IKA®RV 10 control
3859400a_RV10c_032010:Layout­1­­15.04.10­­14:08­­Seite­1
38 594 00 a
IKA®RV 10 control
032010
Reg.-No. 4343-01
Betriebsanleitung
DE
5
Operating instructions
EN
32
Mode d’emploi
FR
59
Instrucciones de manejo
ES
86
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EG-KONFORMITÄTSERKLÄRUNG
DE
Wir erklären in alleiniger Verantwortung, dass dieses Produkt den Bestimmungen der Richtlinien 2006/95/EG, 98/37/EG und 2004/108/EG entspricht und
mit den folgenden Normen und norminativen Dokumenten übereinstimmt: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 und DIN
EN IEC 61326-1.
CE-DECLARATION OF CONFORMITY
EN
We declare under our sole responsibility that this product corresponds to the regulations 2006/95/EC, 98/37/EC and 2004/108/EC and conforms with the
standards or standardized documents DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 and DIN EN IEC 61326-1.
DÉCLARATION DE CONFORMITÉ CE
FR
Nous déclarons sous notre propre responsabilité que ce produit est conforme aux réglementations 2006/95/CE, 98/37/CE et 2004/108/CE et en conformité
avec les normes ou documents normalisés suivant DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 et DIN EN IEC 61326-1.
ES
DECLARACION DE CONFORMIDAD DE CE
Declaramos por nuestra responsabilidad propia que este producto corresponde a las directrices 2006/95/CE, 98/37/CE y 2004/108/CE y que cumple las
normas o documentos normativos siguientes: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 y DIN EN IEC 61326-1.
CE-CONFORMITEITSVERKLRING
NL
Wij verklaren in eigen verantwoordlijkheid, dat dit produkt voldoet ann de bepalingen van de richtlijnen 2006/95/EG, 98/37/EG and 2004/108/EG en met
de volgende normen of normatieve dokumenten overeenstemt: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 and DIN EN IEC
61326-1.
CE-DICHIARAZIONE DI CONFORMITÀ
IT
Dichiariamo, assumendone la piena responsabilità, che il prodotto è conforme alle seguenti direttive: 2006/95/CE, 98/37/CE e 2004/108/CE, in accordo
ai seguenti regolamenti e documenti: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 e DIN EN IEC 61326-1.
CE-KONFORMITETSFÖRKLARUNG
SV
Vi förklarar oss ensamt ansvariga för att denna produkt motsvarar bestämmelserna i riktlinjerna 2006/95/EG, 98/37/EG och 2004/108/EG och att den överensstämmer med följande normer eller normativa dokument: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 och DIN EN IEC
61326-1.
DA
CE-KONFORMITETSERKLÆRING
Vi erklærer, at dette produkt öpfylder bestemmelserne i direktiverne 2006/95/EF, 98/37/EF og 2004/108/EF og at det er overensstemmende med følgende
normer eller normgivende dokumenter: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 og DIN EN IEC 61326-1.
NO
CE-KONFORMITETSERKLÆRING
Vi erklærer på helt og holdent eget ansvar at dette produktet er i samsvar med bestemmelsene i forskriftene 2006/95/EF, 98/37/EF og 2004/108/EF, og at
de er i overensstemmelse med følgende normer eller normative dokumenter: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 og DIN EN
IEC 61326-1.
FI
CE-STANDARDINMUKAISUUSTODISTUS
Ilmoitamme täysin omalla vastuullamme, että tämä tuote vastaa EU-direktiivejä 2006/95/EY, 98/37/EY sekä 2004/108/EY ja on seuraavien normien tai ohjeasiakirjojen mukainen: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 sekä DIN EN IEC 61326-1.
∆ΗΛΩΣΗ ΑΝΤΑΠOΚΡΙΣΗΣ ΕΕ
EL
Με την παρ ύσα δήλωση ε αιών υνε µε απ κλειστική µας ευθύνη ½τι τ παρ½ν πρ½ϊ½ν ανταπ κρίνεται στ υς καν νισµ ύς των δηγιών
2006/95/EU, 98/37/EU και 2004/108/EU, και ½τι αντιστ ι εί στις ακλ υθες πρ διαγραφές και στα ακ½λ υθα ν µ καν νιστικά έγγραφα
DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 και DIN EN IEC 61326-1.
DECLARAÇÃO DE CONFORMIDADE DA CE
PT
Declaramos sob nossa responsabilidade exclusiva que este produto corresponde às determinações estabelecidas nas directivas 2006/95/CE, 98/37/CE e 2004/108/CE do Conselho e que está de acordo com as seguintes normas e documentos normativos: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1,
-2; EN 60204-1 e DIN EN IEC 61326-1.
DEKLARACJA PRODUCENTA CE
PL
Oświadczamy z pe nà odpowiedzialnościà, że produkt ten spe nia wymagania dyrektyw: 2006/95/WE, 98/37/WE i 2004/108/WE i jest zgodny z nast´pujàcymi normami i dokumentami normatywnymi: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 i DIN EN IEC 61326-1.
CS
PROHLÁŠENÍ O SHODĚ CE
Prohlašujeme se vší zodpovědností, že tento produkt odpovídá ustanovením směrnic 2006/95/ES, 98/37/ES a 2004/108/ES a je v souladu s následujícími
normami a normativními dokumenty: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 a DIN EN IEC 61326-1.
HU
CE MEGFELELŒSÉGI NYILATKOZAT
Felelősségünk teljes tudatában kijelentjük, hogy ez a termék megfelel a 2006/95/EK, 98/37/EK és 2004/108/EK irányelvek rendelkezéseinek, és összhangban van a következő szabványokkal és normatív dokumentumokkal: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 és DIN EN
IEC 61326-1.
IZJAVA O SKLADNOSTI IN CE-ZNAK
SL
Pod izkljuãno odgovornostjo izjavljamo, da ta izdelek ustreza doloãilom direktiv 2006/95/ES, 98/37/ES in 2004/108/ES ter naslednjim standardom in standardizacijskim dokumentom: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 in DIN EN IEC 61326-1.
VYHLÁSENIE O ZHODE S NORMAMI EÚ
SK
Vyhlasujeme na svoju zodpovednosť, Ïe tento v˘robok zodpovedá poÏiadavkám 2006/95/ES, 98/37/ES a 2004/108/ES a nasledujúcich noriem a normatívnych dokumentov: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 a DIN EN IEC 61326-1.
ET
CE-VASTAVUSDEKLARATSIOON
Kinnitame täielikult vastutades, et käesolev toode vastab direktiivide 2006/95/EL, 98/37/EL ja 2004/108/EL sätetele ning järgmistele standarditele ja
normdokumentidele: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 ja DIN EN IEC 61326-1.
CE ATBILSTĪBAS DEKLARĀCIJA
LV
Ar pilnu atbildību apliecinām, ka produkts atbilst direktīvu 2006/95/ES, 98/37/ES un 2004/108/ES noteikumiem un ir saskaņā ar šādām normām un normatīvajiem dokumentiem: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 un DIN EN IEC 61326-1.
EB ATITIKTIES DEKLARACIJA
LT
Prisiimdami atsakomybę pareiškiame, kad šis gaminys atitinka direktyvų 2006/95/ES, 98/37/ES ir 2004/108/ES ir šių normų bei normatyvinių dokumentų
reikalavimus: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 ir DIN EN IEC 61326-1.
DECLARAŢIE DE CONFORMITATE CE
RO
Declarăm pe propria răspundere că acest produs corespunde prevederilor directivelor 2006/95/CE, 98/37/CE şi 2004/108/CE precum şi următoarelor
norme şi documente normative: DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 şi DIN EN IEC 61326-1.
BG
ЕО дЕкларация за съОтвЕтствиЕ
Декларираме­на­собствена­отговорност,­че­този­продукт­съответства­на­разпоредбите­на­директиви­2006/95/EИО, 98/37/EИО и 2004/108/EИО
и­отговаря­на­следните­стандарти­и­нормативни­документи:­DIN EN IEC 61010-1, -2-051; DIN EN ISO 12100-1, -2; EN 60204-1 и DIN EN IEC
61326-1.
032010
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RV 10 control
Komplettaufbau mit Zubehör Schutzschild HB 10.1 und Schutzhaube HB 10.2
Device complete, incl. accessories HB 10.1 spray guard and HB 10.2 cover
L’appareil complet, incl. les accessoires HB 10.1 bouclier anti-projections et HB 10.2 capot de protection
Montaje completo con accesorios placa protectora HB 10.1 y cubierta protectora HB 10.2
Pos.
