) and outer flasks 7541100 of both 1/2" and 3/4" sizes. Size information is provided for selecting adapters for older Labconco
(750 ml) and 7541000 (1200 ml).
models and other freeze dryers.
See Tube Holder accessories on page 61.
60
Lyph-Lock Flasks
®
Borosilicate glass
adapters with
either 19/38 or
24/40 standard taper
joints have 90° bend.
(Required — order
separately.)
7555000
7554800
Compatible
with all major
brands of laboratory freeze
dry apparatus.
7554900
7550400
7550000
7554600
Only three pieces
per flask — no
hooks or springs.
The complete
Lyph-Lock Flask
includes: • a flask top of
high strength
borosilicate glass
• a flexible, noncontaminating
silicone rubber
seal
• a flask bottom of
borosilicate glass
to withstand
extreme temperatures and high
vacuum.
7550200
Lyph-Lock Flasks
Select the Lyph-Lock Flasks based on your sample sizes. Flasks should
be filled to no more than one-third of their volume so that maximum
surface area is achieved and efficient lyophilization is ensured. A complete Lyph-Lock Flask includes a glass top and bottom and a rubber ring
seal. Tops, bottoms and seals are available separately as replacement components. Adapters are required to attach flasks to freeze dry valve ports.
Available
in seven
convenient
sizes.
7552000 7556000 7559000 7557200 67 mm x 34 mm
100 ml 75504007554400
7552200 7556200 7559200 7557400 50 mm x 59.2 mm
250 ml 75506007554600
7552200 7556200 7559200 7557600 110 mm x 59.2 mm
500 ml 75508007554800
7552400 7556400 7559400 7557800 103 mm x 90.2 mm
750 ml 75509007554900
7552400 7556400 7559400 7557900 145 mm x 90.2 mm
1000 ml 75510007555000
7552400 7556400 7559400 7558000 187 mm x 90.2 mm
Flat bottom
reduces spills,
provides better
balance.
Entire
flask may be
autoclaved.
Flask Complete Complete Flask
Flask Lyph-Lock Flask
Dimensions
Size Flask
Flask
Top
Top
Seal
Bottom Flask Bottom
19/38 STJ 24/40 STJ 19/38 STJ 24/40 STJ
H x ID
25 ml 75500007554000 7552000 7556000 7559000 7557000 37 mm x 34 mm
50 ml 75502007554200
Silicone rubber
seal grasps top
and bottom.
The flexible ring
holds securely
together during
pre-freezing and
lyophilization.
Provides a high
vacuum seal
for efficient lyophilization.
Adapters
Add the Adapters for connecting the Lyph-Lock Flasks to the valve
ports on your drying chamber or manifold.
7442600 Tube Holder
Stainless steel. Accommodates up to 15 each 12 or
13 millimeter diameter tubes in an upright position
inside a 750 ml or larger Fast-Freeze Flask or LyphLock Flask (tubes and glassware are not included).
144 mm h x 83.3 mm diameter. Shipping weight
1.0 lb. (0.5 kg)
90° Bend
Adapter
7442700 Tube Holder
Stainless steel. Accommodates up to 30 each 2.0 ml
microcentrifuge tubes in an upright position inside
a 750 ml or larger Fast-Freeze Flask or Lyph-Lock
Flask (tubes and glassware are not included).
139 mm h x 83.3 mm diameter. Shipping weight
1.0 lb. (0.5 kg)
Description
7568000
Connects 19/38 STJ Flask Top to 1/2" valve*
7568200
Connects 19/38 STJ Flask Top to 3/4" valve*
7568400
Connects 24/40 STJ Flask Top to 1/2" valve*
7568600
Connects 24/40 STJ Flask Top to 3/4" valve*
*Valves on the freeze dry systems, drying chambers and manifolds offered in this catalog fit adapters
of both 1/2" and 3/4" sizes. Size information is provided for selecting adapters for older Labconco
models and other freeze dryers.
61
Serum Bottles & Vials
Threaded Vials
Stoppers and Threaded Vials
with Screw Caps are supplied
in packages of 200.
Size
5 ml
10 ml
Vials with
Screw Caps
Stoppers
77623007762200
77626007762200
Accessories
Serum Bottles
Perfect for long term storage of freeze dried samples. Labconco Serum
Bottles and Threaded Vials are specifically designed for lyophilization
applications. Their uniform thin wall construction ensures even freezing and drying. Bottles and vials are ideal containers for use in the
FreeZone Stoppering Tray Dryer. Serum bottles also connect to valve
ports on drying chambers and manifolds. Serum Bottles, Stoppers and
Seals are supplied in packages of 100.
Seal Crimpers
Secure tear-away Aluminum Seals.
