Laboratory Rotary Evaporation Solutions Convincing

Laboratory Rotary Evaporation Solutions Convincing
Laboratory Rotary Evaporation Solutions
Convincing solutions from the market leader
BUCHI offers dedicated solutions for laboratory rotary evaporation whether you operate in
R&D or quality control. Based on our experience and knowledge we offer tailor-made solutions to cover a wide range of distinct needs and achieve highest convenience.
Core messages to our customers
BUCHI creates added value with “Quality in your hands”
“Quality in your hands” is the guiding principle that shapes our philosophy and our actions. It
challenges us to provide outstanding services that are precisely tailored to your needs. This means
that we must stay in close contact with our customers. That is why we keep in touch and continue
to work very hard to understand you and your business even better.
We help you by providing high-quality products, systems, solutions, applications and services that
offer you added value. This allows you to focus entirely on your processes and your work.
Easy
You handle complex processes, do challenging work and want to
focus on what is essential. We support you by providing carefully
designed solutions as well as instruments and systems that are
easy to operate.
Competent
You need products, systems, solutions, applications and services
that are precisely tailored to your needs. We have the technological
expertise and decades of experience needed to provide competent
support and work with you to continually improve our market services.
Reliable
You want to be able to rely completely on your partner for products, systems, solutions, applications and services. We guarantee
the quality and functionality of our equipment and will continue to
help you quickly and efficiently whenever something does not operate to your satisfaction.
2
Cost-effective
You want to achieve the best possible results using efficient solutions. We help you to handle your jobs and processes economically.
We strive to create a high level of economic benefit and maximum
added value for you.
Safe
You are working in an environment in which safety is a high priority.
By collaborating closely with you, we do everything in our power to
make our products, systems, solutions, applications and services
as safe as possible for people and the environment.
Global
You value personalized service and short communication channels.
As an international family-owned business with our own subsidiaries and qualified distributors, we have a presence wherever our
customers are located. Our local staff and the large number of satisfied customers around the world give you the assurance that you
are working with the right partner.
Sustainable
You prefer a partner who acts responsibly when it comes to current
environmental challenges. We support environmentally friendly
processes and manufacture products that have a long service
life. We utilize advanced technologies in order to conserve energy
and water and leave the smallest environmental footprint possible.
3
Laboratory rotary evaporation solutions
Benefit from decades of expert knowledge
In 1957 BUCHI introduced the first commercial rotary evaporator. With the technological expertise
and profound customer interaction, we further developed the Rotavapor® to an intelligent and fully
integrated system. Our carefully conceived solutions meet the various needs whether you operate in
R&D or quality control (QC) for a wide range of industries.
Pharmaceutical
For various applications in
QC as well as for laboratory
scale formulations in R&D
departments:
∙∙ Distillation
∙∙ Concentration
∙∙ Drying
Food/Beverage
4
Chemical
Academia/Education
For every day’s application in
QC and R&D laboratories:
For a wide range of applications in academic education:
∙∙ Concentration
∙∙ Reflux reaction
∙∙ Re-crystallization
∙∙ Full range of evaporation
applications
Feed
Used for QC in the food and
beverage industry as well as
for the development of new
ingredients and components:
Used for QC in the feed industry as well as for the development of new ingredients
and components:
∙∙ Distillation
∙∙ Concentration
∙∙ Drying
∙∙ Distillation
∙∙ Concentration
∙∙ Drying
Environmental Analysis
Required for sample preparation in order to monitor the
environmental pollution:
∙∙ Soxhlet extraction
∙∙ Concentration
Our dedicated solutions for your specific needs
Many criteria determine the choice of the most suitable rotary evaporator for you. BUCHI meets your specific
needs with a wide range of tailor-made solutions covering essential needs, as well as highest demands in convenience and productivity. Assess your requirements with the web chart shown below.
