User manual | iCAP 6000 Series - Pre

iCAP 6000 Series
Pre-Installation Manual
Version 4.2
Part number 8499 400 30001
2007 Thermo Fisher Scientific. All rights reserved.
Registration No. 441506
SOLAAR House
19 Mercers Row,
Cambridge CB5 8BZ,
United Kingdom.
Telephone +44 (0) 1223 347400,
Fax +44 (0) 1223 347402,
http://www.thermofisher.com
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Thermo Fisher Scientific
iCAP 6000 Series Pre-Installation Manual v4.2 ii
Contents
Contents ............................................................................................iii
Thermo Fisher Scientific
Chapter 1
Introduction....................................................................................1-1
Chapter 2
System Accessories.........................................................................2-2
Chapter 3
Transportation ...............................................................................3-1
Package Size .................................................................................3-1
Short Term Storage .......................................................................3-2
Transit Damage.............................................................................3-2
Warranty .......................................................................................3-2
Chapter 4
Working Area Requirements........................................................4-1
Introduction...................................................................................4-1
Location ........................................................................................4-1
Environmental Requirements........................................................4-2
Electrical .......................................................................................4-2
Spectrometer Size .........................................................................4-4
Gas Requirements .........................................................................4-5
Water Temperature Control ..........................................................4-5
Waste Storage ...............................................................................4-6
Spectrometer Fume Extraction .....................................................4-6
Sample Fume Extraction...............................................................4-8
Chapter 5
Communications Interface............................................................5-9
On the Spectrometer .....................................................................5-9
On the Data Station.......................................................................5-9
Chapter 6
Pre-Installation Checklist............................................................6-11
Chapter 7
Special Agreements........................................................................7-1
iCAP 6000 Series Pre-Installation Manual v4.2
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iv
iCAP 6000 Series Pre-Installation Manual v4.2
Thermo Fisher Corporation
Chapter 1
Introduction
This manual is designed to help ensure that your iCAP 6000 Series
ICP-OES Spectrometer will be installed efficiently and will be able
to meet your requirements quickly and completely.
It will minimise installation time if the services and facilities detailed
here are available before the equipment is delivered.
Properly installed and maintained, your system will provide you with
years of reliable service. Please inform your local Thermo Fisher
organisation what aspects of support are most important to you and a
tailored agreement can be provided to prolong the life of your
instrument.
This manual describes the environment and the resources required at
the installation site of the iCAP 6000 Series ICP-OES Spectrometer
and associated equipment. Safety requirements for the installation are
also detailed.
WARNING: The installation of all services must comply with the
appropriate rules and regulations required by the local authorities
responsible for those services in the workplace, at the installation
site. An installation engineer is not responsible for the fitting, or
compliance of the facilities, or services.
The choice of an operating site for the instrument will be influenced
by local considerations for example, ease of access and availability
of electrical power.
Logical planning of the installation can save both time and money.
The objective of this manual is to provide information that will
enable the best site to be chosen and to highlight the essential
requirements.
If further information or advice is required, contact your local
Thermo Fisher organisation. A list of Thermo Fisher organisations
and agents can be found on http://www.thermofisher.com.
Installation of the system will include some familiarisation training;
however comprehensive method development and software training
will require additional training that should be ordered separately.
Thermo Fisher Scientific
iCAP 6000 Series Pre-Installation Manual v4.2
1-1
System Accessories
Package Size
Chapter 2
System Accessories
Required:
Recirculating chiller unit (see specification)
Data Station (see specification)
Optional:
Cetac ASX-520 Autosampler (requires dedicated RS232 on Data
Station)
Cetac ASX-260 Autosampler (requires dedicated RS232 on Data
Station)
Cetac EXR-8 Autosampler (requires dedicated RS232 on Data
Station)
Cetac ASX 1400 Autosampler (Stirring)
Cetac U-6000AT+ Ultrasonic Nebuliser
Elemental Scientific, Inc. SC SC4 Autosampler
Elemental Scientific, Inc. SC4 Fast Autosampler
Argon Humidifier
SSEA – Solid sampling device (requires dedicated RS232 on
Data Station and iCAP 6000 accessory board)
Laser – Solid sampling device (requires dedicated RS232 on Data
Station and iCAP 6000 accessory board)
High Solids Sample Introduction kit
HF Acid Sample Introduction kit
Organics Sample Introduction Kit
Volatile Organics Sample Introduction kit
Please request site requirement guides for any purchased accessories
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Thermo Fisher Scientific
Chapter 3
Transportation
The spectrometer is supplied with all compatible accessories that
have been purchased to meet the customer's system requirements.
