MR 3001, MR 3001 K, MR 3001 K8 MR 3002, MR 3002 S8

MR 3001, MR 3001 K, MR 3001 K8 MR 3002, MR 3002 S8
MR 3001, MR 3001 K, MR 3001 K8
MR 3002, MR 3002 S8
HG 3001, HG 3001 K
Betriebsanleitung
Instruction Manual
Mode d’Emploi
Instrucciones de
Empleo
2
DEUTSCH
D
ENGLISH
E
FRANCAISE
F
ESPAGNOL
ES
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Thank you for purchasing a Heidolph Instruments product. This item has been designed, manufactured
and inspected in compliance with DIN EN ISO 61010 for continuous operation and long life performance.
SUMMARY
SUMMARY.............................................................................................................................................14
STANDARD EQUIPMENT & ACCESSORIES........................................................................................15
GENERAL INFORMATION ....................................................................................................................16
SAFETY INFORMATION .......................................................................................................................16
SET-UP ..................................................................................................................................................17
1. Set-up...............................................................................................................................................17
2. Electric hook-up................................................................................................................................17
3. Connect EKT 3001 / EKT 3001 G temperature controlon the MR 3001 K / MR 3001 K8 / MR 3002 /
MR 3002 S8 / HG 3001 K .................................................................................................................17
4. Connect a contact thermometer on the MR 3001 K / MR 3001 K8 / MR 3002 / MR 3002 S8 /
HG 3001 K........................................................................................................................................18
5. Set-up with tank adapter...................................................................................................................19
OPERATION AND CONTROLS .............................................................................................................19
1. Turn item ON ....................................................................................................................................19
2. Set stirring speed..............................................................................................................................19
3. Heat medium in absence of a detached control ................................................................................19
4. Heat medium using the EKT temperature control or a contact-type thermometer
(MR 3001 K / MR 3001 K8 / MR 3002 / MR 3002 S8 / HG 3001 K only) ...........................................20
CLEANING & SERVICING .....................................................................................................................20
UNINSTALL, FORWARD & STORE.......................................................................................................21
DISPOSAL .............................................................................................................................................21
MALFUNCTION & REMEDY ..................................................................................................................21
SPECIFICATIONS .................................................................................................................................22
WARRANTY, LIABILITY & COPYRIGHT ...............................................................................................23
QUESTIONS / REPAIR WORK ..............................................................................................................23
CE-DECLARATION OF CONFORMITY .................................................................................................23
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STANDARD EQUIPMENT & ACCESSORIES
Standard Equipment
product
quantity
P/N
P/N
230 V / 50/60 Hz
115 V / 60 Hz
MR 3001 or
1
504-10000-00
504-10000-01
MR 3001 K or
1
504-10100-00
504-10100-01
MR 3001 K8 or
1
504-10108-00
-----
MR 3002 S or
1
504-20100-00
504-20100-01
MR 3002 S8 or
1
504-20108-00
-----
MR 3002 C or
1
504-20110-00
504-20110-01
MR 3002 G or
1
504-20120-00
504-20120-01
HG 3001 or
1
504-40000-00
504-40000-01
HG 3001 K
1
504-40100-00
504-40100-01
Instruction Manual
1
01-005-002-92
01-005-002-92
power cord
1
14-007-003-81
14-007-003-89
Accessories
Item
P/N
EKT 3001 temperature controller incl. pt 100 stainless steel
509-87000-00
EKT 3001 G temperature controller incl. pt 100 glass
509-87100-00
1 liter heating bath, for oil, 250º C max.
504-93000-00
1 liter heating bath, PTFE coated for water, 100º C max.
504-93100-00
2 liter heating bath, for oil, 250º C max.
504-92000-00
2 liter heating bath, PTFE coated for water, 100º C max.
504-92100-00
4 liter heating bath, for oil, 250º C max.
504-91000-00
4 liter heating bath, PTFE coated for water, 100º C max.
504-91100-00
concave block adaptor for 1 liter round-bottom flasks
504-94000-00
stand, 1.4305 (V2A) stainless steel
509-81000-00
stand, 1.4305 (V2A) stainless steel, (for 4 liter heating bath)
509-98000-00
Clamp for temperature sensor
509-67000-00
magnetic stir bars (3 ea), cylindrical, PTFE-coated
509-56000-00
Bath liquid RT up to 240°C
515-31000-00-1
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GENERAL INFORMATION
Unpack your item carefully.
Inspect for damage and report such damage or missing parts to your supplier right away.
Read your Instruction Manual carefully. Take time to save time while working with your item.
Make sure that every user has read and understood the Instruction Manual.
