- Industrial & lab equipment
- Measuring, testing & control
- Mettler Toledo
- O2 transmitter O2 4220X
- Operating instructions
Mettler Toledo O2 transmitter O2 4220X Operating Instruction 110 Pages
advertisement
O
2
Transmitter 4220X
Your Representative:
04/03
52 120 755
Mettler-Toledo GmbH, Process Analytics, Postfach, 8902 Urdorf, Switzerland
Tel. +41 (01) 736 22 11, Fax +41 (01) 736 26 36
O
2
Transmitter 4220X
Warranty
Defects occurring within 3 years from delivery date shall be remedied free of charge at our plant
(carriage and insurance paid by sender).
Accessories: 1 year
Subject to change without notice
TA–196.400–MTE04 061101 Software release: 5.x 01.04.03
Neu ab Softwareversion 5.0 (April 2003):
Geräte mit Option 467 (HART ® -Kommunikation) unterstützen nun auch die Produktkalibrierung
über die HART ® -Schnittstelle.
Der O
2
Transmitter 4220X unterstützt zusätzlich die neuen Mettler-Toledo Sensoren InPro6800 und InPro6900. grau blau nicht beschaltet transparent Kathode gelb/grün rot
Schirm
Bezugselektrode
Anode grün weiß
NTC
NTC
Fühlerleitung
Polarisationsspannung -675 mV
Zusätzliche Verbindung zur Unterdrückung von Störungen, insbesondere bei kleinen Meßwerten
Beschaltungsbeispiel mit Sensoren InPro6800 bzw. InPro6900
New features for software version 5.0 (April 2003):
Units with Option 467 (HART calibration via HART ®
® communication) now also support product interface.
The O
2
Transmitter 4220X supports the new Mettler Toledo InPro6800 and InPro6900 sensors.
gray blue
Not connected transparent Cathode yellow/green red
Shield
Ref.
electrode
Anode
Polarization voltage -675 mV green white
NTC
NTC
Sense line
Additional connection for interference suppression, particularly when measuring low values
Typical wiring with InPro6800 or InPro6900 sensors
Nouveau à partir de la version 5.0 (Avril 2003):
Les appareils avec l'option 467 (communication HART ® ) supportent également le calibrage du produit via l'interface HART ® .
Les nouveaux capteurs Mettler Toledo InPro6800 et InPro6900 sont disponibles pour les appareils Transmetteur O
2
4220X.
gris bleu
Sans connexions transparent Cathode jaune/vert rouge
Blindage
Electrode de réf.
Anode vert blanc
NTC
NTC
Câble sonde
Tension de polarisation -675 mV
Raccordement supplémentaire pour la suppression de parasites, en particulier pour les petites valeurs mesurées
Exemple de câblage avec les capteurs InPro6800 ou InPro6900
Contents
Transmitter 4220X . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1
Transmitter 4220X . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1
Transmitter 4220X . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-1
Contents III
O
2
Transmitter 4220X
Communication . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-23
IV Contents
®
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7-4
Contents V
O
2
Transmitter 4220X
VI Contents
Package contents
The package should contain:
• O
2
Transmitter 4220X
• This instruction manual
• Any accessories ordered with the Transmitter
(For available accessories, see Chap. 9)
Information on this instruction manual
Warnings and notes
Warning
Warning means that ignoring the given instructions may lead to a malfunction of or damage to the instrument and to property damage or personal injuries.
Note
Notes provide important information that should be followed when using the instrument.
Typical representations
The keys of the O
2
Transmitter 4220X are shown like this in the text:
, , , ,
, , , ,
Menus shown in the instruction manual may differ somewhat from the display of your Transmitter.
This depends on which options your Transmitter is equipped with.
If the behavior of your Transmitter deviates from the description in this manual, check whether the manual corresponds to the software version of your
Transmitter: see Pg 6-3, Device Description.
Information VII
O
2
Transmitter 4220X
Safety information
Be sure to read and observe the following instructions!
The safety instructions must always be followed for your own safety.
Failure to follow these instructions may result in injuries
The instrument has been designed in accordance with the state of the art and complying with the applicable safety regulations. When operating the instrument, certain conditions may nevertheless lead to danger for the operator or damage to the instrument.
Whenever it is likely that the protection has been impaired, the instrument shall be made inoperative and secured against unintended operation.
The protection is likely to be impaired if, for example:
• the instrument shows visible damage
• the instrument fails to perform the intended measurements
• after prolonged storage at temperatures above
70 ˚C
• after severe transport stress
Before recommissioning the instrument, a professional routine test in accordance with EN 61010
Part 1 must be performed. This test should be carried out by the manufacturer.
VIII Information
The O
2
Transmitter 4220X is approved for operation in hazardous locations. It has been developed and manufactured in compliance with the applicable European guidelines and standards.
The Declaration of Conformity confirms the compliance with the applicable European guidelines and standards.
The stipulations of EN 60 079-14:1996 and the following must be observed when installing the instrument in a hazardous location. The O
2
Transmitter
4220X may only be connected to certified intrinsically safe circuits. The electrical data are listed in
the EC-Type-Examination Certificate (see Pg XII).
Before commissioning it must be proved that the intrinsic safety is maintained when connecting the instrument to other equipment, such as supply units including cables and lines.
When commissioning, a complete configuration must be carried out.
Manipulations of the instrument other than described in this manual are not permitted.
Assembly/dismantling, installation, operation and maintenance may only be carried out by qualified personnel as defined by the automation industry in compliance with the applicable regulations and this instruction manual. Be sure to observe the specified ambient conditions and installation instructions.
Information IX
O
2
Transmitter 4220X
Proper use
The O
2
Transmitter 4220X is a 2-wire transmitter.
The Transmitter is supplied with power from the
4 to 20 mA loop current, which also transmits the measured variable.
The O
2
Transmitter 4220X is used for continuous measurement of oxygen saturation, concentration and partial pressure, as well as for temperature measurement in liquids. The instrument is designed for industrial use. The enclosure is protected to
IP 65 and allows direct wall mounting on the site.
The instrument shall not be used in a manner not specified by this manual. Any applications not specified in this manual are inadmissible.
X Information
Declaration of conformity
Information XI
O
2
Transmitter 4220X
EC-Type-Examination Certificate
XII Information
Information XIII
O
2
Transmitter 4220X
XIV Information
1 Assembly, installation, and maintenance
Assembly
• The weatherproof enclosure allows direct wall
mounting. See dimension drawing, Fig. 1-1.
• With the ZU 0136 mounting plate and the ZU 0125 bracket kit, the instrument can also be mounted on a post or pipe.
See dimension drawing, Fig. 1-2.
• The ZU 0157 protective hood provides additional protection against direct weather exposure and mechanical damage.
See dimension drawing, Fig. 1-2
For mounting the protective hood, you require the
ZU 0136 mounting plate.
• The ZU 0158 protective case provides optimum protection against dust, moisture, and mechanical damage.
See dimension drawing, Fig. 1-3.
With the ZU 0220 bracket kit, the protective case can also be mounted on a post or pipe.
Assembly 1-1
O
2
Transmitter 4220X
EP
Equipotential bonding
Cable gland
Fig. 1-1 Dimension drawing O
2
Transmitter 4220X
Fig. 1-2 ZU 0136 mounting plate, ZU 0157 protective hood and ZU 0125 bracket kit
1-2 Assembly
Fig. 1-3 Dimension drawing of ZU 0158 protective case
Assembly 1-3
O
2
Transmitter 4220X
Fig. 1-4 ZU 0220 bracket kit for ZU 0158 protective case
EP
Equipotential bonding
Cable gland
Fig. 1-5 Instrument with lockable protective panel (Opt. 432)
1-4 Assembly
Installation and commissioning
• Installation and commissioning of the O
2
Transmitter 4220X may only be carried out by trained experts in accordance with this instruction manual and as per applicable local and national codes.
Be sure to observe the technical specifications and input ratings.
• All parameters must be set by a system administrator prior to commissioning.
• Be sure to observe the safety precautions on
Before connecting the O
2
Transmitter 4220X to a supply unit, make sure that it cannot output more than 30 V DC, 100 mA and 0.8 W.
To connect the O
2
Transmitter 4220X, open the cover of the terminal compartment (lower part of the instrument) by removing the two screws. The terminals are suitable for single wires and flexible leads up to 2.5 mm
2
(AWG 14). On the right-hand side next to the terminals there are two contact holes for connecting a HART
®
hand-held terminal.
As delivered, all terminals are open to allow easy insertion of the connecting wires. If the terminals are only half open, it may occur that the wire is pushed below the contacting element and does not make contact when the terminal is closed.
Connection examples are shown on Pg 2-4 and the
following.
The outer EP terminal must be connected with equipotential bonding to divert electrostatic charges to the front panel overlay.
Assembly 1-5
O
2
Transmitter 4220X
Notes concerning performance
At ambient temperatures below 0 °C the readability of the LC display may be reduced. This does not impair the instrument functions.
The real-time clock, logbook, cal record, and sensor statistics are battery-backed for approx. 1 year.
After longer power outages these data can be lost.
The instrument then displays the message “Warn
Time/Date”, and the date is reset to 01/01/1990.
Time and date must be reentered.
Maintenance and cleaning
The O
2
Transmitter 4220X contains no user repairable components.
To remove dust, dirt and spots, the external surfaces of the meter may be wiped with a damp, lint-free cloth. A mild household cleaner may also be used if necessary.
When operating the instrument in a hazardous area, pay attention to electrostatic discharge!
Only clean the instrument with a moistened cloth!
Also the ZU 0158 protective case and the lockable protective panel (Opt. 432) may only be cleaned with a moistened cloth!
1-6 Assembly
2 Capabilities of O
2
Transmitter 4220X
Overview of O
2
Transmitter 4220X
Commissioning of the O
2
Transmitter 4220X may only be carried out by trained experts in accordance with this instruction manual. Be sure to observe the technical specifications and input ratings during installation.
All parameters must be set by a system administrator prior to commissioning.
The O
2
Transmitter 4220X is approved for operation in hazardous locations.
Membrane-covered oxygen sensors supply a current proportional to the oxygen partial pressure.
With Henry’s Law, the oxygen concentration can be calculated from the oxygen partial pressure via a solubility coefficient.
In the O
2
Transmitter 4220X the solubility coefficient is stored for the respective temperature from
-5 °C to +60 °C as a table in accordance with
EN 25814 1992. In addition, the influence of the salt content (salinity) of the medium on the solubility can be taken into account. The salt content is either specified directly as the salinity or chlorine content, or the conductivity and temperature of the medium are entered. The salinity is calculated from the conductivity and temperature using the International
Oceanographic Tables, Unesco / National Institute of Oceanography of Great Britain Volume 2, Wormley/ Godalming/Surrey.
Capabilities, Connection 2-1
O
2
Transmitter 4220X
®
Fig. 2-1 System functions of O
2
Transmitter 4220X
Fig. 2-1 shows the system functions. The measur-
ing inputs ➀ and ➁ are designed for the connection of all Mettler Toledo dissolved oxygen sensors.
Output 1 ➂ is galvanically isolated and operates as a current sink for the 4 to 20 mA (22 mA) loop current (supply unit required).
It supplies the Transmitter with power from the loop current, analogously transmits the configured measured value and provides for digital HART
®
communication by overlaying an FSK
*
signal. This allows to read out all measured values and status messages from the O
2
Transmitter 4220X.
The galvanically isolated Output 2 ➃ also operates as a current sink for the 0(4) to 20 mA (22 mA) loop current (supply unit required). It can transmit a further user-defined process variable or can be used as a switching or controller output.
Outputs 1 and 2 are additionally capable of transmitting alarm and warning messages as 22 mA signals. Parameter setting is described from Page
4-22 on in the “Alarm processing / NAMUR signals”
chapter.
2-2
*) FSK: Frequency shift keying
Capabilities, Connection
Insert jumper 4, 5 if necessary!
Insert jumper 7, 8 if necessary!
Fig. 2-2 Terminal assignments
Terminal assignments
Capabilities, Connection 2-3
O
2
Transmitter 4220X
Dissolved oxygen measurement
Fig. 2-3 Connection of the O
2
Transmitter 4220X to the Mettler Toledo DO sensors
Electrode connection
Shielding
Possible measurement problems
Grounding terminal 5 is not permitted. Terminals 4 and 5 must always be connected to each other.
