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Moisture Analyzer
Excellence HS153
Excellence
Table of Contents
Conventions and Symbols Used in these Operating Instructions
Definition of Signal Warnings and Symbols
Basic Elements on Touch Screen
Installation and Putting into Operation
Setting Reading Angle of Terminal
Install METTLER TOLEDO RHT sensor
Table of Contents 3
Settings of Switch-off Criterion (SOC)
4 Table of Contents
Graphical Evaluations of Measurement Results
Explanatory note to periodic inspections in accordance with EU Directive
Table of Contents 5
Measurement Principle of Halogen Moisture Analyzer
Notes on Adjustment of Balance and Heating Module
Further Information on Moisture Determination
Recommended Printer Settings (Strip printer)
6 Table of Contents
1 Introduction
Thank you for purchasing a Halogen Moisture Analyzer from METTLER TOLEDO.
Your Moisture Analyzer is fast and reliable. It offers a high level of operating convenience and useful functions to facilitate determination of the moisture content of your samples.
Behind your instrument stands METTLER TOLEDO, a leading manufacturer of not only balances and scales for the lab and production, but also analytical measuring instruments. A customer service network covering the entire globe with well trained personnel is your service at all times, whether you are choosing accessories or require guidance for a specific application to ensure optimum utilization of your instrument.
Your Halogen Moisture Analyzer is used for determining the moisture content of almost any substance. The instrument works on the thermogravimetric principle. At the start of the measurement the Moisture Analyzer determines the weight of the sample, the sample is then quickly heated by the integral halogen heating module and the moisture vaporizes. During the drying process the instrument continually measures the weight of the sample and displays the reduction in moisture. Once drying has been completed, the moisture or solids content of your sample is displayed as the final result.
Of decisive importance in practice is the rate of heating and even heating of the surface of the sample. In com parison with conventional infrared heating or the drying oven method, for example, the halogen heating module of your instrument needs a shorter time to reach its maximum heating power. It also allows use of high temper atures, an additional factor in shortening the drying time. Uniform heating of the sample material ensures good repeatability of the drying results and makes it possible to use a smaller amount of sample.
The Moisture Analyzer conforms with all common standards and directives. It supports stipulations, work tech niques and result records as demanded by all international quality assurance systems, e.g. GLP (Good Labora tory Practice), GMP (Good Manufacturing Practice). The instrument has a CE declaration of conformity and
METTLER TOLEDO as the manufacturer has been awarded ISO 9001 and ISO 14001 certification. This provides you with the assurance that your capital investment is protected in the long term by a high product quality and a comprehensive service package (repairs, maintenance, servicing, adjustment service).
Finding More Information
u www.mt.com/hxhs
Software version
These operating instructions are based on the initially installed firmware (software) version V2.0.
1.1 Conventions and Symbols Used in these Operating Instructions
1
2 …
Key and button designations are indicated by a picture or text in square brackets (e.g. [Save]
These symbols indicate an instruction: prerequisites steps results
Introduction 7
2 Safety Information
2.1 Definition of Signal Warnings and Symbols
Safety notes are marked with signal words and warning symbols. These show safety issues and warnings.
Ignoring the safety notes may lead to personal injury, damage to the instrument, malfunctions and false results.
Signal Words
WARNING
for a hazardous situation with medium risk, possibly resulting in severe injuries or death if not avoided.
CAUTION
Attention
Note
for a hazardous situation with low risk, resulting in damage to the device or the property or in loss of data, or minor or medium injuries if not avoided.
(no symbol) for important information about the product.
(no symbol) for useful information about the product.
Warning Symbols
General hazard Electrical shock
Hot surface
Toxic substance
Inflammable or explosive substance
Acid / Corrosion
2.2 Product Specific Safety Notes
General Safety Information
Your instrument meets the state of the art technology and complies with all recognized safety rules, however, certain hazards may arise in extraneous circumstances. Do not open the housing of the instrument: It does not contain any parts which can be maintained, repaired or replaced by the user. If you ever have problems with your instrument, contact your authorized METTLER TOLEDO dealer or service representative.
Always operate and use your instrument only in accordance with the instructions contained in this manual. The instructions for setting up your new instrument must be strictly observed.
If the instrument is not used according to these Operating Instructions, protection of the instrument may be impaired and METTLER TOLEDO assumes no liability.
Intended Use
Your Moisture Analyzer is used for determining the moisture in samples. Use the instrument exclusively for this purposes. Any other type of use and operation beyond the limits of technical specifications without written con sent from Mettler-Toledo AG, is considered as not intended.
Moisture determination applications must be optimized and validated by the user according to local regula tions. Application-specific data provided by METTLER TOLEDO is intended for guidance only.
It is not permitted to use the instrument in explosive atmosphere of gases, steam, fog, dust and flammable dust (hazardous environments).
8 Introduction
Staff Safety
The Moisture Analyzer may be operated only by trained personnel who are familiar with the properties of the samples used and with the handling of the instrument.
In order to use the instrument, you must have read and understood the operating instructions. Keep the operat ing instructions for further reference.
Never make any modifications to the instrument and use only original spare parts and optional equipment from
METTLER TOLEDO.
Protective Clothing
It is advisable to wear protective clothing in the laboratory when working with the instrument.
A lab coat should be worn.
A suitable eye protection such as goggles should be worn.
Use appropriate gloves when handling chemicals or hazardous substances, checking their integrity before use.
Safety Notes
Risk of electric shock
Your instrument is supplied with a 3-pin power cable with an equipment grounding conduc tor. Only extension cables which meet this relevant standards and also have an equipment grounding conductor may be used. Intentional disconnection of the equipment grounding conductor is prohibited.
The Halogen Moisture Analyzer works with heat!
a) Ensure sufficient free space around the instrument to avoid heat accumulation and over heating (approx. 1 m free space above the heating module).
b) The vent over the sample must never be covered, plugged, taped over or tampered with in any other way.
c) Do not place any combustible materials on, under or next to the instrument since the area around the heating module may be hot.
d) Exercise caution when removing the sample. The sample itself, the sample chamber, the draft shield and any sample vessels used may still be very hot.
e) During operation, you should never open the heating module itself as the ring-shaped heating reflector or its protective glass can reach 400 °C! If you have to open the heating module e.g. for maintenance, disconnect the instrument from the power supply and wait until the heating module has cooled down completely.
f) No modifications must be made within the heating module. It is particularly dangerous to bend any components or remove them or to make any other changes.
Safety Information 9
Certain samples require special care!
With certain types of samples, there is a possibility of danger to personnel or damage of property. Please note that the user always has the responsibility and liability for damage caused by use of any types of samples!
Fire or Explosion
• Flammable or explosive substances.
• Substances containing solvents.
• Substances which evolve flammable or explosive gases or vapors when heated.
a) In cases of doubt, perform a careful risk analysis.
b) Work at a drying temperature that is low enough to prevent the formation of flames or an explosion.
c) Wear protective goggles.
d) Work with small amounts of sample.
e) Never leave the instrument unattended!
Substances which contain toxic or caustic components
Toxic gases produced during drying could cause irritations (eyes, Skin, breathing), illness or death.
– Such substances may be dried only in a fume cupboard.
Corrosion
Substances which evolve corrosive vapors when heated (e.g. acids).
– Work with small amounts of samples as the vapor can condense on cooler housing parts and cause corrosion.
10 Safety Information
3 Design and Function
In order to work with your Moisture Analyzer, you need to familiarize yourself with the instrument layout, drying unit, graphical user interface of the touch screen as well as the terminal.
3.1 Overview
3.1.1 Drying Unit
Description of the components and the external connectors on the back of the drying unit (Weighing unit with heating module).
1 2 3 4
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14
15
16
12
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10
9
8
7
6
5
1 Sample chamber
2 Sample pan handler
3 Sample pan holder
4 Leveling screw
5 Level indicator
6 Draft shield element
7 Contacts for temprature adjustment kit(optional)
8 Power contacts for halogen lamp
9 Temperatur sensor
10 Heating module (with ter mal overload protection)
11 Handles for opening the sample chamber
12 Inspection window and vent
13 Fan
14 Dust filter (optional)
15 Power line fuse
16 Power supply socket
17 Kensington slot for antitheft purposes
18 Humidity sensor connec tion (n.a.)
19 Fastening for terminal stand (optional)
20 System connection (termi nal cable)
21 Aux 2 connection (n.a.)
22 Aux 1 connection (n.a.)
17 18 19 20 21 22 4
Connectivity
20 System connection
19 Power supply socket
Interface for the communication between terminal and drying unit.
Power supply inlet socket for the country-specific power cable.
The socket has a built in fuse compartment containing a replacement fuse.
Design and Function 11
18 RHT sensor connection
Connection for the RHT sensor from METTLER TOLEDO for detecting the current room temperature and relative humidity for SmartCal™ application. Attention
Do not use this port for other purposes!
3.1.2 Terminal
Description of the connections at the terminal (Input and output unit with interfaces).
1
EXCELLENCE
1 WVGA color display (touch screen)
2 Foot
3 USB Host connection
4 Faceplate
5 USB Host connection
6 USB Device connection
7 RS232C connection
8 Ethernet RJ45 connection
(n.a.)
9 System connection (termi nal cable)
10 Memory Card slot for SD
Card
3
2
4 5 6 7 8 9 4
2
10
12 Design and Function
Connectivity
1 System connection
2 RS232C connection
3 USB Host connection
4 USB Device connection
5 Ethernet TCP/IP connection
6
7
WLAN connection
SD Memory Card slot
Interface for the communication between terminal and drying unit.
RS232C interface for connecting the instrument to a peripheral device
(e.g. printer or a PC with a 9-pin male connector).
USB interface for connecting a peripheral device to the instrument
(e.g. memory stick up to 32 GB). Type A Socket.
USB interface for connecting the instrument to a peripheral device with an USB host connection (e.g. PC). Type-B socket.
Ethernet interface for connecting the instrument to a TCP/IP network.
The most simple network can be implemented by connecting the instrument directly to the PC with a cross-over cable (RJ45 Socket).
DHCP and fix IP addresses are supported.
Wireless LAN interface for connecting the instrument to a wireless
TCP/IP network. DHCP and fix IP addresses are supported.
Note
This function is not available in every country.
The memory card slot fits Secure Digital Memory Cards. SD and
SDHC types as well as sizes up to 32 GB are supported. You can use it as an external storage device e.g. to store measured results.
Note
SDXC types are not supported.
Design and Function 13
3.1.3 Keys on Terminal
2
3
1
1 3 2
To switch on or off (standby operation) the instrument.
Note
Do not disconnect the instrument from the power supply except if you will not be using the instrument for an extended period.
Home
To return from any menu level, or other window to the user home screen.
Touch screen area.
14 Design and Function
3.2 User Interface
The colored touch screen is a touch-sensitive WVGA monitor. The touch screen not only displays information, it also allows you to enter commands by touching certain areas on its surface: You can choose the information displayed on the screen, change terminal settings or perform certain operations on the instrument.
Only those elements which are available for the current dialog appear on the display.
Buttons on the Touch Screen
Buttons are software elements on the touch screen (Soft keys).
Do not touch the touch screen with pointed or sharp objects!
This may damage the touch screen.
Design and Function 15
3.2.1 User "Home" Screen
The user Home screen is the main screen and appears after startup or login of the instrument. All screens of the user interface can be accessed from the home screen. Returning to the Home screen is possible from all other screens of the user interface by pressing the [ ] key or tapping the [Home] button.
2
2
1
3
1
2
3
Name
Measurement
Explanation
Start measurement
Prerequisite:
Method is defined and all necessary settings are made.
For further information see My First Measurement (page 31) and Measurement
Results Show results
Under this menu item, all measurement results can be displayed, printed or exported.
For further information see Results (page 93).
Method Definition Define, edit or delete a method
Test/Adjust
Settings
Instrument info
All actions using in a drying method, can be defined under this menu item.
Description of the menu item see Method Definition (page 71).
Adjust or test the instrument
Under this menu item, the integrated balance and the heating module can be adjusted or tested.
Description of the menu item see Test/Adjust (page 61).
Define general settings
All settings of the system can be defined, e.g, system settings, user management or user preferences. These settings are usually made during installation of the instrument.
Description of the menu item see Settings (page 34)
User shortcuts
User-specific shortcuts for frequently used methods. Shortcuts are saved in the user profile.
How to create shortcuts see Using Shortcuts (page 91).
Shows general info about the instrument like type, serial number, software ver sion.
16 Design and Function
3.2.2 Basic Elements on Touch Screen
The graphical user interface consists of the following basic elements.
Screen Areas and their Elements
1
2
3
Name
1
Status Bar
2
Title Bar
3
Content Area
4
Action Bar
4
Explanation
The status bar contains the user name, status icons as well as date and time.
See Status Message Icons (page 17).
The title bar contains elements for the user's orientation and information, as well
as for special functions. See Title Bar Icons (page 17).
The content area is the main working area of the menus and the applications, content depends on application or performed action. The content area also shows graphic illustrations such as the curve diagram of a data set (e.g. drying curve).
The action bar contains action buttons for triggering the actions which are required and available in the current dialog (e.g. Back, ->0/T<-, Print, Save,
Delete, OK). See Action Bar Buttons (page 17).
3.2.3 Icon and Buttons
3.2.3.1 Status Message Icons
Status messages are displayed by means of small icons in the status bar. For the most important messages
see Status Messages (page 106).
By tapping the symbols, the explanation of the symbols will appear in a separate window. By tapping the quick access icon , brightness or sound can be set.
3.2.3.2 Title Bar Icons
The title bar icons only appear when they are active. The icons which appear in the title bar, are listed with their function below:
Explanation
Create a shortcut and add it to your user home screen. Edit or remove an existing shortcut
see Using Shortcuts (page 91).
3.2.3.3 Action Bar Buttons
The action bar contains action buttons for triggering any of the actions which are required and available in the current dialog (e.g. Back, ->0/T<-, Print, Save, Delete, OK). There are up to six action buttons available for a work step. The functions of these buttons are self explanatory and therefore not discussed further.
Design and Function 17
3.2.4 Input Dialogs
3.2.4.1 Entering Text and Numbers
The keyboard dialog allows you to enter characters including letters, numbers and a variety of special charac ters. The country-specific layout of the keyboard is in accordance with the selected language, see Regional Set
1
1
2
2
Name
1
Input field
2
3
Explanation field
Shift
Explanation
The maximum number of characters allowed is indicated.
You can enter lower and upper case letters by toggling . Switch the keyboard by tapping the corresponding button in the action bar, for entering numbers, spe cial characters or letters
– Confirm with [OK] (To exit keyboard tap [Cancel]).
Function
Shift-Lock
Delete last character
Cursor left
Cursor right
Note
It is also possible to place cursor directly in input field by tapping the respective position.
18 Design and Function
3.2.4.2 Entering Numerical Values
The numerical keypad dialog allows you to enter numerical values.
1
2
2
3
3
1
Name
Switch
Explanation
If a switch appears, located on the left side in the title bar; it must be switched on for the entry of a value: O = OFF, I = ON
2
Input field
3
Explanation field The valid input range is indicated.
– Confirm with [OK].
To exit keypad, tap [Cancel].
Function
Delete last character
Cursor left
Cursor right
Design and Function 19
3.2.4.3 Changing Date and Time
This dialog (Picker view) allows you to set the date and time by picking from the built-in calendar/clock.
1
2
2
3
3
Name
1
Pick button
2
Explanation field
3
Pick button
Explanation
Pick button upwards (input control)
Current value
Pick button downwards (input control)
– Confirm with [Set date]. (To exit without changing, tap [Cancel].)
20 Design and Function
3.2.5 Lists and Tables
Simple list view
Basic elements of a simple list including a content title. If necessary, the content area can be scrolled vertically and can be arranged in a different order.
1
2
3
4
5
6
Name
1
Content title
2
Content area
3
Arrow icon
4
5
6
Scrollbar
Further types of lists:
Explanation
[ i] Showing the list in ascending order.
[ h] Showing the list in descending order.
Scrolling up
Scroller
Scrolling down
Accordion panels can be opened or closed by tapping
[ ].
Closable panels can be opened or closed by tapping
[>].
Design and Function 21
3.2.6 Work Screen
The work screen is used for performing main tasks e.g. measurements.
1
4
2
2
3
5
6
Name
1
Name field
2
Shortcut button
3
Value panel
4
Graphics panel
5
ID panel
6
Parameter panel
7
Action buttons
7
7
Explanation
Name of current Method
Adding/editing a shortcut to the home screen for this method
Displays the current measured values of the work process
E.g. graphical illustrations of the drying curves, instructions for the user for per forming tasks, and weighing-in aid
Identifications (IDs) appear after tapping the ID panel for entering or editing val ues (comments). ID panel appears only if identification input is activated in the menu.
Displays the parameters of the current work process. A detailed overview of the method parameters appears after tapping the parameter panel.
Depending on the current context
Measurement in progress
22 Design and Function
3.2.7 Graphics View
Graphical view of single measurement Chart view of series of measurements
For further information see Graphical Evaluations of Measurement Results (page 93)
Design and Function 23
4 Installation and Putting into Operation
In this section you will find information how to put your new instrument into operation.
4.1 Scope of Delivery
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Open the package and remove drying unit, terminal and the accessories. Check the completeness of the deliv ery. The following accessories are part of the standard equipment of your new Moisture Analyzer:
80 aluminum sample pans
1 Sample handler
1 Sample pan holder
1 Draft shield
1 Specimen sample (circular, absorbent glass fibre filter)
1 Power cable (country specific)
1 Terminal cable (Interface Terminal – drying unit)
1 Operating instructions
1 Application brochure «Guide to Moisture Analysis»
1 Production certificate
1 Declaration of conformity
Remove the packaging from the instrument. Check the instrument for transport damage. Immediately inform your METTLER TOLEDO representative if you have any complaints or parts are missing.
Note
Store all parts of the packaging. This packaging guarantees the best possible protection for the transport of your instrument.
4.2 Location
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Your Moisture Analyzer is a precision instrument. An optimum location guarantees accuracy and dependability.
Make sure that the following environmental conditions are met:
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Operate the instrument only indoors and at an altitude of less than 4000 m above sea level.
Before switching on the instrument, allow all its parts to reach room temperature (+5 to 30°C).
Make sure that the relative humidity is between 20% and 80% and non-condensing conditions are met.
The power plug must be easily accessible.
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Firm, horizontal location as free from vibrations as possible.
Avoid direct sunlight.
No excessive temperature fluctuations.
No powerful drafts.
Surroundings as free from dust as possible.
Sufficient clearance around the instrument to allow warm air to dis sipate.
Sufficient distance from heat-sensitive materials in the vicinity of the instrument.
24 Design and Function
Substances which contain toxic or caustic components
Toxic gases produced during drying could cause irritations (eyes, Skin, breathing), illness or death.
– Such substances may be dried only in a fume cupboard.
4.3 Connecting Instrument
Risk of electric shock
a) Use only the 3-pin power cable with equipment grounding conductor which was supplied with your instrument.
b) Only a 3-pin grounded outlet for connecting your instrument must be used.
c) Only extension cables which meet this relevant standards and also have an equipment grounding conductor may be used.
d) Intentional disconnection of the equipment grounding conductor is prohibited.
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Attention
● First, check whether the voltage printed on the type plate of the drying unit matches your local line voltage. If this is not the case, on no account connect the drying unit to the power, but contact your METTLER TOLEDO sales representative or dealer.