Please store the Instruction Manual in a place easily accessible to every user.
IF ALL ELSE FAILS, READ THESE INSTRUCTIONS !
A so-called EURO-plug (DIN 49441 CEE 7/VII 10/ 16 A 250 V) is standard on all of the items.
For the Continental US they feature a US-standard plug (NEMA Pub.No.WDI.1961 ASA C 73.1 .
1961 page 8 15A 125V).
When using the item in a country with deviating outlet / plug systems, we recommend to use
approved adapters or to have an electrician replace the standard plug with one suiting your
needs.
As shipped, the item features a protective ground wire. When replacing the original plug, make
sure to reconnect this protective ground wire in the new plug !
SAFETY INFORMATION
Please comply with all safety and accident-prevention regulations as in force for laboratory work !
Use extra care when working with flammable substances; refer to safety data sheets.
When connecting your item with your local power supply, please make sure your item is
designed for your local supply voltage; go by data plate on the item.
Turn your power switch OFF whenever the item is not used, or before disconnecting the
plug.
Repair work is restricted to technicians approved by Heidolph Instruments.
Use extra care when working in the vicinity of flammable and explosive substances. Motors are of non-sparking type, however, the item itself is not explosion proof
Please do not connect your magnetic stirrer without a protective ground outlet.
Caution ! Hazard of serious burns when running the hot plate over 50°C.
Avoid contact with hot plate, heating bath and fluid.
Caution ! When heating flammable substances, adjust hot plate nominal temperature to a
lower level than the substance’s flashpoint.
Your item requires a solid stand.
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SET-UP
1. Set-up
Please locate the item on a sturdy, horizontal surface. For reasons of safety, keep the area around the
stirrer module clear of other items.
2. Electric hook-up
4
2
1
2
4
1
4
2
3
3
MR 3001 / MR 3001 K
MR 3002 / MR 3002 S8
Electric hook-up MR 3001 / MR 3001 K / MR
3001 K8 / MR 3002 / MR 3002 S8
Do the following checks before connecting:
- power switches (1 + 2) OFF (“0”); when ON,
toggle switch lights GREEN;
- control knobs (3 + 4) in extreme left position
(CCW)
HG 3001 / HG 3001 K
Electric hook-up HG 3001 / HG 3001 K
Do the following checks before connecting:
- power switch (2) OFF (“0”); when ON, toggle
switch lights GREEN;
- control knob (4) in extreme left position (CCW)
6
6
rear panel, MR 3001 / HG 3001
rear panel, MR 3001 K / HG 3001 K
MR 3001 K8 / MR 3002 / MR 3002 S8
Connect item with mains by plugging the power cord in the plug connector (6) located in the item’s rear
panel and your outlet.
3. Connect EKT 3001 / EKT 3001 G temperature control with MR 3001 K / MR 3001 K8 /
MR 3002 / MR 3002 S8 / HG 3001 K
In addition to the hot plate temperature control, the EKT 3001 / EKT 3001 G is used to control substance
temperature.
7
Connect the EKT 3001 / EKT 3001 G with the socket (7) located
on the item’s rear panel.
For more details please refer to the EKT 3001 Instruction Manual.
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4. Connect a contact-type thermometer with the MR 3001 K / MR 3001 K8 / MR 3002 / MR 3002 S8 /
HG 3001 K
In addition to the hot plate temperature control, a contact-type thermometer is used to control substance
temperature.
For running the item with the contact-type thermometer, we recommend to use
a safety thermometer only.
DIN 12878 contact thermometer wiring
The contact-type thermometer needs to be fitted
with a 4-pin DIN 41524 plug. For wiring information refer to above diagram.
7
8
Contact thermometer without glass breakage
detector wiring
When using a contact-type thermometer not featuring a glass breakage detector, you need to
jumper pins 5 & 3.
Connect your contact-type thermometer with the socket (7)
located in the item’s rear panel. Any time you don’t use either
an EKT or contact-type thermometer, you need to close the
socket (7) with a dummy plug (8).
rear view MR 3001 K/HG 3001 K/
MR 3001 K8/MR 3002/MR 3002 S8
The following optional attachment accessories for the contact-type thermometer are available:
Thermometer- or temperature sensor holder
(P/N 509-67000-00).
stand (P/N 509-81000-00)
Set your contact-type thermometer for the medium temperature required..
Set-up includes stand and holder
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5. Set-up with tank adapter
If you are going to use a heating bath (refer to “Accessory“ section) make
sure bottom rim of your bath properly fits over the hot plate.