Convenience
∙∙ Push and go operation
∙∙ Plug & play installation
∙∙ Push notifications on mobile devices
∙∙ Easy cleaning and maintenance
3
2
1
Versatility
Reproducibility
∙∙ Scale up possibilities
∙∙ Controlled vacuum
∙∙ High bath temperatures
∙∙ Display of vapor temperature
∙∙ Unattended distillation of
∙∙ Data recording
foaming samples
∙∙ Display of lift position
Extendibility
Productivity
∙∙ Seamless extension with peripherals
∙∙ Automatic distillation
∙∙ Wide range of glass assemblies
∙∙ Wide range of accessories
(e.g. sensors, shield, lid)
∙∙ Instant distillation
∙∙ Purchasing costs
1
Selection
Solution
Rotavapor ®
Dynamic Pro
∙∙ Guided operation
Initial investment
applicable
2
more applicable
Interface
Pump
Chiller
Assessories
R-300
I-300 Pro
V-300
F-308
Included:
Foam sensor,
AutoDest sensor, protection
shield, lid
R-300
I-300
V-300
F-305
Optional:
Foam sensor,
AutoDest sensor, protection
shield
R-100
I-100
V-100
F-105
Optional:
Protection
shield, lid
(p. 6, 10)
Rotavapor ®
Essential
most applicable
Rotavapor
(p. 6, 8)
Rotavapor ®
Dynamic
3
(p. 12)
5
Platform «Rotavapor ® Dynamic»
Central control and flexible extension at any time
The Interface I-300 / I-300 Pro is the central control unit for all process parameters of a Rotavapor®
R-300 system. Rotation speed, temperature (heating, cooling, vapor) and pressure are perfectly
synchronized to optimize the distillation process while increasing efficiency and convenience.
Less time in front of the Rotavapor ®
The Rotavapor® App notifies the operator with push notifications and live view
of all process parameters on mobile devices when manual interaction is required. This frees up valuable time for other tasks.
Download at App Store
www.buchi.com/rotavaporapp
6
Create your specific solution
The “Rotavapor® Dynamic” solution is a fully extendable system with intelligent, seamless integration of every
product. Based on the Rotavapor® R-300 simply add the matching interface, heating bath, vacuum pump or
recirculating chiller at any time. The most convenient plug & play concept does not require any further
installation.
ti o
ies
AutoDest and
foam sensor
Lid and
protection shield
Int
I-300 Pro:
V-300:
Final
Final
vacuum
vacuum
1.5 mbar
5 mbar
on
e
I-300:
Navigation knob
Rotavapor ® R-300
ti
Op
fac
Touch screen
ns
V-600:
er
s
t
Op
ion
s
F-305:
F-308:
cooling
cooling
capacity
capacity
550 W
900 W
Op
ti o
Recirculatin g chiller
Vacuum pump
Op
or
Options
c
Ac
s
es
ns
B-301: up to 95 °C, max. flask
1 L, fast heat-up time
B-305: up to 220 °C, max. flask 5 L
Examples
Heating bath
The following configurations exemplifies how a basic Rotavapor® R-300 can be extended continuously whenever it is
needed.
Extendability
Configure your individual Rotavapor® system:
www.buchi.com/rotavapor
7
Solution «Rotavapor ® Dynamic Pro»
The most convenient and efficient way of rotary evaporation
You expect the most convenient operation and high reproducibility. With the “Rotavapor® Dynamic
Pro” solution we offer full automation, method-based guided operation, data recording and realtime charting.
Level sensor
Vacuum Pump V-300
Rotavapor® R-300 with
Heating Bath B-305
Interface I-300 Pro
Recirculating Chiller F-308
Configure your individual Rotavapor® system:
www.buchi.com/rotavapor
8
Your most important benefits
Convenient
∙∙ Easy to use with touch screen providing all process parameters at a glance
∙∙ Guided operation with programmable methods including push notifications on mobile devices when manual interaction is required
∙∙ Unattended automatic operation thanks to the AutoDest and foam sensor
∙∙ No harmful emissions due to post-pump secondary condenser with optional level sensor that alerts potential overflow of the receiving flask
Economical
∙∙ Time saving due to:
∙∙ Instant start thanks to automatic and dynamic pressure adjustment without waiting until heating bath
and chiller reach their set temperature
∙∙ Charting of all process parameters even remotely on mobile devices
∙∙ Efficient operation and increased sustainability with centrally controlled recirculating chiller and speed
controlled vacuum pump
Reproducible
∙∙ Comprehensive recording of all process parameters on SD card for easy analysis on Microsoft Excel
∙∙ Push notification in case of an unexpected event
Your solution «Rotavapor ® Dynamic Pro»
∙∙ Rotavapor® R-300 with Heating Bath B-305
∙∙ Interface I-300 Pro
∙∙ Vacuum Pump V-300
∙∙ Recirculating Chiller F-308
∙∙ AutoDest, foam and level sensor
∙∙ Options: Heating Bath B-301, Vacuum Pump
V-600, Recirculating Chiller F-305, protection
shield, lid
∙∙ Dedicated application support
∙∙ Workshop trainings
∙∙ Service hotline
∙∙ Preventive maintenance
∙∙ FDA compliant components
∙∙ Service and documentation (IQ/OQ)
“The method-based guided operation simplifies the evaporation task. Thus, we can entrust the lab assistants to safely perform a reproducible purification process using the Rotavapor ® system and dedicate ourselves to other tasks.”