The shielding of the sensor cable (yw/gn at terminal
3) ends at the sensor connector.
On the connection side, it must end within the ESD
shield (see Fig. 2-4). Terminal 3 may be grounded
(as close to the measuring point as possible).
Interferences can be injected into the sensor via the sensor body, which is particularly disturbing with low measured values. To remedy this problem, make an additional connection from terminal 3 to the sensor body or to a suitable point near the sensor, which is conductively linked to the sensor body.
Do not connect terminal 5 to ground!
2-4 Capabilities, Connection
Fig. 2-4 Installation of sensor cable within O
2
Transmitter 4220X to prevent injection of electrostatic discharges (ESD)
Temperature detection
Why temperature compensation?
The detection of the temperature of the process or calibration solution is important for two reasons:
• Compensation of the temperature dependence of the sensor membrane: The oxygen permeability of the membrane increases as the temperature rises. Therefore, the temperature is detected and the measured value compensated.
• Temperature-corrected display of oxygen concentration: The oxygen solubility in water and the water-vapor partial pressure are temperaturedependent.
Temperature compensation
The temperature is automatically detected with the temperature probe integrated in the sensor (Mettler
Toledo DO sensors: NTC 22 k
Ω
) and included in
the measured-value calculation (see Fig. 2-3).
The O
2
Transmitter 4220X allows to work with manual temperature specification or with a separate
Pt 100 / Pt 1000 temperature probe.
Capabilities, Connection 2-5
O
2
Transmitter 4220X
Passive output 2
If your Transmitter is equipped with Option 487
(second current output, passive), an additional output is available to you.
This output is passive. It must be supplied by an additional power supply ( e.g. WG 20 isolated supply).
Output 2 can be used either as 0 – 20 mA (22 mA) current output or as switching output (alarm contact or limit contact).
As a current output it can be defined for the various process variables. In addition, a message for failure, warning, and functional check can be output as
22 mA signal.
If your Transmitter is also equipped with Option 353
(Controller function), you can use the output as an analog or switching controller output .
Fig. 2-5 Connection of output 2 as current output with WG 20
Fig. 2-6 Connection of output 2 as switching output with WG 25
(Observe the technical specifications of WG 25.)
2-6 Capabilities, Connection
Typical wiring
Keypad
EP
Equipotential bonding
Fig. 2-7 Dissolved oxygen measurement with recorder evaluation, control and connection to a process control system
Connect EP terminal to equipotential bonding!
See Fig. 1-3 and Fig. 1-5 on Pg 1-3 and the follow-
ing.
This page has been left empty for technical reasons.
Capabilities, Connection 2-7
O
2
Transmitter 4220X
2-8 Capabilities, Connection
3 Operating O
2
Transmitter 4220X
The O
2
Transmitter 4220X may only be commissioned by trained experts in accordance with this instruction manual and as per applicable local and national codes.
All parameters must be set by a system administrator prior to commissioning.
User interface
METTLER TOLEDO
Fig. 3-1 User interface of the O
2
Transmitter 4220X
Capabilities, Connection 3-1
O
2
Transmitter 4220X
Measuring mode
In the measuring mode, two different types of numerical displays are available. If your unit is equipped with Option 448 (Measurement recorder), the variation of any two measured values can also be represented graphically. By pressing you can switch between the different display types.
The display consists of the following elements:
1 The measured value in the main display is se-
lected during Parameter Setting (see Pg 4-3).
2 The measured values in the secondary displays are selected using and .
3 The selection symbol indicates which secondary display can be edited.
By pressing or you can switch between the two secondary displays.
4 NAMUR messages: Warning (maintenance required) and failure
5 Tag number or note (Switch with
6 Current time
)
7 Reference to dependencies of process variables
8 Limit values exceeded
9 HART
®
Multidrop mode is active. Output current 1 is permanently set to 4 mA. The FSK
(HART
®
) signal is modulated onto the current.
3-2 Capabilities, Connection
Keypad assignment in measuring mode switches between the two different types of measured value display. With Option 448 also to the measurement recorder.
activates Calibration, Parameter Setting, Maintenance, or Diagnostics.
switches between tag number and note.
select secondary display for changing the process variable.
change process variable in the secondary display.
Refer to Page 4-3 for an overview of the process
variables that can be displayed.
Capabilities, Connection 3-3
O
2
Transmitter 4220X
Measurement recorder
With the integrated measurement recorder (Option
448), the O
2
Transmitter 4220X provides you with a two-channel “on-site recorder”. For process visualization or, for example, for controller optimizing, the measurement recorder continuously registers two user-defined process variables and simultaneously displays them graphically next to each other in the system display. Process variable, measurement range, recording method, and time feed (scanning interval) parameters can be set within broad limits
see Pg 4-3. The last 500 measured values are
stored with time and date in the recorder memory of your unit. You can also display them numerically
The option (Measurement recorder) can be retrofit-
Keypad assignment for measurement recorder switches to measurement display.
activates Calibration, Parameter Setting, Maintenance, or Diagnostics.
jumps to current entry.
scroll to next or previous page.
scroll to next or previous line.
jumps to current entry.
jumps to oldest entry.
3-4 Capabilities, Connection
Menu structure
Fig. 3-2 Menu structure
Capabilities, Connection 3-5
O
2
Transmitter 4220X
Menu operation
When Calibration, Maintenance, Parameter Setting or Diagnostics are active, the display shows the respective menu for operating the functions.
Operator guidance is supported by a 7-line plaintext display with information texts. During operation, the measured value display (4) and the active status messages (3) remain visible.
3-6 Capabilities, Connection
The menu display consists of the following elements:
1 The abbreviation shows you which menu you are in: view opl
Parameter Setting, Viewing level
Parameter Setting, Operator level
Administrator level
Diagnostics menu diag language selection
2 The heading indicates the current menu level.
3 The status display shows active warning ( and/or failure messages (
F
).
W
)
4 The measured value is also visible in the menus.
5 The » symbol indicates that this menu item contains a submenu.
6 The marker setting is only visible in the Parameter Setting menu. At the Administrator level you can block individual menu items for
the Operator level (see Pg 4-2).
7 In longer menus it is not possible to display all lines at the same time. The and symbols indicate that there are further menu lines.
Keypad assignment for menu operation:
Exits the menu system and returns to measuring mode. In the Calibration or Maintenance menus you are prompted to confirm that your equipment is ready for measurement.
Cancel: To cancel an entry (without storing) or to exit a submenu, you can use the corresponding menu key. That means: Parameter Setting can be canceled by pressing , Diagnostics by press-
How to select a menu item:
Select the desired menu item using the scrolling keys. The selected line is marked by a dark bar (reverse video).
The scrolling keys provide a repeat function: When a key is held down, the lines are scrolled through.
Pressing or menu level.
accesses the next (lower)
How to change a setting:
Pressing a cursor key changes the setting. The selected position is shown in reverse video.
The entry position flashes, as it has been modified but not yet stored.
Pressing stops.
stores the new setting. Flashing
Pressing the menu key (e.g.
restores the old setting.
) instead of
Capabilities, Connection 3-7
O
2
Transmitter 4220X
How to change numerical values:
Moves the cursor within the entry area. With these keys, you select the entry position.
When the entry value has a sign, it can be selected by pressing .
If you edit a numerical value with an entry area covering several decades (e.g. conductivity), the symbol appears in front of the numerical value.
Now you can displace the decimal point using the cursor keys.
Pressing a scrolling key scrolls the numbers from 0 through 9 or changes the sign.
Pressing stores the edited setting.
Pressing the menu key (e.g.
restores the old setting.
) instead of
How to select parameters in a pull-down menu:
Pressing or accesses pull-down selection. An inverted menu is displayed.
Select the desired menu line using the scrolling keys. The selected line is highlighted.
The entry line flashes, as it has been modified but not yet stored.
Pressing stores the edited setting.
Pressing the menu key (e.g.
restores the old setting.
) instead of
3-8 Capabilities, Connection
4 Parameter setting
Commissioning of the O
2
Transmitter 4220X may only be carried out by trained experts in accordance with this instruction manual.
All parameters must be set by a system administrator prior to commissioning.
Language selection
When you access the Parameter Setting level, you can select the language for the displays and menu texts. German, English, French, Italian and Spanish are available.
(Optionally Swedish instead of Spanish)
The three levels of parameter setting
The Parameter Setting menu is divided into the
Viewing, Operator and Administrator levels according to the user’s degree of specialization.
• At the Viewing level the settings can be displayed but not edited.
• At the Operator level only the marked menu items can be edited.
• At the Administrator level all parameter setting functions can be accessed. In addition, markers can be set for each menu item to create an optimal user menu for the Operator level.
Passcodes protect the Operator and Administrator level against unauthorized access. The passcode protection for the Operator level can be switched off if required.
The levels are identified by abbreviations in the upper left corner of the display.
view – Viewing level opl – Operator level adm – Administrator level
Access to the Operator level can be protected with a passcode if necessary. Access to the Administrator level is always protected with a passcode.
Parameter setting 4-1
O
2
Transmitter 4220X
4-2 Parameter setting
Viewing level
At the Viewing level you can have a look at all settings of the Transmitter.
The settings cannot be edited!
Operator level
At the Operator level you can only edit those parameters (menu items) which have been enabled at the Administrator level.
Whether a menu item has been enabled is indicated by the dot preceding the corresponding menu line.
This menu item can be edited.
This menu item is locked: It cannot be edited.
The menu item is skipped during scrolling.
However, it can be accessed at the Viewing level.
Access to the Operator level can be protected with a passcode if necessary.
Administrator level
At the Administrator level you can edit all instrument settings including the passcodes. In addition, the marker function allows you to lock individual menu items to prevent access from the Operator level.
As delivered, all menu items are enabled.
Access to the Administrator level is always protected with a passcode.
Marker setting
An information text explains the marker setting at the Administrator level.
By setting markers you can enable or lock individual menu items at the highest level of the Parameter
Setting menu (except “Passcode Protection”) for the Operator level:
This menu item has been enabled:
It can be edited at the Operator level.
This menu item is locked:
It cannot be edited at the Operator level.
However, it can be accessed at the
Viewing level.
How to set a marker
Press to select the marker.
Press or to enable ( ) or lock ( ) the menu item. Confirm the setting with .
Factory setting
At the Administrator level, you can reset all settings to the initial factory setting.
Before the O
2
Transmitter 4220X is started again, a complete parameter setting procedure must be performed by a system administrator.
Measurement display
During parameter setting you can define which measured value is to appear in the large display in measuring mode. The following process variables can be displayed:
• Oxygen saturation (referred to air) (%AIR)
• Oxygen saturation (referred to pure oxygen)
(%O
2
)
• Oxygen concentration (mg/l or ppm)
• Oxygen partial pressure (mbar)
• Temperature (°C)
• Time
•
The following variables can be shown in the secondary displays:
• MAN
• p
• OUTP1
• OUTP2
• CTIME
Manual measuring temp (°C)
Barometric pressure, manual
Output current 1
Output current 2
(with Option 487 only)
Sensor current in nA
Calibration timer in h
(with Option 483 and active controller)
(with Option 483 and active controller)
• DATE Date
See Pg 3-2 for how to select the process variables
for the secondary displays.
Parameter setting 4-3
O
2
Transmitter 4220X
The “Viewing Angle” menu item allows you to adjust the viewing angle of the display.
When the Transmitter is mounted at a very high or a very low position, you can adjust the viewing angle for optimum display readability.
Select the desired viewing angle (+ means viewing angle upwards and – means viewing angle downwards) and confirm your choice. You see the change immediately in the display.
Input filter
To increase the immunity to interference during measurement, an input filter can be switched on.
When the filter is switched on, momentary interference pulses will be suppressed, slow changes in the measured value will be detected.
If fast measured-value changes are to be detected, you must switch off the input filter.
Pressure correction
The signal delivered by the DO sensor is directly proportional to the oxygen partial pressure. Since the partial pressure changes with the total pressure
(barometric pressure), the O
2
Transmitter 4220X must detect the total pressure and take it into account to obtain the percent saturation as a pressure-independent process variable.