Two different versions of drying units with country-specific power cable are available (110 V AC or
230 V AC).
The power plug must be always accessible.
Before operating, check all cables for damage.
Guide the cables so that they cannot become damaged or interfere with the measuring process.
Connecting the Terminal to the Drying Unit
Drying unit and terminal are at the final location.
1 Connect one end of the supplied terminal cable to the system connection socket on the terminal, see Termi
2 Screw the connector firmly.
4 Screw the connector firmly.
Connecting the Drying Unit to the Power Supply
Terminal – drying unit interface is connected.
1 Connect one end of the power cable to the power supply socket on the drying unit, see Drying Unit
2 Connect the other end to the power line outlet.
Installation and Putting into Operation 25
4.4 Setting up Drying Unit
3 1 2
Terminal and drying unit are connected.
1 To switch on the Instrument, press [ ].
2 Open the sample chamber.
3 Place the draft shield element (1). Only one position is possible.
4 Insert the sample pan holder (2) carefully. Check that the sample pan holder is hooked correctly.
5 Insert the sample pan handler (3).
Note
When putting into operation for the first time or if the instrument is disconnected from the power over a longer period, leave the instrument connected to the power supply for at least 5 hours to allow the built-in recharge able battery to charge up! This battery ensures that the date and time are not lost when the instrument is dis connected from the power. This battery can not be replaced by the user. Please contact a METTLER TOLEDO representative.
4.5 Leveling Drying Unit
Exact horizontal positioning and stable installation are prerequisites for repeatable and accurate results. To compensate for small irregularities or inclinations (±2 %) at the location, the instrument must be leveled.
26 Installation and Putting into Operation
For exact horizontal positioning, the drying unit has a level indicator
(level) and 2 leveling screws. When the air bubble in the level indica tor is exactly in the center, the instrument is standing perfectly horizon tally. To level it, proceed as follows:
1 Position your Moisture Analyzer at the selected location.
2 Turn the two leveling feet until the air bubble is in the center of the level indicator.
L = left foot
R = right foot
L
R
Air bubble at "12 o'clock" turn both feet clockwise
Air bubble at
Air bubble at
Air bubble at
"3 o'clock"
"6 o'clock"
"9 o'clock" turn left foot clockwise, right foot counterclock wise turn both feet counter clockwise turn left foot counterclock wise, right foot clockwise
Note
The drying unit should be re-leveled each time its location is changed.
Leveling the drying unit with optional stand for terminal mounted.
Stand for terminal see Accessories and Spare Parts (page 115).
The drying unit is positioned at the selected loca tion.
1 To loose the clamps for the safety feet of the stand, turn them outwards.
2 Level the drying unit as previously described.
3 To lock the clamps for the safety feet, turn them inwards as far as they will go.
Installation and Putting into Operation 27
4.6 Anti-theft Device
For protection against theft, your drying unit is fitted with a Kensington security slot for an anti-theft device.
To find a suitable anti-theft cable see Accessories and
4.7 Setting Reading Angle of Terminal
– To change the reading angle, fold out the two tilt feet.
4.8 Setting Date and Time
Navigation: Home > Settings > System settings > Regional Settings
When you put your new instrument into operation for the first time, you should enter the current date and time as well as the country in which the instrument is operated. These settings are retained even if you disconnect your instrument from the power supply.
Note
Various languages are available for the dialog with your instrument and can be selected in the menu:
Navigation: Settings > User preferences, see User Preferences.
Set the current date
Regional Settings is selected.
1 Tap Date.
2 Set day, month and year.
3 Confirm with [Set date].
Set the current time
Regional Settings is selected.
1 Tap Time.
2 Set Hours and minutes.
3 Confirm with [Set time].
Set the country in which the instrument is operated.
Regional Settings is selected.
1 Tap Country.
2 Set the country (region).
3 Confirm with [Save].
28 Installation and Putting into Operation
Note
For changing the format for date and time, see Regional Settings (page 37).
4.9 Adjustment
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To obtain accurate measuring results, it is necessary to adjust the integrated balance as well as the heating module.
Adjusting is necessary: before the instrument is used for the first time.
at regular intervals.
after a change of location.
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The following adjustment options are possible:
Balance adjustment with external weight (accessory).
Temperature adjustment with temperature adjustment kit (accessory).
For more information to perform these operations see Test/Adjust (page 61).
4.10 Install METTLER TOLEDO RHT sensor
The RHT sensor from METTLER TOLEDO allows the automatic detection of relative humidity and temperature values for SmartCal tests, see SmartCal test.
Note
Not delivered with every model.
Installation on the Drying Unit
1 Loosen the two screws.
2 Remove screws and cover.
3 Retain these for later use.
1 Take the sensor out of its packing.
2 Retain the packing for later use.
3 Connect the RHT sensor to the drying unit with sensor opening (A) facing down.
A
Installation and Putting into Operation 29
– Tighten the two screws to secure the RHT sensor.
Attention
Please observe the following instructions to avoid wrong SmartCal measurements.
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Do not install the RHT sensor on the terminal.
Be sure that the sensor opening is clean.
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Do not touch the sensor opening with sharply pointed objects.
After installing, RHT sensor must be acclimatized in working area for about one hour, before using.
Exposure to acids, bases or volatile compounds (e.g. solvents) at high concentration or long exposure time must be avoided.
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The RHT sensor must be stored in the original, sealed anti-static bag.
For storage temperature shall be in the range of 10°C…50°C and humidity at 20…60%rH.
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We recommend to remove the RHT sensor from the drying unit after a SmartCal measurement and to store it in the original, sealed anti-static and bag.
Settings see Equipment.
30 Installation and Putting into Operation
5 My First Measurement
After you have successfully put your new Moisture Analyzer into operation for the first time, you can immediate ly perform your first measurement. In doing so, you will become familiar with the instrument.
Use the supplied specimen sample (absorbent glass fiber filter) for your first measurement to determine the moisture content. During your first measurement the instrument operates with the factory settings.
Switching on
The instrument is connected to the mains.
– To switch on, press [ ].
Create a method
1 Tap Method Definition.
Method Definition menu appears.
2 To define a new method, tap [New...].
The keypad appears.
3 Enter a name for your first method e.g. My first method.
4 Confirm with [OK].
5 To store your new method with factory settings, tap [Save].
6 Tap [Home].
User home screen appears.
Select the method for measuring
1 Tap [Measurement].
The methods list is displayed.
2 Tap My first method.
The work screen of the method My first method appears.
3 Open the sample chamber.
Placing sample pan
The display now prompts you to load the empty sample pan and tare the balance.
1 Place the empty sample pan in the sample pan handler.
2 Place the sample pan handler in the sample chamber. Ensure that the tongue of the pan handler fits exactly in the slot of the draft shield element. The sample pan must lie flat in the pan holder.
Note
We advise you to work with the sample pan handler at all times. The pan handler is ergonomic, automatic positioning, safe and provides protection against possible burns due to the hot sample pan.
My First Measurement 31
Taring the balance
1 Close the sample chamber.
The instrument tares the balance (Starting mode: Automatic).
2 After taring, open the sample chamber.
Start measuring
1 Place the specimen sample in the sample pan.
2 Wet the specimen sample with a few drops of water.
3 Close the sample chamber.
The drying process starts automatically.
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Drying process
You can follow the measurement process on the display, see Work Screen (page 22).
The drying process is continuously displayed graphically.
The current temperature in the heating module is displayed as well as the elapsed drying time and the cur rent drying value.
The display shows the selected settings.
The drying process can be aborted by tapping [Stop drying].
At the end of the drying process you can read the moisture content of your sample on the display. If you have defined the control limits in the method, passed, warned or failed status is shown.
Danger of burns
Sample, sample pan and sample pan holder may still be hot.
32 My First Measurement
Remove Sample
The drying process is completed.
1 Open the sample chamber.
2 Carefully remove the sample pan handler from the sample cham ber.
Note
To remove the sample pan from the handler, lift the pan slightly from below and pull it sideways out of the handler.
3 • To perform a further measurement with the current method, tap
[Next Sample].
• To perform a measurement with a new method, tap [Methods].
• To return to the home screen, press [ ].
Congratulations!
You have just performed your first measurement with your new Moisture Analyzer. In the following sections you will find more information about the extensive functions of this instrument.
My First Measurement 33
6 Settings
Navigation: Home > Settings
In this section you will find information how to define the general settings of your instrument.
Menu structure
Main menu
User preferences
System settings
Application settings
Quality management
Submenu
Languages
Screen
Sound
Password
Regional Settings
Peripherals
Network interfaces
Default settings
Company information
Touch screen adjustment
Identifications management
Print and export management
Test / Adjustment settings
User management
System and data management
Groups
Users
Account policies
Export / Import
Back up / Restore
Export event logs
Reset
Update
Further information
see Regional Settings (page 37)
see Network Interfaces (page 41)
see Default Settings (page 39)
see Company Information (page 40)
see Touch Screen Adjustment
see Identifications Management
see Print and Export Management
see Test / Adjustment settings
see Account Policies (page 55)
see Back up / Restore (page 57)
see Export event logs (page 58)
34 My First Measurement
6.1 User Preferences
Navigation: Home > Settings > User preferences
This menu item defines the basic settings for each user. This settings are stored under the active user profile and apply when working within this profile. When a user profile is called up (login user account), the relevant
settings are loaded automatically. See User Management (page 52).
You can define the following parameters:
Menu item
Languages
Screen
Explanation
Defines your preferred display and keyboard lan guage.
Defines the brightness and the color scheme of the display
Further Information
6.1.1 Languages
Navigation: Home > Settings > User preferences > Languages
Select your preferred language for operating the terminal.
Factory setting: Generally, the language of the destination country (if available) or English is set.
You can define the following parameters:
Parameter
Display lan guage
Explanation
Defines user-specific screen language.
Keyboard lan guage
Defines user-specific layout of the Keypad.
Values
English | Deutsch |
Italiano | Français |
Español | Português |
Polski | Magyar |
Český | P усский |
日本語 | 中文 |
한국어/조선말
English | Deutsch |
Italiano | Français |
Español | Português |
Polski | Magyar |
Český
6.1.2 Screen
Navigation: Home > Settings > User preferences > Screen
You can define the following parameters:
Parameter
Brightness:
Explanation
Defines user-specific brightness of the display.
Color scheme
Defines user-specific display color scheme.
Values
10…100 %
(80 %)*
Blue* | Green |
Orange | Grey
* Factory setting
Settings 35
6.1.3 Sound
Navigation: Home > Settings > User preferences > Sound
You can define the following parameters:
Parameter
Sound
Explanation
Activate / deactivate of audible feedback and adjust the volume.
●
●
●
Audible feedback: when tapping a button.
upon measurement completed.
when an error message appears.
Values
OFF* | ON |
0…100 %
(50 %)*
6.1.4 Password
Navigation: Home > Settings > User preferences > Password
In this menu item you can change the user password. It is also possible to create a password for protection or to deactivate the password protection.
You can define the following parameters:
Parameter
Password
Explanation
Change an existing (Old password) and create a New
password.
ON = for entry of a new login password.
OFF = no password protection.
Values
ON | OFF | any
36 Settings
6.2 System Settings
Navigation: Home > Settings > System settings
This menu item defines the basic settings for the system. The system settings apply to the entire system and therefore to all user profiles and applications.
You can define the following parameters:
Menu item
Regional set tings
Peripherals
Explanation
Defines the settings of date & time, keypad and country options.
Defines the configuration of printers and other devices.
Defines network connections.
Network inter faces
Default settings
Defines the default settings of your instrument.
Company infor mation
Defines company specific information.
Touch screen adjustment
Adjusts the touch screen.
Further Information
see Regional Settings (page 37)
see Network Interfaces (page 41)
see Default Settings (page 39)
see Company Information (page 40)
see Touch Screen Adjustment
6.2.1 Regional Settings
Navigation: Home > Settings > System settings > Regional Settings
This menu item defines the settings of date & time.
You can define the following parameters:
Parameter
Date
Time
Date format
Time format
Country
Explanation
Sets the date of the clock of the instrument.
Sets the clock time of the instrument.
Defines the date format.
D = Day
M = Month
Y = Year
Defines the time format.
M = Minutes
Defines the country in which the instrument is operated.
Values
Day | Month | Year
Hours | Minutes
D. MMM YYYY* |
MMM D YYYY |
DD.MM.YYYY |
MM/DD/YYYY |
YYYY/MM/DD |
YYYY-MM-DD
24:MM* | 12:MM |
24.MM | 12.MM
Europe | China |
Japan | US |
Other *
* Factory setting
Note
Date and time of a connected printer will be ignored. Date and time of instrument is relevant.
6.2.2 Peripherals
Navigation: Home > Settings > System settings > Peripherals
In this menu item you can configure one printer and one host connection.
PCs
The MT-SICS host connection (remote client) is enabled by default and only usable with the METTLER TOLEDO specific protocol MT-SICS.
Settings 37
38 Settings
MT-SICS commands and functions can be transmitted via the RS232 interface (COM1 port) or the USB device interface (COM4 port). The use of the USB device interface requires the installation of an USB device driver on
the PC, see Installing USB Device Driver (page 122).
Commands and further information please refer to the Reference Manual MT-SICS Interface Commands for
Halogen Moisture Analyzers downloadable from the internet.
u www.mt.com/hxhs
Printers / PCs
No printer is installed by default. To install a printer:
The desired printer is properly connected to the terminal.
Note
Do not attempt to connect a printer to the drying unit!
1 Tap [New...]
Peripheral type list appears.
2 Select device.
Note
Currently supported devices from METTLER TOLEDO with preset parameters:
• RS-P42 Strip Printer, see RS232 parameters
• RS-P25 Strip Printer, see RS232 parameters
• Local PCL printer, see USB parameters
• Network PCL printer, see network parameters
• LabX Direct Moisture, see RS232 parameters
3 Set the parameters.
4 To store the settings, tap [Save].
5 To activate the interface, tap [ON].
Status changes from Disabled to Enabled.
●
●
●
●
Note
A printer or host connection can also be deleted.
For strip printer settings see Recommended Printer Settings (Strip printer) (page 121).
For defining the printouts see Print and Export Management.
Only one printer can be installed. To install another printer, you have to delete the old printer first.
RS232 parameters
You can define the following parameters:
Parameter
Device Name
Device Port
Baudrate
DataBits
Parity
StopBits
Explanation
Defines a name for the device.
Defines the device port.
COM1: RS232 / COM4: USB Device (Driver required)
Note
It is possible to use an USB-to-Serial adapter. If such an adapter is connected, these devices are shown as e.g.SOU1, SOU2 (SOU stands for serial over USB)
Defines the speed of the data transmission (data transfer rate /
Baud rate).
Defines the number of data bits.
Defines the variant of parity bit.
Defines the stop bits of the transmitted data.
Values any
COM1* | COM 4
1200 | 2400 | 4800 |
9600* | 19200 |
38400 | 57600 |
115200
7 | 8*
None* | Odd | Even
1 StopBit* |
2 StopBits
Flow Control
* Factory setting
Defines the type of flow control (Handshake).
USB parameters
● Supported A4 Printer: OKI B411 USB
● Supported printer command language: PCL 3 or higher
You can define the following parameters:
Parameter
Device Name
Explanation
Defines a name for the device.
Network parameters
You can define the following parameters:
Parameter
Device Name
IP address
Port
Explanation
Defines a name for the device.
Defines the IP address of the printer.
Default address*: 192.168.000.004
Defines the printer's port.
Note
Usually the default value is used.
* Factory setting
None | Xon/Xoff*
Values any
Values any
Default address* | any
9100 * | any
6.2.3 Default Settings
Navigation: Home > Settings > System settings > Default settings
Define the default settings of your instrument.
You can define the following parameters:
Menu item
Default lan guages
Default screen settings
Explanation Further Information
Defines a default display and keyboard language.
see Default Languages (page 39)
Defines the default brightness and color scheme.
see Default Screen Settings
6.2.3.1 Default Languages
Navigation: Home > Settings > System settings > Default settings > Default languages
Select the default language for operating the terminal. Factory setting: Generally, the language of the destination country (if available) or English is set.
You can define the following parameters:
Parameter
Default display language
Explanation
Defines default screen language.
Default key board language
Defines default layout of the keyboard.
Values
English | Deutsch |
Italiano | Français |
Español | Português |
Polski | Magyar |
Český | P усский |
日本語 | 中文 |
한국어/조선말
English | Deutsch |
Italiano | Français |
Español | Português |
Polski | Magyar |
Český
Settings 39
6.2.3.2 Default Screen Settings
Navigation: Home > Settings > System settings > Default settings > Default screen settings
You can define the following parameters:
Parameter
Brightness:
Explanation
Defines default brightness of the display.
Color scheme
Defines default display color scheme.
Values
10…100 %
(80 %)*
Blue* | Green |
Orange | Grey
* Factory setting
6.2.4 Company Information
Navigation: Home > Settings > System settings > Company information
In this menu item you can define optional specific company informations for using on printouts and reports.
You can define the following parameters:
Parameter Explanation
Company name
Entry of the company name.
Department
Entry of the company department.
Instrument ID
Entry of the company specific instrument identification
Entry of the location of the instrument.
Instrument loca tion
Instrument responsible
Entry of the name of the responsible person for the instrument.
Values any any any any any
6.2.5 Touch Screen Adjustment
Navigation: Home > Settings > System settings > Touch screen adjustment
If the alignment of the touch-sensitive areas of the screen correspond not exactly with the position of the buttons e.g. after a software update was performed, then you can solve this error by executing this function.
Do not touch the touch screen with pointed or sharp objects!
This may damage the touch screen.
Menu System settings appears.
1 Choose Touch screen adjustment and tap [Start].
Adjustment screen appears.
2 Touch and hold a touch screen stylus (resistive) on the center of the target until it moves to the next position on the screen.
3 Repeat this procedure until a message appears (New calibration
settings have been measured).
4 Tap the screen to confirm or wait for 30 seconds for canceling
(timeout).
A message box appears.
5 To store the setting, tap [OK].
40 Settings
Note
●
Tap the center of the target as accurately as possible otherwise the process has to be repeated several times.
●
●
Make sure not to touch any other locations on the screen and the fix key areas while doing this adjustment.
Make sure not to touch the screen with your hand.
●
●
Keep accurate angle for your usage.
The adjustment process cannot be aborted.
6.2.6 Network Interfaces
Navigation: Home > Settings > System settings > Network interfaces
In this section you will find information how to define network connections and other terminal interfaces.
Menu structure
Main menu
Host name
Ethernet
WLAN
Submenu
Defines the host name of the instrument
Activates and sets Ethernet connection.
Activates and sets wireless local area network
(WLAN) connection.
Further information
Host Name
Navigation: Home > Settings > System settings > Network interfaces > Host name
The Host name is the name of your instrument and is a unique identifier on a network (Ethernet, WLAN). If using multiple devices, you should ensure that the host name of each instrument is unique. If necessary, con tact the network administrator of your IT department or your IT support.
You can define the following parameters:
Parameter
Host name
Explanation
Defines the host name. The host name must be unique on a net work.
Default host name*: Model name and serial number of the instru ment.
Values any
* Factory setting
Ethernet
Navigation: Home > Settings > System settings > Network interfaces > Ethernet
Ethernet interface for connecting the instrument to a TCP/IP network. The most simple network can be imple mented by connecting the instrument directly to the PC with a cross-over cable (RJ45 Socket). DHCP and fix IP addresses are supported.
Note
●
We recommend to use the default setting DHCP (automatic network settings).