Items may be shipped in separate packages.
WARNING: All items should be transported to the installation site
on pallets, in their original packaging and the right way up. Under no
circumstances may any package be moved without its pallet unless
under the direct control of an authorised Thermo Fisher service
engineer.
Proposed routes from the customer receiving area to the installation
site must be checked for suitability. The largest pallet size should be
used to calculate clearances.
WARNING: The boxed Spectrometer should be moved using a
mechanical lift. Five people should be used if it has to be moved by
hand taking appropriate precautions. Care should be taken in
doorways, corridors or when lowering to avoid trapping fingers.
Package Size
The instrument will be supplied inside especially designed
packaging. The dimensions are:
Table 3–1. Packaged Dimensions and Weight
Width
Depth
Height
Weight
980 mm
900 mm
920 mm
95 Kg
(38.6 in)
(35.4 in)
(36.2 in)
(210 Ib)
Transportation to some destinations may necessitate additional
packaging, for example a packing crate. Dimensions and exact
specifications may vary.
Thermo Fisher Scientific
iCAP 6000 Series Pre-Installation Manual v 4.0
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Transportation
Short Term Storage
Short Term
Storage
To maintain the instrument in serviceable condition and to comply
with the conditions of warranty, ensure that storage of each item is
maintained within the stated parameters detailed for the Working
Area Requirements below. Make sure that the packages are stored
the correct way up.
Note: Do not open the Packages without the permission of the
Thermo Fisher engineer
When the packages are opened prior to installation, the contents will
be checked against the packing list(s).
Transit Damage
Before accepting delivery of any equipment, the packages should be
inspected for signs of obvious damage. The nature of the damage
should be noted on the delivery notice and signed by the carrier's
representative.
Within the time stated in the Thermo Fisher terms and conditions an
inspection should be made for concealed damage. The local Thermo
Fisher organisation should be advised of any damage in writing and,
on receipt of specific instructions, the customer should return the
equipment complete and in the original packing material.
Warranty
Note that the instrument is warranted against defects in material and
workmanship for a period of 12 months from installation, or 15
months from shipment, whichever comes first. This warranty does
not cover damage sustained as a result of improper storage by the
customer prior to installation, or resale to a third party.
Note: Warranty is not transferable to a third party without Thermo
Fisher approval.
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Thermo Fisher Scientific
Chapter 4
Working Area Requirements
The choice of site will be influenced by the dimensions and weights
of the spectrometer and accessories. Other factors are the
environment and the availability of electricity, water and gas
supplies, as well as the need for a suitable ventilation system to
dispose of the exhaust gases. All of these factors are covered in the
following sections.
Pre-installation visits can be made on request, but may be
chargeable.
Introduction
Prior to installation make sure that the proposed area is compatible
with the conditions specified. The laboratory must offer a dry, even
temperature and dust-free conditions, with no possibility of
condensation forming. Sample preparation activities and corrosive
materials should be located in a separate room to avoid problems due
to corrosive fumes.
A comprehensive ‘Risk Assessment’ should be carried out that is
specific to the handling of solvents, samples and sample preparation.
Particular consideration should be taken to avoid direct sunlight,
proximity to heat sources, draughts and vibration. Do not locate the
system where sudden changes in temperature can occur, for
example near a door or window, care should be taken with the
location of items such as air conditioning vents and heating vents.
Location
The instruments are designed for use on a normal laboratory bench.