Automatic pressure detection
The pressure detection methods used during measurement and during calibration can be set independently. Select whether pressure detection during measurement or during calibration is to be set.
Manual pressure specification
If “manual” has been selected, the pressure can be entered and confirmed with .
4-4 Parameter setting
The integrated pressure sensor detects the ambient air pressure (p amb
).
In closed containers the pressure must be measured directly in the gas-filled space of the container. You can enter the pressure value manually.
Measurement in an open container: p = p amb
[p amb
= ambient air pressure] p amb
is automatically detected by the integrated pressure sensor.
Measurement in a closed container: p = p tank
[p tank
= pressure in gas-filled space of container]
The pressure in the gas-filled space of the container p tank
) can be entered manually in the Transmitter.
Salt content
Membrane-covered oxygen sensors supply a current proportional to the oxygen partial pressure.
With Henry’s Law, the oxygen concentration can be calculated from the oxygen partial pressure via a solubility coefficient. The solubility coefficient is dependent on both the medium in which the oxygen is dissolved and on the salt content and temperature of the medium.
The influence of the medium’s salt content (salinity to EN 25814 1992) on the solubility can be taken into account by the O
2
Transmitter 4220X.
The salt content is either specified directly as the salinity or chlorine content, or the conductivity and temperature of the medium are entered. The salinity is calculated from the conductivity and temperature using the International Oceanographic Tables,
Unesco / National Institute of Oceanography of
Great Britain Volume 2, Wormley/ Godalming/
Surrey.
Parameter setting 4-5
O
2
Transmitter 4220X
How to set the salt content parameters
Open a Parameter Setting menu and select “Salt
Content”.
Select whether you want to enter the salinity directly or specify the chlorine content or a conductivity value (Cond).
Enter the selected value.
If you specify a conductivity value, you can also enter the temperature value.
The corresponding salinity value is calculated from the chlorine content or the conductivity value and then used for correcting the oxygen concentration value.
Temperature detection
The temperature is automatically detected with the temperature probe integrated in the sensor (Mettler
Toledo DO sensors: NTC 22 k
Ω
) and included in the measured-value calculation.
Automatic temperature compensation
The Mettler Toledo dissolved oxygen sensors have an integrated NTC 22 k
Ω
temperature probe.
Select the NTC 22 k
Ω
probe in the Temp Probe menu.
The process temperature is automatically detected with the integrated temperature probe and taken into account for compensation.
Manual temperature compensation
The O
2
Transmitter 4220X allows to work with manual temperature specification or with a separate
Pt 100 / Pt 1000 temperature probe.
4-6 Parameter setting
Sensor data
The sensor data for the Mettler Toledo dissolved oxygen sensors are preset in the O
2
Transmitter
4220X.
• Polarization voltage
During amperometric oxygen measurement the oxygen is cathodically reduced. Therefore, the required polarization voltage is negative. It is
-675 mV.
• Temperature probe
(Default setting: NTC) The SE 704 and SE 705 sensors are equipped with an NTC 22 k
Ω
.
• Sensocheck
®
(Default setting: Off)
The Sensocheck
®
sensor monitoring function has been optimized for the Mettler Toledo dissolved oxygen sensors.
With Sensocheck
®
switched on, the impedance between the anode and cathode is monitored.
Rapid impedance changes, e.g. due to mechanical stress on the membrane, trigger the message
“Warn Sensocheck”. You can acknowledge (reset) this message in the Maintenance menu or perform a new calibration (and maintenance, if required) of the DO sensor. Appearance and disappearance of this message is recorded in the logbook. Slow impedance changes have no effect.
Sensocheck
®
has been optimized for automatic temperature compensation. When using manual temperature compensation, Sensocheck
®
should be switched off to prevent false alarms.
Parameter setting 4-7
O
2
Transmitter 4220X
Output 1
Output 1 is galvanically isolated and operates as a current sink for the 4 to 20 mA loop current (supply unit required).
It supplies the Transmitter with power from the loop current and analogously transmits the configured process variable.
The output current can be shown in a secondary
The output current can be assigned to one of the following process variables:
• Oxygen saturation (referred to air) (%AIR)
• Oxygen saturation (referred to pure oxygen)
(%O
2
)
• Oxygen concentration (mg/l or ppm)
• Oxygen partial pressure (mbar)
• Measured temperature (°C)
The output current is frozen at its last value:
• during calibration
• in the current source function (manual entry)
• in the “ Meas. Point Maint.” menu
• during a wash cycle
4-8 Parameter setting
oxygen saturation referred to air
Output curves of the current output
There are four output curves to choose from for the current output:
• Linear
• Trilinear (bilinear)
• Function
• Chart (Option 449)
If the initial value is lower than the end value, a rising output curver will result.
To define a falling output curve, set the lower value as the end value and the higher value as the initial value of the process variable.
Linear output curve
To determine the span corresponding to the current range 4 – 20 mA, set an initial and an end value for the process variable.
For permissible spans, refer to the Specifications,
Chapter 11.
Oxygen saturation referred to air [%AIR]
Parameter setting 4-9
O
2
Transmitter 4220X
Oxygen saturation referred to air [%AIR]
Bilinear output curve
To define a bilinear output curve, set the same X and Y values for the two corner points of a trilinear curve.
To determine the span corresponding to the current range 4 – 20 mA, set an initial and an end value for the process variable.
In addition, you can define a corner point. It divides the output curve into two regions of different slopes.
Example:
1st corner X:
1st corner Y:
2nd corner X:
2nd corner Y:
End:
85 %AIR
40 %
85 %AIR
40 %
100 %AIR
Oxygen saturation referred to air [%AIR]
Trilinear output curve
To determine the span corresponding to the current range 4 – 20 mA, set an initial and an end value for the process variable.
In addition, you can define two corner points. They divide the output curve into three regions of different slopes.
Example:
1st corner X:
1st corner Y:
2nd corner X:
2nd corner Y:
85 %AIR
40 %
95 %AIR
60 %
4-10 Parameter setting
Oxygen saturation referred to air [%AIR]
Output curve “function”
If low oxygen values are to be measured with a high resolution but also high oxygen values are to be detected, it is advisable to measure over several decades.
With the output curve “function”, a nonlinear output current characteristic can be implemented. By defining a 50% point, you can spread the beginning and compress the end of the range as required.
This allows you to create a good approximation of a logarithmic output curve.
To determine the span corresponding to the current range 4 – 20 mA, set an initial and an end value for the process variable. In addition, you can define a 50% point (at 12 mA).
Between the initial and end value, the output current is calculated from the following equations:
Output current (4 to 20 mA) =
(1 + K) x
1 + K x
K =
E + I - 2 X50%
X50% - I x =
M - I
E - I
16 mA + 4 mA
I: Initial value at
X50%: 50% value at
E: End value at
4 mA
12 mA
20 mA
Example: logarithmic output curve over one decade
Approximation of a logarithmic output curve in the range 10 to 100%AIR (one decade):
50% point: 31.6 %AIR
Example: logarithmic output curve over two decades
Approximation of a logarithmic output curve in the range 1 to 100%AIR (one decade):
50% point: 10.0 %AIR
Parameter setting 4-11
O
2
Transmitter 4220X
Output curve via user-defined chart
(Option 449)
If your O
2
Transmitter 4220X is equipped with Option 449, you can enter the parameters of the current output curve in this chart in 1 mA steps.
The slope of the entered curve must be either positive (rising) or negative (falling) throughout its whole length. The O
2
Transmitter 4220X checks whether there are points of inflection in the curve and gives a warning if the case arises.
Setting beginning and end of output current
In addition to the process variable and curve, the start and end values for the output current must be defined.
22mA message
Current output 1 can be defined for output of the
NAMUR signals Failure, Warning and Functional check (22 mA message). The output current is then set to 22 mA in the case of a message.
(Also see Alarm processing on Pg 4-22)
During Multidrop mode of the HART
®
interface output current 1 is permanently set to 4 mA.
In Multidrop mode the Transmitter momentarily draws a current of approx. 22 mA when switched on.
4-12 Parameter setting
Error messages for output settings
The output current is linearly output (determined only by initial and end value). The alarm message
“Warn Current Para” is generated if the settings fulfil one of the following conditions:
Trilinear (bilinear) curve
(rising, beginning < end):
• 1st corner X
≤
beginning
• 2nd corner X
≥
end
• 1st corner X > 2nd corner X
• 1st corner Y
≤
0 %
• 2nd corner Y
≥
100 %
• 1st corner Y > 2nd corner Y
Bilinear curve (rising, beginning < end):
• 1st corner X = 2nd corner X and
1st corner Y
≠
2nd corner Y
Trilinear (bilinear) curve
(falling, beginning > end):
(Beginning is always at 0 %
End is always at 100 %
1st corner X is always at beginning
2nd corner X is always at end)
• 1st corner X
≥
beginning
• 2nd corner X
≤
end
• 1st corner X < 2nd corner X
• 1st corner Y
≤
0 %
• 2nd corner Y
≥
100 %
• 1st corner Y < 2nd corner Y
Bilinear curve (falling, beginning > end):
• 1st corner X = 2nd corner X and
1st corner Y
≠
2nd corner Y
Curve “function” (rising, beginning < end):
• 50% point
≤
beginning
• 50% point
≥
end
Curve “function” (falling, beginning > end):
• 50% point
≥
beginning
• 50% point
≤
end
Parameter setting 4-13
O
2
Transmitter 4220X
Output 2
If your Transmitter is equipped with Option 487, you can use an additional output. The galvanically isolated output 2 also functions as a 0 (4) – 20 mA current sink (supply unit required). It serves to transmit an additional definable process variable, can be used as a switching output for limits or alarms or as wash contact.
If your Transmitter is also equipped with Option 353
(Controller function), you can use the output as a controller output.
Set as a current output
If output 2 is set as a current output, one of the following process variables can be output:
• Oxygen saturation (referred to air) (%AIR)
• Oxygen saturation (referred to pure oxygen)
(%O
2
)
• Oxygen concentration (mg/l or ppm)
• Oxygen partial pressure (mbar)
• Measured temperature (°C)
Select the output current range 0 - 20 mA or
4 - 20 mA
You can define the curve as linear, trilinear, or as a
function (also see Pg 4-9 and the following).
Define the beginning and end of scale for the desired process variable.
Current output 2 can be defined for output of the
NAMUR signals Failure, Warning and Functional check (22 mA message). The output current is then set to 22 mA in the case of a message.
(Also see Alarm processing on Pg 4-22)
Output 2 is passive. It must be supplied by an additional power supply (e.g. WG 21 isolated supply).
4-14 Parameter setting
Set as a limit contact
If output 2 is set as a limit contact, it can be controlled by the following process variables:
• Oxygen saturation (referred to air) (%AIR)
• Oxygen saturation (referred to pure oxygen)
(%O
2
)
• Oxygen concentration (mg/l or ppm)
• Oxygen partial pressure (mbar)
• Measured temperature (°C)
You can define the contact as follows:
• The variable controls the limit contact.
• The effective direction specifies whether the contact will be activated when the measured value falls below (Min) or exceeds (Max) the limit value.
• The limit define the switching threshold.
• The hysteresis specifies how far the measured value must fall below (Max) or exceed (Min) the limit value before the contact switches back.
• N/O or N/C contact specifies whether the active contact is closed
(N/O) or open (N/C).
When the measured value falls below or exceeds the set limit, “Limit” appears in the display.
Output 2 is active.
During calibration the limit contact is inactive!
Parameter setting 4-15
O
2
Transmitter 4220X
Set as an alarm contact
The alarm contact is used to output the NAMUR signals Failure, Warning and Functional check.
These are triggered by alarm processing.
You can choose between a normally-open and a normally-closed contact.
(Also see Alarm processing on Pg 4-22)
Set as an analog controller
You can only make use of the controller function if your Transmitter is equipped with Option 483.
The analog controller can only operate unilaterally because only output 2 is available for outputting the manipulated variable. Therefore, you must select the range in which the controller is to operate:
• Range below setpoint:
• Range above setpoint:
0 to +100 %
0 to –100 %
The controller only operates bilaterally when actuating a 3-way mixing valve.
For a pure P controller (reset time = 0), you only need to define the control range used. For the range not used, however, it is necessary to enter reasonable parameters as otherwise the error message “Warn Control Para” will be output.