●
Ensure that the host name of the instrument is unique, see Host Name (page 41).
●
For installing and configuring an Ethernet interface you need to have basic knowlege of TCP/IP-based net works and of network technology in general. If necessary, contact the network administrator of your IT department or your IT support.
You can define the following parameters:
Parameter Explanation
Configuration
Defines whether the settings are made automatically (dynamic,
DHCP) or manually (static).
Values
DHCP assignment |
Manual assignment
Settings 41
42 Settings
DHCP assign ment
Manual assign ment
IP address
Subnet
Dynamic Host Configuration Protocol to assign all necessary net work parameters on this interface automatically (Dynamic assignment).
Manually assign all the necessary network parameters on this interface. (Static assignment)
Defines the IP address of this instrument. Only setable when
DHCP is disabled.
Default address*: 192.168.002.100
none
IP address | Subnet
Default address* | any
The IP address unique numeric identifier for a device which par ticipates on a network.
If DHCP is enabled, the automatically assigned IP address is dis played.
Defines the subnet mask within the ethernet interface is address able. Only setable when DHCP is disabled.
Default subnet mask*: 255.255.255.000
Default value* | any
* Factory setting
Note
The addresses are written as four dot-separated decimal integers in the range from 0 to 255. Leading zeros need not be written.
WLAN
Navigation: Home > Settings > System settings > Network interfaces > WLAN
Wireless LAN interface for connecting the instrument to a wireless TCP/IP network. DHCP and fix IP addresses are supported.
●
●
●
●
Note
WLAN is not available in every country.
The following WLAN authentications are supported:
Open
WEP
WPA-PSK
WPA2-PSK (tkip only)
You can define the following parameters:
Parameter
WLAN
* Factory setting
Explanation
Activates or deactivates WLAN radio transmitter.
Values
OFF* | ON
Note
After activating WLAN, it takes some time until WLAN is active.
●
●
●
WLAN Network Settings
Navigation: Home > Settings > System settings > Network interfaces > WLAN > Settings > WLAN configu
rations
We recommend to use the default setting DHCP (automatic network settings).
Ensure that the host name of the instrument is unique, see Host Name (page 41).
For installing and configuring an Ethernet interface you need to have basic knowlege of TCP/IP-based net works and of network technology in general. If necessary, contact the network administrator of your IT department or your IT support.
You can define the following parameters:
Parameter Explanation
Configuration
Defines whether the settings are made automatically (dynamic,
DHCP) or manually (static).
DHCP assign ment
Manual assign ment
IP address
Dynamic Host Configuration Protocol to assign all necessary net work parameters on this interface automatically (Dynamic assignment).
Manually assign all the necessary network parameters on this interface. (Static assignment)
Defines the IP address of this instrument. Only setable when
DHCP is disabled.
Default address*: 192.168.002.100
Values
DHCP assignment |
Manual assignment none
IP address | Subnet
Default address* | any
Subnet
The IP address unique numeric identifier for a device which par ticipates on a network.
If DHCP is enabled, the automatically assigned IP address is dis played.
Defines the subnet mask within the ethernet interface is address able. Only setable when DHCP is disabled.
Default subnet mask*: 255.255.255.000
Default value* | any
* Factory setting
Note
The addresses are written as four dot-separated decimal integers in the range from 0 to 255. Leading zeros need not be written.
Networks
Receivable networks are displayed.
Entries for WLAN:
Parameter
WLAN name
(SSID)
Password
Autoconnect
Explanation
Displays the name of the selected WLAN (SSID, service set identi fier)
Entry for the required password.
Activate or deactivate automatic connecting to the preferred net work upon startup of the device.
Note
Only for one network possible.
Establish a connection:
Values
not editable
any
(deactivated)* |
(activated)
1 Touch the desired network.
Note
If the device is connected to a network, the WiFi icon indicates the signal strength. The more bars displayed, the stronger the connection.
2 Enter your password.
3 Enable automatic connection if needed.
4 Touch [connect] to establish the connection.
Settings 43
6.3 Applications Settings
Navigation: Home > Settings > Application settings
You can define the following parameters:
Menu item
Identifications management
Print and export management
Explanation
Defines identifications and their use in order to comment measurements.
Defines the default settings for the printouts.
Further Information
see Identifications Management
see Applications Settings (page 44).
6.3.1 Identifications Management
Navigation: Home > Settings > Application settings > Identifications management
Identifications (ID) contain descriptive text for individual measurements, which enables samples to be easily allocated to specific tasks or customers. This feature allows you to define identifications in order to comment measurements, such as company id, id badge, id sample. In the ID panel on the work screen, the values
on all measurements, regardless of methods. The IDs are included on printouts or can be exported to a PC.
Menu structure
Main menu
Identifications usage
Identifications
Submenu
Identifications input
Clear input after measurement
no submenu
You can define the following parameters:
Parameter
Identifications input
Explanation
Defines the method for entering comments.
ON = activates ID panel on work screen.
Further information
see below
Free input = the IDs appear after tapping on the ID panel (work screen) for entries or changes of values (comments).
Values
OFF* | ON |
Free input |
Guided input
Guided input = each ID is displayed individually in order of defi nition (ID1 to ID10) before measurement, to make entries or changes of values (comments).
Clear input after measurement
Defines the ID whose value (comment) is deleted after measure ment.
OFF* | ON |
ID selection:
| |
- | +* | any
Identifications
Defines general identifications in order to comment measure ments.
+ = New identifications (max. 10 IDs, 1…20 characters)
- = Remove identifications (selectable)
* Factory setting
44 Settings
6.3.2 Print and Export Management
Navigation: Home > Settings > Application settings > Print and export management
You can define the following parameters:
Menu item
Print manage ment (Strip)
Print manage ment (A4)
Explanation Further Information
Defines the settings for printouts on strip printers.
see Print management (page 45).
Defines the settings for ISO A4 printouts on PCL printers.
see Print management (page 45).
Also see
●
●
●
●
Recommended Printer Settings (Strip printer) (page 121)
Information on Printouts (page 95)
Print and Output Settings (page 51)
Print management
Print management (Strip)
Navigation: Home > Settings > Application settings > Print and export management > Print management
(Strip)
If a strip printer is connected and activated, results can be automatically printed out. The interim values are printed out in the pre-selected intervals and the final results are logged at the completion of the measurement.
The printout contains information to the instrument, time, date as well as the method and results, depending of the protocol. The level of detail depends on the selected type of printout (short, standard) and the activated pro tocol items (settings or method), see Information on Printouts.
Note
● The definitions in this menu item are the default settings for the printouts. These parameters are displayed at every initialization of a Printout and can be modified again.
●
The setting for printout language in this menu item has no impact on test or adjustment printouts, see Print and Output Settings.
●
●
Not all languages are compatible with some printers, and also depending on the settings of the printer, see
Recommended Printer Settings (Strip printer) (page 121).
For installing and defining a printer see Peripherals (page 37).
Settings 45
46 Settings
You can define the following parameters:
Parameter
Printout type
Printout lan guage
Explanation
Selects a detailed printout or in a short form.
Defines the language for general printouts.
Note
No impact on test or adjustment printouts.
Values
Standard* | Short
English | Deutsch |
Italiano | Français |
Español | Português |
Polski | Magyar |
Český | P усский |
日本語 | 中文 |
한국어/조선말
(deactivated)* |
(activated)
Print results automatically after measure ment
Include interme diate results to printout
* Factory setting
Print results automatically after measurement if activated.
Defines the time intervals at which interim results are transferred to the printer.
OFF* | 10 s | 30 s |
1 min | 2 min | 10 min
Print management A4
Navigation: Home > Settings > Application settings > Print and export management > Print management
(A4)
If a PCL printer is connected and activated, results can be manually or automatically printed out on ISO A4
Note
● The definitions in this menu item are the default settings for the printouts. These parameters are displayed at every initialization of a Printout and can be modified again.
●
The setting for printout language in this menu item has no impact on test or adjustment printouts, see Print and Output Settings.
●
For installing and defining an A4 printer, see Peripherals (page 37).
You can define the following parameters:
Parameter
Printout lan guage
Explanation
Defines the language for general printouts.
Note
No impact on test or adjustment printouts.
Print results automatically after measure ment
Print results automatically after measurement if activated.
Values
English | Deutsch |
Italiano | Français |
Español | Português |
Polski | Magyar |
Český | P усский |
日本語 | 中文 |
한국어/조선말
(deactivated)* |
(activated)
Export management
Navigation: Home > Settings > Application settings > Print and export management > Export management
If a PC or WLAN is connected and activated, final results can be automatically exported. The export contains information to the instrument, time, date, method, result as well as the graphical curve.
You can define the following parameters:
Parameter Explanation
File name prefix Defines the name of the new data file. Date and time are auto matically added by the system.
File type
Printout lan guage
Export manage ment
Export target
Defines the type of the data file.
Defines the language for general printouts.
Note
No impact on test or adjustment printouts.
Export results automatically after measurement if activated.
Defines the destination of data transfer.
Values any
CSV* | PDF
English | Deutsch |
Italiano | Français |
Español | Português |
Polski | Magyar |
Český | P усский |
日本語 | 中文 |
한국어/조선말
Selection:
* |
Peripheral |
Network (FTP)
* Factory setting
Export target: Peripheral
Parameter Explanation
Location
Finds the location on the storage device.
* Factory setting
Values
Browse and select
Export target: Network (FTP)
For data transfer over a network (Ethernet and WLAN) the File Transfer Protocol FTP is used. The receiving serv er is defined by entry of the appropriate IP address. If necessary, contact the network administrator of your IT department or your IT support.
Parameter
IP address
Port
Password
User name
* Factory setting
Explanation
Defines the IP address of the receiving server.
Defines the Port for communication with the server.
Note
Usually the default value is used.
Entry for the password needed for server login.
Entry for the user name needed for server login.
Values any
21* | any
any any
Settings 47
6.4 Quality Management
Navigation: Home > Settings > Quality management
In this menu you can define all settings related to the adjustment and Test of the instrument. Periodic adjust ments or tests ensure accurate measurement results.
You can define the following parameters:
Menu item
Test / Adjust ment settings
Explanation
Defines the equipment for adjusting and the work flow for testing or adjusting.
Further Information
see Test / Adjustment settings
6.4.1 Test / Adjustment settings
Navigation: Home > Settings > Quality management > Test / Adjustment settings
This section describes all the menu options available for defining the parameters relating to the adjustment and testing of your instrument.
For performing test and adjustments see Test/Adjust (page 61).
Menu structure
Main menu
Equipment
Submenu
Test weight 1
Test weight 2
Temperature kit
External humidity sensor
Test settings
Adjustment settings
Print and output settings
Weight test - external
Temperature test
SmartCal test
Weight adjustment - external
Temperature adjustment
Printout language
Print results automatically after test/adjustment
Further information
see Adjustment Settings (page 50)
see Print and Output Settings
6.4.1.1 Equipment
●
●
●
●
●
Navigation: Home > Settings > Quality management > Test / Adjustment settings > Equipment
This menu item defines the equipment which are required for the following tests:
Weight adjustment
Weight test
Temperature adjustment
Temperature test
SmartCal test (optional)
For performing temperature adjustment or temperature test, you need the optional temperature adjustment kit,
see Accessories and Spare Parts (page 115).
48 Settings
You can define the following parameters:
Parameter
Test weight name
Explanation
Defines a name that is in an easily recognizable form as an alter native to the ID. A name should be unique and unambiguous.
Nominal weight
Defines the nominal weight in grams.
Values any
Identification
30.000…150.000 g
(100 g)*
any
Defines the identification (ID) of the weight. The ID of the weight is provided on the Weight Certificate. The ID may contain your company specific identification number. This ID is stored in the adjustment or test history and shows up on the printouts.
* Factory setting
Temperature Adjustment Kit
You can define the following parameters:
Parameter
Temperature kit name
Identification
Explanation
Defines a name that is in an easily recognizable form as an alter native to the ID. A name should be unique and unambiguous.
Defines the identification (ID) of the Temperature kit. The ID is provided on the Certificate. The ID may contain your company specific identification number. This ID is stored in the adjustment or test history and shows up on the printouts.
Values any any
6.4.1.2 Test Settings
Navigation: Home > Settings > Quality management > Test / Adjustment settings > Test settings
Weight test external
You can define the following parameters:
Parameter
Test weight
Tolerance
Explanation
Selects the predefined Test weight.
Test weight 1 / Test weight 2 = defined in the menu item Equip
ment
Defines the measuring tolerance of the weight.
Values
Test weight 1 |
Test weight 2
0.0001…0.1000 g
(0.0010 g)*
* Factory setting
Temperature test
You can define the following parameters:
Parameter Explanation
Temperature kit
Shows the name of the Temperature kit which was defined in the menu item Equipment.
Temperature 1
Enables or disables the lower test temperature.
Values
none
Tolerance
Temperature 2
Tolerance
Defines the tolerance of the test temperature.
Enables or disables the upper test temperature.
Defines the tolerance of the test temperature.
OFF | ON
(100 °C)*
1…5 °C
(3 °C)*
OFF | ON
(160 °C)*
1…5 °C
(3 °C)*
* Factory setting
Settings 49
SmartCal test
You can define the following parameters:
Parameter
Lot number input
Clear lot num ber after mea surement
Temperature
Explanation
Defines the type of input for the Lot number. The Lot number can be found on the product label.
Free input: Input is not required
Guided input: Input is required.
Enabled or disabled the function for clearing the Lot number after test measurement.
Defines the test temperature.
Note
●
●
The setting of the temperature influences the setting of the control limits.
If custom temperatur is set, the controll limits will be off.
Values
ON* | OFF |
Free input |
Guided input *
(enabled) |
(disabled)*
70 °C | 100 °C* |
130 °C | 160 °C |
Custom temperature...
40 °C…230 °C
(105 °C*)
Use cSmartCal Sets the controll limits to the correct values for using of cSmart
Cal.
Note
Enabling of cSmartCal affects only the protocol entry but has no effect to the values of the control limits, if custom temperature was set.
(enabled) |
(disabled)*
Control limits
Defines the control limits. The values of the control limits are in dependence of the temperature setting. The recommended values are automatically set. The values can also be changed.
The recommended values are (lower - upper limits):
70 °C: 3.2-4.4 %MCN (cSmartCal: 3.3 - 4.3 %MCN)
100 °C: 5.2-6.4 %MCN (cSmartCal: 5.3 - 6.3 %MCN)
130 °C: 7.4-8.8 %MCN (cSmartCal: 7.5 - 8.7 %MCN)
160 °C: 9.9-11.7 %MCN (cSmartCal: 10.0 - 11.6 %MCN)
Note
Control limits are switched off if custom temperature was set.
values see explanation |
OFF
* Factory setting
6.4.1.3 Adjustment Settings
Navigation: Home > Settings > Quality management > Test / Adjustment settings > Adjustment settings
Weight adjustment external
You can define the following parameters:
Parameter
Test weight
Explanation
Selects the predefined Test weight.
Test weight 1 / Test weight 2 = defined in the menu item Equip
ment
Values
Test weight 1 |
Test weight 2
Temperature adjustment
You can define the following parameters:
Parameter Explanation
Temperature kit
Shows the name of the Temperature kit which was defined in the menu item Equipment.
Values
none
50 Settings
6.4.1.4 Print and Output Settings
Navigation: Home > Settings > Quality management > Test / Adjustment settings > Print and output set
tings
This menu item allows you to set specific printer functions for test or adjustment printouts.
●
●
●
The setting for printout language in this menu item has impact on test or adjustment printouts only. For set
ting the general printout language, see Print and Export Management (page 45).
Not all languages are compatible with any printer, and also depending on the settings of the printer, see
Recommended Printer Settings (Strip printer) (page 121).
For installing and defining a printer see Peripherals (page 37).
You can define the following parameters:
Parameter
Printout lan guage
Explanation
Defines the printout language for test or adjustment printouts.
Print results automatically after test/adjust ment
* Factory setting
Activated or deactivated function.
Values
English | Deutsch |
Italiano | Français |
Español | Português |
Polski | Magyar |
Český
(enabled) |
(disabled)*
Settings 51
6.5 User Management
Navigation: Home > Settings > User management
The security system of the instrument is based on a "Users and Groups" concept. Every real user of the instru ment should be represented by a user account on the instrument which holds particular settings of the respec tive user. Every user belongs to a particular group and inherits the access rights assigned to that group.
You can define the following parameters:
Menu item
Groups
Explanation
Defines groups and their access rights.
Users
Defines the user accounts.
Account policies Set default startup user.
Further Information
see Account Policies (page 55)
6.5.1 Groups
Navigation: Home > Settings > User management > Groups
In this menu you can create, delete, or edit user groups and define their access rights.
Four predefined groups are available. The default group with all access rights is administrator. The administra tor group can not be edited or deleted. All other groups can be edited or deleted.
Predefined groups
Default access rights
User Pref erence set tings
System set tings
Edit Meth ods
Run Tests Run Adjust ments
Quality manage ment
User and data man agement
Administra tor
Supervisor
Quality
Manager
Operator
Creating a new group
Menu Groups selected.
1 Tap [New...].
2 Enter the name of the new group and confirm with [OK]. Name should be unique and unambiguous.
3 Edit the properties of the new group.
Deleting a group
Menu Groups selected.
1 Select the group you wish to delete.
2 Tap [Delete]. Confirm the message box.
Note
Editing a group
Menu Groups selected.
1 Select the group you wish to edit.
2 Edit the group parameters. Store the settings with [Save].
52 Settings
You can define the following parameters:
Parameter Explanation
Group properties Name and (optional) description of the group. Name should be unique and unambiguous.
Access rights
Defines the access rights to menus or operations.
Values any
User Preference set
tings | System settings
| Edit Methods | Run
Tests | Run Adjust
ments | Quality Man
agement | User and
data management none Group members
(%1)
History
Displays the users assigned to this group (no editing can be done here, the assignment is done when setting up or editing a user).
Displays the date and time of the last modifications made to this group (no editing here).
Influence of access rights
Access rights
User Preference settings
System settings
Edit Methods
Run Tests
Run Adjustments
Quality management
User and data management none
Impact on
User preferences
Navigation: Home > Settings > User preferences
See User Preferences (page 35)
System settings
Navigation: Home > Settings > System settings
Method definition
Navigation: Home > Method definition
See Method Definition (page 71)
Application settings
Navigation: Home > Settings > Application settings
See Applications Settings (page 44)
Tests
Navigation: Home > Test/Adjust > Tests
Adjustments
Navigation: Home > Test/Adjust > Adjustments
Quality management
Navigation: Home > Settings > Quality management
See Quality Management (page 48)
User management
Navigation: Home > Settings > User management
System and data management
Navigation: Home > Settings > System and data management
See System- and Data Management (page 56)
Deleting results
See Graphical Evaluations of Measurement Results (page 93)
Note
●
●
If password protection is mandatory requirement, the access right User Preference settings must be dis abled.
If a user does not have the appropriate access rights, the respective navigation elements are not shown (on
Home screen) or are disabled (greyed out).
Settings 53
6.5.2 Users
Navigation: Home > Settings > User management > Users
In this menu you can create, edit, or delete user accounts.
Attention
Important note for the Administrator password.
We recommend that you note down your administrator password and keep it in a safe place. If you forgot the password for the default administrator access, it is not possible to regain access to the moisture analyzer. In this case contact your METTLER TOLEDO representative.
Creating a new user account
Note
The user account name must be unique.
Menu Users selected.