A
B
C
D
E
F
G
Bezeichung
HB 10.2 Schutzhaube
HB 10.1 Schutzschild
HB 10 Heizbad
RV 10 Antrieb control
Glassatz
Halter
Woulff’sche Flasche
Item Designation
A
HB 10.2 Cover
B
HB 10.1 Spray guard
C
HB 10 Heating bath
D
RV 10 Drive control
E
Glassware
F
Bracket
G
Woulff bottle
A
G
B
Pos
A
B
C
D
E
F
G
F
C
Désignation
HB 10.2 Capot de protection
HB 10.1 Bouclier anti-projections
HB 10 Bain chauffant
RV 10 Entraînement control
Verrerie
Support
Flacon de Woulfe
E
Pos.
A
B
C
D
E
F
G
D
Fig. 1
Designación
HB 10.2 Cubierta protectora
HB 10.1 Placa protectora
Baño calefactor HB 10
Accionamiento RV 10 control
Equipo de vidrio
Soporte
Botella de Woulfe
Funktionstasten / Function keys / Touches de fonction / Teclas de función RV 10 control
6
5
1
2
3
4
Fig. 2
Pos.
1
2
3
4
5
6
­4
Bezeichung
Taste “Power”
Taste Liftposition ““
Taste Liftposition ““
Dreh-/ Drückknopf
Taste “Set”
Taste “Esc”
Item
1
2
3
4
5
6
Designation
“Power” key
Lift position ““ key
Lift position ““ key
Rotating/ Pressing knob
“Set” key
“Esc” key
Pos.
1
2
3
4
5
6
Designation
Touche “Power”
Touche de position du
dispositif de levage ““
Touche de position du
dispositif de levage ““
Bouton rotatif/ Bouton-poussoir
Touche “Set”
Touche “Esc”
Pos.
1
2
3
4
5
6
Designación
Tecla “Power”
Tecla de la posición
del elevador ““
Tecla de la posición
del elevador ““
Mando giratorio/Botón pulsador
Tecla “Set”
Tecla “Esc”
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Contents
EN
Seite
CE-Declaration of conformity
Safety instructions
Correct use
Unpacking
Useful information
Setting up
Drive RV 10 control
Heating bath
Glassware
Hose system
3
32
33
33
34
35
Interfaces and outputs
Commissioning
Maintenance and cleaning
Accessories
Error codes
Technical data
Solvent table (excerpt)
Warranty
42
44
54
55
57
58
58
58
Safety instructions
­32
For your protection
• Read the operating instructions in full before starting up and
follow the safety instructions
• Keep the operating instructions in a place where they can be accessed by everyone.
• Ensure that only trained staff work with the appliance.
• Follow the safety instructions, guidelines, occupational health and
safety and accident prevention regulations. When working under
a vacuum in particular!
• Wear your personal protective equipment in accordance with the
hazard category of the medium to be processed. Otherwise there
is a risk of:
- splashing liquids,
- body parts, hair, clothing and jewellery getting caught,
- injury as a result of glass breakage.
• CAUTION! Inhalation of or contact with media such as poisonous
liquids, gases, spray mist, vapours, dusts or biological and microbiological materials can be hazardous to user.
• Set up the device in a spacious area on an even, stable, clean,
non-slip, dry and fireproof surface.
• Ensure that there is sufficient space above the device as the glass
assembly may exceed the height of the device.
• Prior to each use, always check the device, accessories and especially the glass parts for damage. Do not use damaged components.
• Ensure that the glass assembly is tension-free! Danger of cracking
as a result of:
- stress due to incorrect assembly,
- external mechanical hazards,
- local temperature peaks.
• Ensure that the stand does not start to move due to vibrations respectively unbelance.
• Beware of hazards due to:
- flammable materials,
- combustible media with a low boiling temperature,
- glass breakage.
• CAUTION! Only process and heat up media that has a flash point
higher than the adjusted safe temperature limit of the heating bath
that has been set.
The safe temperature limit of the heating bath must always be
set to at least 25 °C lower than the fire point of the media used.
• Do not operate the appliance in explosive atmospheres, with hazardous substances or under water.
• Only process media that will not react dangerously to the extra
energy produced through processing. This also applies to any
extra energy produced in other ways, e.g. through light irradiation.
• Electrostatic discharges could pose a direct danger.
• Tasks with the device must only be performed when operation
is monitored.
• Operation with excess pressure is not permitted (for cooling
water pressure see "Technical Data").
• Do not cover the ventilation slots of the device in order to ensure
adequate cooling of the drive.
• There may be electrostatic discharges between the medium and
the drive which could pose a direct danger.
• The appliance is not suitable for manual operation.
• Safe operation is only guaranteed with the accessories described
in the ”Accessories” chapter.
• Refer to the operating instructions for the HB 10 heating bath.
• Refer to the operating instructions for the accessories, e.g. vacuum pump.
• Position the positive pressure outlet of the vacuum pump under
a fume hood.
• Use the HB 10.2 cover or the HB 10.1 spray guard.
• Only use the device under an all side-closed exhaust, or a comparable protective device.
• Adapt the quantity and the type of distilland to the size of the distillation equipment. The cooler must work properly. Monitor
the coolant flow rate at the cooler outlet.
• The glass equipment must always be ventilated when working
under normal pressure (e.g. open outlet at cooler) in order to
prevent a pressure build-up.
• Please note that dangerous concentrations of gases, vapours or
particulate matter can escape through the outlet at the cooler. Take
appropriate action to avoid this risk, for example, downstream cold
traps, gas wash bottles or an effective extraction system.
• Evacuated glass vessels must not be heated on one side; the
evaporating flask must rotate during the heating phase.
• The glassware is designed for operation under a vacuum of up to 10
mbar. The equipment must be evacuated prior to heating (see chapter ”Commissioning”). The equipment must only be aired again
after cooling. When carrying out vacuum distillation, uncondensed
vapours must be condensed out or safely dissipated. If there is a
risk that the distillation residue could disintegrate in the presence
of oxygen, only inert gas must be admitted for stress relief.
• CAUTION! Avoid peroxide formation. Organic peroxides can accumulate in distillation and exhaust residues and explode while
decomposing!
Keep liquids that tend to form organic peroxides away from light,
in particular from UV rays and check them prior to distillation and exhaust for the presence of peroxides. Any existing peroxides must
be eliminated. Many organic compounds are prone to the formation
of peroxides e.g. dekalin, diethyl ether, dioxane, tetrahydrofuran,
as well as unsaturated hydrocarbons, such as tetralin, diene, cumene and aldehydes, ketones and solutions of these substances.
• DANGER OF BURNING! The heating bath, tempering medium,
evaporator piston and glass assembly can become hot during operation and remain so for a long time afterwards! Let the components cool off before continuing work with the device.
• ATTENTION! Avoid delayed boiling! Never heat the evaporating
flask in the heating bath without switching on the rotary drive!Sudden foaming or exhaust gases indicate that flask content is beginning to decompose. Switch off heating immediately. Use the lifting
mechanism to lift the evaporator piston out of the heating bath.
Evacuate the danger zone and warn those in the surrounding area.
• Automatic operation: Always check evaporation processes before starting automatic operation. Automatic operation must not be
used for unfamiliar evaporation processes.
The following automatic modes are available in addition to manual
mode:
- 100% distillation,
- Volume-/quantity-dependent distillation.
• When the device is switched off or the power supply disconnected, the internal safety lift removes the evaporator piston from the
heating bath. The maximum load (evaporator piston and contents)
is 1.5 kg for a permissible safety lift with no power.
• CAUTION! Never operate the device when the evaporator piston
is rotating and the lift is raised. Always lower the evaporator piston
into the heating bath first before starting the rotation drive. Otherwise hot tempering medium may be sprayed out!
• A vacuum may form inside the glassware in case of power outage.
The device will vent automatically when it is switched on again.
• Set the speed of the drive so no tempering medium is sprayed
out as a result of the evaporator piston rotating in the heating bath.
If necessary reduce the speed.
• Do not touch rotating parts during operation.
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• Imbalance may result in uncontrolled resonance behaviour of the
device or assembly. Glass apparatus may be damaged or destroyed
In the event of unbalance or unusual noises, switch off the appliance immediately or reduce the speed.