7578000 Seal Crimper. For 13 mm corkage. Shipping weight 3 lbs. (1.4 kg)
7578100 Seal Crimper. For 20 mm corkage. Shipping weight 3 lbs. (1.4 kg)
Size
20 mm
Corkage
13 mm
Corkage
Split
Stoppers
Aluminum
Seals
2 ml
75750107576010 7577010
3 ml
75752107576010 7577010
7593000 Vacuum Stoppering Adapter. Connects to a valve port
for manual stoppering of a 20 mm corkage serum bottle under original
vacuum. The stopper and serum bottle are inserted into the adapter
body and lyophilization begins. After the process is completed, the
researcher slides the stopper into position so when the valve is turned
from vacuum to vent the serum bottle is tightly sealed by the stopper. The ejector tube is then used to force the serum bottle out of the
adapter. Shipping weight 1 lb. (0.4 kg)
Sleeve-Type Stoppers
5 ml
7573010
75762107577110 7577510
10 ml
7573210
75762107577110 7577510
20 ml
7573410
75762107577110 7577510
30 ml
7573610
75762107577110 7577510
50 ml
7573810
75762107577110 7577510
100 ml
7574010
75762107577110 7577510
125 ml
7574210
75762107577110 7577510
Stoppering Adapter Body
Serum Bottle
Valve Port
Vent Hole
Ejector Tube
62
Stopper
Ampules & Miscellaneous Accessories
Ampules
7439300 Microcentrifuge
Tube Holder. 3.0" w x 2.25"
d x 1.0" h (7.6 cm x 5.7 cm x
2.5 cm), anodized aluminum
block with twelve bore holes
that accommodate 1.7 ml
microcentrifuge tubes. Holder
may be placed on any flat
freeze drying surface such
as inside Clear Chambers,
the built-in vacuum drying
chamber of FreeZone Console Systems; or on FreeZone Stoppering or
Bulk Tray Dryer Shelves, Product Shelves, or Heated Product Shelves.
One each. Microcentrifuge tubes are not included. Shipping weight
0.6 lb. (0.3 kg)
Labconco Ampules are fabricated of highest quality borosilicate glass for
strength and durability. Ampules are supplied in packages of 100.
Size
Straight
Pre-Scored
Flat Bottom
Digital Electronic Vacuum
Gauges Provide a LCD
display of vacuum measurement in mBar, PA or Torr.
Range is 0.02 mBar to 5
mBar. Stainless steel and
glacier white epoxy-coated
steel casing, 8.1" w x 4.1" d
x 6.4" h. Include a cord with
3/8" to 1/2" OD adapter for
connection to either vacuum
tubing or a valve on a drying chamber. All FreeZone Freeze Dry Systems
include a digital vacuum gauge. The Dry Ice Benchtop Freeze Dry System
or other freeze dryers may use the Digital Electronic Vacuum Gauge as an
accessory.
75727107570610
2 ml
7570810
5 ml
7571010
10 ml
7571210
1 ml
7578500 Oxygen/Natural Gas Sealing Torch. Specifically designed
for flame sealing freeze dry ampules. Seals all types of heat-resistant
glass. Connects to natural gas, butane or propane and oxygen with
1/4" ID hose connectors. Shipping weight 3 lbs. (1.4 kg)
Catalog
Number
Electrical
Requirements
7395000
115 volts, 60 Hz, 0.4 A
230 volts, 50 Hz, 0.2 A
7395001*
Shipping
Weight
10 lbs. (4.5 kg)
10 lbs. (4.5 kg)
7814300 Bleed Valve
Bleeds vacuum when all valves are in use on the Dry Ice Freeze Dry
System. 1/2" OD connections. Shipping weight 0.5 lb. (0.3 kg)
7593401 Ampule Valve Adapters. Connect
ampules to valve ports or stainless steel stems. Ten
per package. Shipping weight 0.5 lb. (0.2 kg)
7509600 Replacement Valve
For drying chambers and manifolds manufactured after March, 1996.
Consists of neoprene body and gaskets, molded plastic knob and fittings.
Accommodates both 1/2"
and 3/4" adapters. Shipping
weight 1 lb. (0.4 kg)
7762700 Three Way Adapter. Permits attachment of three ampules to a single valve port.
Ampules are attached using Ampule Valve
Adapters or 1/8" surgical tubing (not provided).
Cavity in adapter body can be filled with cotton fiber media to help prevent contamination
between samples. Shipping weight 3 oz. (0.1 kg)
7543800 29/32 Stainless Steel
Adapter. Allows connection of 29/32
round bottom flasks to valve ports on
drying chambers and manifolds. Shipping
weight 1 lb. (0.45 kg)
63
Miscellaneous Accessories
7645900 Replacement Neoprene
Tubing
For Dry Ice Benchtop Freeze Dry System
connections, 5/16" ID, 3' length. Shipping
weight 5 lbs. (2.3 kg)
RS-232 Cables
Provide connection from the RS-232 port on any FreeZone 2.5, 4.5, 6,
12 or 18 Liter Freeze Dry System or FreeZone Bulk Tray Dryer to an
IBM-compatible, user-supplied computer. An RS-232 Cable may also be
connected to the RS-232 port on the FreeZone Stoppering Tray Dryer
connected to a computer; however, the Interconnect Cable 7353403
included with the Stoppering Tray Dryer is recommended since it allows
the Stoppering Tray Dryer to communicate with the Freeze Dry System.