1 Tap [New...].
2 Enter the name of the new user account and confirm with [OK].
3 Edit the properties of the new user account.
Editing an existing user account
Menu Users selected.
1 Select the user account you wish to edit.
2 Select menu User properties.
3 Edit the user account parameters.
4 To store the settings, tap [Save].
You can define the following parameters:
Parameter
User name
Full name
Description
Explanation
Name of the user account. Name should be unique and unam biguous.
Full name of the user (optional).
Descriptive text for the user account (optional).
Account active
Activate or deactivate the user account. Inactive user accounts are not available for login.
Password
Create a new or change an existing password. OFF = no pass word protection.
Group
Assign the user account to a particular group.
* Factory setting
Values any any any
(deactivated)* |
(activated)
OFF* | ON | any
available groups
Note
●
To view the date and time of last modification made to a user account, select the respective account and tap [History].
● If password protection is mandatory requirement, the access right User Preference settings must be dis
Deleting a user account
Menu Users selected.
1 Select the user account you wish to delete.
2 Tap [Delete]. Confirm the message box.
Note
You cannot delete the Administrator account or the account that is currently active.
54 Settings
6.5.3 Account Policies
Navigation: Home > Settings > User management > Account policies
In this menu you can set the default startup user.
You can define the following parameters:
Parameter
Default startup user
Explanation
Select the default user account for login at startup.
* Factory setting
Note
If a non-standard user logs out, the default startup user profile is automatically activated.
Values
OFF | ON* |
available user accounts
Settings 55
6.6 System- and Data Management
Navigation: Home > Settings > System and data management
This menu item allows you to export or import settings and methods to or from an external USB storage device, as well as to restore the system (depending on the user rights).
Menu structure
Main menu
Export / Import
Back up / Restore
Export event logs
Reset
Update
Submenu
Export settings and methods to external storage devices...
Import settings and methods from external storage device...
Back up your system on external storage device...
Restore your system from selected back up...
Further information
see Back up / Restore (page 57)
Export all event information
no submenu
see Export event logs (page 58)
Update your instrument software
Note for using USB memory sticks
● Memory sticks up to 32 GB are supported.
●
●
Recommended formatting: FAT32 (NTFS not supported).
Max. cluster size: 32 KB.
●
●
●
Max. file size: 32 MB.
Make sure that the stick is fully inserted.
Make sure that the write protection is deactivated if present.
6.6.1 Export / Import
Navigation: Home > Settings > System and data management > Export / Import
This menu item allows you to export or import settings and methods to or from an external storage device.
These data can be transferred to other instruments of the same type and can be useful to configure multiple instruments with the same specifications.
Note
●
●
●
Software Version must be equal or higher.
Data transfer from HX models to HS models is limited. Features which are not supported by HS models can not be imported, e.g. Step drying or high resolution.
Export / import of methods can also be performed from the menu Method Definition.
Export settings and methods to external storage devices...
You can define the following parameters:
Parameter
File name
Location
Explanation
Defines the name of the new data file.
Finds the location on the storage device.
Values any
Browse and select
56 Settings
Export selection Defines the data for export.
Note
●
●
User management and user preferences contains: User management settings, user preferences
System, application and QM settings contains: System set tings, application settings, quality management settings
All* |
ences |
User manage
ment and user prefer
System, application
and QM settings |
Methods (%1)
* Factory setting
An external storage device is connected e.g. memory stick.
Settings are made.
– To start, tap [Export].
To abort, tap [Cancel].
Import settings and methods from external storage device...
You can define the following parameters:
Parameter
Import from file
Location
Explanation
Defines the data to be imported.
Shows the location of the import file.
Import selection Defines the data for import.
* Factory setting
Import settings and methods from external storage devices – is selected.
An external storage device is connected e.g. memory stick.
1 Tap Browse and select
Import from file appears.
2 Select Device and import file.
Full menu of Import settings and methods from external storage devices appears.
3 Tap Import selection and select the data for import if needed.
4 To start, tap Import button and follow the instructions in the message window.
To abort, tap [Cancel].
Values
Browse and select
–
All* | User manage
ment and user prefer
ences |
System, application
and QM settings |
Methods (%1)
6.6.2 Back up / Restore
Navigation: Home > Settings > System and data management > Back up / Restore
This menu item allows you to create a recovery point of the system and to store them on an external storage device. We advise you to create a recovery point of the system regularly. So you are able to restore the system with all data in fault.
Attention
●
●
After restoring, the system is in backup status. That means, that newer data such as settings, methods or results are lost.
Restore is only possible on the same instrument as the back up was carried out.
Settings 57
Backup
You can define the following parameters:
Parameter
File name
Location
Procedure:
Explanation
Defines the name of the new data file.
Finds the location on the storage device.
An external storage device is connected e.g. memory stick.
Back up your system on external storage device... – is selected.
1 Define the name of the new data file.
2 Define the location on the storage device.
3 To confirm, tap [OK].
4 To start, tap [Backup].
To abort, tap [Cancel].
Restore
You can define the following parameters:
Parameter Explanation
Restore from file Finds the location on the storage device and selects the file for restoring.
Procedure:
Restore your system from selected back up... – is selected.
An external storage device is connected e.g. memory stick.
Values any
Browse and select
Values
Browse and select
1 Tap Restore from file... (Browse and select).
Storage device appears.
2 Select the file for restoring.
3 To start, tap [Restore].
To abort, tap [Cancel].
Confirmation window appears.
4 Confirm with [Restore].
The system will restore the data and then perform a restart. Wait until the system has completely started up again.
6.6.3 Export event logs
Navigation: Home > Settings > System and data management > Export event logs
This menu item allows you to export a log file (Zip format) with all relevant data to an external storage device.
These data can be used for example, to support METTLER TOLEDO for troubleshooting.
You can define the following parameters:
Parameter
File name
Export target
Explanation
Defines the name of the new data file.
Defines the destination of data transfer.
Values any
Peripheral |
Network (FTP)
Export target: Peripheral
Parameter Explanation
Location
Finds the location on the storage device.
* Factory setting
Values
Browse and select
58 Settings
Export target: Network (FTP)
For data transfer over a network (Ethernet and WLAN) the File Transfer Protocol FTP is used. The receiving serv er is defined by entry of the appropriate IP address. If necessary, contact the network administrator of your IT department or your IT support.
Parameter
IP address
Port
Password
User name
File type
Explanation
Defines the IP address of the receiving server.
Defines the Port for communication with the server.
Note
Usually the default value is used.
Entry for the password needed for server login.
Entry for the user name needed for server login.
Defines the type of the data file.
Values any
21* | any
any any
CSV* | PDF
* Factory setting
6.6.4 Reset
Navigation: Home > Settings > System and data management > Reset
This menu item allows you to reset the Instrument to factory settings. Date, time, weight and temperature adjustments/history are not affected.
Data loss after system reset.
After resetting, the instrument is in state as delivered. That means, that all data such as set tings, methods or results are lost.
– We recommend you, first save the appropriate data on an external storage device, see
Export / Import (page 56) and Back up / Restore (page 57).
You can define the following parameters:
Parameter
Reset
Explanation
Resets the instrument to factory settings.
Values none
6.6.5 Update
Navigation: Home > Settings > System and data management > Update
Note
This function is not available with approved instruments. For update, contact your METTLER TOLEDO represen tative.
METTLER TOLEDO is continuously improving its instrument firmware (software) for the benefit of customers. So that the customer can benefit quickly and easily from further developments, METTLER TOLEDO makes the latest firmware versions available on the Internet. The firmware made available on the Internet has been developed and tested by Mettler-Toledo AG using processes that meet the guidelines of ISO 9001. Mettler-Toledo AG does not, however, accept liability for consequences that might arise from using the firmware.
Operating Principle
If you register on the following METTLER TOLEDO website, you will find all relevant information and updates for your instrument:
www.mettler-toledo-support.com
Settings 59
60 Settings
Update Procedure
Data loss after system update.
During update of the system, the existing data such as settings, methods or results are migrated. It may happen that data are lost or the update fails.
– We advise you, first create a recovery point of the system on an external storage device,
see Back up / Restore (page 57).
For each software update, the following steps must be performed:
Step 1 Backup system data.
See Back up / Restore (page 57), procedure Backup.
Step 2 Execute software update (see below).
Step 3 Restore system data if needed.
See Back up / Restore (page 57), procedure Restore.
Execute software update
This menu item allows you to update the Instrument.
You can define the following parameters:
Parameter Explanation
Update from file Finds the location on the storage device and selects the file for updating.
Back up of the system data is already performed.
Values
Browse and select
1 Insert USB stick with software for update.
2 Select Home > Settings > System and data management > Update.
Update screen appears.
3 Tap Update from file. Browse and select the software update package file on the USB stick.
4 Tap [Update]
Screen Confirm Software Update appears.
5 Read the Information on the screen.
– If an update is needed, tap [Update].
– If the software is up-to-date, tap [OK].
6 Wait until the software update is completely finished, i.e. the system returned to the home screen (the instrument might reboot up to twice in between).
Attention
Do not remove the USB stick before the instrument has completely restarted.
Also see
●
Touch Screen Adjustment (page 40)
7 Test/Adjust
Navigation: Home > Test/Adjust
This function offers you to adjust or test the integrated balance and the heating module. For the relevant settings
see Test / Adjustment settings (page 48).
Menu structure
Main menu
Adjustments
Submenu
Weight adjustment - external
Tests
History
Temperature adjustment
Weight test - external
Temperature test
SmartCal test
Further information
see Weight Adjustment - External
see Temperature Adjustment
see Weight Test - External (page 65)
see Temperature Test (page 65)
see Test Printout Examples
Weight test history
Weight adjustment history
Temperature adjustment history
Temperature test history
SmartCal test history
Also see
●
Adjustment Printout Examples (page 64)
7.1 Adjustments
Navigation: Home > Test/Adjust > Adjustments
In this menu item you can adjust the balance as well as the heating module of your instrument. For relevant
settings see Test / Adjustment settings (page 48).
Attention
● To obtain accurate results, the balance must be adjusted at the point of use under measuring condition in order to match the gravitational acceleration at its location. The instrument must be connected to the power supply for approximately 60 minutes in order to reach operating temperature before adjusting. Adjusting is necessary:
• before the instrument is used for the first time.
• after a change of location.
● We advice you to wait at least 30 minutes after a drying operation (or previous heating module adjustment) before performing the adjustment.
7.1.1 Weight Adjustment - External
Navigation: Home > Test/Adjust > Adjustments > Weight adjustment - external
This function allows you to adjust the balance using an external weight. We recommend to use certified weights so that full traceability is guaranteed.
Perform this function as follows:
Test weight and Adjustment settings are defined.
see Test / Adjustment settings (page 48)
1 Have required test weight ready.
2 Tap the item Weight adjustment - external.
Test/Adjust 61
The adjustment screen appears.
3 Clear sample pan holder and tap [Start adjustment].
Note
We recommend not to use a pan.
The required value flashes and prompts you to load the weight, e.g. "100.00 g".
4 Load the required test weight in the center of sample pan holder.
The balance indicates the adjustment process, "––––––" appears.
5 When the display flashes "000.00" remove the test weight.
The balance is adjusted and ready to use for further measurements. The display shows the adjustment results. The results can be printed out by tapping [ ]
Note
After a timeout the error message appears Weight out of range.. The adjustment has been aborted. The adjustment was not executed.
1 Confirm with [OK].
2 Remove the test weight for unloading.
3 Repeat the adjustment.
7.1.2 Temperature Adjustment
●
●
●
Navigation: Home > Test/Adjust > Adjustments > Temperature adjustment
This function allows you to adjust the temperature control of the heating module. You need the optional Temper
ment of the heating module is necessary, see Notes on Adjustment of Balance and Heating Module
adjustment) before performing the adjustment.
Note
●
The duration of the temperature adjustment is 30 minutes. (15 minutes for each measuring temperature).
The sample chamber must be less than 50 °C before a further adjustment or test can be done.
It is also possible to perform a test first, and then to transform the test into an adjustment if required. Only
possible for tests conducted with 2 temperatures, see Temperature Test (page 65).
For temperature adjustment settings see Adjustment Settings (page 50).
Danger of burns
Sample chamber may still be hot.
– Cool down instrument before setting up.
Adjustment settings are defined, see Adjustment Settings (page 50).
– Tap menu item Temperature adjustment.
Work screen Temperature adjustment appears.
62 Test/Adjust
Setting up Drying Unit
Have required Temperature kit ready.
Instrument is on
Sample chamber is open.
Instrument is cooled down.
1 Remove sample pan handler (with pan) (1).
2 Remove sample pan holder (2).
3 Contact areas (3) should be clean. Clean them if needed.
Note
Do not remove draft shield.
– Insert Temperature kit (4).
1 2 3
4
Start adjustment
Draft shield is installed.
Temperature kit is inserted.
1 Tap [Start adjustment].
Note
The adjustment process takes 30 minutes.
The instrument starts the adjustment process. The screen shows the current temperature and the remain ing time.
The instrument heats up to the target temperature 1 for determining the predefined lower temperature.
After 15 minutes, the instrument adjusts the lower temperature and continues with the process.
The instrument heats up to the target temperature 2 for determining the predefined upper temperature.
After 15 minutes, the instrument adjusts the upper temperature and concludes the adjustment.
2 • To print out the results, tap [ ].
• To display or print out the results of previous adjustments, tap [History].
• To return to the home screen, tap [ ].
Test/Adjust 63
3 After cooling down, remove Temperature kit and set up drying unit for measurement.
See History and Setting up Drying Unit (page 26)
Note
Your calibrated temperature adjustment kit can be re-calibrated. Please contact your local METTLER TOLEDO representative for more information.
7.1.3 Adjustment Printout Examples
Weight adjustment external Temperature adjustment
-WEIGHT ADJUST EXTERNAL-
14.10.2011 11:51
METTLER TOLEDO
Halogen MoistureAnalyzer
Type HS153
SNR(Drying Unit) 2345
SNR(Terminal) 6788
SW(Drying Un 0.60.09
SW(Terminal) 4.20628
User name Administrator
Weight ID
ECW-100/1
Nominal Weight
100.000 g
Cell temperature
25.20 °C
Adjustment done
Signature
........................
---------- END ---------
-TEMPERATURE ADJUSTMENT-
14.10.2011 11:51
METTLER TOLEDO
Halogen MoistureAnalyzer
Type HS153
SNR(Drying Unit) 2345
SNR(Terminal) 6788
SW(Drying Unit) 0.60.09
SW(Terminal) 4.20628
User name Administrator
Temp Kit ID MT-414/A
Temp1 target 100 °C
Temp1 actual 97 °C
Temp2 target 160 °C
Temp2 actual 162 °C
Adjustment done
Signature
........................
---------- END ---------
64 Test/Adjust
7.2 Tests
Navigation: Home > Test/Adjust > Tests
In this menu item you can check the adjustment of the balance as well the temperature of the heating module.
For relevant settings see Test / Adjustment settings (page 48).
7.2.1 Weight Test - External
Navigation: Home > Test/Adjust > Tests > Weight test - external
This function allows you to test the balance using an external weight. Perform this function as follows:
Test weight and Adjustment settings are defined.
see Test / Adjustment settings (page 48)
1 Have required test weight ready.
2 Open sample chamber.
3 Tap the item Weight test - external.
The adjustment screen appears.
4 Clear sample pan holder and tap [Start test].
Note
We recommend not to use a pan.
The required value flashes and prompts you to load the weight.
5 Load the required test weight.
The balance indicates the adjustment process, "––––––" appears.
6 When the display flashes "000.00" remove the test weight.
When the test process is done, the display shows the test results and indicates whether the test is passed or failed according to defined tolerances. The results can be printed out by tapping [ ].
Timeout
After a timeout of 75 seconds the error message appears Weight out of range. The test has been aborted.
The test was not executed.
1 Confirm with [OK].
2 Repeat the test.
7.2.2 Temperature Test
Navigation: Home > Test/Adjust > Tests > Temperature test
This function allows you to test the temperature control of the heating module. You need the optional Tempera
you to wait at least 30 minutes after a drying operation (or previous heating module adjustment) before per forming a test.
Note
● The duration of the temperature test is 15 minutes for each measuring temperature.
●
●
●
The sample chamber must be cooled down below 50 °C before a further adjustment or test can be done.
It is possible to perform a test and then subsequently to transform the test into an adjustment if required.
This is only possible for tests conducted with temperatures 1 and 2.
Temperature test settings see Test Settings (page 49).
Test/Adjust 65
Setting up the Drying Unit for temperature test
Same procedure as for temperature adjustment, see Temperature Adjustment (page 62).
Danger of burns
Sample chamber may still be hot.
– Cool down instrument before setting up.
Performing temperature test
Test settings are defined, see Test Settings (page 49).
Setting up the drying unit for temperature testing has been carried out.
1 Tap menu item Temperature test.
Work screen Temperature test appears.
2 Tap [Start test].
Note
The testing process takes 15 minutes for each temperature (depending on the settings).
The instrument starts the testing process. The screen shows the current temperature and remaining time.
The instrument is heating up to the target temperature 1 for determining the predefined lower tempera ture.
After 15 minutes, the instrument displays and stores the measured lower temperature and continues with the process.
The instrument is heating up to the target temperature 2 for determining the predefined upper tempera ture.
After 15 minutes, the instrument displays and stores the measured upper temperature.
The test is done and indicates whether the test has passed or failed according to defined tolerances.
3 Decide if an adjustment is needed.
4 • To return to the menu Tests, tap [Tests].
• To print out the results, tap [ ].
• To display or print the results at any time, tap [History].
• To return to the home screen, press [ ].
5 After cooling down, remove temperature adjustment kit and set up drying unit for measurement, see Setting
66 Test/Adjust
7.2.3 SmartCal test
What is SmartCal™?
Proper operation of the Halogen Moisture Analyzer can be quickly verified with a SmartCal test. SmartCal is a granular test material with a defined moisture value after a specified time at a defined drying temperature.
SmartCal is available for four test temperatures. There are control limits for each test temperature. If the mea sured and normalized moisture value is within the control limits, the instrument has passed the functional test.
If value is outside the control limits, there may be a problem with the instrument or the test conditions may not have been met.
Test temperatures and control limits
cSmartCal (certified) and SmartCal can be used for testing at any temperature between 70 °C and 230 °C.
METTLER TOLEDO provides established control limits for testing at 70 °C, 100 °C, 130 °C and 160 °C.
Select the temperature closest to the drying temperature normally used.
Temperature
70 °C
100 °C
130 °C
160 °C
cSmartCal™
3.3 - 4.3 %MCN
5.3 - 6.3 %MCN
7.5 - 8.7 %MCN
10.0 - 11.6 %MCN
SmartCal™
3.2 - 4.4%MCN
5.2 - 6.4 %MCN
7.4 - 8.8 %MCN
9.9 - 11.7 %MCN
MCN = Normalized moisture content (Calculated value in consideration of temperature and humidity)
Note about using SmartCal
●
Store SmartCal at room temperature.
●
Do not open the blister pack before use.
●
Shelf life: The expiry date is printed on the blister pack and on the stick (e.g. Exp08.2013).
●
Disposal: Can be disposed of as normal waste. Observe local and national environmental regulations.
Additional information on using SmartCal, e.g. SmartCal user guide, see u www.mt.com/smartcal
Performing SmartCal™ test
Navigation: Home > Test/Adjust > Tests > SmartCal test
The test is carried out in the same way as a measurement. The duration of the test is 10 minutes.