• The appliance does not start up again automatically following a cut
in the power supply.
• The device is only disconnected from the power supply network
if the device power switch is off or the plug is pulled out.
• The socket for the mains cord must be easily accessible.
For protection of the equipment
• The voltage stated on the type plate must correspond to the mains
voltage.
• Socket must be earthed (protective ground contact).
• Removable parts must be refitted to the appliance to prevent the
infiltration of foreign objects, liquids etc.
• Protect the appliance and accessories from bumps and impacts.
• The appliance may only be opened by experts.
Correct use
• Use
4Together with the accessories recommended by IKA, the device
is suitable for:
- quick and gentle distillation of liquids
- evaporation of solutions and suspensions
- crystallisation, synthesis or cleaning of fine chemicals
- drying of powder and granulate material
- recycling of solvents
The safety of the user cannot be guaranteed if the appliance is operated with accessories that are not supplied or recommended by
the manufacturer or if the appliance is operated improperly contrary
to the manufacturer’s specifications.
Mode of operation: Tabletop device
• Range of use
- Laboratories
- Pharmacies
- Schools
- Universities
Unpack
• Unpacking
- Please unpack the device carefully
- In the case of any damage a fact report must be set immediately (post, rail or forwarder)
032010
x x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
x
optional:
RV 10.4001 Vacuum valve for central vacuum system
RV 10.4002 Vacuum valve for laboratory vacuum system
RV 10.4003 Pump controller with vacuum valve for
individual operation on vacuum pump
or
x
x
x
x
or
RV 10 control V
RV 10 control VC
RV 10 control D
RV 10 control DC
or
Drive RV 10 control
Heaing bath HB 10
Vertical glassware RV 10.1
Vertical glassware RV 10.10 coated
Diagonal glassware RV 10.2
Diagonal glassware RV 10.20 beschichtet
Woulff bottle
Bracket
Cooler locking device, compl.
Vacuum hose (2x0,55 m)
Water discharge hose (1x1 m)
Operating instructions
Ring spanner wrench
Handhold
• Delivery scope
see table
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Useful information
Distillation is a thermal separating process for liquid compounds based
on substance-specific, pressure-dependent boiling points through evaporation and subsequent condensation.
The boiling point temperature decreases with decreasing external
pressure which means that work is usually done under reduced
pressure. In this way the heating bath can be maintained at a constant temperature (e.g. 60 °C). Using the vacuum, the boiling point
is set with a steam temperature of approx. 40 °C. The cooling water
for the condensation cooler should not be warmer than 20 °C (6040-20 rule).
A chemical resistant membrane pump with a vacuum controller
should be used to create the vacuum. The pump is protected from
solvent residue by the addition of a Woulff bottle and/or a vacuum
separator.
Working with a jet pump to create a vacuum can only be recommended to a limited extent as the solvents may contaminate the
environment when using these systems.
Speed, temperature, piston size and system pressure all affect the
evaporator air capacity.
The optimum capacity of the flow-through condenser is approx. 60%.
This corresponds to condensation on approx. 2/3 of the cooling coil.
With larger capacities there is the risk that the uncondensed solvent
vapour will be extracted.
In order to prevent this, the condenser loading safety monitoring system can be activated. Before activating the safety monitoring, first
carry out several distillations, noting the value given under menu
“Settings”, menu option “Drive”, item “Maximum heat rejection
rate”. Now calculate the heat rejection rate using the following formula:
Heat rejection rate threshold = maximum heat rejection rate * 1.3
Enter this value under menu “Settings”, menu option “Distillation”,
item “Heat rejection rate threshold”. The device will now stop the
measurement and issue an error message if the threshold for the
condenser is exceeded. If the configuration of the condenser equipment or the distillation process is modified, then it may be necessary
to re-evaluate the maximum condenser loading.
The factory setting for this value is 900 W.
The device is equipped with a piston-operated safety mechanism. A
vacuum may form in the glassware assembly if there is a power outage; this will be vented when the system is switched on again. If
the power cuts out, the evaporator piston is automatically lifted out
of the heating bath by an integrated gas spring.
CAUTION! The maximum load (evaporator piston and contents) is
1.5 kg for a permissible safety lift with no power for glass apparatus
with diagonal or vertical condenser.
When using other types of condensers such as dry ice or intensive
condensers as well as when using return distillation distributors with
slip-on condensers, it may be necessary to reduce the mass of the
media to compensate for the mass of this additional glassware.
Thus, prior to distillation, check whether the lift goes up without
power when laden with the glass and distillation material.
In addition to offering a full range of manual and semi-automatic
evaporation operating modes, the RV 10 control rotary evaporator
can also be used for fully automatic, quantity-controlled evaporation processes. Standard fittings for fully-automatic operation include a two-position vacuum controller, a cooling water
differential temperature measurement sensor, and a cooling
water flow rate meter. The device is designed for operation with
a cooling water supply system (e.g. laboratory thermostat), but
can also be run off a water supply line. Please refer to the Technical Data for information on cooling water pressure, temperature
constancy, and flow rate.
We recommend using the RV 10.5001 water regulator valve when
operating directly off a water supply line.
This valve allows the cooling water flow rate to be adjusted and automatically cuts off the cooling water supply on completion of the distillation process.
The RV 10.5002 water filter can be used to prevent particles of dirt
passing from the water supply line into the valve mechanism.
If pressure reduction is required, we recommend fitting the
RV 10.5003 pressure regulator valve in the pipe immediately
downstream of the pick-off point.
Automatic volume-dependent distillation: The apparatus must
be brought up to operating temperature. This is achieved by conducting a test distillation.
Please observe the specified values during automatic distillation (see
“Technical specifications”).
Vacuum equipment: The RV 10 control rotary evaporator is fitted as standard with a two-position vacuum controller and a pressure measuring chamber with bleed valve.
The correct vacuum valve must be selected from the following list and installed according to the type of vacuum source used at the
customer site.
Vacuum source
­34
Code
Valve
Central vacuum system
Large-scale vacuum source for
multiple consumers of different
types across a site;
generally a fixed-pipe installation.
RV 10.4001
Laboratory vacuum system
Laboratory-based RV vacuum pump
with multiple similar consumers,
e.g. 2 rotary evaporators/1 pump.
RV 10.4002
Single pump system
One rotary evaporator with one pump/
desktop operation.
Pump is deactivated when target pressure
reached and reactivated automatically.
RV 10.4003
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Setting up
 Remove the clamping device for the angle setting of the rotation
drive on the right side of the lift by rotating the knurled screw
counter clockwise (gently press and rotate the knurled screw (E)
at the same time to move it further in or out).
 Set the drive at an angle of approx. 30° (fig. 7).
Drive RV 10 control
ATTENTION! Loosen transportation lock (fig. 4a)!
Fig. 4a
 Hold the lift with your hand on the height position and remove the
thumb screw on the back of the appliance (A).
 Once the transportation lock has been removed, the lift moves
slowly to its upper end position. The distance is approx. 140 mm.
E
 Connect the device to the power supply (B) using the supplied
power cord (B).
Fig. 7
 Then secure the rotation drive from being accidentally turned by
tightening the knurled screw in a clockwise direction.
Adjustable base (fig. 4b)
Heating bath HB 10
CAUTION! Refer to the chapter entitled "Commissioning" in the heating bath instruction manual!
 Place the heating bath on the stand of the rotation drive and push
it into the left position (fig. 8).
F
Fig. 4b
Mounting the Woulff bottle (Fig. 5)
 Fit the hose connecting piece (C) on the left side of the lift.
 Mount the holder (D) onto the hose connecting piece (C).
Fig. 8
Note: Data is exchanged between the drive unit and the heating
bath by means of an infrared link (F). Please note that reliable communication is only guaranteed when the infrared beam has clear
line-of-sight to the detector.
C
Glassware
Fig. 5
D
 Release the locking device on the steam pipe by turning it 60°
counter clockwise (G), (fig. 9).
 Insert the bottle and attach the supplied hose connectors to the
bottle (fig. 6).
G
H
Fig. 6
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Fig. 9
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 Feed the steam pipe in until it stops.
 Then lock the locking device by turning it clockwise by 60°
(fig. 10).
First use - Fitting the seal RV 06.15/RV 06.13
 Insert vapour tube (1).