See page 38 for more information.
Catalog
RS-232 Cable
Number
7537800
7373436 Vacuum Tubing
For vacuum pump connection to the
Freeze Dry System, 3/4" ID, 3' length. Wire-reinforced PVC. Shipping
weight 5 lbs. (2.3 kg)
Shipping
Weight
For connection to computer
with 9-pin serial data port
0.5 lb. (0.2 kg)
7537801
For connection to computer
with 25-pin serial data port
0.5 lb. (0.2 kg)
7579000 Rubber Tubing Clamp
Clamp completely seals heavy wall vacuum tubing up to 3/4" ID for use
in leak detection. Shipping weight 5 lbs. (2.3 kg)
7426400 Support Shelves
Attach easily without tools
to the sides of the FreeZone
1, 2.5 or 4.5 Liter Freeze Dry
System or left-hand side of
the FreeZone Triad System
cabinet to provide support for
large flasks attached to the
drying chamber or manifold.
Multiple rows of perforations
on the sides of the FreeZone
cabinet allow for height adjustment of the shelves to support various sizes
of flasks. One pair. Glacier white epoxy-coated steel. Each shelf is 7.4" w x
12.0" d (18.7 cm x 30.5 cm). Shipping weight 2 lbs. (0.9 kg)
8025000 Portable Table
May be used to support
FreeZone 1, 2.5 or 4.5 Liter
Benchtop Freeze Dry System
on the top shelf while supporting a Rotary Vane or
Combination Rotary Vane/
Diaphragm Vacuum Pump
on the lower shelf. Glacier
white epoxy-coated tubular
steel. 4" diameter casters,
two with toe locks. Extruded rubber handle grips. Supports loads up to
400 pounds. Lifetime guarantee. Dimensions: 34.9" x 19.0" x 36.4" h.
(37.4 cm x 48.3 cm x 92.5 cm). Shipping weight 44 lbs. (20 kg)
Corrosion-resistant Lids
Replace the acrylic lids
included with FreeZone
Freeze Dry Systems and
Drying Chambers. Provide
additional protection from
solvents and corrosives
that attack acrylic, such as
acetonitrile. Lids 7439903,
7439902 and 7439900 are glass. Lid 7386800 is stainless steel. Include
neoprene gasket.
Catalog For Use With:
Diameter
Number
7439903
7439902
7439900
7386800
FreeZone 4.5 Liter Systems
FreeZone 6, 12 & 18 Liter Systems
16-Port Drying Chamber
12-Port Drying Chamber
FreeZone 1 & 2.5 Liter Systems
FreeZone Plus 4.5 Liter Systems
FreeZone -105° C 4.5 Liter Systems
8075000 Variable Height
Bench
May be used to support a
FreeZone 6 Liter Benchtop
Freeze Dry System with
any drying accessory except
the Stoppering Tray Dryer
mounted on top. Glacier
white epoxy-coated tubular
steel. Phenolic board with
melamine high-pressure
laminate surface. Height is adjustable from 29.6" to 37.4" (75.1 cm to
94.9 cm) using steel pins with nuts inserted in vertical frame members.
5" diameter, non-marking, toe-locking casters with bearings. Supports
loads up to 540 pounds. Lifetime guarantee. Work surface dimensions:
38.0" x 28.0" x 1.1" thick (96.5 cm x 71.1 cm x 2.8 cm). Shipping
weight 111 lbs. (50 kg)
Shipping
Weight
10.12"
14.00"
2.5 lbs. (1.1 kg)
3.5 lbs. (1.6 kg)
9.25"
10.12"
2.0 lbs. (0.9 kg)
5.0 lbs. (2.3 kg)
64
Contact Labconco for more information about
these quality products for your laboratory.
HEPA-Filtered Biological
Safety Cabinets, Enclosures
& Clean Benches
Fume Hoods &
Ductless Enclosures
Balance & Bulk Powder
Enclosures
Laboratory Animal
Research Stations
Nanotechnology
Enclosures
Forensic Enclosures
Glove Boxes
Glassware
Washers
Water Purification
Systems
Vacuum Concentrators &
Cold Traps
Bio-Concentrators
Multiple Sample
Evaporation Systems
Laboratory
Carts & Benches
Blood Drawing
Chairs
Vacuum
Desiccator
Labconco Corporation
8811 Prospect Avenue
Kansas City, Missouri 64132-2696
816-333-8811 or 800-821-5525
FAX 816-363-0130
[email protected]
www.labconco.com
© 2012 by Labconco Corporation
Printed in the U.S.A.
Product design subject to change without notice.
3-30-5/12-Graphx-4M-R1
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