The Instrument is acclimatized in working area, cooled and connected to AC power for at least one hour.
The SmartCal package is acclimatized in working area.
The expiration date of the Smart Call sample has not been reached.
The METTLER TOLEDO RHT sensor is properly installed and acclimatized in working area after installing for at least one hour. If no RHT sensor is available, room temperature and humidity must be enter manually,
see Install METTLER TOLEDO RHT sensor (page 29).
Alternatively:
– you can use a certified RHT sensor from Testo, see note at the end of this Chapter.
– you can enter the temperature and humidity manually.
Identification of the METTLER TOLEDO RHT sensor if needed, see Equipment (page 48).
Test temperature and control limits are set, see Test Settings (page 49).
1 Tap SmartCal test.
2 Open sample chamber.
3 If no RHT sensor is used, enter current room temperature and humidity. Tap [OK]
4 Enter SmartCal lot number if needed. Tap [OK]
5 Place the sample pan handler with the aluminum sample pan in the instrument.
Test/Adjust 67
6 Tap [->0/T<-] to tare the balance.
7 Remove a SmartCal stick from the blister pack, tear it open, and distribute the entire contents evenly over the sample pan. If necessary, carefully rotate and tilt the sample pan until it is fully and uniformly covered with granulate.
8 Close sample chamber.
9 Start the test immediately by tapping start drying.
SmartCal test is performing.
The test is done and indicates whether the test has passed or failed. The display shows the normalized result.
●
●
Passed: Your instrument works properly and is ready for other measurements.
Failed: Your instrument works not properly. Action are required:
•
See What to Do if…
•
We recommend not to use this instrument further until the problem is resolved. In this case contact your
METTLER TOLEDO representative.
– • To return to the menu Tests, tap [Tests].
• To print out the results, tap [ ].
• To display or print the results at any time, tap [History].
• To return to the home screen, press [ ].
Note
SmartCal tests do not supersede the recommended periodic weight or temperature tests.
Certified RHT sensors
The RHT sensor from METTLER TOLEDO in not available as a certified version. If an certified version is required, the following RTH models from testo are supported: testo 435-2, testo 435-4, testo 635-2, testo 735-2.
The Testo RHT sensor has to be connected on the USB port on the terminal. If both RHT sensors are connected, the testo RHT sensor has priority.
For more information about Testo, see u http://www.testo.com
68 Test/Adjust
7.2.4 Test Printout Examples
Weight test external
--WEIGHT TEST EXTERNAL--
14.10.2011 11:51
METTLER TOLEDO
Halogen MoistureAnalyzer
Type HS153
SNR(Drying Unit) 2345
SNR(Terminal) 6788
SW(Drying Unit) 0.60.09
SW(Terminal) 4.20628
User name Administrator
Weight ID
ECW-100/1
Nominal Weight
100.000 g
Actual 100.001 g
Difference 0.001 g
Tolerance +/- 0.002 g
Cell temperature
23.83 °C
Test passed
Signature
........................
---------- END ---------
Temperature test
----TEMPERATURE TEST----
14.10.2011 11:51
METTLER TOLEDO
Halogen MoistureAnalyzer
Type HS153
SNR(Drying Unit) 2345
SNR(Terminal) 6788
SW(Drying Unit) 0.60.09
SW(Terminal) 4.20628
User name Administrator
Temp Kit ID MT-414/A
Temp1 target 100 °C
Temp1 actual 99 °C
Temp1 tolerance
+/- 2 °C
Temp2 target 160 °C
Temp2 actual 159 °C
Temp2 tolerance
+/- 2 °C
Test passed
Signature
........................
---------- END ---------
Test/Adjust 69
7.3 History
Navigation: Home > Test/Adjust > History
●
●
●
The instrument always records all test or adjustment operations that have been made and saves them in a memory which is specially protected against power failure (limited to the last 50 records per history selection).
Note
Aborted adjustments or tests will not be saved.
When the History is selected, a list appears with the history selection as follows:
Weight test history
Weight adjustment history
Temperature test history
●
●
Temperature adjustment history
SmartCal test history
The following information is displayed:
Weight test history
Weight test external
Calibration weight identification
Nominal weight
Actual weight
Difference
Tolerance
Temperature g g g g
°C
Weight adjustments history
Weight adjustment external
Calibration weight name
Calibration weight identification
Nominal weight
Temperature g
°C
Temperature adjustment/test history
Temperature adjustment
Adjustment kit identification
Temperature 1
Temperature 2
Temperature test
Adjustment kit identification target - actual Temperature 1 target - actual Temperature 2
Free temperature
Tolerances for each temperature
SmartCal test history
SmartCal test
User name
SmartCal Identification
Start weight
Total test time
Dry weight
Test result
Date and time
Leveling information g minutes
%MCN passed / failed
The selected individual results can be printed out by tapping [ ].
target - actual target - actual target - actual
°C
70 Test/Adjust
8 Method Definition
Navigation: Home > Method definition
What is a method?
Methods simplify and accelerate your daily work. A method contains all settings for measuring the moisture content of a particular sample (substance). It can be recalled by tapping a measurement button or a shortcut and your instrument immediately operates with the corresponding settings.
The optimal setting of parameters and the drying time depends on the type and size of the sample and the desired accuracy of the measurement result. The exact parameters can only be determined experimentally, see
How to Obtain Best Results (page 120). Your Instrument helps you to determine the settings.
Method definition
This function offers you to define new methods and to change, delete, export or import existing methods depending on the user rights. It allows you to store up to 99 individual methods.
All parameters using in a drying method, can be defined under this menu item.
Note
● In most cases it is sufficient to set Main measurement parameters.
● You will find more information about defining methods in the delivered application brochure «Guide to Mois
ture Analysis» or see How to Obtain Best Results (page 120).
Prerequisite
The parameter menu appears only if a method already exists and is selected in the method definition dialog or create a new method.
Menu structure
Main menu
Main measurement parame ters
Result and value handling
Workflow handling
General method properties
Submenu
Drying program
(including temperature and switch-off criteria)
Display mode
Start weight
Further information
see Settings of Drying Program
see Settings of Display Mode
see Settings of Start Weight
Control limits
Free factor
Starting mode
Method name
Method Definition 71
Defining a new Method
Note
A method name can only exist once.
Method definition is selected.
1 Tap [New...].
The keypad appears.
2 Enter a name for the new method. Name should be unique and unambiguous.1 to 30 characters are possi ble (including spaces).
3 Confirm with [OK].
The parameter menu for the new method appears.
4 Set the desired parameters e.g. Main measurement parameters.
5 To store the method, tap [Save].
Editing an existing method
Method definition is selected.
1 Tap the method in the list you want to edit.
The parameter menu for the selected method appears.
2 Edit the desired parameters e.g. Main measurement parameters.
3 To store the method, tap [Save].
Copying an existing method
Method definition is selected.
1 Tap the method in the list you want to copy.
The parameter menu of the desired method appears.
2 Tap [Save as...].
The keypad appears.
3 Enter a new name for the copied method. Name should be unique and unambiguous.1 to 30 characters are possible.
4 To store the method, tap [Save].
Removing an existing method
Note
All results of this method are also removed.
Method definition is selected.
1 Tap the method in the list you want to remove.
The parameter menu of the desired method appears.
2 Tap [Delete].
A message box appears.
3 Confirm with [Delete].
The desired method is removed.
Note
A possible shortcut to this method is not removed.
For removing shortcuts see Using Shortcuts (page 91)
8.1 Main Measuring Parameters
Navigation: Home > Method Definition > Method name > Main measurement parameters
72 Method Definition
These parameters are relevant for measuring and must be determined for all samples. Most samples can be determined with these parameters.
You can define the following parameters:
Menu item Explanation
Drying program
Defines the drying program which is best suited for the specific sample. (including temperature and switch-off criteria)
Further Information
see Settings of Drying Program
Display mode
Defines the type of value for displaying and printing. see Settings of Display Mode
Start weight
Defines a start weight so that the samples always have approximately the same weight .
see Settings of Start Weight
8.1.1 Settings of Drying Program
Navigation: Home > Method Definition > Method name > Main measurement parameters > Drying pro
gram
This function offers you different predefined drying programs for optimum matching of the drying characteristics to the sample used. Furthermore, the drying temperature, switch-off criterion as well as the start weight can be set. Carry out a test measurement for determining the appropriate switch-off criterion, if you do not know the
behavior of the sample. For carry out a test measurement see Testing a Method (page 87).
●
●
●
Note
You will find more information about defining methods in the delivered application brochure «Guide to Moisture
Analysis».
You can define the following parameters:
Parameter Explanation
Drying program
Defines the drying program which is best suited for the specific sample.
Values
Standard* |
Rapid |
Gentle |
* Factory setting
Further information:
Standard drying see Setting Standard drying (page 73)
Rapid drying see Setting Rapid drying (page 74)
Gentle drying see Setting Gentle drying (page 75)
8.1.1.1 Setting Standard drying
Standard drying
This drying program is set in the factory and is suitable for most samples. The sample is heated to the drying temperature.
Factory setting
Drying temperature = 105 °C, Switch-off criterion 3 = 1 mg / 50 s
Method Definition 73
You can define the following parameters:
Parameter
Drying tempera ture
Switch-off crite rion
SOC delay
Explanation
Defines the drying temperature.
Values
40…230 °C
(105 °C *)
Defines the criterion when the instrument should end the drying.
1 (1 mg / 10 s) |
2 (1 mg / 20 s) |
3 (1 mg / 50 s)* |
4 (1 mg / 90 s) |
5 (1 mg / 140 s) |
Timed... |
Free (mg / s)... |
Free (% / s)...
Activates and defines the delay for the starting time of the switchoff criterion.
OFF* | ON |
0…99 min
OFF = no delay applied.
Setting the Drying Temperature
Navigation: Method Definition > Name of method > Main measurement parameters > Drying temperature
In this menu item you can set the final drying temperature.
Note:
The admissible input range for the drying temperature is indicated.
1 Start of drying
2 Final temperature
Setting Switch-off criterion
see Settings of Switch-off Criterion (SOC) (page 76)
8.1.1.2 Setting Rapid drying
Rapid drying
This drying program is primarily suitable for samples with a moisture content over 30%.
Following the start, the selected temperature is exceeded by 40% for 3 minutes (however, is possible up to maximum 230°C) to compensate for the cooling due to vaporization and accelerate the drying process. The drying temperature is then lowered to the set value and maintained.
Factory setting
Drying temperature = 105 °C, Switch-off criterion 3 = 1 mg / 50 s
74 Method Definition
You can define the following parameters:
Parameter
Drying tempera ture
Switch-off crite rion
Explanation
Defines the drying temperature.
Values
40…230 °C
(105 °C *)
Defines the criterion when the instrument should end the drying.
1 (1 mg / 10 s) |
2 (1 mg / 20 s) |
3 (1 mg / 50 s)* |
4 (1 mg / 90 s) |
5 (1 mg / 140 s) |
Timed... |
Free (mg / s)... |
Free (% / s)...
* Factory setting
Setting the Drying Temperature
Navigation: Method Definition > Name of method > Main measurement parameters > Drying temperature
In this menu item you can set the final drying temperature.
Note:
The admissible input range for the drying temperature is indicated.
1 Start of drying
2 Final temperature
Setting Switch-off criterion
see Settings of Switch-off Criterion (SOC) (page 76)
8.1.1.3 Setting Gentle drying
Gentle drying
This drying program is suitable for the gentle drying of substances which tend to form a
skin (e.g. substances containing sugar or volatile substances). With this program the tem perature is continuously increased and attains the selected drying temperature only after
the elapse of the so-called ramp time. The «ramp», i.e. the time that should elapse between the start of drying and attainment of the final temperature can be pre-set.
Factory setting
Drying temperature = 105 °C, Ramp time = 3:00 min,
Switch-off criterion 3 = 1 mg / 50 s
Method Definition 75
You can define the following parameters:
Parameter
Drying tempera ture
Ramp time
Switch-off crite rion
Explanation
Defines the drying temperature.
Values
40…230 °C
(105 °C *)
0…480 min Defines the time in minutes that should elapse between the start of drying and attainment of the final temperature for Gentle dry ing.
Defines the criterion when the instrument should end the drying.
1 (1 mg / 10 s) |
2 (1 mg / 20 s) |
3 (1 mg / 50 s)* |
4 (1 mg / 90 s) |
5 (1 mg / 140 s) |
Timed... |
Free (mg / s)... |
Free (% / s)...
* Factory setting
Setting the Drying Temperature
Navigation: Method Definition > Method name > Main measurement parameters > Drying
programGentleDrying temperature
In this menu item you can set the desire final drying temperature.
1 Start of drying
2 Final temperature
Setting the ramp time
Navigation: Method Definition > Method name > Main measurement parameters > Drying programGentle
> Ramp time
In this menu item you can define the Ramp time, i.e. the time that should elapse between the start of drying and attainment of the final temperature. The ramp is started once the temperature reaches 50 °C.
1 Start of drying
2 Final temperature
3 Ramp time
Setting Switch-off criterion
see Settings of Switch-off Criterion (SOC) (page 76)
8.1.1.4 Settings of Switch-off Criterion (SOC)
Navigation: Home > Method Definition > Method name > Main measurement parameters > Drying pro
gram
This function offers you different switch-off criteria. A switch-off criterion defines when the instrument should end the drying or should start the next step ("Step drying"). Switch-off criteria ensure that measurements are finished in the same condition (weight loss per unit of time) every time, ensuring repeatable measurements.
Note
Accurate results require same start weights, see Settings of Start Weight (page 82).
76 Method Definition
●
●
●
You can define the following parameters:
Parameter
Switch-off crite rion
Explanation Values
Defines the criterion when the instrument should end the drying.
1 (1 mg / 10 s) |
2 (1 mg / 20 s) |
3 (1 mg / 50 s)* |
4 (1 mg / 90 s) |
5 (1 mg / 140 s) |
Timed... |
Free (mg / s)... |
Free (% / s)...
* Factory setting
Weight loss per unit of time (5 preprogrammed settings)
Free switch-off criterion (2 different settings)
Timed switch-off
Weight loss per unit of time
The switch-off defines in which drying condition, the measurement is completed. This switch-off is based on a weight loss per unit of time. As soon as the mean weight loss is less that a preset value during a specified time, the instrument considers drying as complete and automatically discontinues the measurement process.
Note
The switch-off criterion is inactive during the first 30 sec.
The following 5 preprogrammed settings are available
Switch-off criterion
3
4
1
2
5
Δ g
1 mg
1 mg
1 mg
1 mg
1 mg
Δ t
10 s
20 s
50 s
Description
This setting is suitable for fast measurements to determine a trend.
This setting is suitable for quick drying samples.
This is the factory setting. It is suitable for most kind of samples.
90 s This setting is suitable for samples which dry moderately quickly or for samples with higher accuracy requirements.
140 s This setting is suitable for samples which dry very slowly (trapped moisture, skin formation) or for samples with very low moisture con tent e.g. plastics. Not suitable for very temperature sensitive samples.
The graph below exemplifies the mode of operation of the switch-off operation (not to scale).
Method Definition 77
W
W
1)
= =
2)
∆ t
∆g
∆t
(10 s)
∆g
∆t
(50 s) ∆g
∆t
(140 s)
1
(1 mg / 10 s)
3
(1 mg / 50 s)
5
(1 mg / 140 s)
t
t = time
W = weight of sample
1, 3, 5 = switch-off criteria shown as an example
1) = equal area
2) = mean weight loss per unit of time
●
●
Free switch-off criterion
The free switch-off criterion is based on a user-defined mean weight loss per unit of time.
The following 2 settings are available:
Switch-off criterion > Free (mg / s)... (weight loss per unit of time)
Switch-off criterion > Free (% / s)... (weight loss in percent per unit of time)
Timed switch-off
With this switch-off criterion the measurement lasts until the present drying time has elapsed. The display pro vides you with continuous information in the drying time.
Performing Test measurements
78 Method Definition
8.1.1.5 Settings of SOC Delay
Navigation: Home > Method Definition > Method name > Main measurement parameters > SOC delay
With this function you can delay the starting time of the switch-off criterion. This can be useful for samples with low moisture content which need extended time until they evaporate moisture e.g. plastics.
●
●
Note
SOC delay is only available for the following drying programs:
Standard
QuickPredict
You can define the following parameters:
Parameter
SOC delay
Explanation
Activates and defines the delay for the starting time of the switchoff criterion.
OFF = no delay applied.
* Factory setting
Values
OFF* | ON |
0…99 min
8.1.2 Settings of Display Mode
Navigation: Home > Method Definition > Method name > Main measurement parameters > Display Mode
With this function you can select the desired type of result display. You also define what type of values are printed on the records.
You can define the following parameters:
Parameter Explanation
Display Mode
Defines the type of value for displaying and printing.
Values
%MC* | %DC | %AM |
%AD | g| g/kg MC |
g/kg DC | –%MC
●
●
●
●
●
●
●
●
* Factory setting
%MC – Moisture Content (calculated value)
%DC – Dry Content (calculated value)
%AM – ATRO Moisture Content (calculated value)
%AD – ATRO Dry Content (Wet weight, calculated value)
g – Weight in Grams
g/kg MC – Moisture Content (calculated value)
g/kg DC – Dry Content (calculated value)
–%MC – Moisture Content (negative value, calculated value)
Note
Calculated values are indicated with an asterisk in the display.
Detailed information:
Method Definition 79
%MC – Moisture Content
The moisture content of the sample is displayed (and printed out) as a percentage of the wet weight (WW = initial weight = 100 %). This is the
factory setting.
WW
During the measuremnet the value is constantly displayed in percent and as a graphical drying curve. The measured value is marked by "%MC"
(Moisture Content, e.g. 11.35 %MC) also for the printed results.
Before drying
MC
=
WW – DW
WW
· 100 %
MC = Moisture Content [0…100 %]
WW = wet weight
DW = dry weight
%DC – Dry Content
The dry content of the sample is displayed (and printed out) as a per centage of the wet weight (WW = initial weight = 100 %).
During the measuremnet the value is constantly displayed in percent and as a graphical drying curve. The measured value is marked by "%DC"
(Dry Content, e.g. 88.65 %DC) also for the printed results.
Before drying
DC
=
DW
WW
· 100 %
DC = dry content [100…0 %]
WW = wet weight
DW = dry weight
DW
After drying
MC
After drying
80 Method Definition
%AM – ATRO Moisture Content
1)
The moisture content of the sample is displayed (and printed out) as a percentage of the dry weight (DW = final weight = 100 %)
During the measuremnet the value is constantly displayed in percent and as a graphical drying curve. The measured value is marked by "%AM"
(ATRO Moisture Content, e.g. 255.33 %AM) also for the printed results.
Before drying
AM
=
WW – DW
DW
· 100 %
AM = ATRO moisture content [0…1000 %]
WW = wet weight
DW = dry weight
After drying
%AD – ATRO Dry Content (Wet weight)
1)
The wet weight of the sample is displayed (and printed out) as a per centage of the dry weight (DW = final weight = 100 %)
During the measuremnet the value is constantly displayed in percent and as a graphical drying curve. The measured value is marked by "%AD"
(ATRO Dry Content, e.g. 312.56 %AD) also for the printed results..
Before drying
AD =
WW
DW
· 100 %
AD = ATRO dry content [100…1000 %]
WW = wet weight
DW = dry weight
After drying
1)
Comment on the ATRO display mode
If the current measured value in the ATRO display mode is greater or less than the predefined limit value (i.e.
greater than 999.99 %AD or less than –999.99 %AM), the ATRO result values are limited to 999.99%.
g – Weight in Grams
The weight of the sample is displayed (and printed out) in grams. With this setting, the Moisture Analyzer is used as a precision balance.