When using the controller as a PI controler (reset time
≠
0), it is absolutely necessary to define the unused range. The manipulated variable (controller output) is influenced by both control ranges due to the integration time.
The following controller types are available:
• 3-way mixing valve
• Straightway valve
The following controlled variables can be defined:
• Oxygen saturation (referred to air) (%AIR)
• Oxygen saturation (referred to pure oxygen)
(%O
2
)
• Oxygen concentration (mg/l or ppm)
• Oxygen partial pressure (mbar)
• Measured temperature (°C)
4-16 Parameter setting
The current value of the controller output (CTL-Y
[%]) and the controller setpoint (X w
) can be shown in the secondary display in measuring mode.
With the definable feed time alarm, you can monitor the time during which the controller output is at
+100 % or –100 %, i.e. how long the valve is fully open.
If this time is exceeded, this may be due to a shortage of air flow or a defective valve, for example.
Control characteristic
Fig. 4-1 Control characteristic
Fig. 4-1 shows the characteristic of the controller in
the O
2
Transmitter 4220X. All points of the curve can be defined.
• The control range specifies the range in which the controller is active: above or below the setpoint
X w
(not for 3-way mixing valve)
• Values are adjusted toward the setpoint.
• Beginning of control and
• End of control define the control range.
Outside the control range the controller output remains at +100 % or -100 %.
Parameter setting 4-17
O
2
Transmitter 4220X
4-18 Parameter setting
• In the neutral zone no control takes place.
The neutral zone is symmetrical to the setpoint and its width can be defined.
• With corner X and corner Y you can define a corner point for each control range ( : controlled variable < setpoint and : Controlled variable > setpoint). This allows you to define two different slopes to obtain an optimal control characteristic for strongly nonlinear curves, for example.
• The reset time specifies the I-action component of the controller. If you set “ Reset Time 0000 s”, the
I-action component is turned off. The reset time can be defined separately for both control ranges
( : Controlled variable < setpoint and : Controlled variable > setpoint).
• With Cal/Maint active, you select whether the controller output is frozen at its last value (Y = const) or whether it goes to 0 % (Y = 0 %) during calibration and maintenance.
For test purposes, you can manually enter the con-
troller output Y in the Maintenance menu (see
Controller output (manipulated variable)
The manipulated variable (controller output) is output via output 2 as a current of either 0 to 20 mA or
4 to 20 mA. The valve type determines the behavior of the output current. You can choose between a 3-way mixing valve or a straightway valve.
With the 3-way mixing valve, output 2 operates over the entire control range:
• Y = –100 to +100 % corresponds to 0 (4) to 20 mA
When set as a straightway valve, you must select the output range:
• Control range below setpoint X
W
:
Controller output range 0 to +100 % corresponds to 0 (4) to 20 mA
• Control range above setpoint X
W
:
Controller output range 0 to -100 % corresponds to 0 (4) to 20 mA
The current controller output and the setpoint can
be shown in the secondary display (see Pg 3-2).
3-way mixing valve
For the 3-way mixing valve, output 2 is used for the entire control range. A controller output Y = 0 % then corresponds to a current of 10 or 12 mA, resp.
For example: For temperature control
Straightway valve
In the straightway valve mode an analog control valve or a pump is actuated with 0 (4) to 20 mA.
You define the output range in the Parameter Setting menu.
Output range below setpoint X
W
The analog controller output then operates in the range 0 to +100 % with +100 % corresponding to a current of 20 mA. The controller only outputs the manipulated variable below the setpoint. Above the setpoint the manipulated variable cannot be output and the output remains at 0 (4) mA.
For example: For controlling the air flow in fermentors
Output range above setpoint X
W
The analog controller output then operates in the range 0 to -100 % with -100 % corresponding to a current of 20 mA.
The controller only outputs the manipulated variable above the setpoint. Below the setpoint the manipulated variable cannot be output and the output remains at 0 (4) mA.
Parameter setting 4-19
O
2
Transmitter 4220X
Error messages for controller settings
The controller will be switched off (manipulated variable Y = 0 %) and the alarm message “Warn
Control Para” will be activated if any of the following conditions applies:
All controller types:
• Beginning
≥
setpoint – neutral zone / 2
• Corner X < beginning
• Corner X > setpoint – neutral zone / 2
• End
≤
setpoint + neutral zone / 2
• Corner X < setpoint + neutral zone / 2
• Corner X > end
• Corner Y>100 %
• Neutral zone < 0
• Corner Y>100 %
With the definable feed time alarm (see Pg 4-21)
you can monitor the time during which the controller output is at +100 % or –100 %, i.e. how long the valve is fully open. If this time is exceeded, this may be due to a shortage of air flow or a defective valve, for example.
Set as a wash contact
If output 2 is set as a wash contact, the DO sensor can be automatically cleaned using an appropriate probe.
Wash interval and wash time are freely definable.
If either of the two parameters is set to 0, the function is disabled.
During calibration and maintenance a wash interval is not started.
During the wash time the NAMUR Functional
Check signal is active, the output currents are frozen at their last values or set to 22 mA.
4-20 Parameter setting
Alarm settings
The O
2
Transmitter 4220X allows you to monitor up to 10 different measured values by warning and failure messages. These alarms are numbered from 0 through 9. For each alarm, you can separately define the process variable and the high and low limits for warning and failure messages. In addition, each alarm can be switched on or off. The alarm limits remain stored even when the alarm is switched off.
You can set warning and failure limits for each of the following process variables:
• Oxygen saturation (referred to air) (%AIR)
• Oxygen saturation (referred to pure oxygen)
(%O
2
)
• Oxygen concentration (mg/l or ppm)
• Oxygen partial pressure (mbar)
• Measured temperature (°C)
• Pressure (mbar)
• Calibration timer (h)
• Zero point (nA)
• Slope (pA/mbar)
You can define four independent alarm limits for each of these variables:
• Failure Limit Lo
If the measured value falls below the defined limit,
“FAIL” appears in the display.
• Warning Limit Lo
If the measured value falls below the defined limit,
“WARN” appears in the display.
• Warning Limit Hi
If the measured value exceeds the defined limit,
“WARN” appears in the display.
• Failure Limit Hi
If the measured value exceeds the defined limit,
“FAIL” appears in the display.
You can view the currently active alarm messages
in the “Message List” of the Diagnostics menu (see
Parameter setting 4-21
O
2
Transmitter 4220X
Alarm processing / NAMUR signals
Fig. 4-2 Alarm processing
The defined alarms 0 to 9 and the system ➁ generate the NAMUR signals Failure and Warning.
In addition, the system ➁ also generates the Functional Check signal during parameter setting, calibration and maintenance.
These signals are immediately entered in the message list and logbook ➂ (Opt. 354).
In the NAMUR Signals menu ➃ , you can define individual delay times for these messages.
4-22 Parameter setting
For functional check, the defined delay time acts as a fall delay!
This has the advantage that, for example, any temperature or measurement settling times following a sensor calibration can be bridged with a correspondingly defined fall delay time.
The messages can be output via output current 1
➄ or output 2 ➅ (if current 2 is active) as a 22 mA signal.
To do so, all three messages can be activated separately or in any combination in the 22 mA Message submenu.
If output 2 is set as an alarm contact, it can be used to output these messages. In this menu the alarm contact can be set as a normally open or a normally closed contact.
Cal timer
The cal timer allows you to monitor whether the sensor is calibrated regularly.
The cal timer counts the time passed since the last calibration. When the preset time is reached, a message is released.
In the “Alarm Settings” menu you can preset one interval each for a warning and a failure message.
The cal timer count can be shown in the secondary
HART
®
Communication
With Option 467 “HART
®
Communication” you can, for example, communicate with the O
2
Transmitter
4220X via the loop current using a handheld terminal or from the control room. Device data, measured values, messages and parameters are retrievable.
The O
2
Transmitter 4220X can be addressed from the master in two different ways: via a long, permanent address, which is unique world-wide, or via a selectable short address.
Parameter setting 4-23
O
2
Transmitter 4220X
Device address
Short address
Write protection
HART
®*
commands
The device address is unique world-wide for each device. It is composed of the manufacturer ID, the device type and the serial number.
The short address has two functions. You select the address 00 for a point-to-point connection. The output current then continues to be controlled by the measurement signal. In the bus mode (multidrop) each connected device must have a unique short address. The addresses 01 to 15 are used for this purpose. All devices supply a constant 4 mA at the current output. The data are transmitted completely via the HART
®
signal.
The write protection protects the settings from being changed via the HART
®
interface. The write protection can only be switched on or off via the menu.
When activated, the write protection also prevents the short address from being changed with the
HART
®
commands.
You can select the short address of the Transmitter and activate or deactivate the write protection.
From pull-down menus, you can select the respective process variables for the HART
®
“Secondary
Variable”, “Tertiary Variable” and “4th Variable”.
The “Primary Variable” is always assigned to the process variable of output current 1.
The selected process variables can be read out with the HART
®
command #3 (Read Dynamic Variables and P.V. Current). This allows to transmit and evaluate up to four selectable process variables using standard HART
®
programs (without Device Description).
A list of the HART
®
commands for the O
2
Transmitter 4220X can be found in the enclosed “Process
Unit 77 (X)... Transmitter-Specific Command
Specification” (with Option 467 only).
*) HART
®
is a registered trademark of the HART Communication Foundation
4-24 Parameter setting
Setting the clock
In the Date Format pull-down menu, you can select the desired type of display.
On pressing entered value.
, the clock starts running at the
Pressing cancels the entry (Undo). The clock then keeps the old time.
Point of measurement/note
In the Point of Measurement menu, you can specify the point of measurement according to DIN 19227
(ISO 3511) by entering a tag number. In addition, you can enter a note.
Each entry may be up to 16 characters long.
In measuring mode, there is a display with the tag number or note beneath the secondary displays.
Pressing switches between the displays.
With the “HART
®
Descriptor” you can, for example, enter operating instructions as a note, which is then shown in the display. With HART
®
communication, only the first 8 characters of the tag number are used (HART
®
Specification).
Device diagnostics
The O
2
Transmitter 4220X can perform an automatic self test (memory test) at regular intervals. In the case of a defective memory, the “Warn Device
Diagnostics” message is output.
The automatic self test is only carried out when the
Transmitter is in measuring mode and the interval time is not set to 0000 h. During the testing, measurement is countinued in the background. All outputs remain active.
The device tests can be executed manually in the
“Device Diagnostics” menu. The respective results
Parameter setting 4-25
O
2
Transmitter 4220X
“On-site recorder”
Measurement recorder
If you want to use the measurement recorder, but your Transmitter is not equipped with Option 448, you can retrofit the option.
See Release of options on Page 4-29.
For process visualization or, for example, for controller optimizing, the measurement recorder continuously registers two user-defined process variables and simultaneously displays them graphically next to each other in the system display.
Process variable, measurement range, recording method and time feed (scanning interval) parameters can be set within broad limits. The last 500 measured values are available with time and date in the form of a graph and as numerical values.
The measurement recorder can be adjusted like an ordinary recorder: The right and left channel can be separately defined. The feed (scanning interval) applies to both channels.
You can choose feed rates from 2 seconds up to 10 hours per recorder entry. With a rate of 2 seconds, the recorder shows the data of the last 16 minutes, with a 10 hour rate, it shows the data of the last 7 months.
Right and left channel:
Select the controlling process variable from the
Variable pull-down menu.
The following process variables are available:
• Oxygen saturation (referred to air) (%AIR)
• Oxygen saturation (referred to pure oxygen)
(%O
2
)
• Oxygen concentration (mg/l or ppm)
• Oxygen partial pressure (mbar)
• Measured temperature (°C)
• Pressure
• OUTP1 Output current 1
• OUTP2 Output current 2
(with Option 487 only)
Beginning and End define the recorder range.
These value only refer to the graphic representation in the display. All measured values are stored with their complete number of digits.
4-26 Parameter setting
In the Recording pull-down menu, you can choose between four methods:
• Snapshot
The currently measured value is recorded after expiration of the feed time.
• Min Value
Each measured value is checked in the measurement recorder. The lowest value within the feed time is entered in the recorder memory.