Ideally the instrument should be placed on a moveable bench with
0.5 meters of access behind the instrument. The mounting surface
must be level and the instruments must not be placed on any type of
cushioning as this could block ventilation.
The mounting arrangements should be capable of supporting the
weight of the spectrometer and its accessories. Make sure that the
working surface is sufficiently rigid to prevent vibration as this may
affect the optical alignment of the spectrometer and accessories.
To avoid the possibility of liquid ingress into the top of the
spectrometer the location should ensure it is not possible to store
sample or other liquids directly above the instrumentation.
Organic or volatile solvents should not be stored, even for a short
time, near the instrument.
Thermo Fisher Scientific
iCAP 6000 Series Pre-Installation Manual v 4.2
4-1
Working Area Requirements
Do not position the equipment so that it is difficult to operate the
extraction, electrical supply, cooling water, purge gas and plasma gas
controls.
Environmental
Requirements
The atmospheric temperature requirement is 15 to 35°C (60 to 95°F),
the temperature should not change by more than 2°C per hour.
Atmospheric humidity should be 20 to 80% m/v for an ambient
temperature between 15 and 30°C and 20 to 60% m/v for an ambient
temperature between 30 and 35°C. Atmospheric conditions must be
non-condensing. The instrument room should be at a positive
pressure with respect to rooms with a corrosive atmosphere.
Warning: Argon is an asphyxiant; if the extraction is turned off
sufficient air must be supplied to prevent the concentration of Argon
reaching a harmful level.
Electrical
The spectrometer will require an electrical supply at 200 to 240 VAC
4 KVA 50/60 Hz. The spectrometer will be supplied with a 2.5m
mains cord.
For customers in the USA and Canada the mains cord supplied will
terminate in a NEMA L6-20P Twist&Lock plug. (Coding is black (X
– ac high), white (Y – ac low), green (G – earth/ground).
Figure 4–1. NEMA L6-20P plug for USA/Canada
For customers in the rest of the world the mains lead is shipped with
no terminating plug, but with wires ready for a suitable 20 A plug.
Coding is blue (neutral), brown (live), green/yellow (earth/ground).
Connection to the laboratory supply should be with an appropriately
rated plug conforming to local electrical guide lines and local
requirements. It must be possible to electrically isolate the
instrumentation.
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Additional standard mains sockets will be required for the Data
Station PC, and for an autosampler, chiller, printer or any other
additional accessory required.
Each electrical outlet must have an effective earth/ground
connection. This protection must not be negated by the use of an
extension cable without a protective earth conductor.
Thermo Fisher Corporation
iCAP 6000 Series
Working Area Requirements
Spectrometer
Size
Width
Depth
Height
Weight
832 mm
744 mm
589 mm
85.5 Kg
(32.7 in)
(29.3 in)
(23.2 in)
(188 lbs)
Table 4–2. Spectrometer Dimensions and Weight
831.2mm
510mm
Figure 4–2. iCAP 6000 Series Front View
Figure 4–3. iCAP 6000 Series Top View
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Gas
Requirements
The spectrometer will require argon at 6 bar (87psi) (minimum
quality of 99.998% pure with less than 10ppm water and less than
10ppm oxygen - used for operation and optical path purge). The
maximum flow requirement will be 25 l/min during installation
For purging the optical path in the spectrometer nitrogen at 5.5 bar
(80psi) (minimum quality of 99.995% pure with less than 10ppm
water and less than 10ppm oxygen) can be used, instead of argon.
The maximum flow requirement will be 15 l/min during installation.
For optimum performance, a quality of 99.998% pure nitrogen is
recommended.
If an additional gas accessory is required (optional), clean oil free air
is required at a pressure of 2.5 bar (35psi) and a flow of approx
100ml.min-1
The instrument will be supplied with gas tubing terminating in 6mm
outside diameter gas connections (contamination free, refrigeration
grade copper for the purge and plastic for the plasma gas).
Connection to the laboratory gas supply should be within 1 metre of
the instrument. A regulator should be close to the connection.