During the measuremnet current weight is constantly displayed in grams.
g/kg MC – Moisture Content
The moisture content of the sample is displayed (and printed out)in g/kg of the wet weight (WW = initial weight = 1000 g/kg).
During the measuremnet the current measured value is constantly dis played in percent and as a graphical drying curve. The measured value is marked by "g/kg MC" (Moisture Content, e.g. 11.35 g/kg MC) also for the printed results.
WW
Before drying
MC =
WW – DW
WW
· 1000 g/kg
MC = Moisture Content [0…1000 g/kg]
WW = wet weight
DW = dry weight
DW
After drying
MC
Method Definition 81
g/kg DC – Dry Content
The dry content of the sample is displayed (and printed out) in g/kg of the wet weight (WW = initial weight = 1000 g/kg).
During the measuremnet the current measured value is constantly dis played in percent and as a graphical drying curve. The measured value is marked by "g/kg DC" (Dry Content, e.g. 88.65 g/kg DC) also for the printed results.
DC =
DW
WW
· 1000 g/kg
DC = dry content [1000…0 g/kg]
WW = wet weight
DW = dry weight
Before drying
–%MC – Moisture Content
The moisture content of the sample is displayed (and printed out) as a percentage of the wet weight (WW = initial weight = 100 %).
During the measuremnet the value is constantly displayed in percent and as a graphical drying curve. The measured value is marked by "-%MC"
(Moisture Content, e.g. -11.35 -%MC) also for the printed results and shown as a negative value.
WW
Before drying
MC = –
WW – DW
WW
· 100 %
MC = Moisture Content [0…100 %]
WW = wet weight
DW = dry weight
After drying
DW
After drying
MC
8.1.3 Settings of Start Weight
Navigation: Home > Method Definition > Method name > Main measurement parameters > Start weight
The start weight affects both the duration of the measurement as well as the accuracy of the results. A small weight results in a shorter duration of the measurement but will decrease the accuracy of the result. With this function you can define a start weight so that the samples are approximately of equal weight thus improving the repeatability of the measurements. The weighing-in aid assists you in weighing-in the sample. At most of the samples the target weight is in the range of 2–5 g (plastics 30 g). We recommend to cover the whole surface of the sample pan with a thin uniform layer of sample.
You can define the following parameters:
Parameter
Start weight
Start weight tol erance
Weigh-in aid
Explanation
Defines a start weight so that the samples always have approxi mately the same weight .
Defines the tolerance of the Start weight.
10 %, recommended for sample weights up to 5 g.
Defines monitoring of target weight and tolerance.
Passive = tolerance is displayed.
Active = tolerance is monitored. If the startweight is out of toler ance, the measurement cannot be started.
Values
OFF* | ON
(0.100…200.000 g)
1…25 %
(10 %)*
Passive* | Active
* Factory setting
82 Method Definition
8.2 Result and Value Handling
Navigation: Home > Method Definition > Method name > Result and value handling
You can define the following parameters:
Menu item Explanation
Control limits
Defines the acceptable range for measuring results in the unit of the selected display mode.
Further Information
8.2.1 Control limits
Navigation: Home > Method Definition > Method name > Result and value handling > Control limits
With this function you can set warning and intervention limits for the quality and process monitoring. You can also set limits for distinguish passed or failed.
You can define the following parameters:
Parameter Explanation
Control limits
Defines the acceptable range for the measuring results in the unit of the selected display mode.
Values
OFF* | ON
(0.00…100.00)
OFF = no limits applied.
T1+ (Upper warning limit)
T1- (Lower warning limit)
T2+ (Upper intervention lim it)
T2- (Lower intervention lim it)
* Factory setting
Defines the upper warning limit in the selected unit of the display mode. Measurement passed with warning (!).
Value range in ATRO mode (%AD, %AM) up to 1000.
Defines the lower warning limit in the unit of the selected display mode. Measurement passed with warning (!).
Value range in ATRO mode (%AD, %AM) up to 1000.
Defines the upper intervention limit in the unit of the selected dis play mode. Measurement failed (X).
Value range in ATRO mode (%AD, %AM) up to 1000.
Defines the lower intervention limit in the unit of the selected dis play mode. Measurement failed (X).
Value range in ATRO mode (%AD, %AM) up to 1000.
OFF* |
0.01…100.0 (1000)
OFF* |
0.01…100.0 (1000)
OFF* |
0.01…100.0 (1000)
OFF* |
0.01…100.0 (1000)
Setting the limits
1 2 3
MC%
0
4 5 6
MC%
0
Method Definition 83
Limits
T2+ (Upper intervention limit)
T1+ (Upper warning limit)
T1- (Lower warning limit)
T2- (Lower intervention limit)
(X)
(!)
(!)
(X)
1
Off
Off
2
Off
Off
Off
3
Off
Off
Off
4 5
Off
Off
6
Off
Off
( ✓) Measurement is within the warning limits: passed (displayed in green)
(!) Measurement is between the warning limits and the intervention limits: passed with warning (displayed in yellow)
(X) Measurement is outside the intervention limit: failed (displayed in red)
Control limits is off = no limits applied (displayed in blue)
Testing the limits
See Testing a Method (page 87).
8.2.2 Free Factor
Navigation: Home > Method Definition > Method name > Result and value handling > Free factor
This function allows you to multiply the result by a method-specific factor in the selected display mode. Further more, it allows you changing the result by an offset entry in the unit of the selected display mode. It is used to calculate a corrected final result (e.g. in order to compensate for systematic deviations from the reference result).
Note
● Free factor is not available in display mode "g" (weight).
●
●
The calculation is carried out continuously during the measurement and displayed with the graphical drying curve.
With free factor, the results are calculated and marked with an asterisk in the display.
You can define the following parameters:
Parameter
Free factor
Explanation
Defines the settings for free factor.
OFF = no free factor applied.
Factor
Defines the multiplication factor.
Values
OFF* | ON
Offset
Format
Defines the offset value in the selected display mode.
Defines the number of decimal places of the calculated final results, for displaying and printing.
-10.000…+10.000
(1.000)*
-1000.000…
+1000.000
(0.000)* x | x.x | x .xx | x.xxx*
* Factory setting
84 Method Definition
8.3 Workflow Handling
Navigation: Home > Method Definition > Method name > Workflow handling
With this functions you can define the workflow for the measurement
You can define the following parameters:
Menu item Explanation
Starting mode
Defines how the sample chamber is operated.
Further Information
8.3.1 Starting Mode
Navigation: Home > Method Definition > Method name > Workflow handling > Starting mode
In this menu you can choose whether the sample chamber performs automatic or manual functions (e.g. tare, stop drying).
You can define the following parameters:
Parameter Explanation
Starting mode
Defines how the sample chamber is operated.
Values
Automatic* |
Manual
* Factory setting
Automatic
Your instrument is set in the factory to the automatic operating mode. This mode can be used for most kind of samples. When closing the sample chamber, the weight of the sample is recorded and the measurement is started.
Manual
We advise you to use the manual operating mode for samples which contain readily volatile substances. In contrast to the automatic operating mode, in the manual operating mode the sample chamber does not auto matically close when the [Start drying] button is tapped. However, the initial weight (wet weight) important for the determination of the moisture content is recorded. In the manual operating mode you have time for further preparation of the sample (e.g. mixing with quartz sand or even distribution of the sample) while weight losses due to evaporation during the preparation time are measured from the outset. As soon as the sample is ready for drying, close the sample chamber. As soon as the automatic sample chamber is closed, drying starts. In the manual operating mode you can open the sample chamber during a drying operation e.g. in standby mode. In contrast to the automatic mode, drying will not be stopped but simply interrupted until the automatic sample chamber is closed again.
Method Definition 85
8.4 General Method Properties
Navigation: Home > Method Definition > Method name > General method properties
8.4.1 Method name
Navigation: Home > Method Definition > Method name > General method properties > Method name
You can define the following parameters:
Parameter Explanation Values
Method name
Renaming a method. Name should be unique and unambiguous. any
86 Method Definition
8.5 Testing a Method
Test a method
This function allows you to test the settings during the definition phase of a method. Testing is possible at any time. Test measurements are recorded in the journal and marked as test results. If you wish to work with the switch-off criterion «weight loss per unit of time» and are not familiar with the behavior of the sample, the test measurement will help you select the suitable setting. For more information about switch-off criteria, see Set
tings of Switch-off Criterion (SOC) (page 76).
The diagram illustrates the progress of a drying. The points at which the individual switch-off criteria were reached (1-5) are marked.
MC (%)
20
15
10
1
2
3
4
5
5
0 t
0 1 2 3 4 5 6 7 8 9 10 11
During this measurement, the measured values are recorded the switch-off criteria 1 to 5 and maybe one of a free-defined switch-off criterion. The measurement terminates after the defined time (default 30 minutes). Note that the start weight affects the switch-off criterion. The test time can also be switched off. In this case the mea surement terminates after reaching the predefined switch-off criterion. Nevertheless, all switch-off criteria are recorded.
By comparing the measured values with values of a reference method e.g. drying oven and the standard devia tion, you can define the appropriate parameter settings. For more information see the application brochure
«Guide to Moisture Analysis».
Carry out all measurements under Home > Method Definition > Method name > Tests before releasing a method. The results of test measurements are specifically marked.
Attention
Before releasing the method, check if the determined switch-off criterion is set.
Performing a Test measurement
You perform a test measurement just like any other measurement. How to perform the measurement see Mea
Changing the test time
Work screen for testing is displayed.
1 Tap Test time in the work screen.
Test time in min appears.
2 Confirm with OK.
Displaying the parameter
Work screen for testing is displayed.
– Tap the parameter in the work screen.
The parameter list appears.
Printing results of the determined switch-off criteria
For a printout example , See Information on Printouts section «Special events».
Displaying results of the determined switch-off criteria
See Graphical Evaluations of Measurement Results
Method Definition 87
9 Measurement
This function offers you to perform a measuring using previously defined methods. After choosing the measure ment method, the measurement process can be started. The work screen guides you step by step through the measuring process.
The following functions are available:
●
●
●
●
On the work screen, you can create a shortcut. This allows you to start a method directly from the home screen.
See Using Shortcuts (page 91).
After completion of a measuring you can perform a further measuring with same method by tapping [Next
Sample] or with an other method by tapping [Measurement].
For graphical evaluations of measurement results tap [Results]. If you have defined the control limits in the method, passed, warned or failed status is shown.
A detailed overview of the method parameter can you call up by tapping the parameter panel.
Also see
●
●
●
9.1 Performing a Measurement
You are now familiar with all the parameters of your instrument and have defined all values for your sample.
The instrument is now ready for the determination of your samples. In this Section you will learn how to perform measurements and how to stop the measurement process.
Switching on
The instrument must be connected to the power supply for approxi mately 60 minutes in order to reach operating conditions.
1 To switch on the Instrument, press [ ].
2 Log-in with your password, if needed.
Selecting method for measurement
1 Tap Measurement.
The methods list is displayed.
2 Select the method to determine your sample.
The work screen of the method appears.
3 Open the sample chamber.
88 Method Definition
Placing sample pan
The display now prompts you to load the empty sample pan and tare the balance.
1 Place the empty sample pan in the sample pan handler.
2 Place the sample pan handler in the sample chamber. Ensure that the tongue of the pan handler fits exactly in the slot of the draft shield element. The sample pan must lie flat in the pan holder.
Note
We advise you to work with the sample pan handler at all times. The pan handler is ergonomic, automatic positioning, safe and provides protection against possible burns due to the hot sample pan.
Taring the balance
1 Close the sample chamber.
The instrument tares the balance (Starting mode: Automatic).
2 After taring, open the sample chamber.
Starting measurement
After taring, the display prompts you to add the sample to the sam ple pan.
1 Add the sample to the sample pan. If you have defined a start weight, weigh the sample using the weighing-in aid.
2 Close the sample chamber.
3 Tap [Start drying].
The drying process starts.
●
●
●
●
Drying process
You can follow the measurement process on the display, see Work Screen (page 22).
The drying process is continuously displayed graphically.
The current temperature in the heating module is displayed as well as the elapsed drying time and the cur rent drying value.
The display shows the selected settings.
The drying process can be aborted by tapping [Stop drying].
At the end of the drying process you can read the moisture content of your sample on the display. If you have defined the control limits in the method, passed, warned or failed status is shown.
Removing Sample
Danger of burns
Sample, sample pan and sample pan holder may still be hot.
Measurement 89
The drying process is completed.
The sample chamber is open.
1 Carefully remove the sample pan handler from the sample cham ber.
Note
To remove the sample pan from the handler, lift the pan slightly from below and remove it from the handler.
2 • To perform a further measurement with the current method, tap
[Next Sample].
• To perform a measurement with a new method, tap [Measure-
ment].
• To return to the home screen, press [ ].
Stop drying
When you stop the measuring process by tapping [Stop drying], you can chose between two possibilities:
●
●
Abort without saving
Abort without saving of any data collected until now.
Abort measurement and save data
Already sampled data are stored and an entry will be made in the results. The result is marked as aborted.
Adding a comment
At the end of a measurement you can add a comment to the result of the measurement. This comment is stored in the measurement result and can be printed. A comment can only be entered before leaving the current mea surement.
1 To create a comment, tap [Note].
The keyboard dialog appears.
2 Enter a comment.
3 Confirm with [OK].
9.2 Work with Weighing-in Aid
The weighing-in aid can be defined for each method and facilitates weighing in of the sample to a target value.
This is particularly necessary if you require all the samples of a method you wish to process to have same weight in order to improve the repeatability of the measurement results. In addition, the weighing-in aid can be set as active so that the drying process cannot be started if the weight of sample is outside the set tolerance.
You are therefore compelled to weigh-in the correct quantity of sample. If all sample weighed are within toler ances then this will improve the repeatability. The weighing-in aid is available only if start weight has been acti
vated. For further information see Settings of Start Weight (page 82).
90 Measurement
Icon Function
Lower weight limit (tolerance range)
Target weight
Icon Function
Upper weight limit (tolerance range)
9.3 Using Shortcuts
Navigation for managing shortcuts: Home > Measurement > Method name > [ ]
Shortcuts allow you to start methods directly from the home screen. Shortcuts are user-specific, i.e. each indi vidual user can have his own shortcuts for the most common tasks.
You can define the following parameters:
Parameter Explanation
Shortcut name
Defines a name for the shortcut. It is recommended to choose a short name because only approx. 8 characters are displayed on the shortcut. Name should be unique and unambiguous.
Method name
Shows the name of the method. The name of the method is the target of the shortcut and can not be changed.
Values any none
Defining a shortcut
Menu Measurement is activated.
The method is selected.
1 Tap [ ].
Window My shortcuts appears.
2 Tap Add a shortcut to my home for this method.... (To abort, tap [X].)
New shortcut appears.
3 To enter a name for the shortcut if needed, tap Shortcut name.
Note
It is recommended to choose a short name because only approx. 8 characters are displayed on the short cut. Name should be unique and unambiguous.
4 Confirm with [OK].
5 To store the setting, tap [Save].
To abort, tap [Cancel].
The shortcut is added to the home screen.
Editing a shortcut
The method is selected.
1 Tap [ ].
Window My shortcuts appears.
2 Tap Edit this shortcut.... (To abort tap [X].)
Shortcut properties appears.
3 To edit the name of the shortcut, tap Shortcut name.
4 Confirm with [OK].
5 To store the setting, tap [Save].
To abort, tap [Cancel].
Removing a shortcut
The method is selected.
1 Tap [ ].
Window My shortcuts appears.
Measurement 91
2 Tap Edit this shortcut.... (To abort, tap [X].)
Shortcut properties appears.
3 To remove the shortcut, tap [Remove].
A message window appears.
4 Confirm with [Remove]. (To abort, tap [Cancel].)
The shortcut is removed from the home screen.
92 Measurement
10 Results
10.1 Graphical Evaluations of Measurement Results
Navigation: Home > Results
This function allows you to manage and evaluate measurement results.
1
3
2
4
5a
5b
Test measurement
Results 93
94 Results
1 Method list
– Tap the method you want to evaluate.
The journal view appears.
2 Journal view
The journal view allows you to start different graphical evaluations from a measurement series. You can per form the following functions:
– To start filter function, tap [ ].
The filter menu appears.
– To start chart view, tap [Chart].
The chart view of the series of measurement appears (4).
– To start graphic view, tap a measurement result.
The graphic view appears (5).
●
●
●
●
●
●
3 Filter menu
The filter function allows you to evaluate the measurement series according to various criteria. You can select the following criteria:
All (No filter)
Today
This week
Date range (Begin - End)
Last 10 measurements / tests*
Last 20 measurements / tests
– Tap [X] to close filter menu.
* Factory setting
4 Chart view
This view allows you to display the results of a series of measurements depending on the filter settings. If you have defined the control limits in the method, they are diagramed in the results.
The marked measuring point is displayed with date, time, and the measurement result. You can perform fol lowing functions:
– To jump forward to the next measurement result, tap [ -> ].
– To jump backwards to the previous measurement result, tap [ <- ]. Alternatively, tap directly on the desired measurement point.
– To recall the full measurement curve of the corresponding measurement, tap [ ].
5a Graphics view
With this function you can display a graphical view of the detailed results of a single measurement. If you have defined the control limits in the method, passed, warned or failed status is shown, see Control limits
You can perform the following functions:
Printing result
– To print the result, tap [ ].
Exporting result
– To export the result, tap [Export].
See Exporting Results (page 97).
Deleting result
– To delete this measurement result, tap [Delete] (depending on user rights).
More data
– To display more measurement data, tap [More data]
5b Displaying results of test measurements
For test measurements see Testing a Method (page 87).
This view allows you to display the results of the determined switch-off criteria. Each criterion is marked as a measuring point and displayed with its result. You can perform following functions:
– To jump forward to the next measurement result, tap [ -> ].
– To jump backwards to the previous measurement result, tap [ <- ]. Alternatively, tap directly on the desired measurement point.
10.2 Information on Printouts
The illustrations in this chapter show examples of a standard measurement printout (factory setting) and a short measurement printout. The level of detail on the printouts depends on the selected settings in the menu.
Results 95
96 Results
Structure of the standard printout type
-MOISTURE DETERMINATION-
METTLER TOLEDO
Halogen MoistureAnalyzer
Type HS153
SNR(Drying Unit)
B206684647
SNR(Terminal)
B206684647
SW(Drying Unit) 1.10
SW(Terminal) 1.20
Method name NEG
Drying prog Standard
Drying temp 105 °C
Switch Off 3(1mg/50s)
Display mode %MC
Start weight OFF
Control limits OFF
Start mode Automatic
User name Administrator
Start weight 0.487 g
Total time 0:22 min
Dry Weight 0.470 g
Moisture content
0.017 g
End result 3.29 %MC
Note
Signature
........................
14.10.2011 12:01
---------- END ---------
Structure of the short printout type
-MOISTURE DETERMINATION-
METTLER TOLEDO
Halogen MoistureAnalyzer
Type HS153
SNR(Drying Unit)
B206684647
SNR(Terminal)
B206684647
SWK(Drying Unit) 1.10
SWT(Terminal) 1.20
Method name NEG
Drying prog Standard
Drying temp 105 °C
Switch Off 3(1mg/50s)
User name Administrator
Start weight 0.487 g
Total time 0:22 min
End result 1.79 %MC
Note
14.10.2012 12:01
---------- END ---------
Special events
The sample chamber was opened and closed during drying process. When the sample chamber is open, drying is interrupted and then continued when the chamber is closed.