Dr. Yasuhiro Shirai, Group Leader Photovoltaic Polymer Materials, GREEN, Japan
9
Solution «Rotavapor ® Dynamic»
Convenient rotary evaporation with full extendibility
You aim to conveniently evaporate your samples with the option to seamlessly extend your
BUCHI rotary evaporator to a fully automated system at any time. The “Rotavapor® Dynamic”
solution with a centrally controlled vacuum pump offers automatic evaporation and can be
upgraded to a “Rotavapor® Dynamic Pro” solution.
Protection shield
Interface I-300
Rotavapor® R-300 with
Heating Bath B-301
Plastic coated glass (P+G)
VacuBox
Vacuum Pump V-300
Configure your individual Rotavapor® system:
www.buchi.com/rotavapor
10
Your most important benefits
Convenient
∙∙ Easy to use interface providing all process parameters and push notification on your mobile device
∙∙ Unattended automatic operation thanks to the AutoDest and foam sensor
∙∙ User-friendly and ergonomic design of all components of the system
∙∙ Easy cleaning thanks to wide opening on the condenser
Versatile
∙∙ Individual requirements are covered by a wide range of accessories:
∙∙ Seven different glass assemblies for various applicative demands
∙∙ Plastic coating (P+G) and protection shield for extended safety
∙∙ Optional heating bath for 5 L flask achieving high temperatures
Extendable
∙∙ Intuitive plug & play extension for all components of the system
∙∙ Seamless integration of the Recirculating Chiller F-305 / F-308 saves cooling water
∙∙ Expandable to the Rotavapor® Dynamic Pro solution adding the Interface I-300 Pro and optional sensors
Your solution «Rotavapor ® Dynamic»
∙∙ Rotavapor® R-300 with Heating Bath B-301
∙∙ Interface I-300
∙∙ Vacuum Pump V-300
∙∙ Options: extendable to the full solution
"Rotavapor® Dynamic Pro" including various
accessories
∙∙ Dedicated application support
∙∙ Workshop trainings
∙∙ Service hotline
∙∙ Preventive maintainance
∙∙ FDA compliant components
∙∙ Service and documentation (IQ/OQ)
“I have been using BUCHI Rotavapor ® for more than 10 years, ever since my postgraduate research. It’s
very user-friendly and a lot of thought has clearly been put into the design details."
Dr. Ella Xiang, Nu Skin Enterprise, China
11
Solution «Rotavapor ® Essential»
Evaporation covering essential needs
You are looking for an economical and complete high-quality evaporation solution. The
“Rotvapor® Essential” solution integrates a Rotavapor®, an interface, a regulated vacuum pump
and a recirculating chiller to cover the main evaporation applications efficiently.
Vacuum Pump V-100
Optional: Plastic
coated glass (P+G)
Interface I-100
Rotavapor® R-100
Recirculating Chiller F-105
Configure your individual Rotavapor® system:
www.buchi.com/rotavapor
12
Your most important benefits
Economical
∙∙ Unique and affordable system for essential needs
∙∙ Small footprint saves valuable lab space
∙∙ Saves resources thanks to integrated system
Efficient
∙∙ Centrally regulated vacuum pump and recirculating chiller
∙∙ Process control due to precise vacuum regulation
∙∙ Reproducible yield thanks to stable parameters
∙∙ Heating bath temperature
∙∙ Vacuum pressure
∙∙ Cooling temperature
Convenient
∙∙ Ease of use due to smooth and ergonomic handling
∙∙ Maximum comfort thanks to integrated system
Your solution «Rotavapor ® Essential»
∙∙ Rotavapor® R-100
∙∙ Interface I-100
∙∙ Vacuum Pump V-100
∙∙ Recirculating Chiller F-105
∙∙ Optional: Plastic coated glass (P+G)
∙∙ Application support
∙∙ Workshop trainings
∙∙ Service hotline
∙∙ Preventive maintenance
“The solution is easy to use. The equipment is very useful due to various applications for sample preparation
or quality determination.”