 Insert seal RV 06.15 (2).
 Slide the union nut (3b) over the flange on the condenser (3a).
 Also slide the annular spring (3c) over the flange on the condenser (3a).
 Position the condenser (3a) on top of the seal (2).
 Tighten the union nut (3b) by hand onto the threaded flange. Run the
device for 20 minutes at 120 rpm. Finally, retighten the union nut (3b) by
hand.
Note: Follow the mounting instructions for the glassware
3a
H
3b
2
1
Fig. 10
 Check the axial locking device on the steam pipe.
Push-off mechanism
The plastic screw nut (H) helps loosen tight-fitting piston ground-in
connections (Fig. 9).
 Hold the locking device and loosen the plastic screw nut (H).
 To do so, hold the tight-fitting evaporator piston and turn the plastic screw nut (H) until the evaporator piston neck.
Fig. 11c
Before using the device, hand-tighten the plastic screw nut (H)
against the left-hand stop. This will hold the steam pipe locking device (G) firmly in place.
3c
Fitting the condenser seal
 Place the RV 06.15 or RV 06.13 condenser seal in the condenser
receptacle and fit the glassware to the device according to the assembly instructions (Fig. 11 a,b, c and d).
Fig. 11d
Assembling the vertical glassware cooler locking device
Fig. 11a
 Assemble the condenser locking device according to the diagram
(fig. 12).
 Mount the plate (I) using the thumb screw (J).
 Put the support rod (L) on the plate (I) and attach it with the screw
nut (K).
 Attach the rubber protector (M).
 Fasten the Velcro band (N) to the support rod (L).
 Secure the vertical glassware with the Velcro band (N).
M N
L
I
K
Fig. 11b
J
­36
Fig. 12
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Mounting the glassware
4
Glassware
RV 10.2 diagonal
RV 10.20 diagonal, coated
5
Glassware
RV 10.1 vertical
RV 10.10 vertical, coated
7
8
13
6
7
12
8
12
13
6
15
16
15
4 5
9
9
3
3
2
2
10
10
NS2
9/32
NS2
9/32
11
16
100
0 ml
1
100
0 ml
Rotary head
11
Rotary head
1
Item
Designation
1
2
3
4
5
6
7
8
9
10
11
12
13
15
16
Receiving flask
Clamp NS 29 (stainless steel)
Steam pipe
Stopcock
Pipe tube
Condenser
Connection
Clamp NS 29 (plastic)
Seal RV 06.13/ RV 06.15
Evaporator piston 1000 ml
Ball joint clamp RV 05.10
Screw joint cap
Hose connection
Locking nut
Spring ring
Quantity
diagonal glassware
Quantity
vertical Glassware
1
1
1
1
1
1 Diagonal condenser
1 Introduction sleeve
1
1
1
1
4
4
1
1
1
1
1
1
1
1 Vertical condenser
1 Vacuum connection
1
1
1
1
4
4
1
1
Removing the condenser
Description of special condensers
 Use the ring spanner provided to loosen union nuts that are tightly
fitted.
 Loosen the union nut by turning anticlockwise.
• RV 10.3 Vertical-intensive condenser with manifold
This vertical-intensive condenser features a double jacket design
for particularly efficient condensation.
Also available with coating (RV 10.30)
• RV 10.4 Dry ice condenser
Dry ice condenser for distilling low-boiling solvents.
Cooling by dry ice, no cooling water required. Maximum condensation thanks to low temperatures.
Also available with coating (RV 10.40)
If a dry ice condenser is used, then the flow rate control system
must be switched of in menu “Distillation”, menu option “Flow
rate control”; see also “Commissioning” section.
• RV 10.5 Vertical-condenser with manifold and cut-off valve for
reflux distillation
Also available with coating (RV 10.50)
• RV 10.6 Vertical-intensive condenser with manifold and cutoff valve for reflux distillation
This vertical-intensive action condenser features a double jacket
design for particularly efficient reflux distillation.
Also available with coating (RV 10.60)
Fig.13
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Hose system
Schematic view of hose system (rear view)
RV 10.5001
Water regulator valve,
optional
Water
Vacuum
2x T1,6A 250V
Water
Fig. 14
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Vacuum
 Fit one of the optional RV 10.4001, RV 10.4002 or RV1 0.4003 vacuum valves, as appropriate for the type of vacuum system used, in
the bracket provided for this purpose and connect the vacuum hose
to the valve (Figure 15a, b, c).
Connection RV 10.4003
Connection RV 10.4001
Power
supply
pump
Fig. 15c
Solenoid rotates freely
Fig. 15a
Solenoid rotates freely
Direction of suction
corresponds to the
arrow marking.
Always check for correct orientation.
Connection RV 10.4002
Direction of suction
corresponds to the
arrow marking.
Always check for correct orientation.
Connection RV10 temperature sensor (dT)
Fig. 15d
dT
Fig. 15b
Note the direction of the arrow.
Solenoid rotates freely
Direction of suction
corresponds to the
arrow marking.
Always check for correct orientation.
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Water
 Connect the water inlet to the water supply (Figure 16a; Figure 16b
with optional RV 10.5001 water regulator valve). Please refer to the
technical specifications relating to the water supply.
The RV 10.5001 water regulator valve is not suitable for use on the
condenser unit because it would reduce the flow rate too greatly.
 Connect the water outlet hose (supplied) by pushing it onto the
nipple until the stop inside the connection socket is reached
(fig. 18).
Caution! Ensure that the condenser inlet and condenser outlet
are connected correctly.
Automatic distillation cannot be carried out if the water inlet and
outlet hoses are not fitted according to the instructions and illustrations acc. fig. 14, since this would cause the temperature readings for the inlet and outlet to be measured incorrectly.
Inlet
condenser
Water
inlet
Outlet
condenser
Fig. 16a
RV 10.5001
Water
inlet
Fig. 18
 Release the hose connection using the supplied tool.
Fig. 16b
 Connect the water hoses to the glass condenser (short hose (O)
= lower outlet, long hose (P) = upper inlet) and fix hoses in place
(fig. 17).
Note: For special condensers see “Description of special condensers”
section.
Fig. 19
P
O
Fig. 17
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Schematic view of connections (rear view)
 Insert the valve connector cable (RV 10.5001 or RV 10.4001/2 resp. RV 10.4003 Valve) resp. the network cable (RV 10.4003 pump control) ) into the
appropriate socket (fig. 20).
RV10.4003
Pump control
RV10.5001
RV10.4001/2
RV10.4003 Valve
dT
RS 232
Fig. 20
 Connect the pressure sensor to the Woulff bottle and the Woulff
bottle to the vacuum connector on the condenser using the vacuum hoses supplied. Please note that the vacuum must always
be connected to the highest connection point on the condenser
(fig. 21).
032010
Fig. 21
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Interfaces and outputs
HB 10
Data is exchanged between the heating bath and the drive unit by
means of an infrared link. These are located on the left display side
of the heating bath or on the right side of the drive unit. Do not place
any objects between the two operating units as otherwise the data
transfer may be interrupted (fig. 22)!
Serial interface RS 232 (V24)
Configuration
- The functions of the interface lines between the device and the
automation system are a selection from the signals specified in
the EIA standard RS232 C, as per DIN 66 020 Part 1.
- For the electrical characteristics of the interface and the allocation
of signal status, standard RS 232 C applies in accordance with DIN
66 259 part 1.
- Transmission procedure: asynchronous character transmission in
start-stop mode.
- Type of transmission: full duplex.
- Character format: character representation in accordance with data
format in DIN 66 022 for start-stop mode. 1 start bit; 7 character
bits; 1 parity bit (even); 1 stop bit.
- Transmission speed: 9600 bit/s.
- Data flow control: none
- Access procedure: data transfer from the device to the computer
takes place only at the computer’s request.
Fig. 22
RV 10 control
The device can be operated in “Remote” mode via an RS 232 or USB
interface using labworldsoft® laboratory software.
The RS 232 interface at the back of the device, see fig. 20, is fitted
with a 9-pole SUB-D jack and can be connected to a PC. The pins
have serial signals. The USB interface is located on the left-hand
side of the display on the drive unit and can be connected to a PC
using the USB cable supplied.
Note: Please note the system requirements as well as the operating
instructions and help section included with the software.