01:00 min 2.26 %MC
01:20 min opened
01:28 min closed
02:00 min 3.49 %MC
The drying process has been aborted by tapping
[Stop drying] and the measurement result at the time of the abort is not recorded as it could be wrong.
01:00 min 2.26 %MC
02:00 min 3.49 %MC
ABORTED
14.10.2011 12:01
Printing the test measurement
During the test measurement a record is printed which explains exactly when and with what measurement result each switch-off criterion was reached.
Switch-off crit. 3
Time 01:21 min
Dry weight 3.385 g
Moisture content
0.53 %MC
10.3 Exporting Results
Results can be exported to an external storage device e.g. memory stick as well via network to a server. Data in
CSV format can be imported into e.g. MS Excel for further evaluations.
Note
Results cannot be imported in a Moisture Analyzer.
Sample procedure
Result is activated.
An external storage device is connected e.g. memory stick.
1 To start, tap [Export]
Export results appears.
2 Tap Export target > Peripheral
3 Tap Location > Browse and select.
Location appears.
4 Select location for file and confirm with [OK].
5 Enter new file name, if needed.
6 To start export, tap [Export].
10.3.1 Single Result Export
You can define the following parameters:
Parameter
File name
File type
Language
Explanation
Defines the name of the new data file.
Defines the type of the data file.
Defines the language for export files.
Export target
Defines the destination of data transfer.
Values any
CSV* | PDF
English | Deutsch |
Italiano | Français |
Español | Português |
Polski | Magyar |
Český | P усский |
日本語 | 中文 |
한국어/조선말
Peripheral |
Network (FTP)
Results 97
Peripheral
Parameter
Location
* Factory setting
Explanation
Finds the location on the storage device.
Values
Browse and select
Network (FTP)
For data transfer over a network (e.g. Ethernet, WLAN) the File Transfer Protocol FTP is used. The receiving server is defined by entry of the appropriate IP address. If necessary, contact the network administrator of your
IT department or your IT support.
Parameter
IP address
Port
Password
User name
* Factory setting
Explanation
Defines the IP address of the receiving server.
Defines the Port for communication with the server.
Note
Usually the default value is used.
Entry for the password needed for server login.
Entry for the user name needed for server login.
Values any
21* | any
any any
10.3.2 Multiple Result Export
●
Summary export
• The summary export contains method parameters and the end results per measurement. The intermediate values are not exported.
• If the method has step drying, the summary export also includes the results per step.
• If the test measurement was executed, then the summary export also includes the results for each switchoff criteria reached during the test measurement.
●
Multiple export
• The multiple export contains method parameters, method data, intermediate values and end results per measurement.
• Each measurement is exported as a single file.
You can define the following parameters:
Parameter Explanation
File name prefix Defines the name of the new data file. Date and time are auto matically added by the system.
File type
Language
Export content
Defines the type of the data file.
Defines the language for export files.
Export selection Custom selection of multiple results for the export from selected measurements. The selection can be made via the filter function.
Defines the content of the multiple results export.
Summary export (one file, no intermediate values): Results as summary report in one file.
Multiple export (one file per measurement): Results with inter mediate measurement values as separate files with the same lay out as for the single result export.
Values any
CSV* | PDF
English | Deutsch |
Italiano | Français |
Español | Português |
Polski | Magyar |
Český | P усский |
日本語 | 中文 |
한국어/조선말
Selection:
|
Summary export |
Multiple export
98 Results
Export target
Defines the destination of data transfer. Peripheral |
Network (FTP)
Peripheral
Parameter
Location
* Factory setting
Explanation
Finds the location on the storage device.
Values
Browse and select
Network (FTP)
For data transfer over a network (e.g. Ethernet, WLAN) the File Transfer Protocol FTP is used. The receiving server is defined by entry of the appropriate IP address. If necessary, contact the network administrator of your
IT department or your IT support.
Parameter
IP address
Port
Password
User name
* Factory setting
Explanation
Defines the IP address of the receiving server.
Defines the Port for communication with the server.
Note
Usually the default value is used.
Entry for the password needed for server login.
Entry for the user name needed for server login.
Values any
21* | any
any any
10.4 Information on Exports
The illustrations in this chapter show examples for the level of details of a PDF single result export and a PDF summary result export.
METTLER TOLEDO
Method
Batch (ID1)
Sample (ID2)
Date & Time
Measured Values & Drying Curve
End result
%MC
100
Moisture Determination
Standard
17.Feb 2012 / 12:46
ID3
ID4
User-ID
100.00%MC
Duration
Administrator
03:59 min
50
0
0 01:00
Comment:
Start weight
Dry weight
Moisture content
Method parameters & Instrument Data
Main parameter
Drying program
Drying Temp
Switch off criterion
Start weight Tol
Result and value handling
Instrument Data
Type
SNR (Drying unit)
SW (Drying unit)
Last Weight Adjustment
Adjustment Time
02:00
0.361 g
0.000 g
100.00%MC
03:00
Inclinometer
Workflow handling
Resolution
Start mode
Standard
230 °C
1(1mg/10s)
OFF
HX204
0123456789
1.2.1.27409
Instrument-ID
SNR (Terminal)
SW (Terminal)
Last Temperature Adjustment
Adjustment Time min levelled
Standard
Automatic
9876543210
1.3.1.28465
METTLER TOLEDO
Method
Measured Values & Drying Curve
End Results
%MC
100
50
0
1
Measured data
Date
Time
Batch (ID1)
Sample (ID2)
ID3
ID4
End result measured %MC
Status
Duration min.
Start weight g
Inclonometer
Username
Measured data
Date
Time
Batch (ID1)
Sample (ID2)
ID3
ID4
End result measured %MC
Status
Duration min.
Start weight g
Inclonometer
Username
2
Moisture Determination
Standard
Summary report
17.Feb 2012 / 12:46 - 8.Apr 2013 / 09:52
3
1
8.Apr 2013
09:52
4
2
30.Jan 2013
10:13
5
3
9.Jan 2013
11:12
6
4
3.Jul 2012
16:00
5
17.Feb 2012
14:49
TEST
0.11
00:46 min
11.110
levelled
Administrator
6
17.Feb 2012
12:46
12.06
11:10 min
12.484
levelled
Administrator
12.32
10:44 min
12.513
levelled
Administrator
0.15
00:42 min
5.886
levelled
Administrator
0.16
01:00 min
1.225
levelled
Administrator
100.00
03:59 min
0.361
Comment
Date / Signature
Page 1/1
Review Date / Signature
Version 1.00 2013_03
Comment
Date / Signature
Page 1/2 print 12.Aug 2013 / 15:56
Review Date / Signature
Version 1.00 2013_03
Results 99
11 Maintenance
Risk of electric shock
– The instrument must be disconnected from the power supply, before cleaning or other maintenance work to be performed.
– Use only the power cord from METTLER TOLEDO, if it needs replacing.
●
●
Note
The thermal overload protection can not be reset by the user.
The halogen lamp can not be replaced by the user.
In such cases, contact your METTLER TOLEDO representative.
11.1 Cleaning
Danger of burns
The interior parts of the heating module as well as the parts in the sample chamber could be very hot.
– Wait until the heating module has cooled down completely.
To obtain precise measurement results, we recommend you to clean the temperature sensor and the protective glass of the halogen lamp regularly. Please note the following directions for cleaning your instrument.
●
●
●
General
Your Moisture Analyzer is made from high quality, resistant materials and can therefore be cleaned with a com mercially available, mild cleaning agent e.g. isopropanol.
Attention
●
●
Use a lint-free cloth for cleaning.
Ensure that no liquids enters the interior of the instrument.
Heating Module
Clean the exterior of the heating module with a mild cleaning agent although the housing is extremely rugged and resistant to solvents.
Terminal
On no account use cleaning agents, which contain solvents or abrasive ingredients, as this can result in damage to the terminal overlay.
Never open the housing of the instrument – it contains no components, which can be cleaned, repaired or replaced by the user.
Note
After the temperature sensor or the protective glass have been cleaned, we recommend adjusting the heating
module using the temperature adjustment kit, see Temperature Adjustment (page 62).
100 Results
11.1.1 Sample Chamber
Sample chamber is open.
1 Remove the sample pan handler (1), the sample pan holder (2) and the draft shield (3) for clean ing.
2 Carefully remove any deposits from the black tem perature sensor (4).
11.1.2 Heating Module
3
2
4
1
1 2 3 4
1 Reflector ring
2 Protective glass
3 Reflector with inspection window glass
4 Halogen lamp
Maintenance 101
To clean the protective glass, the reflector as well as the reflector ring, you should first open the heating mod ule.
Attention
Avoid touching the round halogen lamp. If you have to remove any splashes, deposits, or spots of grease from the halogen lamp, it is advisable to use a weak organic solvent such as, for example ethanol. Ensure that the lamp is cool. Do not remove the halogen lamp!
Opening heating module for cleaning
Sample chamber is open.
1 Inside, there is a locking device on each side. Push both outwards
(together) for unlocking.
Note
Do not hold the module while unlocking it.
The upper part has been unlocked on both sides.
2 Open the heating module.
Removing reflector ring for cleaning
Note
For cleaning the protective glass, removing the reflector ring is not mandatory.
Heating module is open.
1 On both sides and at the same time, pull the two lugs outwards.
2 Unhook the ring and remove it from the bracket.
Removing reflector with inspection window glass for cleaning
Reflector ring is removed.
1 To unlock, pull the spring clip forwards.
2 Pull out the reflector upwards off the bracket.
102 Maintenance
Removing protective glass for cleaning
Reflector is removed.
– Pull out the protection glass upwards off the bracket.
Reassembling after cleaning
Reassemble all parts in the opposite order.
All parts are cleaned.
1 Insert the protective glass.
2 Insert the reflector with inspection window glass (until it clicks).
Note
The lamp must be located in front of the reflector. Do not touch the lamp with your fingers.
3 Insert the reflector ring.
Attention
Observe the correct position! Assure that the ring is properly fitted.
4 Close the heating module (until it clicks).
11.1.3 Fan Grill
The air inlet of the fan is located at the rear of the instrument and its exterior should be cleaned from time to time to free it from any dust deposits.
11.2 Dust Filter
If you use the Moisture Analyzer in a dusty environment with an dust filter, check the filter at regular intervals. Replacement Filters see
Accessories and Spare Parts (page 115).
– Replace the filter, if needed.
Maintenance 103
11.3 Replacing Power Line Fuse
Safety risk or damage of the instrument
Do not use a fuse of a different type or rated value, or short out (bridge) the fuse, because this can put your safety at risk and damage the instrument!
If the display of your terminal remains dark after switching on, in all probability the power line fuse of the drying unit is blown.
The power line fuse is located on the back of the drying unit. To change the fuse, proceed as follows:
1 Pull out the power cord.
2 Slide out the fuse holder (1) with a suitable tool such as a screw driver.
3 Remove the fuse (3) and check its condition.
4 If the fuse is blown, replace the fuse with one of the same type and the same rated value (5 x 20 mm, T6.3H 250 V).
Note:
A spare fuse is located in the holder (2).
1 2 3
Fuse see General Technical Data (page 109)
11.4 Disposal
In conformance with the European Directive 2002/96/EC on Waste
Electrical and Electronic Equipment (WEEE) this device may not be dis posed of in domestic waste. This also applies to countries outside the
EU, per their specific requirements.
Please dispose of this product in accordance with local regulations at the collecting point specified for electrical and electronic equipment. If you have any questions, please contact the responsible authority or the distributor from which you purchased this device. Should this device be passed on to other parties (for private or professional use), the content of this regulation must also be related.
Thank you for your contribution to environmental protection.
104 Maintenance
12 Troubleshooting
Errors can occur during operation of your instrument. This section describes how you can rectify these errors.
12.1 Error Messages
Most error messages appear in plain text directly in the respective application, and usually accompanied by a text describing how to correct the error. Error messages of this type are self-explanatory and therefore are not mentioned below. The following error messages can appear instead of the weighing result.
Error Message
Weight display
Cause Rectification
Overload – The weight on the pan exceeds the weighing capacity of the balance.
– Reduce the weight of the sample.
Underload – Sample pan holder is missing.
– Insert sample pan holder.
If needed, reboot the system by dis connecting and connecting to the mains.
– Remove the weight.
0.0000
Weight display flashes / Out of zero
range – When the instrument was switched on or upon zeroing, one or more limits were exceeded. The usual reason for this message to appear is when there is a weight on the weighing pan when the balance is switched on.
Adjustment
Unstable weight.
No stability during adjustment.
●
●
●
●
Ensure ambient conditions and an optimum location.
Take care that no part of the sample or the sample pan touches the draft shield or the sample pan handler.
Ensure that the sample pan holder is correctly installed as well as not defect.
Highly volatile substances in the sample also prevent a stable weigh ing result being detected since the sample is continuously losing weight.
Weight out of range.
Either no weight, or the wrong weight, has been placed on the sample pan dur ing adjustment. (This message is also displayed if you do not remove the weight when prompted to do so by the instrument.)
– Repeat the adjustment process and load the required adjustment weight.
Troubleshooting 105
12.2 Status Messages
Status messages are displayed by means of small icons in the status bar of the display. For further information
see Status Message Icons (page 17). The status icons indicate the following:
Cause
Hot surface
Indicates that the temperature inside the sample chamber is over approximately 50°C. The parts in the sample chamber and the sample itself can be very hot and there is a risk of burns.
The battery in your instrument must be replaced.
This battery ensures that the date and time are not lost when the instrument is disconnected from the power supply.
Your instrument is due for servicing.
Rectification
The status icon will disappear as soon the temper ature inside the sample chamber is less than approximately 50°C.
– Contact your METTLER TOLEDO representative as soon as possible.
A service technician will change the battery.
Quick Access icon is displayed continuously.
– Contact your METTLER TOLEDO representative as soon as possible to have a technician ser vice your instrument.
Quick setting of brightness and sound.
WLAN connection status.
WLAN connection status.
The instrument is connected to the network. If the device is connected to a network, the WiFi icon indicates the signal strength. The more bars dis played, the stronger the connection.
WLAN connection failed. The instrument is not connected to the network.
106 Troubleshooting
12.3 What to Do if…
Symptom
Display remains dark after switching on
Keys and buttons do not respond
●
●
Countermeasure
● Ensure that the terminal is properly connected to the drying unit.
● Ensure that the instrument is connected to the power supply and the power is actually supplied.
●
●
Check the power line fuse of the drying unit and replace if necessary, see
Replacing Power Line Fuse (page 104).
If the problem persists, contact a METTLER TOLEDO representative.
Reboot the system by disconnecting and connecting to the mains.
If the problem persists, contact a METTLER TOLEDO representative.
Printer that is connected does not print
●
●
●
Ensure that the printer is properly connected to the terminal (do not con nect the printer to the drying unit).
Ensure that the printer is on and enabled in the menu. See Peripherals
Check the printer settings. See Recommended Printer Settings (Strip
Incorrect characters are printed ● Change the bit/parity setting of the printer and the instrument to 8/NO.
● Check if both instruments have the same baud rate setting, see Peripher
●
Use the correct character sets, see Recommended Printer Settings (Strip
Measurement takes too long
●
●
●
●
●
●
You have selected an unsuitable switch-off criterion, see Settings of
Switch-off Criterion (SOC) (page 76).
An excessive amount of sample can also be the cause of slow drying, likewise samples which tend to form a skin which hinders vaporization.
Perform a measurement at higher temperature.
Enlarge the surface of the sample, e.g. by crushing or grinding.
Use absorbent glass fiber filters for liquids.
If the sample is very temperature sensitive and decomposes, reduce the temperature.
If measuring is unstable, check correct positioning of pan, sample han dler, sample, draft shield or sample holder.
Instrument does not heat after the start
● Halogen lamp is defective or the heating module is overheated and the thermal overload protection has switched off the heating. In this case, contact your METTLER TOLEDO representative.
Troubleshooting 107
Symptom
Measurement results are not repeatable
Countermeasure
●
Support on which the instrument is standing is not sufficiently stable. Use a stable support.
● Surroundings are very unstable (e.g. vibrations, air draft, humidity). Pro vide better environmental conditions.
●
Sample has more or less moisture between sampling and starting the drying process.
●
●
Sample is not evenly dispersed on the pan.
Start weight has not always the same value.
●
●
●
●
Samples are not homogeneous, i.e. they have different compositions.
The more inhomogeneous a sample, the larger the amount of sample needed to obtain a repeatable result.
Selected drying time is too short for the "Timed switch-off" criterion.
Extend the drying time or select a suitable switch-off criterion "Weight loss per unit of time".
Sample does not become completely dry (e.g. awing to skin formation).
Dry the sample with the aid of glass fiber discs.
Selected temperature is too high and the sample has oxidized or decom posed. Lower the drying temperature.
●
●
●
●
●
Sample boils and the splashed drops continuously change the weight.
Lower the drying temperature.
Granulation is not homogeneous or too large.
Insufficient heating power because the protective glass of the halogen
lamp is dirty. Clean the protective glass, see Cleaning (page 100).
Temperature sensor is contaminated or faulty. Clean the temperature
sensor, see Cleaning (page 100).
If the problem persists, contact a METTLER TOLEDO representative.
SmartCal test fails
●
●
●
●
●
●
●
Ensure that the test prerequisites are met.
Ensure that entries of room temperature and humidity are correct (check
RTHSensor)
Ensure that the sample pan is fully and uniformly covered with the test granulate.
Perform the temperature test, see Temperature test
Perform the weight test, see Tests
Repeat the test with new sample.
If the problem persists, contact a METTLER TOLEDO representative.
WLAN usage is not possible.
●
Ensure you have set the correct country setting, see Regional Settings
● If the problem persists, possibly there is no authorization in your country for WLAN usage with this instrument. For more information, contact a
METTLER TOLEDO representative.
108 Troubleshooting
13 Technical Data
13.1 General Technical Data
Drying Unit
Heating Module
Temperature range
Temperature step
Temperature programs
Balance
Maximum capacity
Readability
Minimum sample weight
Weighing technology
Adjustment
Halogen ring-shaped radiator
40–230 °C
1 °C standard, rapid, gentle
150 g
1 mg
0.1 g
Monobloc
External weight
Moisture Content
Readability 0.01%
Repeatability (sd) with 2 g sample 0.05%
Repeatability (sd) with 10 g sample 0.01%
Materials
Drying Unit
Housing
Inspection window grill
Protective glass
Halogen lamp
Reflector
Reflector bracket
Draft shield, interior bottom plate
Terminal
Top housing
Bottom housing
Plastic, PBT, Crastin SO653-GB20
Plastic, PEEK-HT G22 (UL94-V0)
Glass ceramics
Quartz glass
Stainless steel, X2CrNiMo17-2 (1.4404)
Plastic, PEEK-HT G22 (UL94-V0)
Stainless steel, X2CrNiMo17-2 (1.4404)
EN ZL-ZnAl4Cu1 (EN Zl-0410)
PA12 GB30
Protection and Standards
Overvoltage category
Degree of pollution
Standards for safety and EMC
Range of application
Environmental Conditions
Height above sea level
Ambient temperature range
Relative air humidity
Class II
2 see Declaration of Conformity (part of standard equipment) for use in dry interior rooms up to 4000 m
5 °C to 40 °C
10% to 80% at 31 °C, linearly decreasing to 50 % at 40 °C, noncondensing
Technical Data 109
Warm-up time At least 60 minutes after connecting the instrument to the power supply; when switched on from standby, the instrument is ready for operation immediately.