Dr. Rungnaphar Pongsawatmanit, Associate Professor, Kasetsart University – Faculty of Agro-Industry,
Thailand
13
The best solution for your need
Comparison by customer needs, application and characteristics
Rotavapor ®
R-100
Needs / Solutions
R-300
Interface
I-100
I-300
I-300 Pro
Page
8
•
«Rotavapor ® Dynamic»
10
•
«Rotavapor ® Essential»
12
«Rotavapor ® Dynamic Pro»
•
•
•
•
Characteristics
Temperature range [°C]*
20 – 95
20 – 95
20 – 220
Lift mechanism
manual
manual/
automatic
Available condensers
V/C
7 cond.
Evaporating flask [mL]*
50 – 4000
50 – 1000
50 – 5000
Receiving flask [mL]
50 – 3000
50 – 3000
Integrated display for
heating
temp.
heating
temp.,
rotation,
lift position
ECO-mode bath
•
•
•
Compatible with Rotavapor ® App
•
•
Solvent library
•
•
Dynamic distillation for instant start
•
•
Automatic distillation / foam
•
•
Timer function
detection
Guided operation (methods)
•
Data recording and charting
•
* B-301: max. temperature: 95 °C / max. flask size: 1 L, B-305: max. temperature: 220 °C / max. flask size: 5 L
14
•
Vacuum Pump
V-100
V-300
Recirculating Chiller
V-600
F-100
F-105
F-305
•
F-308
•
•
•
•
Characteristics
1.5
1.8
3.1
Vacuum capacity [m3/h]
10
5
1.5
Final vacuum [mbar]
40 - 52
32 - 57
40 - 64
•
•
60
60
54
55
Noise level [dB]
Observation / supervision through glass
window
Cooling range [°C]
fix 10
-10 – 25
-10 – 25
-10 – 25
300
390
440
730
Cooling capacity [W] at 10 °C
-
120
250
450
Cooling capacity [W] at 0 °C
•
•
Temperature lock
Combination with BUCHI interfaces
I-100
•
I-300
I-300
I-300 Pro
I-300 Pro**
•
•
•
•
•
•
I-100
•
Recommended interface
I-300
I-300
I-300 Pro
I-300 Pro
•
•
Automatic start / stop
•
•
Temperature setting / control
Speed controlled
•
•
Power save mode / ECO-mode
** In combination with LegacyBox
15
Rotavapor ® Dynamic
Configure your extendable solution for highest convenience
Your Rotavapor® Dynamic solution consists of: Rotavapor® R-300 (with P+G coated glassware),
Interface I-300 or I-300 Pro, Vacuum Pump V-300 and a Recirculating Chiller F-305 or F-308
(optional).
1
1
S
R
3
0
0
Rotavapor®
1 Manual lift
2 Electronic lift
Heating baths
1 B-301: 20 °C to 95 °C (water),
max. flask size 1 L
5 B-305: 20 °C to 220 °C,
max. flask size 5 L
Glass assembly
1 Standard joint 29/32
2 Standard joint 24/40
V Vertical condenser: Used along with chiller or tab water
C Cold trap: Used for low boiling solvents along with e.g. dry ice
Interfaces
S I-300: Navigation knob and function keys; operating modes:
manual, timer, solvent library, automatic distillation, drying
P I-300 Pro: Touch screen and navigation knob; operating modes:
like I-300 plus guided operation, recording, charting
Recirculating chiller
0 Without chiller
1 F-305: -10 to 25 °C, cooling capacity 550 W at 15 °C
2 F-308: -10 to 25 °C, cooling capacity 900 W at 15 °C
Voltage
1 220 – 240 V
2 100 – 120 V
Vacuum pump
The Vacuum Pump V-300 is an integrated part of every Rotavapor® R-300
system.
Configure your individual Rotavapor® system:
www.buchi.com/rotavapor
16
Rotavapor ® Essential
Configure your solution covering essential needs
Your Rotavapor® Essential solution consists of: Rotavapor® R-100, Interface I-100, Vacuum Pump V-100,
Recirculating Chiller F-100 or F-105 (optional).