Care should be taken to ensure that laboratory gas lines do not
contaminate the gases used for the iCAP.
If liquid argon is not used it is recommended that banks of cylinders
be used with switch over valves so that the gas supplies can be used
continuously.
Warning: Nitrogen and argon gas may cause asphyxiation at high
concentrations, appropriate care should be taken.
PLEASE NOTE: GAS REQUIREMENTS ARE
NOT THE SAME AS FOR PREVIOUS
THERMO FISHER ICP SPECTROMETERS.
Water
Temperature
Control
A recirculating chiller should be used to remove waste heat from the
spectrometer. The water temperature should be set to 5°C below the
ambient temperature.
The water used in the chiller must be distilled water containing 5%
by volume of the correct inhibitor (included with maintenance kit
which can be order from your local Thermo Fisher organisation).
Temperature variation must be less than 0.2°C per hour
The flow requirement of the spectrometer is 5 l/min and a cooling
capacity in excess of 900 W.
Thermo Fisher Corporation
iCAP 6000 Series
Working Area Requirements
A suitable chiller (ThermoFlex 900) can be supplied from your local
Thermo Fisher organisation.
Requirements for ThermoFlex 900:
Power: 230 V, 50 Hz, 7 A; or 115 V, 60 Hz, 13 A
Dimensions: 69.6 x 36.1 x 62.7cm (27.4 x 14.2 x 24.7in)
The spectrometer will be supplied with plastic connecting tubing that
has a 12mm outside diameter.
Connection to the water chiller should be within 3 meters of the
instrument, or insulated tubing must be used.
Waste Storage
Spectrometer
Fume
Extraction
The analysis of a sample, by ICP-OES, usually involves production
of a fine mist from a liquid sample. Waste will be produced that
could be corrosive and toxic, or an organic solvent. An appropriate
container is required that is solvent proof, shatterproof and vented
away from the instrument. Ensure the waste container does not
constitute a spill or trip hazard. It may be necessary to neutralise
waste to prevent any toxin build up. Appropriate facilities should be
provided for the disposal of any waste which should be disposed of
following local procedures and regulations.
This instrumentation is designed for operation in clean air
conditions. The laboratory must be free of all contaminants that
could have a degrading effect on the instrument components.
Dust, acid and organic vapours must be excluded from the work area.
The warranty will be void if the equipment is operated in substandard
conditions.
WARNING: The spectrometer must never be operated without an
effective fume extraction system attached to the torch compartment
chimney.
Hot fumes, which may be corrosive and toxic, are discharged from
the instrument chimney during operation. To ensure a safe working
environment and safe removal of waste combustion products, an
effective extraction system must be installed, this should include
appropriate filtering of hazardous toxic fumes.
The extraction must be capable of exceeding the minimum required
velocity, measured in the centre of the extraction tube at the
spectrometer end, while disconnected from the instrument, as
shown in figure 4-3 below. The extraction tube has an inlet
diameter of 125 mm (5 in).
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An iCAP 6000 Duo instrument will require an
extraction of 10 m/s (33 ft/s; 22.4 mph).
An iCAP 6000 Radial instrument will require an
extraction of 5 m/s (16 ft/s; 11.2 mph).
The extraction flow must be adjustable to 50% of the maximum to
allow optimization during installation. This can be achieved with a
butterfly valve, or an adjustable gate as shown in figure 4-3 below.
The extraction system must not be affected by external weather
conditions, or other uses the system may be used for.
Measure flow rate at
instrument end of
extraction system
Figure 4–4. iCAP 6000 Extraction System
PLEASE NOTE: EXTRACTION
REQUIREMENTS ARE NOT THE SAME AS
FOR PREVIOUS THERMO FISHER ICP
SPECTROMETERS.