Power Supply
110 V AC Version
230 V AC Version
Voltage fluctuations
Power load
Power line fuse
Interfaces
Drying Unit
100 V–120 V, 50/60 Hz, 4 A
220 V–240 V, 50/60 Hz, 2 A
-15%+10% max. 450 W during drying process
5 x 20 mm, T6.3H 250 V
Terminal
●
●
1x System (Terminal – drying unit)
1x Connection for METTLER TOLEDO RHT sensor
●
●
●
●
●
●
1 x RS232C (9-pin socket)
2x USB Host (Type A socket), USB 1.1
Supported memory sticks up to 32 GB
1x USB Device (Type B socket), USB 1.1
1x Slot for memory cards SD/SDHC up to 32 GB (SDXC not supported)
Ethernet: TCP/IP, DHCP, static IP, 100 Mbit/s, RJ45
WLAN: TCP/IP, DHCP, static IP, IEEE 802.11b/g/n, open,
WEP, WPA-PSK, WPA2-PSK (tkip only)
Data
Export data format of results
●
●
CSV (Comma-separated values)
Hardware
Drying unit
Sample chamber opening/closing
Leveling
Sample pan
Thermal overload protection
Dimensions (w x h x d)
Weight, ready to measure
Terminal
Display
Reading angle
Dimensions (w x h x d)
Weight manual
2 leveling screws
Ø 90 mm
Bimetallic-element switch in heating module
199 x 139 x 428 mm
6.8 kg
WVGA color display, resistive touch-sensitive
Adjustable, 2 folding feet
200 x 63.5/79.5 x 134.5 mm
1.2 kg
110 Technical Data
13.1.1 Explanatory note to periodic inspections in accordance with EU Directive 2001/95/EC
This instrument is provided with a 3-pin plug. The earth conductor is led into the instrument and con nected to the bottom and the rear panel. The other accessible metal parts are not connected to the earth conductor. These parts are reinforced insulated and must not be connected to the earth conductor accord ing to current European standards.
The earth connection must be checked on the metallic rear panel.
Further information about conformance of this instrument can be found in the Declaration of Conformity which is coming with the product or can be downloaded from the internet.
uwww.mt.com/hxhs
Technical Data 111
13.2 Dimensions
(all dimensions in mm)
13.2.1 Drying Unit
21.2
346.5
405
428
247
17.4
112 Technical Data
13.2.2 Terminal
METTLER TOLEDO
63.5
79.5
200
13.3 Interfaces Specification
13.3.1 RS232C
Schematic
GND
5
9
RxD
TxD
DATA
IN
OUT
1
6
CTS
RTS
HAN D
SHA KE
IN
OUT
Item Specification
Interface type Voltage interface according to EIA
RS-232C/DIN66020 CCITT V24/V.28)
Max. cable length 15 m
Signal level Outputs:
+5 V … +15 V (RL = 3–7 kΩ)
–5 V … –15 V (RL = 3–7 kΩ)
Inputs:
+3 V … +25 V
–3 V … -25 V
Connector
Operating mode
Sub-D, 9-pole, female
Full duplex
Transmission mode Bit-serial, asynchronous
Transmission code ASCII
Baud rates
Bits/parity
Stop bits
Handshake see setting options see setting options see setting options
None, XON/XOFF, RTS/CTS (software selectable)
Technical Data 113
13.3.2 USB Host
Schematic
13.3.3 USB Device
Schematic
1 VBUS (+5 VDC)
2
3
D– (Data –)
D+ (Data +)
4 GND (Ground)
Shield Shield
Item
Standard
Speed
Power usage
Connector
Pin assignment
Specification
In conformity with USB Specification Revision
1.0/1.1
Full speed 12 Mbps (requires shielded cable)
Max. 500 mA
2
3
Type A
1
4
Shell
VBUS (+5 V DC)
D- (Data -)
D+ (Data +)
GND (Ground)
Shield
Item
Standard
Specification
In conformity with USB Specification Revision
1.1
Full speed 12 Mbps (requires shielded cable) Speed
Function CDC (Communication Device Class) serial port emulation
Power usage Suspended device: Max 10 mA
Connector Type B
114 Technical Data
14 Accessories and Spare Parts
Description
Power supplies
Country-specific 3-Pin power cable with grounding conductor.
Power cable AU
Power cable BR
Power cable CH
Power cable CN
Power cable DK
Power cable EU
Power cable GB
Power cable IL
Power cable IN
Power cable IT
Power cable JP
Power cable TH, PE
Power cable US
Power cable ZA
Cables for RS232C interface
RS9 – RS9 (m/f): connection cable for PC, length = 1 m
Part No.
00088751
30015268
00087920
30047293
00087452
00087925
00089405
00225297
11600569
00087457
11107881
11107880
00088668
00089728
11101051
Cables for USB interface
USB (A –B) connection cable for connection to PC, length = 1 m
Cables for terminal
Terminal cable, length = 0.68 m
Printers
RS-P25 printer with RS232C connection to instrument
Paper roll, set of 5 pcs
Paper roll, self-adhesive, set of 3 pcs
Ribbon cartridge, black, set of 2 pcs
12130716
30003971
11124300
00072456
11600388
00065975
Accessories and Spare Parts 115
Prin ter
1
1
0.506 g
5.876
1.098
6.554
g
7 g g
5 g
17.37
8.003
3 g
g
g
g
METTLER
TOLEDO
RS-P42 printer with RS232C connection to instrument
Paper roll, set of 5 pcs
Paper roll, self-adhesive, set of 3 pcs
Ribbon cartridge, black, set of 2 pcs
Sample Pans
Aluminum sample pan, HA-D90, set of 80 pcs
00229265
00072456
11600388
00065975
00013865
Professional aluminum sample pan, extra strong, set of
80 pcs
11113863
Stainless steel reusable sample pan 6 mm, DA-DR1, set of 3 pcs
00214462
Textile weighing pan HA-CAGE, 1 pcs 00214695
Down holder, prevents slipping of the sample during measure ment,1 pcs
00214758
Adjustment / Test Parts
Certified adjustment weight, 100 g (F1) 11119531
OIML / ASTM Weights (with calibration certificate) see www.mt.com/weights
116 Accessories and Spare Parts
Temperature adjustment set HA-ETCC, certified
RHT sensor for detecting of humidity and temperature
Anti-theft devices
SmartCal™, Moisture Analyzer Reference Substance cSmartCal™, certified, 12 tests cSmartCal™, certified, 24 tests
SmartCal™, 12 tests
SmartCal™, 24 tests
Steel cable
Miscellaneous
Glass fiber filter (for Liquids), set of 100 pcs
Dust filter, set of 50 pcs
Protective cover for Terminal
Transport case
00214464
30020838
30003957
30020836
30020851
30020850
30005793
30005791
30005792
30005790
11600361
Accessories and Spare Parts 117
Excellence Plus
Stand for terminal
Printer holder for mounting on the stand for terminal.
Spare Parts
Sample pan handler
Draft shield
Sample pan holder
Reflector without inspection glass
Inspection glass for reflector
Reflector ring
30018474
30066692
30020852
30007150
11148108
11148330
11148421
30006700
118 Accessories and Spare Parts
Protective glass
Leveling foot
11148416
11106323
Accessories and Spare Parts 119
15 Appendix
15.1 How to Obtain Best Results
In this Section you will find important information on how to obtain optimum results. You will discover which parameters influence the measurement process and how you can optimize the settings of your instrument to achieve the best measurement results.
15.1.1 Measurement Principle of Halogen Moisture Analyzer
Your instrument performs measurements based on the thermogravimetric principle, i.e. the moisture is deter mined from the weight loss of a sample dried by heating.
120 °C
In principle, your instrument thus comprises two instruments: An ana lytical balance and a heating module. In contrast to other thermogravi metric methods (drying oven, infrared, microwave), the Halogen Mois ture Analyzer operates with halogen heating technology. This ensures fast heating of the sample and thus guarantees rapid availability of the measurement results.
●
●
●
●
Irrespective of the measurement method, a correct preparation of the sample and the correct choice of the fol lowing measurement parameters improve the quality of the measurement result:
Sample size
Drying temperature
Switch-off mode
Drying time
Attention
Inappropriate setting of these parameters can cause the results to be incorrect or misleading. For this reason, check that the results for each type of sample are what might reasonably be expected.
You will find detailed information on the relationships between these parameters in the delivered application
brochure «Guide to Moisture Analysis» or see Accessories and Spare Parts (page 115).
In practice not only the quality of the measurement results, but also the speed of the measurement process is important. Thanks to its drying principle (heat generated by a halogen radiator), the Halogen Moisture Analyzer is very fast. You can increase the speed even further through optimum setting of the instrument, e.g. using the
Drying program Rapid.
The optimum drying temperature and the drying time are dependent on the nature and size of the sample and on the desired accuracy of the measurement results. These can be determined only by experiment. The Halogen
Moisture Analyzer supports you in this task: It offers result recording of test measurements in the menu Method
Definition.
15.1.2 Notes on Adjustment of Balance and Heating Module
The balance and the heating module in your drying unit can be adjusted using the appropriate accessories, see
adjustment). The user can define a test weight or the test temperature, together with permissible tolerances for this test. A test report can be printed out showing the test result has passed or failed.
A Moisture Analyzer is typically used in place of or in addition to the drying oven method. In an oven heat ener gy is transferred by the flow of air, which establishes an equilibrium between the sample temperature and the ambient temperature. This is not the case in a Moisture Analyzer. The actual sample temperature primarily depends on the specific absorption properties of the sample (dark samples absorb more heat), which can change during the measurement process. There can also be differences between the temperature at the surface of the sample and the temperature inside the sample. The heat output is therefore not dependent on the true sample temperature but instead is regulated by a temperature sensor underneath the halogen heating module.
120 Accessories and Spare Parts
●
●
For the reasons explained above, the sample temperature will be slightly different than the temperature shown on the instrument display. By regularly testing or adjusting the drying unit, you will ensure a consistent and reproducible heat output for the entire lifetime of your instrument.
Note:
METTLER TOLEDO offers an adjustment service – please contact your METTLER TOLEDO representative.
We recommend to adjust the instrument exclusively under operating conditions.
●
After the temperature sensor or the protective glass have been cleaned, we recommend adjusting the heat
cedure for testing or adjusting the drying unit (balance/heating module), see Test/Adjust (page 61).
15.1.3 Optimum Sample Preparation
Preparation of the sample is decisive for the speed of the measurement process and the quality of the measure ment results.
Note:
Basic rules for the preparation of your sample:
The amount of sample you select should be as small as possible and only as large as necessary.
Excessive amounts of sample require more time for drying and thus prolong the measurement process. If the amount of sample is too small, the measurement result may possibly not be representative of the true moisture content. The following always holds: The greater the inhomogeneity of the sample, the larger the amount of sample needed to obtain a repeatable result .
Distribute the sample evenly over the sample pan
You thus increase the surface area of the sample and facilitate heat absorption. The base of the pan should be evenly covered.
With liquid, fat-containing, melting and highly reflecting samples, you should use the sample with the glass
samples which form a skin on their surface when heated. The glass fiber filter ensures even and rapid heat dis tribution and prevents the formation of a skin on the sample surface.
15.1.4 Further Information on Moisture Determination
You will find further information on the moisture determination, the importance of the parameters and the prepa ration of the samples in the delivered application brochure «Guide to Moisture Analysis» dealing with moisture
determination, see Accessories and Spare Parts (page 115).
Useful tips and a variety of example methods (comparison between Halogen Moisture Analyzer results and the oven drying method) can be downloaded from: u www.mt.com/moisture u www.mt.com/moisture-methods u www.moisture-guide.com
If you require information on specific applications, your METTLER TOLEDO Customer Service will be pleased to help you.
Attention
Moisture determination applications must be optimized and validated by the user according to local regula tions. Application-specific data provided by METTLER TOLEDO is intended for guidance only.
15.2 Recommended Printer Settings (Strip printer)
English, German, French, Spanish, Italian, Polish, Czech, Hungarian
Printer
RS-P25
Model Char Set
IBM/DOS
Auto baudrate
Off
Balance feature
Disable
Appendix 121
Printer
RS-P42
Instrument / Printer
Model
RS-P25
RS-P42
Brazil Portuguese
Printer
Model
RS-P25
RS-P42
Instrument / Printer
RS-P25
RS-P42
Model
IBM/DOS
Baudrate
9600
1200
Char Set
IBM/DOS
—
Baudrate
9600
—
2)
2)
1)
1)
Printer settings not available.
2)
Required font for this language not available.
Bit / Parity
8/NO
8/NO
Bit / Parity
8/NO
—
2)
—
Auto baudrate
Off
—
Stop Bits
1
1
Stop Bits
1
—
2)
—
Handshake
Xon/Xoff
Xon/Xoff
Balance feature
Disable
—
Handshake
Xon/Xoff
—
2)
15.3 Installing USB Device Driver
For transmitting MT-SICS commands via USB Device interface, a driver needs to be installed on the connected
PC. You can find the USB driver installer for download on the METTLER-TOLEDO website: u www.mettler-toledo-support.com
Requirements
●
PC with Microsift Windows
®
Windows Vista, Windows 7)
operating system (Windows 32-Bit & 64-Bit: Windows 2000, Windows XP,
●
●
Internet connection and Web browser (e.g. MS Internet Explorer)
PC to instrument USB connection cable.
Installing USB Driver
Navigation: www.mettler-toledo-support.com > login > Customer Support > HS153/HX204 Moisture Ana
lyzers
122 Appendix
1 Click USB Driver.
2 Click USBDriverInstaller.exe.
3 Click [Run] to install (recommended) or [Save] to download.
4 Click [Run]
5 Click [Next] and follow the installer's instructions.
Installing Instrument
1 Switch off moisture analyzer
2 Connect the moisture analyzer to the preferred USB Port on the PC.
3 Switch the moisture analyzer on.
4 Follow the instructions of the wizard and install the software auto matically (recommended).
Note
The wizard appears again for each USB port, either on your PC or if another moisture analyzer is connected.
Attention
Do not click [Cancel] as for the connected USB port, it might not be possible anymore to perform the installa tion process.
15.4 Third Party License/Notice
This section contains Third Party Software Notices and/or Additional Terms and Conditions for licensed third party software components included within SOFTWARE PRODUCT.
This SOFTWARE PRODUCT is based in part on the work of:
Appendix 123
124 Appendix
●
●
●
●
●
Qwt project
For user's guide see http://qwt.sf.net
For LGPL license V2.1 see http://www.gnu.org/licenses/old-licenses/lgpl-2.1.html
KompexSQLite
For LGPL license V3 see http://www.gnu.org/licenses/lgpl.txt
Qt library 4.8
For LGPL license V2.1 see http://qt-project.org/doc/qt-4.7/lgpl.html
For GPL license V3 see http://qt-project.org/doc/qt-4.7/gpl.html
decNumber
For ICU license V3.68 see http://source.icu-project.org/repos/icu/icu/trunk/license.html
RapidXML
For MIT license see http://www.opensource.org/licenses/mit-license.php
Index
A
Access rights
Accessories
Account
Policies
User
Adding comments
Adjustment
Balance
Heating module
Notes
Printouts
Settings
Touch screen
Weight
Weight external
Anti-theft
Appendix
Asterisk
Automatic sample chamber
B
Back up
Basic elements
Battery
Brightness
C
Calculated values
Certified RHT sensor
Chart
Chart view
Cleaning
Color
Comments to measurement
Commissioning
Company information
Settings
Connecting the Instrument
Connectivity
Control limits
Copy
Method
Country
CSV
CSV format
D
Data
Data management
Date
Default settings
Define
Method
Shortcut
Delete
see Remove
Dimensions
Display language
Display mode
Disposal
Drying
Temperature
Unit dimensions
Drying program
Gentle
Rapid
Standard
Dust filter
E
Edit
Method
Shortcut
Entering
Numerical values
Text and numbers
Error messages
Ethernet
Event logs
Export
Export
Result
Settings and methods
Export management
F
I
Factor
Fan
Filter
Firmware update
First measurement
Free factor
Fuse
G
General method properties
General safety information
General settings
Gentle drying
Graphics panel
Graphics view
Groups
H
Heating module
History
Home screen
Host name
Host settings
Identifications
Identifications panel
Import
Index 125
126 Index
Settings and methods
Installation
Intended Use
Interface
Interim results
Introduction
J
Journal
K
Kensington slot
Keyboard text and numbers
Keyboard language
Keypad numerical values
Keys on the terminal
L
M
Maintenance
Cleaning
Dust filter
Heating module
Power line fuse
Measurement
First
Measurement principle
Memory Card
Memory stick
Method
Copy
Definition
Edit
Export and import
Name
New
Properties
Remove
Renaming
Test
MT-SICS
N
LabX Direct
Languages
Printout
Leveling
Limits
Lists
Location
Log file
Login
Networks
New method
Numbers
Numerical values
O
P
Q
QuickAccess
R
Parameter panel
Password
PCL printer
Peripheral settings
Power line fuse
Power supply
Print management
Printer
Printout
Settings
Intermediate results
Language
Short
Standard
Protective clothing
Ramp time
Rapid drying
Reading angle
Remove
Method
Replace
Shortcut
Dust filter
Power line fuse
Reset
Restore
Result
Export
Result and value handling
Results
RHT sensor
Installation
RS232C
S
Out of zero range
Overload
Safety Information
General
Intended use
Protective clothing
Signal words
Staff safety
Warning Symbols
Sample preparation
Scope of delivery
Screen settings
SD card
Selecting the location
Settings
Adjustment
Date
Export and import
Host
Peripheral
Regional
Screen
System
Temperature Test
Time
Weight adjustment
Weight test
Shortcuts
Define
Edit
Remove
Show results
Signal words
SmartCal
General
RHT sensor
Test
Test settings
SOC
SOC delay
Software update
Sound
Spare parts
Staff Safety
Stand for terminal
Standard drying
Standard equipment
Standby
Start measurement
Start weight
Starting mode
Startup user
Status icon
Status messages
Stop drying
Switch button
Switch ON/OFF
Switch-off criterion
System
System management
System settings
T
Tables
TCP/IP
Temperatur
Adjustment settings
Temperature
Switch-off criterion
Test
Test settings
Terminal
Terminal dimensions
Test
Balance
Heating device
Measurement
Method
Temperature
Time
Weight external
Text
Thermogravimetric
Time
Touch screen
Touch screen adjustment
Troubleshooting
U
Underload
Unpacking
Update
USB
USB Device
USB Driver
Installation
USB Host
USB Memory stick see memory stick
User
Account
Groups
Home screen
Interface
Management
Profile see User manage ment
Shortcuts
V
Value panel
W
Warning Symbols
Weighing-in aid
Weight
Adjustment external
Test external
Weight adjustment
Settings
Weight test
Settings
Wireless LAN interface
WLAN
Settings
Work screen
Workflow handling
Index 127
Mettler-Toledo AG, Laboratory & Weighing Technologies
CH-8606 Greifensee, Switzerland
Tel. +41 (0)44 944 22 11
Fax +41 (0)44 944 30 60 www.mt.com
Subject to technical changes.
© Mettler-Toledo AG 10/2013
30019588B en
www.mt.com/hxhs
For more information
*30019588*
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