• Max Value
Each measured value is checked in the measurement recorder. The highest value within the feed time is entered in the recorder memory.
• Average
The measurement recorder calculates a mean value of all values measured, i.e. the value entered in the recorder memory is the arithmetical mean of all values measured within the feed time.
Passcode entry
Access to the Calibration and Maintenance menus and to parameter setting at the Operator and Administrator levels can be protected with passcodes.
You can set or disable each passcode individually
(the Administrator passcode cannot be disabled).
When a passcode is disabled, there is no protection against unauthorized access to the corresponding menu!
For safety reasons, you should not use the standard passcodes!
The factory-set passcodes are the same for all
Transmitters. Therefore, you should define your own passcodes.
The “Change passcode” line only appears when a passcode is enabled. The passcode remains stored even if it has been disabled.
Parameter setting 4-27
O
2
Transmitter 4220X
Setting the Administrator passcode
If you have lost the Administrator passcode, system access is locked! The Administrator level cannot be accessed for parameter setting. All menu items locked for the Operator level can no longer be edited.
In this case, please contact:
Mettler-Toledo GmbH
Hotline
Im Hackacker 15
8902 Urdorf/Switzerland
Phone: +41-1-736 22 14
Telefax: +41-1-736 26 36
After having entered the Administrator passcode, you are prompted to repeat the input for safety reasons.
If the second entry does not correspond to the first entry or if you cancel by pressing istrator passcode will not be changed.
, the Admin-
When you set the Administrator passcode to
“0000”, the Administrator level can be accessed without passcode entry by pressing passcode prompt.
at the
When you set the Administrator passcode to
“0000”, menus and device settings will not be protected against unauthorized access!
Improper changing of the device settings may lead to malfunctions of the O
2
Transmitter 4220X and to incorrect measured-value outputs!
Factory-set passcodes
As delivered, the following passcodes are set in the
O
2
Transmitter 4220X:
• Calibration passcode: 1147
• Maintenance passcode: 2958
• Operator passcode: 1246
• Administrator passcode: 1989
4-28 Parameter setting
Release of options
You can retrofit software options at any time on the site without dismantling the Transmitter. To do so, you require a device-specific, unique transaction number (TAN).
To release an option, you require:
• the desired option number,
• the model designation
(O
2
Transmitter 4220X)
• and the serial number of your Transmitter.
Please refer to the Diagnostics/Device Description
menu (see Pg 6-3) for this information. The price of
the option depends on the currently valid price list.
A list of available options is provided on Page 9-1.
The transaction number (TAN) can be obtained from your Mettler Toledo representative.
Option release with transaction number (TAN):
1: Select the desired option from the Option pulldown menu. Contact your Mettler Toledo representative specifying the option number, model designation and serial number.
2: Enter the transaction number you have received and confirm your entry by pressing
.
3: With the correct TAN you can enable or disable the option. The transaction number can be used repeatedly with this O
2
Transmitter
4220X to enable or disable the option at any time.
Parameter setting 4-29
O
2
Transmitter 4220X
This page has been left empty for technical reasons.
4-30 Parameter setting
5 Calibration
Why do you have to calibrate?
Every dissolved oxygen sensor has its individual slope and zero point. Both values are altered, for example, by electrolyte consumption. For sufficiently high accuracy of oxygen measurement, the
Transmitter must be regularly adjusted for the sensor data (calibration).
Calibration medium is water with a known oxygen saturation (referred to air) or air. The sensor is immersed in the calibration medium.
Then the O
2
Transmitter 4220X measures the sensor current and medium temperature and automatically calculates the sensor slope and zero point.
Without calibration every dissolved oxygen meter delivers an imprecise or wrong output value!
Particularly after having replaced the sensor, electrolyte or sensor membrane, you must perform a calibration.
Monitoring functions for calibration
The O
2
Transmitter 4220X provides functions for monitoring proper calibration performance and the sensor condition. This allows documentation for quality management to ISO 9000 and GMP.
• Sensocheck
®
recognizes mechanical stress of the membrane that might modify the calibration data.
• Regular calibration can be monitored by the cal
• The calibration record provides all relevant data of
the last calibration (GMP) (see Pg 6-1).
• The sensor statistics show the behavior of the sensor parameters during the last three calibrations compared to the first calibration
• The logbook provides time and date stamped records of calibrations performed within the last
Calibration 5-1
O
2
Transmitter 4220X
• You can define limits for warning and failure mes-
sages for the sensor slope and zero point (see
Pg 4-21). This permits automatic monitoring of
the sensor state using the calibration data.
Calibration menu
Pressing accesses the Calibration menu.
If calibration is protected with a passcode, you must enter the correct passcode to access the Calibration menu. The calibration passcode can be defined or disabled at the Administrator level.
Four different calibration methods are available:
• Automatic calibration in water
• Automatic calibration in air
• Manual entry of saturation
• Calibration be data entry
The NAMUR “functional check” signal is active during calibration.
If you press before having performed a calibration, you are prompted to confirm your decision to abort calibration.
If you abort, the old calibration data remain valid.
What does “First Calibration” mean?
During first calibration, the sensor data are stored as reference values for sensor statistics.
The “Sensor Statistics” Diagnostics menu shows the deviations in the slope and zero point, as well as the values for calibration temperature, calibration pressure and response time of the last three calibrations with date and time with respect to the reference values of the first calibration. This allows evaluation of the drift behavior and aging of the sensor.
5-2 Calibration
When do you have to perform a First Calibration?
Each time the sensor, electrolyte or membrane is replaced, a First Calibration must be performed.
How do you perform a First Calibration?
Select the corresponding calibration method, set
“First Calibration Yes” and confirm with .
If you do not want to perform a First Calibration, press to proceed to the next step of the calibration sequence.
One-point or two-point calibration?
For the calibration methods
• Automatic – Water
• Automatic – Air you can choose between one- and two-point calibration.
One-point calibration
The sensor is only calibrated using 100 % medium.
This determines the present slope of the sensor.
The old zero point remains unchanged.
One-point calibration is sufficient for most of the cases.
Two-point calibration
The sensor is calibrated using two media with different oxygen saturation values (100 % and 0 %).
This determines the slope and zero point of the sensor.
Two-point calibration is only necessary if the measured oxygen value is low or near the sensor zero.
Calibration 5-3
O
2
Transmitter 4220X
Automatic calibration in water or air
Calibration can be performed as one- or two-point calibration either in water or in air.
The calibration value is always the oxygen saturation (referred to air).
First, the slope is corrected using the 100 % value.
Then, also a zero-point correction can be carried out using the 0 % value.
All calibration data are converted using a reference temperature of 25 °C.
During calibration, the NAMUR functional check signal is active, the output currents are frozen at their last values, the limit contact is inactive, the controller output can either be frozen or set to zero
(see Pg 4-18), a wash interval is not started.
What you have to know for calibration
For calibration in water:
• Ensure sufficient medium flow to the sensor.
• The calibration medium must be in equilibrium with air. Oxygen exchange between water and air is very slow. Therefore, it takes a relatively long time until water is saturated with atmospheric oxygen.
For calibration in air:
• The sensor membrane must be dry, as adhering water drops falsify the measured oxygen value.
Make sure that the oxygen saturation of the calibration medium is correct and remains constant during calibration.
Ensure that all other parameters, e.g. temperature and pressure, are constant.
5-4 Calibration
If there is a temperature difference between the calibration medium and the measured medium, the sensor must be kept in the respective medium for several minutes before and after calibration in order to deliver stable measured values.
The type of calibration pressure detection is preset
during parameter setting (see Pg 4-4).
Automatic calibration in air
In the “Automatic – Air” submenu you can correct the calibration pressure manually preset at the Pa-
rameter setting level (see Pg 4-4).
In addition, you can specify the relative humidity of the air.
If you do not know the exact value of the relative humidity of the air used, you can take the following standard values for a sufficiently precise calibration:
• Normal ambient air: 50 %
• Bottled gas: 0 %
If you do not want to perform a First Calibration (see above), press to proceed to the information text.
The information text again shows calibration medium used and the corresponding oxygen saturation referred to air.
To start calibration, select “Calibration Start” using
.
The oxygen saturation indicated for air calibration is a hypothetical value which, however, corresponds
(at 100 % relative air humidity) to the oxygen saturation of water (equilibrium between water and air).
The Transmitter automatically recognizes when the sensor current is stable. The response time indicates how long it takes for the sensor to provide a stable current value. After a minimum response time of 1 min the sensor drift is checked and calibration is stopped if appropriate.
If you are sure that the sensor current has stabilized earlier, you can stop calibration after 10 sec by pressing .
An unstable sensor current reduces the accuracy of the calibration values!
Calibration 5-5
O
2
Transmitter 4220X
If the sensor current fluctuates or drifts strongly, calibration is stopped after 10 min. This may be caused by:
• insufficient sensor polarization
(see operation instructions for sensor)
• unstable measured values
• insufficient temperature equalization between sensor and environment (observe equalization
For one-point calibration, press
“Calibration End”.
to select
For two-point calibration, place the sensor in oxygen-free medium (e.g. 99.98 % nitrogen) and confirm “Calibration Start” with .
After a successful calibration the values calculated for slope and zero point are displayed.
End the calibration or repeat it if necessary with
“Calibration Repeat”.
Dissolved oxygen sensors often demonstrate a minor drift at the zero point over a longer period of time. However, the automatic calibration stops the zero-point calibration at a relatively early point in time due to the specified drift criterion and to avoid extremely long calibration times. The accuracy achieved in this way is sufficient for most applications. If a more exact and stable zero point value is required, the zero point should be calibrated as described under “Calibration by data entry”.
If an error message appears, you have to repeat calibration (service the sensor if necessary).
Automatic calibration in water
The calibration sequence in air is identical to the calibration sequence in air. Only adjustment of the relative humidity is omitted.
The calibration media are 100% air-saturated water and O
2
-free water (water flown through by inert gas such as N
2
, Ar etc.).
5-6 Calibration
Calibration with manual entry of saturation
When calibrating with manual entry of saturation, you can correct the measured value by directly entering the actual process value.
This permits a fast correction of slope without starting a complete calibration sequence.
With manual entry of saturation, slope is corrected without checking the drift. Therefore you should only make use of this method for corrections between two calibrations.
It cannot replace regular calibrations!
All calibration data are converted using a reference temperature of 25 °C.
During calibration, the NAMUR functional check signal is active, the output currents are frozen at their last values, the limit contact is inactive, the controller output can either be frozen or set to zero
(see Pg 4-18), a wash interval is not started.
What you have to know for calibration
Make sure that the oxygen saturation of the solution is correct and remains constant during calibration.
Ensure that all other parameters, e.g. temperature and pressure, are constant.
Calibration sequence
Place the sensor in a medium with known oxygen saturation. Select “Manual – Entry of Saturation” from the Calibration menu and confirm with .
The currently measured value for oxygen saturation referred to air is displayed.
Enter the actual process value.
The O
2
Transmitter 4220X stores the value and displays it in the measured value display.
Calibration 5-7
O
2
Transmitter 4220X
Calibration by data entry
If the current values for slope and zero point of a sensor are known, they can be entered directly.
Data entry may be of particular advantage for calibrating the zero point when measuring in the range of low oxygen concentrations. Place the DO sensor in an oxygen-free medium (such as 99.98 % nitrogen) and watch the sensor current. When the current sensor is stable (this may take more than 10 minutes), enter it as a zero point in the Data entry menu.
All calibration data are converted using a reference temperature of 25 °C.
During calibration, the NAMUR functional check signal is active, the output currents are frozen at their last values, the limit contact is inactive, the controller output can either be frozen or set to zero
(see Pg 4-18), a wash interval is not started.
Calibration sequence
Enter the data for zero point and slope in the Data
Entry menu and confirm with .
5-8 Calibration
6 Diagnostics menu
The Diagnostics menu provides all relevant information on the instrument status.
During diagnostics all measuring functions of the
O
2
Transmitter 4220X continue to be active. All outputs continue to be operated and warning and failure message are output.
If no key is pressed within 20 minutes, the Diagnostics menu is automatically exited.
Message list
The message list shows the number of currently activated messages and the individual warning or failure messages in plain text.
For explanations of the individual messages please refer to Chapter 8.