USB Interface
The Universal Serial Bus (USB) is a serial bus system used to connect the RV 10 control with the PC (Fig. 23). Devices that support
USB can be connected to each other whilst they are running (hot
pluggable) and provide automatic recognition of the connected devices and their properties.
Use the USB interface in conjunction with labworldsoft® for operation in “Remote” mode to update the solvent library. Navigate to
http://www.ika.net/ika/lws/download/RV10.cfg to update.
Command syntax and format
The following applies to the command set:
- Commands are generally sent from the computer (Master) to the
device (Slave).
- The stirrer machine sends only at the computer’s request. Even
fault indications cannot be sent spontaneously from the stirrer machine to the computer (automation system).
- Commands are transmitted in capital letters.
- Commands and parameters including successive parameters are
separated by at least one space (Code: hex 0x20).
- Each individual command (incl. parameters and data) and each response are terminated with Blank CR Blank LF (Code: hex 0x20
hex 0x0d hex 0x20 hex 0x0A) and have a maximum length of 80
characters.
- The decimal separator in a number is a dot (Code: hex 0x2E).
The above details correspond as far as possible to the recommendations of the NAMUR working party (NAMUR recommendations for the design of electrical plug connections for analogue
and digital signal transmission on individual items of laboratory
control equipment, rev. 1.1).
The NAMUR commands and the additional specific IKA commands serve only as low level commands for communication
between the rotary evaporator and the PC. With a suitable terminal or communications programme these commands can be
transmitted directly to the rotary evaporator. The IKA software
package, labworldsoft, provides a convenient tool for controlling
rotary evaporator and collecting data under MS Windows, and
includes graphical entry features, for motor speed ramps for example.
The following table summarises the (NAMUR) commands understood by the IKA. control equipment.
Fig. 23
Installation
Connect the RV 10 control to the PC using the USB data cable. t. The
RV 10 control will then transmit information to the Windows operating system to tell it which device drivers are required. Windows
will then either:
- Load the driver,
- Install the driver automatically if not already installed,
- Prompt the user to perform a manual installation.
Navigate to http://www.ika.net/ika/lws/download/stmcdc.inf.
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Abbreviations used:
m
=
X
=
2
X
=
3
X
=
4
X
=
60
X
=
61
X
=
62
X
=
63
X
=
66
X
=
70
X
=
74
Numbering parameter (integer)
Temperature heating plate
Safety temperature heating plate
Speed
Interval time (1-99 seconds, 1 <= m >=99)
Timer (1-199 minutes, 1 <= m >=199)
Upper lift position (OUT_SP_62 1-> drive lift up)
Lower lift position (OUT_SP_62 1-> drive lift down)
Value vacuum controller
Vacuum controller hysteresis
Tempering medium (OUT_SP_74 0=Öl, OUT_SP_74 1=Wasser)
NAMUR Commands
Function
IN_NAME
IN_PV_X
X = 2, 3, 4, 66
IN_SOFTWARE
IN_SP_X
X = 2, 3, 4, 60, 61, 66, 70
OUT_SP_X m
X = 2, 3, 4, 60, 61, 62, 63, 66, 70, 74
RESET
START_X
X = 2, 4, 60, 66
STOP_X
X = 2, 4, 60, 66
Request designation
Read actual value
Request software Id-number, date and version
Read target value input
Set target value to m
Switch to normal operation
Switch on appliance (remote) function
witch off appliance function
PC 1.1 Cable
This cable is required to connect the 9-pin connector to a PC. (fig. 24).
Fig. 24
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Commissioning
Basic guide to using the menu system
Functional description (in as-delivered state)
Selecting a menu
 Turn the rotary/push knob to the right/left to select the desired
menu option.
Factory settings
The values specified below correspond to the as-delivered state (display output/factory language setting is English).
Note: The active menu item is shown with a black background on
the display.
Editing values
 Press the rotary/push knob
 Turn the rotary/push knob to change the value (the magnitude of
the change is dependent on the speed at which the knob is turned).
 Press the rotary/push knob again to complete the process.
Exiting a menu
 Press the SET button.
 Current values are stored.
Next-highest menu level is displayed.
 Press the ESC button.
 Current values are not stored.
Next-highest menu level is displayed.
 The system check is performed while the start screen is displayed; this takes no more than 30 seconds.
Note: Some menu items do not contain values that can be stored.
Select SET or ESC to exit the menu.
The main menu will appear after a few seconds
Note: Certain menu items have functionality that varies from or adds
to that described above.
Display screen during the distillation process
Each operating mode has its own dedicated display screen. The following display characteristics are common:
- When a distillation is in progress it is not possible to leave the active display indicated.
- Press SET or ESC to exit the active display mode when no distillation is in progress. This will return the display to the main menu.
Error messages
 Press ESC to acknowledge the fault if an error message appears
on the display.
 The error message will disappear.
Note: In the case of serious faults, an additional display message
will appear indicating that the device must be switched off and only
switched back on again when the fault has been rectified.
 Turn the rotary/push knob to the right/left to select a menu option.
 Confirm the selection by pressing the rotary/push knob.
“Settings“ menu
The unit is ready for service when the
mains plug has been plugged in.
Switching on the device
 Switch on the device on the right side of the device by the mains
plug (fig.25).
 Device functions activated.
The following options are available from the "Settings" menu.
 Turn the rotary/push knob to the right/left to select a menu option.
 Confirm the selection by pressing the rotary/push knob.
Fig.25
Note: The heating bath must also be switched on.
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Distillation settings
Vacuum settings
 Turn the rotary/push knob to the right/left to select a menu option.
 Press the rotary/push knob.
 Turn the rotary/push knob to change the value (the magnitude of the
change is dependent on the speed at which the knob is turned).
 Press the rotary/push knob again to complete the process.
 Turn the rotary/push knob to the right/left to select a menu option.
 Press the rotary/push knob.
 Turn the rotary/push knob to change the value (the magnitude of the
change is dependent on the speed at which the knob is turned).
 Press the rotary/push knob again to complete the process.
SET key: Exit menu and save changes.
ESC key: Exit menu without saving changes.
SET key: Exit menu and save changes.
ESC key: Exit menu without saving changes.
Distillation method
Select between the automatic distillation methods “Volume” and
“100%”. This selection only has an effect during auto-distillation.
Hysteresis
The default settings for the hysteresis (as shown) are suitable for
use in most situations. The (vacuum) hysteresis value describes the
difference between the closing and opening pressures for the vacuum valve.
Volume
The measured values of the cooling water flow rate and the cooling
water temperature difference form the basis for a heat balance calculation used to determine the quantity of distillate at every stage of the distillation. The distillation process is halted when the specified quantity
of distillate has been reached.
Time scaling
The time axis of the vacuum-rotation-time graph is scaled using the
value specified here. If the value = 0, then the time axis is scaled automatically.
100%
The distillation process is stopped when the measured cooling water
temperature difference falls below a threshold value, i.e. as soon as a
solvent has been completely distilled off.
Vacuum scaling
The vacuum axis of the vacuum-rotation-time graph is scaled using
the value specified here. If the value = 0, then the vacuum axis is
scaled automatically.
Drying
The cooling water temperature difference is not monitored if this option
is activated, e.g. use in processes for drying powdered media.
Vacuum meas. unit
Select between the units of measurement for a vacuum: mBar, Torr,
and hPascal.
Heat rejection rate threshold
A limit value can be set for the heat rejection rate that is appropriate for
the condenser used; see "Worth knowing" section. The actual heat rejection rate is calculated during every distillation process. If the threshold
is exceeded, the distillation will be stopped and an error message displayed.
Maximum heat rejection rate
The maximum heat rejection rate achieved during the last distillation is
displayed. This value is for information purposes only.
RV 10.5001 connected?
If no RV 10.5001 is connected, then the cooling water flow rate will not
be monitored.
Flow rate control
It is also possible to deactivate the cooling water flow rate monitoring
when the RV 10.5001 is connected. This is necessary if, for example, a
dry ice cooler is used.
"Auto-distillation" mode is not available if the "Volume" distillation method is selected when flow rate control is switched off.
Quantity meas. unit
Select between millilitre and gram as the unit of quantity.
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Drive settings
Bath settings
 Turn the rotary/push knob to the right/left to select a menu option.
 Press the rotary/push knob.
 Turn the rotary/push knob to change the value (the magnitude of the
change is dependent on the speed at which the knob is turned).
 Press the rotary/push knob again to complete the process.