1
1
1
0
0
Glass assembly
V Vertical condenser: Used along with chiller or tab water
C Cold trap: Used for low boiling solvents along with e.g. dry ice
Standard joint
1 Standard joint 29/32
2 Standard joint 24/40
Protective coating
Plastic coated glassware protects against mechanical
damage and prevents sample loss.
0Without
1 Safety coating
Recirculating chiller
0 Without Chiller
1 F-100: fix 10 °C, cooling capacity 400 W at 15 °C
2 F-105: 0 to 25 °C, cooling capacity 500 W at 15 °C
Voltage
1 220 – 240 V
2 100 – 120 V
Vacuum pump and interface
The Vacuum Pump V-100 with Interface I-100 is an
integrated part of every Rotavapor® R-100 system.
Configure your individual Rotavapor® system:
www.buchi.com/rotavapor
17
Benefit from the market leader
Valuable and facilitative features of the Rotavapor ® Dynamic solution
Push notifications – Reduce your time in front of the rotary evaporator
The Rotavapor® App for iOS, Android and Windows
offers live view of all process parameters such as
rotation speed, temperature (heating, cooling, vapor) and pressure. Push notifications alert you when
required. In addition, graphical representation of
parameters is possible on the mobile device when
combined with the Interface I-300 Pro.
Methods – Improve reproducibility and free up your time
Until now a distillation process required regular supervision to guarantee smooth operation. The I-300 Pro now
offers user-defined steps that automatically guide the operator through the process. Push notifications alert when
manual interaction is required.
BUCHI’s latest innovation, frees up your time by eliminating the need for on-site supervision.
Example for a typical method:
Distillation
gradient, AutoDest or fixed pressure
Draining
alert user when distillation needs to be
drained
Save time by using methods
Classical
(no methods)
Time used for supervision
Distillation
Drying
Drying
clock and counterclockwise roation
Methodbased
t
Distillation
Drying
Free up your time for other tasks
Aeration
alert user when process is finished
Foam sensor – Handle foaming samples without manual interference
The foam sensor in conjunction with the Interface I-300 / I-300
Pro enables unattended distillation of foaming samples. The sensor automatically aerates the system temporarily to avoid extensive
foam formation, while keeping the vacuum on a constant level.
18
AutoDest – Distill automatically without supervision
The AutoDest sensor in conjunction with the Interface I-300 /
I-300 Pro enables unattended automatic distillation. The vacuum
is automatically optimized according to the cooling capacity of the
condenser. Solvent emissions into the laboratory atmosphere are
thus minimal as the condenser is not overloaded.
B-301 – Reduce the heat-up-time of the bath
The small Heating Bath B-301 consists of an similar heating power
compared to the Heating Bath B-305. Since the volume of the
B-301 is 2.5 times smaller, the bath reaches the set temperature
within a very short period of time.
B-305
4 min to 50 °C
8 min to 50 °C
Pmax 1’100 W
Pmax 1’300 W
1 L flask
5 L flask
Tmax 95 °C
Tmax 220 °C
Temp. [°C]
B-301
B-301
B-305
95
50
4
8
22
Time [min]
V-100/V-300/V-600 – Choose from various performance options
BUCHI’s chemical-resistant PTFE diaphragm pumps form an integral part of a Rotavapor® R-300 or R-100 system.
Centrally controlled by the corresponding interface, they feature different performance levels covering a wide range of
application needs.
V-100
V-300
V-600
Ultimate vacuum
10 ± 2 mbar
5 ± 2 mbar
1.5 ± 1 mbar
Suction capacity
1.5 m3/h
1.8 m3/h
3.1 m3/h
19
Benefit from the market leader
Frequently asked questions
Which is the right glass assembly for my application?
The glass assembly is chosen according to individual applicative requirements, solvent and sample
properties as well as condenser characteristics.
A
C
Diagonal Cold trap
V
S
Vertical
Reflux
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
Applications
CR
E
Cold trap Expansion
reflux
BY
Double
jacket
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
• •
M–H
L–M
M–H
M–H
L–M
M–H
M–H
•
•
•
•
•
• •
Cooling
CL
CM
CL
CL
CM
CL
CL
Cooling temperature range
H
M
H
H
M
H
H
Suitable for high throughput
•
•
•
•
•
Distillation
Drying
Concentration
Reflux reaction
Soxhlet extraction
Re-crystallization
Solvent/Sample properties
Boiling point range
Bumping or foaming
1
1
1
1
1
1
Characteristics
Vapor temperature sensor
Available Available
•
Foam sensor
•
•
•
•
HS
HS
HS
HS
HS
HS
500
1500
1500
1500
500
1300
•
•
•
•
•
•
•
•
Automatic distillation
Suitable for limited space
2
VS
Condenser surface max. [cm2] 1500
Available for R-300
Available for R-100
•
Available Available
•
2
3
H = High M = Medium L = Low VS = Limited vertical space HS = Limited horizontal space
CL = Cooling liquid CM = Coolant mixtures (e.g. dry-ice/acetone)
1
With Reitmeyer adapter 2 Possible with AutoDest sensor only 3 Limited features
20
•
Where is the rotation speed displayed?