When using the item with a 4 liter bath accessory, you may attach the temperature sensor to a special stand (X) (P/N 509-98000-00) designed for the
4 liter heating bath.
X
Set-up features 4 liter heating bath, clamp for temperature sensor and special stand
OPERATION AND CONTROLS
1. Turn item ON
Place your container or heating bath with the magnetic stir bar and fluid on the active surface of your
magnetic stirrer. Magnetic stir bars are available from Heidolph Instruments as an optional accessory.
1
1
3
MR 3001 / MR 3001 K
3
MR 3002
Prior to turning the power switch (1) ON, rotate speed control (3) to its extreme left position (CCW).
When turning power switch to ON, stirrer is going to start running at its preset speed immediately.
2. Set stirring speed
set speed to meet your needs with the rotary speed control (3) on the front panel.
Note:
HG 3001 and HG 3001 K do not feature a stirrer drive mechanism.
3. Heating medium in the absence of a detached control
5
4
MR 3001 / MR 3001 K
2
5
MR 3002
4
2
5
2
4
HG 3001 / HG 3001 K
Prior to turning the power switch (2) to ON, rotate hot plate temperature control fully CCW. At this point
you can turn the heating circuit ON with the power switch (2).
Use rotary control (4) to adjust hot plate temperature between ambient and 300°C; make reference to
front panel temperature marks.
A yellow LED (5) confirms heating current ON.
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Note regarding temperature adjustment:
Due to the thermal coefficient of different vessels, the different solvent quantities and radiation losses of the solvent temperature will always be slightly below
the hot plate temperature.
We recommend to select a SET temperature with the control knob of approx.
1.5 to 4 times of the solvent temperature required.
This factor could turn out even higher for large volumes or high thermal conductivity solvents.
Important Note regarding heat-up time:
The higher the SET temperature, the faster your Heidolph Magnetic Stirrer will
heat up.
4. Heating medium using the EKT temperature control or a contact-type thermometer
(MR 3001 K / MR 3001 K8 / MR 3002 / MR 3002 S8 / HG 3001 K only)
Make reference to „set-up“, para. 4, and connect a contact-type thermometer as described.
For heating, make reference to „2a“ „heating in absence of a detached temperature control“ and set your
nominal temperature on the EKT or contact-type thermometer.
Important Note regarding heat-up time:
The higher the SET temperature, the faster your Heidolph Magnetic Stirrer will
heat up. However, if SET temperature is set too high, (either on the Magnetic
Stirrer or on the Heidolph temperature control EKT 3001) your solvent may heat
up too fast and the temperature will overshoot.
To avoid an overshoot temperature situation, please adjust the SET temperature very carefully.
CLEANING & SERVICING
Cleaning: wipe housing surfaces clean with a damp cloth (add some sort of mild liquid soap).
Note
To avoid damage to the surface finish, avoid using chlorine bleach, chlorinebased detergents, abrasive substances, ammonia, rags or cleaning agents
containing metal particles.
The item is maintenance-free. Repair work is limited to technicians authorized or appointed by Heidolph
Instruments. Please call your local Heidolph Instruments Dealer or a Heidolph Instruments Field Representative (also refer to page 23).
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UNINSTALL, FORWARD & STORE
Uninstall
Turn the item OFF and disconnect mains plug.
Forward & Store
1. We recommend to store the item and its components in its original box, or a similar container that
offers adequate protection against damage in transit. Tape the box securely.
2. Store the item in a dry place.
Caution
Do not jolt or shake the item during transport.
DISPOSAL
For disposal, please comply with your local or national regulations.
Split by metal, plastic, etc.
Packing material to be treated as described above (material split).
MALFUNCTION & REMEDY
1. Power switch dim:
check power supply and power cord
2. Won’t stir (magnetic stirrers only):
8
– no magnetic stir bar in container
– speed control knob in extreme left (CCW) position
rear view MR 3001 K / HG 3001 K / MR
3. Won’t heat:
3001 K8 / MR 3002 / MR 3002 S8
– jumper (8) not installed
– EKT 3001 or contact-type thermometer not connected
– EKT 3001 or contact-type thermometer broken (sensor broken)
– thermal circuit breaker in hot plate dropped
(allow hot plate to cool off)
In case of a malfunction and you cannot repair as described above, contact your authorized Heidolph
Instruments Dealer.