 Turn the rotary/push knob to the right/left to select a menu option.
 Press the rotary/push knob.
 Turn the rotary/push knob to change the value (the magnitude of the
change is dependent on the speed at which the knob is turned).
 Press the rotary/push knob again to complete the process.
SET key: Exit menu and save changes.
ESC key: Exit menu without saving changes.
SET key: Exit menu and save changes.
ESC key: Exit menu without saving changes.
Right/left interval
Setting a particular value X for the right/left interval will cause the drive
to change the direction of rotation every X seconds.
Medium bath
Select either water or oil as the medium for the heating bath.
Note: In interval mode the maximum speed is limited to 200 rpm.
Language
Timer
The timer value determines the time after which a manual distillation
will be stopped.
Time scaling
The time axis of the vacuum-rotation-time graph is scaled using the
value specified here. If the value = 0, then the time axis is scaled automatically.
Rotation scaling
The rotation axis of the vacuum-rotation-time graph is scaled using the
value specified here. If the value = 0, then the rotation axis is scaled automatically.
 Turn the rotary/push knob to the left/right to select the language.
 Confirm the selection by pressing SET.
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Service
 Fill water at room ambient temperature into a glass beaker (approx.
500 ml). Fully submerge both sensors into the water, see fig. 27.
 Turn the rotary/push knob to the right/left to select a menu option.
 Press the rotary/push knob.
 Turn the rotary/push knob to change the value (the magnitude of the
change is dependent on the speed at which the knob is turned).
 Press the rotary/push knob again to complete the process.
 Wait until the temperature display in the “Service” menu, menu option “Calibrate” has stabilised, e.g. 0.2K.
 Press the rotary/push knob.
 The temperature difference displayed will be calibrated to zero.
Fig.27
ESC key: Exit menu, all changes to switch settings are reset, the calibration remains unaffected.
Switching valves and pump
To check functionality for servicing purposes, use the Service menu
to activate/deactivate directly the valves included in delivery or optional and the pump, e.g. RV 10.5001.
The RV 10.5001 valve switches the water circuit on and off. This row
also shows the current cooling water flow rate.
Calibrate
The “Calibrate” option is used for calibration of the temperature sensor.
Calibration is only possible within the temperature range +0.5 K to 0.5 K. If the temperature is outside this range, then either a temperature sensor is faulty or connected incorrectly. Please contact the
Service department.
If the characteristics of the cooling water supply deviate significantly
from the specifications given in the “Technical specifications”, with
the result that the initial conditions for automatic distillation are not
achieved, then it may be necessary to recalibrate the temperature
sensors. This may, however, lead to a reduction in the accuracy with
which the distillate quantity is measured in “Auto-distillation” mode.
Operation hours
This value serves as informaton and cannot be changed.
The temperature difference displayed will be calibrated to zero. This action cannot be reversed.
The temperature sensor must be calibrated whenever it is replaced or
changed, or if a new temperature sensor is installed.
Please contact the Service department.
The temperature sensor supplied with the system is calibrated exworks.
Performing calibration
 Activate the “Calibrate” menu option by turning the rotary/push
knob.
 Remove both sensors. To remove a sensor, push back the outer ring
to release the locking device on the push-in connector, while at the
same time pulling the temperature sensor out of the connector, see
fig. 26.
Fig.26
 To reconnect a temperature sensor, push it into the push-in connector until the limit stop is reached; an initial resistance will be felt.
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„Manuel Mode“ menu
“Manuel Mode” display screen
1. Operating mode display
2. Vacuum display (actual value)
3. Vacuum display (target value)
4. Control field for „Start/ Stop“ distillation
5. Timer display
6. Control field for storing the distillation sequence
7. Vacuum-rotation-time graph
8. Display of flow rate, differential temperature, and condenser
heat rejection rate
9. Control field for rotary speed display (target value) and speed
measurement unit
10. Error message in case of fault, otherwise status indicator
Saving the distillation sequence as a procedure on completion of
distillation
 Turn the rotary/push knob to the right/left to select "Save".
 Press the rotary/push knob to display the "Procedures" screen.
Turn the rotary/push knob to the left/right to select one of the ten
procedures. The sequence will be shown graphically.
 Press SET, to overwrite the selected procedure with the current
procedure (the procedure that has just been completed) and exit
the menu.
 Pressing ESC will prevent the selected procedure from being
overwritten.
Note: Distillation sequences saved in this manner can be repeated
at a later dater in the user-defined mode by selecting the corresponding procedure.
Note: If it is necessary to work in manual mode for an extended period (>4 minutes) without performing a distillation (e.g. flask not in
heating bath), or if a drying process is carried out, then “Drying”
mode must be activated in menu “Settings”, menu option “Distillation”, in order to prevent the “No temperature increase” error
message being displayed.
Setting the rotary speed
 Press the rotary/push knob to change the target value.
 Turn the rotary/push knob to the right/left to change the target
value. The magnitude of the change is dependent on the speed
at which the knob is turned.
 Press the rotary/push knob again to save and complete the
change
Note: When you select the speed > 100 rpm, smooth start is automatically activated.
Setting the vacuum
 Press the rotary/push knob to change the target value.
 Turn the rotary/push knob to the right/left to change the target
value. The magnitude of the change is dependent on the speed
at which the knob is turned.
 Press the rotary/push knob again to save and complete the
change
Start
 Turn the rotary/push knob to the right/left to select "Start".
 Press the rotary/push knob to start the distillation..
 The display field will change to "Stop".
Note: If the timer has been configured, then the time will start to
count backwards. If a timer has not been configured then the time
elapsed since the start is shown.
Stop
 Turn the rotary/push knob to the right/left to select "Stop".
 Press the rotary/push knob to stop the distillation.
 The display field will change to "Start".
­48
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Auto-distillation Mode“ menu
User defined solvents
 Select one of the options NewSolvent1 ... NewSolvent5 from the
"Solvents" screen.
 Select one of these solvents and press the rotary/push knob.
"Auto-distillation Mode” display screen
1. Operating mode display
2. Control field for solvent
3. Vacuum display (actual value)
4. Vacuum display (target value)
5. Control field for „Start/ Stop“ distillation
6. Timer display
7. Distillation progress indicator
(% of required quantity of distillate)
8. Vacuum-rotation-time graph
9. Display of flow rate, differential temperature, and condenser
heat rejection rate.
10. Rotary speed display (target value) and speed measurement unit
11. Error message in case of fault, otherwise status indicator
Changing the selected solvent
 Turn the rotary/push knob to the right/left to select the control
field "Solvent".
 Press the rotary/push knob to display a list of the various solvents
available.
All the parameters displayed for the solvent can now be modified.
 Turn the rotary/push knob to the right/left to select the parameter to be changed.
 Press the rotary/push knob.
 Turn the rotary/push knob to the right/left to change the selected
parameter.
 Press the rotary/push knob.
 Press SET to save all values.
 This action selects NewSolvent1 as the current solvent.
Note: It is not possible to return to the selection list.
 Turn the rotary/push knob to the right/left to select a "Solvent".
 Press the SET key.
 The solvent selected will be used for the subsequent distillation.
Note: The display shows the parameters for each of the solvents.
The parameters can only be changed for the user-definable solvents
UserSolvent1 ... UserSolvent5. Please refer to the next section for
instructions on how to do this.
032010
­49
3859400a_RV10c_032010:Layout­1­­15.04.10­­14:09­­Seite­50
Starting automatic distillation
"User-defined Distillation" menu
 Press the rotary/push knob with the “Start” or “Continue” field
selected. If the “100% distillation” or “Drying” options are active,
then the distillation will start immediately, provided that the necessary conditions are fulfilled.
When the “Volume” distillation method is used, a further screen
with additional distillation parameters will be displayed.
 Turn the rotary/push knob to the right/left to select a menu option.
 Press the rotary/push knob.
 Turn the rotary/push knob to change the value (the magnitude of the
change is dependent on the speed at which the knob is turned).
 Press the rotary/push knob again to complete the process.
Distillation
This field indicates the distillation method selected in Settings/Distillation and cannot be changed..
"User-defined Distillation" display screen
1. Operating mode display
2. Control field for distillation procedure
3. Vacuum display (actual value)
4. Vacuum display (target value)
5. Control field for „Start/ Stop“ distillation
6. Timer display
7. Vacuum-rotation-time graph
8. Display of flow rate, differential temperature, and condenser
heat rejection rate
9. Rotary speed display (target value) and speed measurement unit
10. Error message in case of fault, otherwise status indicator
Amount
Enter the amount, which the flask contains.