The rotation speed, as well as heating bath temperature and lift
position, are shown on the integrated bath display. When using an
interface those parameters are shown on both the bath and the
interface.
How can I reduce the noise emission of a vacuum pump?
By choosing a speed-controlled pump. The Vacuum Pump V-100 /
V-300 and V-600 in conjunction with the Interface I-300 / I-300 Pro
are operating only when required. This significantly reduces
the noise emission and extends the lifetime of the pump.
Can I reduce the energy consumption of the evaporation system?
Yes, the ECO-mode is an integral part of the BUCHI Rotavapor®
R-300 system. Both bath and chiller enter a stand-by mode after
a pre-defined period of time and are restarted automatically when
required.
Why should I buy plastic coated glassware?
The transparent plastic coating (P+G) improves the durability and
stability of the glass. It also protects the operator from broken bits
of glass as well as chemicals in case of glass breakage.
21
Benefit from the market leader
Our recommendations to increase the distillation efficiency
The following extract of the BUCHI Evaporation Guide help you to improve the efficiency of your
evaporation process, to save time, to conserve energy and to reduce the environmental impact.
Optimal temperatures
∆ 20 °C rule
∙∙ Heating temperature T1 ≥ 20 °C vapor temperature T2 ≥ 20 °C cooling temperature T3
Advantages
∙∙ Condenser works at its optimum without being overloaded
∙∙ Vapor emissions into the lab atmosphere are minimal
T3
T2
T1
Recommendation: Set the bath temperature to ∆T ≥ 20 °C
50 °C. Applying the ∆ 20 °C rule results in 50/30/10 °C:
∙∙ Bath temperature T1: 50 °C
∙∙ Vapor temperature T2: 30 °C  select pressure for the vapor temperature to equal 30 °C (solvent library;
example: for ethanol set pressure to 102 mbar)
∙∙ Cooling temperature T3: 10 °C
∆T ≥ 20 °C
Immersion angle
Advantages of a flat angle (10 °)
∙∙ Larger percentage of rotating flask is wetted by heating medium
∙∙ Produces maximum turbulence inside flask
Limitations of a flat angle
∙∙ Flask cannot be as deeply immersed in the heating medium
∙∙ Sample is more likely to bump or foam
25 °: best compromise
35 °: best immersion
Recommendation: Use standard position (25 °) for best efficiency without jeopardizing the sample
wetted surface
Download the comprehensive evaporation guide:
www.buchi.com/rotavapor
22
10 °: most effcient
Rotation speed
Evaporation performance
Mean time to mechanical failure
Advantage of high rotation speed
High
∙∙ Produces maximum turbulence inside flask and
bath to achieve maximum evaporation output
Limitations of high rotation speed
∙∙ More vibrations
∙∙ More spillage of heating media
Low
100
250
400
Rotation speed [rpm]
Recommendation: Use 250 to 280 rpm for maximum turbulence at high durability
Evaporating flask size
Advantages of large flasks
∙∙ Larger surface results in greater turbulence inside the flask
and a higher evaporation performance
∙∙ Less bumping and foaming
Limitations of large flask sizes
∙∙ More difficult to transfer
∙∙ Less flexible for changing the immersion angle
Level of
heating
media
large flask
Recommendation: Select a flask that accommodates approximately twice the starting sample
volume
Evaporating flask thickness
Advantage of thin walls
∙∙ Allows better heat transmission from the bath through the glass into the solvent
Limitation of thin walls
∙∙ Higher risk of breaking
Flask content "Solvent"
heat conduction
Glass of
evaporating flask
Heating bath medium
heat transfer
Optimal wall
thinkness range
Low
Glass stability
heat transfer
Evaporation performance
High
1.5
2.0
2.5
Glass thickness [mm]
Recommendation: Use 1.8 mm thick flasks (1 L) for best temperature exchange at high safety
23
Complete your laboratory evaporation portfolio
Complementary and related products
Vacuum Pump
The Vacuum Pump V-100,
V-300 and V-600 are fully
integrable into your evaporation solution. Benefit from
the small footprint and
quiet operation.