Cal record
The Cal Record displays all relevant data of the last sensor calibration for preparing documentation in accordance with ISO 9000 and GMP.
• Date and time of last calibration
• Calibration mode (e.g. Manual)
• Zero point
• Slope
• Relative humidity
• 1st sensor current
• 1st calibration temperature
• 1st calibration pressure
• Response time
• 2nd sensor current
• 2nd calibration temperature
• 2nd calibration pressure
• Response time
For some calibration procedures, such as Data Entry, not all measured values are available. The respective positions are then covered with a gray bar.
Diagnostics 6-1
O
2
Transmitter 4220X
Sensor statistics
When you perform a First Calibration (see Pg 5-2),
the following values are stored as reference val-
ues:
• Date and time of first calibration
• Sensor zero point
• Sensor slope
• Calibration temperature
• Calibration pressure
• Response time
When you then perform further calibrations, the following data will be listed in the sensor statistics for the last three calibrations:
• Date and time of calibration
• Deviation of sensor zero point
• Deviation of sensor slope
• Calibration temperature
• Calibration pressure
• Response time
This provides you with important information on sensor condition, aging and the time for the next due calibration.
If the time between two calibrations is less than 6 minutes, the Transmitter interprets the second calibration as repetition of the first one (e.g. when an error has occurred). It does not create a new record. The last calibration record is overwritten with the new values.
In the Sensor Statistics menu you can read the the respective statistics from the First Calibration and the last three calibrations.
6-2 Diagnostics
Logbook
This option (Logbook) can be retrofitted via TAN
The logbook contains the last 200 events with date and time and displays them.
Error messages occurring during parameter setting, calibration or maintenance are ignored.
The following events are recorded:
• Transmitter in measuring mode
• Transmitter turned on/off
• : Start of warning and failure messages
• : End of warning and failure messages
• Calibration messages
• Parameter setting, calibration, maintenance or diagnostics active
• Entry of a wrong passcode
The logbook entries can be used for quality management documentation to ISO 9000 and GMP.
Logbook entries cannot be edited!
Device description
The Device Description contains information on the model designation, serial number and instrument options.
The display indicates:
• Model designation
• Serial number
• Hardware and software version
• Program module code
• Options
The software version must correspond to the version indicated at the bottom right of the second page of this manual.
Diagnostics 6-3
O
2
Transmitter 4220X
Device diagnostics
The Device Diagnostics feature allows you to perform extensive tests to check the function of the
O
2
Transmitter 4220X.
This permits quality management documentation to
ISO 9000.
Instrument settings and parameters are not affected.
In the Device Diagnostics menu you see when each test was performed and what the result was.
Start the selected test with .
Memory test
Select “RAM Test”, “EPROM Test” or “EEPROM test”.
The Transmitter forms a CRC checksum for the calculated data and compares it with the setpoint.
If “Failure” appears in the menu after the test is completed, the Transmitter must be sent in to the manufacturer for repair.
Display test
Several test patterns will be displayed allowing you to check whether all pixels, lines and columns function properly.
If there are disturbances in the test patterns, the
Transmitter should be sent in to the manufacturer for repair.
Keypad test
Each key must be pressed once during keypad testing. Keys that have been pressed are highlighted.
If “Keypad Test Failure” appears in the menu after the test, the Transmitter must be sent in to the manufacturer for repair.
6-4 Diagnostics
Measurement recorder (listing)
This option (Measurement recorder) can be retrofit-
In addition to the graphic display of the measure-
ment recorder (see Pg 3-4), the Diagnostics menu
provides the last 500 measured value pairs from the recorder memory as a listing. Each recorder entry occupies one display line. The measured values of both channels are recorded with date and time.
The symbols for min ( ), max ( ) or mean value (
∼
) are displayed after the measurement symbol, if applicable.
Entries in the measurement recorder cannot be edited!
Diagnostics 6-5
O
2
Transmitter 4220X
This page has been left empty for technical reasons.
6-6 Diagnostics
7 Maintenance menu
The Maintenance menu provides all functions for sensor maintenance and adjustment of connected instruments.
Access to the Maintenance level can be protected with a passcode.
• In the measurement point maintenance mode you can view the message list, activate the current source or start calibration.
• The sensor monitor allows to observe the sensor current.
• The current source allows manual adjustement of all active output currents for configuring and checking connected peripheral devices (such as indicators or recorders).
• Temperature probe adjustment allows individual calibration of the connected temperature probe.
• If the Transmitter is equipped with the controller function (Option 483) and the controller has been activated, you can manually enter the controller output (manipulated variable Y).
• The “Reset Sensocheck” submenu only appears when Sensocheck
®
has been switched on. It allows to reset a Sensocheck
®
signal.
However, it is better to perform a calibration.
Measurement point maintenance
Measurement point maintenance allows you to remove the sensor. While the Transmitter is in measurement point maintenance mode, you can clean or replace the sensors. The output current is frozen at its last value, the controller output is either frozen or set to zero and the NAMUR “functional check” signal is active.
Maintenance 7-1
O
2
Transmitter 4220X
The Measurement Point Maintenance menu provides the following submenus:
• Message list
In this submenu you can view the message list containing all active messages (without releasing
• Current source
In this submenu you can manually specify the output currents during maintenance (for current
• Calibration
In this submenu you can start a calibration directly from the Maintenance menu without having to re-
lease the outputs (for calibration, see Pg 5-1 and
the following).
Sensor monitor
The sensor monitor allows to observe and evaluate the sensor current during maintenance.
The uncompensated sensor current and the temperature are displayed.
Current source function
During current source function the output currents do not follow the measured value!
The values can be entered manually.
Therefore, you must make sure that the connected devices (control room, controllers, indicators) do not interpret the current value as a measured value!
In the Current Source menu you can manually adjust the values for the output currents, for example to check connected peripheral devices.
During Multidrop mode the output current 1 is permanently set to 4 mA. This is indicated by the word
“HART”.
7-2 Maintenance
Temperature probe adjustment
During temperature probe adjustment you compensate for the individual tolerance of the temperature probe and the influence of the lead resistances.
This increases the accuracy of the temperature measurement.
Adjustment may only be carried out after the process temperature has been precisely measured using a calibrated reference thermometer!
The measurement error of the reference thermometer should be less than 0.1 °C.
To simplify the adjustment procedure, set “Mea-
surement Display: Variable °C” (see Pg 4-3).
When the measurement display has been set accordingly, the temperature measured by the temperature probe is displayed in the upper right corner.
Switch on Installation Adjustment and enter the process temperature measured by the reference thermometer.
Now the compensated temperature from the temperature probe is displayed in the upper right corner.
The permissible adjustment range is ±5 °C from the value measured by the temperature probe.
Manual entry of controller output
If the Transmitter is equipped with the controller function (Option 483) and the controller has been activated, you can manually adjust the controller output (manipulated variable Y) for test purposes or to start a process.
When you manually adjust the controller output, it no longer follows the controlled variable!
Therefore, you must make sure that the connected actuators and the control loop are monitored accordingly!
Maintenance 7-3
O
2
Transmitter 4220X
You can enter the controller output in the range from -100 % to +100 %, for example to check connected actuators.
When you exit manual controller entry, the Transmitter switches back to automatic controller operation.
With a PI controller (reset time
≠
0), switchover is smooth. This allows you to rapidly start processes with large time constants or dead times.
With the definable feed time alarm, you can monitor the time during which the controller output is at
+100 % or –100 %, i.e. how long the valve is fully open. If this time is exceeded, this may be due to a shortage of air flow or a defective valve, for example.
Reset Sensocheck
®
It allows to reset a Sensocheck
®
signal. However, it is preferable to perform a calibration to determine and eliminate possible errors.
If the Sensocheck
®
signal appears following a successful calibration, it is possible that the adjustment of the sensor has changed during installation due to mechanical stress. Therefore, make sure when installing the sensor that it is not subjected to any mechanical stress (impact, friction, tension).
In running water and in agitated vessels free-floating solids can hit the sensor. This may cause a change in the sensor adjustment. Such a sudden change may be the reason for a Sensocheck
®
message.
7-4 Maintenance
8 Error messages
Error message
Fail Hi Zero
Warn Hi Zero
Warn Lo Zero
Fail Lo Zero
Fail Hi Slope
Warn Hi Slope
Warn Lo Slope
Fail Lo Slope
Warn Identical Media
Warn Media Interchged
Fail Hi Conc Value
Warn Hi Conc Value
Warn Lo Conc Value
Fail Lo Conc Value
Warn Current Par
Fail Hi Temp
Warn Hi Temp
Warn Lo Temp
Fail Lo Temp
Fail Hi Cal Time
Warn Hi Cal Time
Warn Current1 Span
Warn Current1 < 4 mA
Warn Current1 > 20 mA
Warn Current2 Span
Warn Current2 < 0/4 mA
Warn Current2 > 20 mA
Warn Cal Temp
Warn Sensor Unstable
Warn Time/Date
Warn Control Para
Fail CRC Error par
Fail Hi Feed Time
Warn Hi Feed Time
Warn Write Protection
Cause
Sensor zero point > 200 nA or above failure limit
Sensor zero point above warning limit
Sensor zero point below warning limit
Sensor zero point < -200 nA or below failure limit
Sensor slope > –50 pA/mbar or above failure limit
Sensor slope above warning limit
Sensor slope below warning limit
Sensor slope < -1 µA/mbar or below failure limit
Calibration with identical media
Sequence of calibration media interchanged
Concentration above failure limit
Concentration above warning limit
Concentration below warning limit
Concentration below failure limit
Current parameter error at output 1, output 2 (see Pg 4-13)
Temperature > 250 °C or above failure limit
Measured temperature above warning limit
Measured temperature below warning limit
Temperature < -50 °C or below failure limit
Cal timer interval above failure alarm limit
Cal timer interval above warning alarm limit
Current output 1: Start and end value too close
Current output 1: Output current below defined start value
Current output 1: Output current above defined end value
Current output 2: Start and end value too close
Current output 2: Output current below defined start value
Current output 2: Output current above defined end value
Calibration temperature out of range
No stable end value for calibration after 12 to 15 min
Time had to be automatically initialized: The clock must be reset
Parameter error for controller, see Pg 4-20
CRC data error during parameter setting: Check all settings at the Administrator level!
Controller: Feed time above failure limit
Controller: Feed time above warning limit
Write protection violation at “WriteProtect” (HART
®
communication)
Error messages 8-1
O
2
Transmitter 4220X
Error message
Warn Device Diag
Fail System Failure
Fail Hi Saturation
Warn Hi Saturation
Warn Lo Saturation
Fail Lo Saturation
Fail Hi Part. Press.
Warn Hi Part. Press.
Warn Lo Part. Press.
Fail Lo Part. Press.
Fail Hi Press. Signal
Warn Hi Press. Signal
Warn Lo Press. Signal
Fail Lo Press. Signal
Warn Sensocheck
Fail Hi
Fail Lo
Impedance
Impedance
Fail Input Range
Warn Temp O
2
-Conc/SAT
Cause
Diagnostics error: Instrument self-test defective
Clock failure, CRC error in factory settings
Saturation > 600 % AIR or above failure limit
Saturation above warning limit
Saturation below warning limit
Saturation < 0 % AIR or below failure limit
Partial pressure > 2000 mbar or above failure limit
Partial pressure above warning limit
Partial pressure below warning limit
Partial pressure < 0 mbar or below failure limit
Barometric pressure > 1100 mbars or above failure limit
Barometric pressure above warning limit
Barometric pressure below warning limit
Barometric pressure < 700 mbars or below failure limit
Sensocheck message
Impedance above failure limit (open circuit)
Impedance below failure limit (short circuit)
Input overdrive, sensor current too large (see Pg 4-7)
Temperature not within stored chart for water vapor pressure or concentration (Temp < –5 °C or > 60 °C)
8-2 Error messages
9 Product line and accessories
Devices
O
2
Transmitter 4220X
Mounting accessories
Mounting plate, extruded profile AlMg3, 20 µm anodized,
(not required for direct wall mounting)
Bracket kit, brackets hot galvanized, screws stainless steel, wing nuts aluminum anodized, (only in conjunction with ZU 0136 mounting plate)
Protective hood, aluminum AlMg1, 25 µm anodized,
(only in conjunction with ZU 0136 mounting plate)
Protective polyester case, IP 65, protective Macrolon panel, complete with mounting kit
Bracket kit for protective case, brackets hot galvanized, screws stainless steel, wing nuts aluminum anodized, (only in conjunction with ZU 0158)
Further accessories
Power supply/isolator for 24 V AC/DC
Repeater power supply for 90 to 253 V AC (optional 24 V AC/DC)
Repeater power supply with HART
®
transmission
IS loop-powered supply with HART
®
transmission
Options
Logbook
Key-lockable protective panel
Measurement recorder
Current characteristic via enterable table
HART
®
communication
Language selection German, English, French, Italian and Swedish instead of German, English, French, Italian and Spanish
Analog controller (only with Opt. 487)
Second current output (passive)
TAN x x x x
Ref. No.