Distillate
Enter the amount, which you want to distill off.
Efficiency
Balancing requires a precise thermal efficiency to be entered.
The efficiency is dependent on a combination of factors that affect
the distillation process, so it must initially be estimated. The first
time a distillation process is carried out should therefore be used
for calibration. Following completion of the distillation process, determine the quantity of distillate produced and calculate the actual
heat rejection rate according to the following formula:
ηP =
ηP
ηth
m(gem)
m (calc)
ηth . m(calc)
m (gem)
Actual efficiency
Estimated efficiency
Measured quantity of distillate
Specified (calculated) distillate quantity
For subsequent distillations, the actual calculated efficiency should
be entered; this will ensure that subsequent automatic distillations
under the same distillation and ambient conditions are performed
with sufficient precision.
End of automatic distillation
Automatic distillation will stop when the following conditions are
met::
 Turn the rotary/push knob to the right/left to select „Procedure“.
 Press the rotary/push knob.
 The display will show the "Procedures" screen.
 Turn the rotary/push knob to the right/left to select a procedure.
 Press the SET button.
 The procedure selected will be used for the subsequent distillation.
Note: The vacuum-rotation-time graph is displayed for each procedure. The parameters can be changed for each procedure. Please
refer to the next section for instructions on how to do this. The sequence used for a manual distillation process can also be saved as
a procedure. see "Manual Mode" section.
Volume controlled
The specified quantity of distillate has been reached.
100% distillation
The measured cooling water temperature has fallen below a target
value, indicating that the solvent is fully evaporated.
The distillation can also be stopped manually:
 Press the rotary/push knob with the “Stop” display field selected..
­50
032010
3859400a_RV10c_032010:Layout­1­­15.04.10­­14:09­­Seite­51
Changing a procedure
 Select the procedure to be changed and press the rotary/push
knob. The “Delete and create” display field will be activated.
 Press the rotary/push knob with the "Delete and create" field selected to delete the procedure.
New vacuum and rotation values can now be entered to define a
new step in procedure.
Vacuum
 Turn the rotary/push knob to the right/left to select "Vacuum" from
the on-screen options.
 Press the rotary/push knob.
 Turn the rotary/push knob to the right/left to enter a value.
 Press the rotary/push knob.
Stopping user-defined distillation
The user-defined distillation will stop automatically once all steps in
the currently active procedure have been completed. It is also possible to stop the process manually by pressing the rotary/push
knob with the “Stop” display field selected.
Stand-by operation
 Press the "Power" button.
 The device will enter stand-by.
 Press the "Power" button again.
 The screen will display “Start” to indicate that the device is ready
for use again.
Duration
 Turn the rotary/push knob to the right/left to select "Duration" from
the on-screen options.
 Press the rotary/push knob.
 Turn the rotary/push knob to the right/left to enter a value.
 Press the rotary/push knob. This will define a new step in the procedure with the pair of values vacuum-duration and add it to the
procedure. The diagram will be updated.
Rotation
 Turn the rotary/push knob to the right/left to select "Rotation" from
the on-screen options.
 Press the rotary/push knob.
 Turn the rotary/push knob to the right/left to enter a value.
 Press the rotary/push knob.
Duration
 Turn the rotary/push knob to the right/left to select "Duration" from
the on-screen options.
 Press the rotary/push knob.
 Turn the rotary/push knob to the right/left to enter a value.
 Press the rotary/push knob. This will define a new step in the procedure with the pair of values rotation-duration and add it to the
procedure. The diagram will be updated.
The vacuum-duration and rotation-duration steps can be repeated a
maximum of twenty times.
SET key: Exit menu, store the newly created procedure and activate
it as the current procedure.
ESC key: Exit menu and reset all changes.
032010
­51
­52
Start up-screen
Main menu
Manual mode
Auto-distillation mode
User-defined mode
Settings
Distillation
Vacuum
Drive
Heating bath
Language
Service
RV10.5001
RV10.4001/2
RV10.4003 Valve
V4 Vacuum venting
RV10.4003 Pump
Calibration
Operating hours
Rotation
Start
English
Deutsch
Français
Español
Rotation, target value
Vacuum, target value
Timer Display
Control field of distillation procedure
Start/Stop, more parameter
Error display
Display of flow rate, differential temperature, cooling capacity
Vacuum-rotation-time graph display
Rotation, target value
Vacuum, target value
Timer Display
Control field of solvents
Start/Stop, more parameter
Error display
Display of flow rate, differential temperature, cooling capacity
Vacuum-rotation-time graph display
Distillation progress display
Rotation, target value
Vacuum, target value
Timer Display
Start/Stop
Confirmation, Control field of procedures
Error display
Vacuum-rotation-time graph display
Bath medium
Water
Oil
Procedure 1
Procedure 2
Procedure 3
Procedure 4
Procedure 5
Procedure 6
Procedure 7
Procedure 8
Procedure 9
Procedure 10
Right/left interval
Timer
Scaling time
Saling rotation
Delete procedure
Vacuum
Duration
Rotation
Duration
Confirmation
Initial quantity
Distillate quantity
Efficiency
100% Distillation
Hysteresis
Scaling time
Scaling vacuum
Vacuum meas. units
Aceton
Water
Toluon
N-Pantenol
Benzol
UserSolvent 1
UserSolvent 2
UserSolvent 3
UserSolvent 4
UserSolvent 5
Distillation method
Drying
Heat rejection rate threshold
Maximum heat rejection rate
RV 10.5001 connected?
Flow rate control
Quantity meas. units
Heating bath temperature
Rotation
Vacuum
Efficiency
C-Value
Evaporation enthalpy
Density
Procedure 1
Procedure 2
Procedure 3
Procedure 4
Procedure 5
Procedure 6
Procedure 7
Procedure 8
Procedure 9
Procedure10
3859400a_RV10c_032010:Layout­1­­15.04.10­­14:09­­Seite­52
Menu system
032010
3859400a_RV10c_032010:Layout­1­­15.04.10­­14:09­­Seite­53
Setting the lower end stop
CAUTION! Depending on the size of the piston, the setting angle of
the rotation drive and the position of the heating bath and lift, the
evaporator piston can be in contact with the bottom of the heating
bath. CAUTION - glass may break!
Limit the lower lift position with the variable end stop.
The lift can be moved to any desired position in manual mode using the
“” and “” keys. There is no automatic cut-off if a collision occurs.
 Press the “” key until the lift reaches the desired position.
Note: The evaporator piston should be 2/3 immersed in the heating
bath.
 To adjust the stop element (Q), press the centre button ((R) on the
front of the lift (fig. 28).
 Slide the limit stop (Q) to the lowest position (Fig. 29).
 Press the “” key until the lift has reached the upper end stop.
Note: The path is limited from 0 – 6 cm.
Filling the evaporator piston
Prior to filling the evaporator piston, a vacuum controller is used to regulate the glass apparatus to the target pressure.
 Now fill the evaporator piston using the backfeed line, see fig. 30.
 Due to the vacuum present, the solvent is suctioned into the evaporator piston. This enables you to keep solvent loss due to suctioning to a minimum.
 You can also fill the evaporator piston manually prior to creating
the vacuum. The evaporator piston should not be filled more than
half its volume.
Note: CAUTION! The maximum allowed load (evaporator piston
and contents) is 3 kg.
R
Fig. 30
Q
Fig.28
Setting up the heating bath
Refer also to the operating instructions for the HB 10 heating
bath!
 Move the lift to the bottom position and check the position of the
heating bath in relation to the evaporator piston. When using larger evaporator pistons (2 or 3 litres) or depending on the angle of
the rotation drive, you can move the heating bath 50 mm to the
right.
 Fill the heating bath with the tempering medium until the evaporator piston is surrounded by tempering medium to 2/3 of its volume.
 Switch on the rotation drive and slowly increase the speed.
Note: Avoid creating waves.
 Switch on the heating bath using the main on/off switch.
Note: Avoid stress on the glass due to different evaporator piston
and heating bath temperatures when lowering the evaporator piston into the heating bath!
Note: If non-original accessories are used that are not supplied by
IKA, then it is possible that the 50 mm travel range provided by the
heating bath will not be sufficient. This applies in particular when
using 3 L evaporator flasks with foam brake.