Glass Assemblies
Make use of the widest
range of glass condensers
and flasks to optimize your
evaporation application.
24
Interface
Recirculating Chiller
I-100, I-300 and I-300 Pro
are central control units for
BUCHI evaporators,
vacuum pumps and
chillers. Different modes of
operation optimize all
process parameters.
BUCHI recirculating chillers
are fully integrable into any
Rotavapor® system. They
guarantee a sustainable
operation of your sample
preparation.
Plastic Coated Glass
Industrial Rotavapor ®
For maximum safety
­BUCHI offers a high quality
plastic coating for virtually every glass to prevent
glass slivering.
Best performance production scale with the
Rotavapor® R-220 Pro.
Parallel Evaporator
The Multivapor™ is a compact 6 or 12 position parallel vortex evaporator that
is designed to optimize
existing personal process
workflows.
Chromatography
Purify your samples using
flash and/or prep chromatography with the
Reveleris® X2 or Prep
systems or our modular
Sepacore® system.
Parallel
Concentrator
The Syncore® Polyvap allows parallel evaporation of
4 to 96 samples, using six
exchangeable racks, available as option.
Spray Dryer
The Mini Spray Dryer
B-290 is the product of
choice to dry solutions
quickly and gently into
particles of the desired
size by spraying.
Glass Oven
Small amounts of solvents
are best distilled on the
B-585 Kugelrohr. The option B-585 Drying allows
for temperatures of up to
300 °C.
Melting Point
Check the purity of your
compounds using the
Melting Point M-560 or
M-565 for melting point or
boiling point determination.
25
Support and customer service
From feasibility to preventive maintenance
You value an efficient and personalized service. Our network of professional application specialists
and service technicians as well as a large number of satisfied customers around the world give you
the assurance that you are working with the right partner.
BUCHI Product and system configurator
Compose your rotary evaporator with the BUCHI Rotavapor® Configurator according to your specific needs. Simply choose from various options and receive your Rotavapor® order code including a
picture of your specific configuration. Share the result with others or
easily get a quote.
Configure your individual Rotavapor® system:
www.buchi.com/rotavapor
Learn about evaporation and concentration
Over more than 50 years of experience in the development of official and customized applications is summarized in practical guides.
In addition, The Laboratory Assistant provides the theoretical background of essential sample preparation steps as well as practical
tips. Profit from a myriad of information.
Discover our literature at:
www.buchi.com/literature
Discover our numerous case studies
BUCHI offers over 130 different case studies. By using real information, the online case studies bring to life the complexities of business
and give you an understanding of the wide range of the applications
supported by our products, systems, solutions and services.
Discover our case studies:
www.buchi.com/casestudies
26
Profit from workshops, trainings and seminars
We regularly offer practical seminars and workshops, often in cooperation with other partners in the field of sample preparation and
analysis. Customer contributions thereby underline how our solutions facilitate the daily routine. We also attend many local and international scientific and industrial congresses.
Find an overview of our activities:
www.buchi.com/events
Use your product most effectively
We help you to set your product properly into operation. We provide thorough Installation/Operation Qualification (IQ/OQ) services
to ensure compliance with FDA, GLP/GMP standards or GAMP
guidelines. Whether it is because of an initial installation, requalification or relocation, we provide professional compliance verification.
Find out more about our services:
www.buchi.com/service-support
Minimize downtimes
Avoid products’ downtimes with preventative maintenance and tailored service packages. We offer a product warranty of two years
and guarantee ten years of spare parts availability.
Get in touch with us:
www.buchi.com/warranty
Global Network
Our subsidiaries and qualified distribution partners ensure proximity where ever you are. Since we are familiar with your requirements, we use our experience and knowledge to provide first-rate
solutions.