Thermo Fisher Corporation
iCAP 6000 Series
Working Area Requirements
Sample Fume
Extraction
4-8
Additional, separate, extraction should be considered if significant
numbers of volatile, or acidic, samples are left in the proximity of the
instrumentation, even those in an autosampler.
iCAP 6000 Series Pre-Installation Manual v3.1
Thermo Fisher Corporation
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Chapter 5
Communications Interface
On the
Spectrometer
On the Data
Station
An Ethernet connection is fitted for Data Station communication
An optional accessory control PCB maybe fitted for additional the
communication requirements for some accessories. The use of each
connection is specified in the user manuals for each accessory.
The Data Station requirements will normally be met by a PC meeting
the minimum specification:
Windows XP Professional (Service pack 2)
20Gb Hard drive
512 Mb RAM
Dedicated Ethernet card for spectrometer communication
Some accessories require a dedicated RS232 port
A separate Ethernet card will be required for networking
A printer port maybe required
A suitable PC is available from your local Thermo Fisher
organisation.
The installation engineer is not responsible for network and customer
specific set-up of the PC.
Thermo Fisher Corporation
iCAP 6000 Series
Communications Interface
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Thermo Fisher Corporation
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Chapter 6
Pre-Installation Checklist
This checklist is to be filled in by the customer to confirm that all relevant factors
concerned with the installation have been considered and dealt with.
On completion of the list, a copy should be forwarded to the local Thermo Fisher
organisation with a request for installation to be carried out. Failure to send the checklist
may result in delays with the instrument installation, any delays may incur extra charge.
Required
Completed
Location
Table dimensions for the spectrometer
Table dimension for the auto sampler (right side of the
machine)
Extraction
900 x 600 mm
600 x 550 mm
Tube diameter for extraction
125 mm
Extraction capability
10 m/s (Duo)
5 m/s (Radial)
Adjustable valve in the extraction tube
Yes
Electrical supply
Plug 200-240 VAC, 32A single phase 4000W, 50Hz
Yes
Standard mains plug 200-240 VAC for each accessory
Yes
Argon Gas
Regulator valve in the wall 0 -10 bars (0 – 100 PSI)
Yes
Gas union dimension at the exit of the regulator valve
6 mm (1/4 inch
adapter supplied
with instrument)
Maximum distance between the instrument and the regulator
2m
valve
Purity of argon (Gas or Liquid)
Pressure required at the input of spectrometer
Thermo Fisher Corporation
99,995% 02<10
ppm H20<10
ppm
6 bars (87 Psi)
iCAP 6000 Series P
Optic nitrogen purge (Optional)
Regulator valve in wall 0 – 10 bars (0 – 100 Psi)
Yes
Gas union dimension at the exit of the regulator valve
6 mm (1/4 inch
adapter supplied
with instrument)
Maximum distance between the instrument and the regulator
2m
valve
99,995% 02<10
Purity of nitrogen (Gas or Liquid)
ppm H20<10
ppm
Pressure required at the input of spectrometer
6 bar (87 Psi)
Waste
Waste container, a minimum of 5 l for liquids waste
Yes
Auto Sampler rinse and waste
Minimum 1l container for the rinse supply station and waste
2 needed
Chiller (if not bought with the instrument)
Maximum distance from the spectrometer
3m
Pipe supply O.D. dimension
12 mm
Cooling capability
900 W
Flow rate
5 l/min
Chiller inhibitor
Yes
PC and printer (if not bought with the machine)
512 Mb RAM, 40 Gb HDD, 2 Ethernet ports, 1 serial port,
USB ports, monitor, ink jet printer
Yes
Windows XP Professional (Service pack 2)
Yes
Caution: The instrument installation will not start before
Thermo Fisher receives this document back completed. In the
case of false information causing the installation to be stopped, a
travel cost may be charged.
I certify the exactness of the information supplied in this document.
Name:
Position:
Signature:
Company stamp:
Date:
Installation Manual v3.1
Thermo Fisher Corporation
Chapter 7
Special Agreements
This section should detail any special agreements, which have been
arranged with your local Thermo Fisher organisation.
Thermo Fisher Scientific
iCAP 6000 Series Pre-Installation Manual v 4.2
7-1

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