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SPECIFICATIONS
stirrer drive
speed range
speed control
temperature control
heating power
hot plate temperature
control hysteresis, hot plate
hot plate made from
MR 3001; MR 3001 K; MR 3001 K8
HG 3001; HG 3001 K
condenser motor, electronic speed
control, thermal circuit breaker
100 – 1250 rpm (MR 3001...)
scale marks (MR 3001...)
capillary tube
600 watts
800 watts (MR 3001 K8)
0 – 300 °C
MR 3002; MR 3002 S8
± 15 K
Silumin (= aluminum alloy)
±5K
MR 3002 S (Silumin)
MR 3002 C (chromium steel)
MR 3002 G (vitrified ceramics)
2 x Pt100
230 volts / 50/60 Hz;
others available on request
0 – 250 °C
YES
temperature sensor, hot plate
supply voltage
capillary tube
230 volts / 50/60 Hz;
others available on request
temperature range, medium
0 – 250 °C
accepts detached temperature MR 3001 K, MR 3001 K8 and HG
control or contact-type ther3001 K: YES
mometer
accuracy of control (with EKT ± 1 K
3001; EKT 3001 G)
safety-circuit
thermal circuit breaker (bimetal) in hot
hot plate temperature
plate, drops at 370°C
power dissipation
625 watts
MR 3001 K8: 825 watts
weight
dimensions (w x d x h)
ambient specifications
chemical resistance
22
3.0 kg
240 mm x 155 mm x 120 mm
0 – 40 °C
at 80 % rel. humidity
housing: encapsulating,
polyamide coating
front panel: polyester
condenser motor, electronic speed control, thermal circuit breaker
0 – 1250 rpm
scale marks
electronic
600 watts
800 watts (MR 3002 S8)
0 – 300 °C
±1K
2 independent circuits (Triac and relay),
drops at 370 °C
630 watts
MR 3002 S8: 830 watts
3.0 kg
240 mm x 155 mm x 120 mm
0 – 40 °C
at 80 % rel. humidity
housing: encapsulating,
polyamide coated
front panel: polyester
E
WARRANTY, LIABILITY &
COPYRIGHT
Warranty
Heidolph Instruments warrants that the present
product shall be free from defects in material (except wear parts) and workmanship for 3 years
from the date shipped off the manufacturer’s
warehouse.
Transit damage is excluded from this warranty.
To obtain such warranty service, contact Heidolph
Instruments (phone: +49 – 9122 - 9920-68) or
your local Heidolph Instruments Dealer. If defects
in material or workmanship are found, your item
will be repaired or replaced at no charge.
Misuse, abuse, neglect or improper installation are
not covered by this warranty promise.
Alterations to the present warranty promise need
Heidolph Instruments’ consent in writing.
Exclusion Clause
Heidolph Instruments cannot be held liable for
damage from improper use or misuse. Remedy for
consequential damage is excluded.
Note
You will receive clearance for sending
your defective item to the following address:
Heidolph Instruments GmbH & Co. KG
Lab Equipment Sales
Walpersdorfer Str. 12
D-91126 Schwabach / Germany
Tel.: +49 – 9122 - 9920-68
Fax: +49 – 9122 - 9920-65
E-Mail: [email protected]
Safety Information
When shipping items for repair that may
have been contaminated by hazardous
substances, please:
advise exact substance
take adequate protective action not
to harm our parts receiving and service personnel
mark the pack IAW Hazardous Materials Act
-
Copyright
Copyright in pictures and wording of the present
Instruction Manual is held by Heidolph Instruments.
QUESTIONS / REPAIR WORK
If any aspect of installation, operation or maintenance remains unanswered in the present Manual, please contact us at the following address:
For equipment repairs, please call Heidolph Instruments (phone: +49 – 9122 - 9920-68) or your
local authorized Heidolph Instruments Dealer.
CE-DECLARATION OF
CONFORMITY
We herewith declare that the present product
complies with the following standards and harmonized documents:
EMC-guideline (89/336/EEC):
EN 61326: 1997 + A1:1998 + A2:2001+ A3 2003
EN 61000-3-2: 2000
EN 61000-3-3: 1995 + 1997 + A1:2001
EN 61326: 1997 + A1:1998 + A2: 2001+ A3 2003
EN 61000-4-3:2002 +A1:2002
EN 61000-4-5:1995 +A1:2001
EN 61000-4-6:1996 +A1:2001
EN 61000-4-11:1994 + A1:2001
Low-voltage guideline (73/23/EWG):
EN 61010-1 + EN 61010-2-010
+ EN 61010-2-051
23
01-005-002-92-0 11/2004
Heidolph Instruments GmbH & Co. KG
Technische Änderungen sind ohne vorherige Ankündigung vorbehalten.
Technical changes reserved. Publication not mandatory.
Sous réserve de modifications techniques sans
notification préalable.
Nos reservamos el derecho de introducir modificaciones técnicas sin previo aviso.
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