Get in touch with us:
www.buchi.com/worldwide
27
Quality in your hands
BUCHI Affiliates:
Europe
Switzerland/Austria
Benelux
France
Germany
BÜCHI Labortechnik AG
CH – 9230 Flawil
T +41 71 394 63 63
F +41 71 394 64 64
buchi@buchi.com
www.buchi.com
BÜCHI Labortechnik GmbH
Branch Office Benelux
NL – 3342 GT Hendrik-Ido-Ambacht
T +31 78 684 94 29
F +31 78 684 94 30
benelux@buchi.com
www.buchi.com/bx-en
BUCHI Sarl
FR – 94656 Rungis Cedex
T +33 1 56 70 62 50
F +33 1 46 86 00 31
france@buchi.com
www.buchi.com/fr-fr
BÜCHI Labortechnik GmbH
DE – 45127 Essen
T +800 414 0 414 0 (Toll Free)
T +49 201 747 49 0
F +49 201 747 49 20
deutschland@buchi.com
www.buchi.com/de-de
Italy
Russia
United Kingdom
Germany
BUCHI Italia s.r.l.
IT – 20010 Cornaredo (MI)
T +39 02 824 50 11
F +39 02 575 12 855
italia@buchi.com
www.buchi.com/it-it
BUCHI Russia/CIS
Russia 127287 Moscow
T +7 495 36 36 495
russia@buchi.com
www.buchi.com/ru-ru
BUCHI UK Ltd.
GB – Oldham OL9 9QL
T +44 161 633 1000
F +44 161 633 1007
uk@buchi.com
www.buchi.com/gb-en
BÜCHI NIR-Online
DE – 69190 Walldorf
T +49 6227 73 26 60
F +49 6227 73 26 70
nir-online@buchi.com
www.nir-online.de
America
Brazil
USA/Canada
BUCHI Brasil Ltda.
BR – Valinhos SP 13271-200
T +55 19 3849 1201
F +55 19 3849 2907
brasil@buchi.com
www.buchi.com/br-pt
BUCHI Corporation
US – New Castle, DE 19720
T +1 877 692 8244 (Toll Free)
T +1 302 652 3000
F +1 302 652 8777
us-sales@buchi.com
www.buchi.com/us-en
Asia
China
India
Indonesia
Japan
BUCHI China
CN – 200233 Shanghai
T +86 21 6280 3366
F +86 21 5230 8821
china@buchi.com
www.buchi.com/cn-zh
BUCHI India Private Ltd.
IN – Mumbai 400 055
T +91 22 667 75400
F +91 22 667 18986
india@buchi.com
www.buchi.com/in-en
PT. BUCHI Indonesia
ID – Tangerang 15321
T +62 21 537 62 16
F +62 21 537 62 17
indonesia@buchi.com
www.buchi.com/id-in
Nihon BUCHI K.K.
JP – Tokyo 110-0008
T +81 3 3821 4777
F +81 3 3821 4555
nihon@buchi.com
www.buchi.com/jp-ja
Korea
Malaysia
Singapore
Thailand
BUCHI Korea Inc.
KR – Seoul 153-782
T +82 2 6718 7500
F +82 2 6718 7599
korea@buchi.com
www.buchi.com/kr-ko
BUCHI Malaysia Sdn. Bhd.
MY – 47301 Petaling Jaya,
Selangor
T +60 3 7832 0310
F +60 3 7832 0309
malaysia@buchi.com
www.buchi.com/my-en
BUCHI Singapore Pte. Ltd.
SG – Singapore 609919
T +65 6565 1175
F +65 6566 7047
singapore@buchi.com
www.buchi.com/sg-en
BUCHI (Thailand) Ltd.
TH – Bangkok 10600
T +66 2 862 08 51
F +66 2 862 08 54
thailand@buchi.com
www.buchi.com/th-th
BUCHI Support Centers:
South East Asia
Middle East
Latin America
BUCHI (Thailand) Ltd.
TH-Bangkok 10600
T +66 2 862 08 51
F +66 2 862 08 54
bacc@buchi.com
www.buchi.com/th-th
BÜCHI Labortechnik AG
UAE – Dubai
T +971 4 313 2860
F +971 4 313 2861
middleeast@buchi.com
www.buchi.com
BUCHI Latinoamérica
S. de R.L. de C.V.
MX – Mexico City
T +52 55 9001 5386
latinoamerica@buchi.com
www.buchi.com/es-es
We are represented by more than 100 distribution partners worldwide.
Find your local representative at: www.buchi.com
11592821G en 1707 /Technical data are subject to change without notice/Quality Systems ISO 9001.
The English version is the original language version and serves as basis for all translations into other languages.
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