O
2
4220X
ZU 0136
ZU 0125
ZU 0157
ZU 0158
ZU 0220
WG 20 A2
WG 21 A7
WG 21 A7 Opt. 470
WG 25 A7
Ref. No.
354
432
448
449
467
477
483
487
Product line 9-1
O
2
Transmitter 4220X
This page has been left empty for technical reasons.
9-2 Product line
10 Sensors
Dissolved oxygen sensors of the InPro
®
6000 series
InPro
®
6000 12 mm sensors with screw cap
InPro
®
6000 12 mm sensors with fixed cable
Sensors 10-1
O
2
Transmitter 4220X
InPro
®
6000 25 mm sensors with screw cap
Spare parts for dissolved oxygen sensors of the InPro
®
6000 series
Order No.
Designation
Membrane module, single
T-96
S-96
Membrane kit (4 membrane modules, replacement O rings, 25 ml electrolyte
T-96
S-96
Coupling sleeve N (without probe guard)
Coupling sleeve P (with probe guard)
52 200 071
52 200 072
52 200 024
52 200 025
52 200 037
52 200 038
Accessories
Designation
Electrolyte (25 ml)
O
2
cable with 4-pole plug and open cable ends
1 m
3 m
5 m
Order No.
34 100 2016
32 248 7501
32 248 7503
32 248 7505
10-2 Sensors
Sensor, 12 mm dia.
Installation length a = 120 mm a = 220 mm a = 320 mm a = 420 mm
Spare parts for sensor, 12 mm dia.
T membrane kit (replacement O rings, 4 membrane modules, 25 ml electrolyte)
T membrane module, single
S membrane kit (replacement O rings, 4 membrane modules, 25 ml electrolyte)
S membrane module, single
O
2
electrolyte (25 ml)
Sensor, 25 mm dia.
Installation length a = 70 mm a = 150 mm a = 320 mm
Order no. T type Order no. S type
34 100 3045 34 100 3049
34 100 3046
34 100 3047
34 100 3048
34 100 3050
34 100 3051
34 100 3052
Order no.
34 100 2021
34 100 3040
34 100 3041
34 100 2022
34 100 2016
Spare parts for sensor, 25 mm dia.
Membrane kit (replacement O rings, 4 membrane modules, 25 ml electrolyte)
Membrane module, single
O
2
electrolyte (25 ml)
Order no.
32 275 6800
32 275 6801
32 275 6802
Order no.
32 202 5114
32 204 8617
34 100 2016
Accessories
O
2
cable with 4-pole plug and open cable ends
1 m
3 m
5 m
Order no.
32 248 7501
32 248 7503
32 248 7505
Sensors 10-3
O
2
Transmitter 4220X
This page has been left empty for technical reasons.
10-4 Sensors
11 Specifications
DO measuring input
EEx ia IIC
Ranges
Measuring current
Meas. error
Polarization voltage
Calibration
Sensocheck
Temp measuring input
EEx ia IIC
Ranges
Meas. error
1 input for Mettler Toledo DO sensors
Saturation
Concentration
Partial pressure
Barometric pressure manual
Salt correction
0.0 to 600.0 % Air
0.0 to 120.0 % O
2
0.0 µg/l to 90.00 mg/l
0.0 ppb to 90.00 ppm
0 to 2000 mbar
700 to 1100 mbar
0 to 9999 mbar
0.0 to 45.0 g/kg
0 to 600 nA, resolution 10 pA **
Measuring current < 0.5 % of meas. value ± 0.02 nA
–675 mV
Operating modes *
• Automatic calibration in air-saturated water
• Automatic calibration in air
• Manual entry of saturation
• Data entry
Monitoring of membrane and electrolyte, can be switched off
1 input for Pt 100 / Pt 1000 / NTC 22 k
Ω temperature probe adjustable
Pt100/Pt1000
NTC 22 k
Ω
–50 to +250 °C;
–20 to +130 °C
Pt100/Pt1000
NTC ***
< 0.2 % meas. value ± 0.3 K
< 0.2 % meas. value ± 0.3 K
Temperature compensation
Output 1 *
(current loop)
EEx ib IIC
Nonlinear, preset for Mettler Toledo DO sensors
Operating modes:
• Automatic with NTC 22 k
Ω
• Manual
4 to 20 mA (22 mA), floating, supply unit required user defined for %Air, %O
2
, mg/l, µg/l, pO
2
, °C
Current characteristic definable: linear, trilinear, function or as chart (with Option 449)
As desired within ranges Start/end of scale *
Spans * Saturation
Concentration
Partial pressure
Temperature
10.0 to 600.0 %; 2.0 to 20.0 % O
2
≥
20.0 µg/l, min. 10 % full scale
20 to 1200 mbar
10.0 to 300.0 °C
Output current error
< 0.3 % meas. value + 20 µA
Current source function
4.00 mA to 22.00 mA
Supply voltage
EEx ib IIC
14.3 to 30 V; I
* User-defined
** Reduced accuracy at temperatures > 100 °C max
= 100 mA; P max
= 0.8 W
Specifications 11-1
O
2
Transmitter 4220X
Output 2, (passive) *
(Option 487)
EEx ib IIC
Start/end of scale *
Spans *
Output current error
Current source function
Supply voltage
Defined as switching output
Loadability
Display
Display options
2-channel measurement recorder *
(Option 448)
Languages *
HART
®
Communication
PI controller (Option 483)
Clock
* User-defined
*** Frequency shift keying
0(4) to 20 mA (22 mA), floating, supply unit required user defined for %Air, %O
2
, mg/l, µg/l, pO
2
, °C
Current characteristic definable: linear, trilinear or function or as analog controller output (Option 353)
As desired within ranges
Saturation
Concentration
Partial pressure
Temperature
10.0 to 600.0 %; 2.0 to 20.0 % O
2
± 20.0 µg/l, min. 10 % full scale
20 to 1200 mbar
10.0 to 300.0 °C
< 0.3 % meas. value + 20 µA
0.00 mA to 22.00 mA
1.3 to 30 V; I max
= 100 mA; P max
= 0.8 W
Switching controller, limit or alarm output
DC V max
= 30 V; I max
= 100 mA;
P max
= 0.8 W, voltage drop: < 1.3 V
Graphic LCD, 240 x 64 matrix
Main display
Secondary display
Dialog display character height approx. 20 mm character height approx. 6 mm
7 lines, character height approx. 4 mm
Main display Secondary display
Saturation
Concentration
Saturation
Concentration
[% Air]; [% O
2
]
[mg/l; µg/l]
Partial pressure
Temperature Temperature
Time
Partial pressure
Pressure
Current output 1
Current output 2
Sensor current
Cal timer
Time
[ppm; ppb]
[mbar]
[°C]
[mbar]
[mA]
[mA]
[nA, µA]
[h]
[h,min]
Date [d,m,y]
Man. temperature
Controller output1
[°C]
[%]
Controller setpoint X w
Graphic representation of two process variables in the display user-defined for %Air, %O
2
, conc., pO
2
, °C, pressure, output 1, output 2,
Span and time base definable,
Recording of: Snapshot, min, max or mean value,
500 measurement points with time and date
German, English, French, Italian, Spanish
Option 477: Swedish instead of Spanish
Digital communication by FSK*** modulation of loop current
(output 1 only), point-to-point connection or Multidrop (bus) *
Continuous controller via output 2 (Option 487) user defined for % AIR and % O
2
Real-time clock with date, self-contained
Date format user-definable
11-2 Specifications
Records
Logbook (Option 354)
Device self-test
Calibration record
Data retention in case of power failure
Explosion protection
EMC
Ambient temperature
Enclosure
Cable glands
Dimensions
Weight
For quality management documentation to ISO 9000.
Recording of function activations, appearance and disappearance of warning and failure messages, with date and time
Storage capacity 200 entries available
Test of RAM, EPROM, EEPROM, display and keypad
All relevant data of the last calibration for documentation to GMP
Parameters and factory settings >10 years (EEPROM)
Logbook, cal record
Clock (reserve power)
> 1 year (lithium battery)
> 1 year (lithium battery)
No battery replacement required according to NAMUR NE 32
II 2 (1) G EEx ib [ia] IIC T6 , PTB 00 ATEX 2190
EN 61326/
EN 61326 /A1
VDE 0843 Part 20: 1998-01
VDE 0843 Part 20/A1: 1999-05
Interference immunity to NAMUR EMC recommendation for process and laboratory control equipment
Operation ****
Transport and storage
-20 to +50 °C
-20 to +70 °C
Case with separate terminal compartment, suitable for outdoor mounting
Material: acrylonitrile butadiene styrene, Front: polyester
Ingress protection: IP 65
Metric cable glands
See dimension drawing
Approx. 1.5 kg
**** At ambient temperatures below 0 °C the readability of the display may be reduced.
This does not impair the instrument functions.
Specifications 11-3
O
2
Transmitter 4220X
This page has been left empty for technical reasons.
11-4 Specifications
12 Oxygen solubility table
c s
(p
N
) Oxygen saturation concentration at normal pressure (p
N
= 1013.25 mbars)
8.42
8.26
8.11
7.97
7.83
7.69
7.56
7.43
c mg/l
9.66
9.47
9.28
9.09
8.91
8.74
8.58
7.30
7.18
7.06
6.95
6.83
6.72
6.61
28
29
30
31
24
25
26
27
20
21
22
23 t °C
17
18
19
36
37
38
32
33
34
35
13.83
13.46
13.11
12.77
12.45
12.14
11.84
11.56
c mg/l
16.98
16.46
15.97
15.50
15.05
14.62
14.22
11.29
11.03
10.78
10.54
10.31
10.08
9.87
8
9
6
7
4
5
2
3
–2
–1
0
1 t °C
–5
–4
–3
14
15
16
10
11
12
13
50
51
52
53
46
47
48
49
42
43
44
45 t °C
39
40
41
58
59
60
54
55
56
57
5.88
5.79
5.71
5.63
5.55
5.47
5.39
5.31
c mg/l
6.51
6.41
6.32
6.23
6.14
6.05
5.96
5.24
5.16
5.08
5.00
4.91
4.83
4.74
Bold: EN 25 814: 1992
Not bold: interpolated and extrapolated values
Oxygen solubility table 12-1
O
2
Transmitter 4220X
This page has been left empty for technical reasons.
12-2 Oxygen solubility tables
13 Glossary
3-wire connection
Administrator level
Administrator passcode
Alarm limit
Alarm processing
Calibration menu
Calibration passcode
Calibration record
Calibration sequence
Cal timer
Concentration
Controlled variable
Connection of the temperature probe with a (third) sense line for compensating for the supply lead resistances. Required for exact temperature measurement with long wires.
“adm”, menu level of the Parameter Setting menu.
All device settings and the passcodes can be defined.
Protects access to the Administrator level. Can be set at the Administrator level.
For each process variable, you can define high and low warning and failure limits. The alarm can be activated individually for each variable. If an alarm limit is exceeded, an error message appears.
In the alarm processing function, delay times can be set for the NAMUR Failure, Warning and Functional Check signals. The delay times are treated separately. Alarms can be output as 22 mA signals
via outputs 1 and 2 (see Alarm processing, Pg 4-22)
Menu key for the Calibration menu
Menu for calibrating the Transmitter
Protects access to calibration. Can be set or disabled at the Administrator level.
The calibration record shows all relevant data of the last calibration for documentation to GMP.
Four different methods are available for calibration:
Automatic calibration in air-saturated water, automatic calibration in air, manual entry of saturation and data entry.
Counts the time passed since the last calibration.
The cal timer count can be monitored with alarm limits.
With Henry’s Law, the oxygen concentration can be calculated from the oxygen partial pressure via a solubility coefficient.
User-defined variable that acts on the controller.
Glossary 13-1
O
2
Transmitter 4220X
Cursor keys
Delay
Diagnostics menu
DO sensor
Failure
Feed time alarm
First calibration
Functional check
GMP
HART
®
Information display
Interval
Language selection
Limit contact
and , serve to select entry positions or digits during number entry.
User-defined time until the NAMUR signals “Warning” and “Failure” react to an alarm message and an off-delay of the NAMUR signal “Functional check”.
Menu key for the Diagnostics menu
Display of all relevant information on the device status.
Dissolved oxygen sensor – O
2
-sensitive sensor
Key for confirming entries
Failure is a NAMUR signal. The limits are set in the
Alarm Settings menu.
Failure means that the equipment no longer operates properly or that a process parameter has reached a critical value.
Monitors the time during which the controller output is at 100 %.
During First Calibration, the sensor data are stored as reference values for sensor statistics.
Functional check is a NAMUR signal. This signal is active during parameter setting, calibration and
maintenance (see Alarm processing, Pg 4-22).
Good Manufacturing Practice: Rules for performance and documentation of measurements.
Digital communication by superimposing digital signals on the loop current.
Information text for operator guidance or indication of device status. Marked with i .
Time from the start of one device test to the start of the next device test, user defined.
In the Parameter Setting menu, you can select the user interface language: The language can be selected without entering a passcode.
Is controlled by a user-defiable process variable.
The limit contact is activated if the measured value falls below or exceeds an alarm limit, depending on the user-defined effective direction.
13-2 Glossary
Logbook
Main display
Maintenance menu
Maintenance passcode
Manipulated variable
Measurement recorder
Measuring mode
Menu
Menu level
Message list
NAMUR
NAMUR signals
The logbook shows the last 200 events with date and time, e.g. calibrations, warning and failure messages, power failure etc. This permits quality management documentation to ISO 9000.
Large measured-value display in the measuring mode. The displayed process variable can be defined. The process variable of the main display is shown in the menus in the upper right corner.
Menu key for the Maintenance menu
The Maintenance menu provides all functions for sensor maintenance and adjustment of connected devices.
Protects access to Maintenance. Can be set or disabled at the Administrator level.
Output variable of the controller, controls output 2.
Menu key. Pressing allows return to measuring mode from all other menus.
Two-channel recorder for optical display of the process development on the system display. One process variable can be assigned to each channel.
When no menu function is activated, the Transmitter is in measuring mode. The selected measured value is displayed. You can always return to the measuring mode by pressing .
Pressing a menu key ( , , or
), gives access to a menu from which you can select the corresponding functions.
The menu is divided into several menu levels.
You can switch between the different levels by pressing the corresponding menu key or a cursor
The message list shows the number of currently activated messages and the individual warning or failure messages in plain text.
German committee for measurement and control standards in the chemical industry
Failure, warning and functional check are NAMUR signals. They can be assigned to outputs 1 and 2 as
22 mA signals. The limits for failure and warning are set in the Alarm Settings menu.
Glossary 13-3
O
2
Transmitter 4220X
Operator level
Operator passcode
Oxygen concentration
Oxygen partial pressure
Oxygen saturation
Parameter Setting menu
Partial pressure
Passcode protection
Percent saturation
Polarization time
Pulse suppression
Recorder
Scrolling key
Secondary display
Sensor slope
13-4 Glossary
“opl”, menu level of the Parameter Setting menu.
You can edit the device settings that have been enabled at the Administrator level.
Protects access to the Operator level. Can be set or disabled at the Administrator level.
See Concentration
See Partial pressure
See Percent saturation
Menu key for the Parameter Setting menu
The Parameter Setting menu is divided into three submenus: Viewing level (view), Operator level
(opl) and Administrator level (adm)
Share of a gas to the total pressure of the gas mixture
Access to the Calibration, Maintenance, Operator and Administrator levels is protected by passcodes.
The passcodes can be defined or disabled at the
Administrator level.
Ratio (in percent) of the measured quantity of O
2
to the highest possible quantity (saturation)
Time after power-on of the Transmitter until the sensor delivers stable measured values (also see operating instructions of sensor)
To increase immunity to interference, a disconnectable input filter suppresses transient interference pulses while slow changes of the measured value are detected immediately.
See Measurement recorder
and : Keys for selecting menu lines or entering numbers.
Two small displays located below the main display in measuring mode. The process variables to be displayed can be selected using / and
/ .
Specified in pA/mbar
Sensor statistics
Slope
Tag number
TAN
Temperature compensation
Viewing level
Warning (maintenance required)
Zero point
The sensor statistics provide the sensor data of the last three calibrations and the first calibration.
See Sensor slope.
Can be defined to identify the Transmitter and can be displayed in the diag menu.
For HART
®
transmission, the first 8 characters are used as “TAG”.
Transaction number for later installation of software options.
Correction of temperature dependence of membrane diffusion
“view”, menu level of the Parameter Setting menu.
Display of all device settings, however no editing possible.
Alarm message, means that the equipment is still operating properly but should be serviced, or that process parameters have reached a value requiring intervention.
Sensor signal which is output when measuring in an oxygen-free medium.
Glossary 13-5
O
2
Transmitter 4220X
This page has been left empty for technical reasons.
13-6 Glossary
14 Index
3-way mixing valve ,
3-wire connection, Explanation ,
A
Accessories ,
Administrator level ,
Explanation ,
Administrator passcode ,
Explanation ,
Alarm contact ,
Alarm limit, Explanation ,
Alarm processing ,
Explanation ,
Alarm settings
Assembly
ATEX Certificate ,
Automatic calibration ,
B
Bracket kit
C
Cal record ,
Cal timer
Explanation ,
cal, Explanation ,
Calibration ,
Automatic ,
Data entry ,
Freeze output currents ,
Manual entry of saturation ,
Monitoring functions
Calibration menu
Explanation
Calibration passcode, Explanation ,
Calibration record
Explanation
Calibration sequence, Explanation ,
Calibration timer alarm
Cleaning ,
Clock, setting ,
Concentration, Explanation ,
Control beginning ,
Control end ,
Controlled variable, Explanation ,
Controller ,
Control characteristic
Controlled variable ,
Controller output
Manual
Parameter setting, Error messages
Corner point ,
Bilinear output curve
Trilinear output curve
Current output
Falling curve ,
Output curve
Settings
Error messages
Span ,
Current output 1
Current output 2
Current source function
Cursor key, Explanation ,
Index 14-1
O
2
Transmitter 4220X
D
Date format ,
Declaration of Conformity ,
Delay, Explanation
Device description
Device diagnostics
diag, Explanation
Diagnostics menu, Explanation ,
Display, Viewing angle ,
DO sensor, Explanation ,
E
EC Declaration of Conformity ,
EC-Type-Examination Certificate ,
Effective direction ,
enter, Explanation ,
Error messages ,
F
Factory setting, reset to ,
Failure, Explanation
Feed time alarm ,
Explanation ,
First calibration ,
Explanation ,
Functional check, Explanation ,
G
Glossary ,
GMP, Explanation ,
H
HART® communication ,
Hysteresis ,
I
Information display, Explanation ,
Input filter
Installation ,
Interval, Explanation
L
Language selection ,
Limit contacts ,
Effective direction
Explanation
Hysteresis ,
Logbook ,
Explanation
M
Main display, Explanation ,
maint, Explanation
Maintenance
Maintenance menu, Explanation ,
Maintenance passcode, Explanation
Manipulated variable, Explanation ,
Marker setting ,
meas, Explanation
Measurement display ,
Measurement point maintenance
Measurement recorder ,
Average
Explanation
14-2 Index
Max Value ,
Min Value ,
Snapshot ,
Measuring mode ,
Explanation ,
Memory test
Menu level, Explanation ,
Menu operation ,
Keypad assignment ,
Menu structure
Menu, Explanation ,
Message list ,
Explanation ,
Mounting plate ,
N
NAMUR signals ,
Explanation ,
NAMUR, Explanation ,
Neutral zone
Note ,
O
One-point calibration ,
Operator level ,
Explanation ,
Operator passcode, Explanation ,
Option release
Options ,
Output 2
Alarm contact ,
Typical wiring ,
Wash contact ,
Output curve
Bilinear ,
Function ,
Linear
Logarithmic ,
Trilinear
User-defined chart
Oxygen concentration alarm ,
Oxygen concentration, Explanation ,
Oxygen partial pressure alarm
Oxygen saturation (referred to air)
Explanation
Oxygen saturation alarm
Oxygen solubility table ,
P
Package contents , VII par, Explanation
Parameter setting
Administrator level
Marker setting ,
Factory setting
Language selection ,
Operator level
Viewing level ,
Parameter Setting menu, Explanation ,
Partial pressure, Explanation ,
Passcode entry
Passcode protection, Explanation ,
Passcode, factory set
Percent saturation, Explanation
Polarization time, Explanation ,
Pressure alarm ,
Pressure correction ,
Product line ,
Proper use
Protective case ,
Protective hood ,
Index 14-3
O
2
Transmitter 4220X
Pulse suppression, Explanation ,
R
Recorder ,
Reset time ,
S
Safety information ,
Salt content ,
Scrolling key, Explanation ,
Secondary display
Explanation ,
Process variables ,
Self test ,
Sensocheck®
Reset ,
Sensor data, Setting ,
Sensor monitor ,
Sensor slope, Explanation ,
Sensor statistics ,
Explanation ,
Sensormonitor
Setpoint
Slope ,
Slope alarm
Software retrofitting
Solubility table ,
Span
Specifications
Straightway valve
T
Tag note ,
Tag number
Explanation
TAN ,
Temp probe adjustment
Temperature alarm ,
Temperature compensation
Automatic
Manual
Temperature detection
Terminal assignments ,
Transaction number
Two-point calibration
U
User interface
V
Viewing angle adjustment
Viewing level ,
Explanation
W
Warning, Explanation ,
Wash contact
Z
Zero point alarm ,
Zero point, Explanation ,
14-4 Index
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Table of contents
- 22 Assembly, installation, and maintenance
- 22 Assembly
- 22 Installation and commissioning
- 22 Notes concerning performance
- 22 Maintenance and cleaning
- 23 Transmitter 4220X
- 23 Transmitter 4220X
- 23 Terminal assignments
- 23 Dissolved oxygen measurement
- 23 Temperature detection
- 23 Passive output
- 23 Typical wiring
- 24 Transmitter 4220X
- 24 User interface
- 24 Measuring mode
- 24 Measurement recorder
- 24 Menu structure
- 24 Menu operation
- 68 Parameter setting
- 68 Language selection
- 68 The three levels of parameter setting
- 68 Factory setting
- 68 Measurement display
- 68 Input filter
- 68 Pressure correction
- 68 Salt content
- 68 Temperature detection
- 68 Sensor data
- 68 Output
- 68 Alarm settings
- 68 Alarm processing / NAMUR signals
- 68 Communication
- 68 Setting the clock
- 68 Point of measurement/note
- 68 Device diagnostics
- 68 Measurement recorder
- 68 Passcode entry
- 68 Release of options
- 69 Calibration
- 69 Why do you have to calibrate?
- 69 Monitoring functions for calibration
- 69 Calibration menu
- 69 What does “First Calibration” mean?
- 69 One-point or two-point calibration?
- 69 Automatic calibration in water or air
- 69 Calibration with manual entry of saturation
- 69 Calibration by data entry
- 77 Diagnostics menu
- 77 Message list
- 77 Cal record
- 77 Sensor statistics
- 77 Logbook
- 77 Device description
- 77 Device diagnostics
- 77 Measurement recorder (listing)
- 78 Maintenance menu
- 78 Measurement point maintenance
- 78 Sensor monitor
- 78 Current source function
- 78 Temperature probe adjustment
- 78 Manual entry of controller output
- 79 Error messages
- 80 Product line and accessories
- 81 Sensors
- 82 Specifications
- 83 Oxygen solubility table
- 84 Glossary
- 85 Index