Use the IKA RV 10.3000 mounting plate to extend the heating bath
travel range by 150 mm.
Fig.29
Check that the limit stop is functioning properly:
 Lower the lift by holding down the “” key.
 The drive stops automatically when the preset desired lower end
position has been reached.
 Move the drive back to the upper position.
032010
­53
3859400a_RV10c_032010:Layout­1­­15.04.10­­14:09­­Seite­54
Maintenance and cleaning
The device is maintenance-free. It is subject only to the natural
wear and tear of components and their statistical failure rate.
The seal on the glass condenser should be checked at regular intervals and replaced if necessary.
For cleaning disconnect the main plug.
To clean the device use only water with a detergent that contains
tensides, or use isopropylalcohol for stubborn soiling.
­54
Spare parts order
When ordering spare parts, please give:
- machine type,
- manufacturing number, see type plate,
- item and designation of the spare part, see www.ika.net, spare
parts diagram and spare parts list.
Repair
In case of repair the device has to be cleaned and free from any materials which may constitute a health hazard.
If you require servicing, return the appliance in its original packaging.
Storage packaging is not sufficient. Please also use suitable transport packaging.
032010
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Accessories
1
2
RV 10.1
RV 10.10
RV 10.2
RV 10.20
NS 29/32 Vertical glassware (1)
NS 29/32 Vertical glassware, coated (1)
NS 29/32 Diagonal glassware (2)
NS 29/32 Diagonal glassware, coated (2)
RV 10.700
RV 10.710
RV 10.800
RV 10.810
NS 29/42 Vertical glassware (1)
NS 29/42 Vertical glassware, coated (1)
NS 29/42 Diagonal glassware (2)
NS 29/42 Diagonal glassware, coated (2)
RV 10.900
RV 10.910
RV 10.1000
RV 10.1010
NS 24/40 Vertical glassware (1)
NS 24/40 Vertical glassware, coated (1)
NS 24/40 Diagonal glassware (2)
NS 24/40 Diagonal glassware, coated (2)
RV 10.3
RV 10.30
RV 10.4
RV 10.40
RV 10.5
Vertical-intensive condenser with manifold
Vertical-intensive condenser with manifold, coated
Dry ice condenser
Dry ice condenser, coated
Vertical-condenser with manifold and cut-off valve
for reflux distillation
Vertical-condenser with manifold and cut-off valve
for reflux distillation, coated
Vertical-intensive condenser with manifold and cut-off valve
for reflux distillation
Vertical-intensive condenser with manifold and cut-off valve
for reflux distillation, coated
RV 10.50
1
2
3
RV 10.6
RV 10.60
1
032010
HB 10.1
HB 10.2
Protection shield (Heating bath HB 10)
Protection cover (Heating bath HB 10)
RV 10.70
RV 10.71
RV 10.72
RV 10.73
NS 29/32 Steam pipe
NS 24/29 Steam pipe
NS 29/42 Steam pipe
NS 24/40 Steam pipe
RV 10.80
RV 10.81
RV 10.82
RV 10.83
RV 10.84
RV 10.85
RV 10.86
NS 29/32 Evaporator piston 50 ml
NS 29/32 Evaporator piston 100 ml
NS 29/32 Evaporator piston 250 ml
NS 29/32 Evaporator piston 500 ml
NS 29/32 Evaporator piston 1000 ml
NS 29/32 Evaporator piston 2000 ml
NS 29/32 Evaporator piston 3000 ml
RV 10.90
RV 10.91
RV 10.92
RV 10.93
RV 10.94
RV 10.95
RV 10.96
RV 10.97
NS 24/32 Evaporator piston 50 ml
NS 24/32 Evaporator piston 100 ml
NS 24/32 Evaporator piston 250 ml
NS 24/32 Evaporator piston 500 ml
NS 24/32 Evaporator piston 1000 ml
NS 24/32 Evaporator piston 2000 ml
NS 24/32 Evaporator piston 3000 ml
NS 24/40 Evaporator piston 1000 ml
RV 10.2001
RV 10.2002
RV 10.2003
RV 10.2004
RV 10.87
RV 10.2005
RV 10.2006
NS 29/42 Evaporator piston 50 ml
NS 29/42 Evaporator piston 100 ml
NS 29/42 Evaporator piston 250 ml
NS 29/42 Evaporator piston 500 ml
NS 29/42 Evaporator piston 1000 ml
NS 29/42 Evaporator piston 2000 ml
NS 29/42 Evaporator piston 3000 ml
RV 10.2007
RV 10.2008
RV 10.2009
RV 10.2010
RV 10.2011
RV 10.2012
RV 10.2013
NS 24/40 Evaporator piston 50 ml
NS 24/40 Evaporator piston 100 ml
NS 24/40 Evaporator piston 250 ml
NS 24/40 Evaporator piston 500 ml
NS 24/40 Evaporator piston 1000 ml
NS 24/40 Evaporator piston 2000 ml
NS 24/40 Evaporator piston 3000 ml
RV 10.100
RV 10.101
RV 10.102
RV 10.103
RV 10.104
RV 10.105
KS 35/20 Receiving flask 100 ml
KS 35/20 Receiving flask 250 ml
KS 35/20 Receiving flask 500 ml
KS 35/20 Receiving flask 1000 ml
KS 35/20 Receiving flask 2000 ml
KS 35/20 Receiving flask 3000 ml
2
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3859400a_RV10c_032010:Layout­1­­15.04.10­­14:10­­Seite­56
­56
1
2
3
4
5
6
RV 10.200
RV 10.201
RV 10.202
RV 10.203
RV 10.204
RV 10.205
KS 35/20 Receiving flask, coated 100 ml
KS 35/20 Receiving flask, coated 250 ml
KS 35/20 Receiving flask, coated 500 ml
KS 35/20 Receiving flask, coated 1000 ml
KS 35/20 Receiving flask, coated 2000 ml
KS 35/20 Receiving flask, coated 3000 ml
RV 10.300
RV 10.301
RV 10.302
NS 29/32 Powder piston 500 ml
NS 29/32 Powder piston 1000 ml
NS 29/32 Powder piston 2000 ml
RV 10.303
RV 10.304
RV 10.305
NS 24/29 Powder piston 500 ml
NS 24/29 Powder piston 1000 ml
NS 24/29 Powder piston 2000 ml
RV 10.2014
RV 10.2015
RV 10.2016
NS 29/32 Powder piston 500 ml
NS 29/32 Powder piston 1000 ml
NS 29/32 Powder piston 2000 ml
RV 10.217
RV 10.218
RV 10.219
NS 24/40 Powder piston 500 ml
NS 24/40 Powder piston 1000 ml
NS 24/40 Powder piston 2000 ml
RV 10.400
RV 10.401
NS 29/32 Evaporator cylinder 500 ml
NS 29/32 Evaporator cylinder 1500 ml
RV 10.402
RV 10.403
NS 24/29 Evaporator cylinder 500 ml
NS 24/29 Evaporator cylinder 1500 ml
RV 10.2020
RV 10.2021
NS 29/42 Evaporator cylinder 500 ml
NS 29/42 Evaporator cylinder 1500 ml
RV 10.2022
RV 10.2023
NS 24/40 Evaporator cylinder 500 ml
NS 24/40 Evaporator cylinder 1500 mll
RV 10.500
RV 10.501
RV 10.2024
RV 10.2025
NS 29/32 Foam brake
NS 24/29 Foam brake
NS 29/42 Foam brake
NS 24/40 Foam brake
RV 10.600
RV 10.601
RV 10.602
NS 29/32 Distillation spider with 6 sleeves
NS 29/32 Distillation spider with 12 sleeves
NS 29/32 Distillation spider with 20 sleeves
RV 10.603
RV 10.604
RV 10.605
NS 24/29 Distillation spider with 6 sleeves
NS 24/29 Distillation spider with 12 sleeves
NS 24/29 Distillation spider with 20 sleeves
RV 10.2026
RV 10.2027
RV 10.2028
NS 29/42 Distillation spider with 6 sleeves
NS 29/42 Distillation spider with 12 sleeves
NS 29/42 Distillation spider with 20 sleeves
RV 10.2029
RV 10.2030
RV 10.2031
NS 24/40 Distillation spider with 6 sleeves
NS 24/40 Distillation spider with 12 sleeves
NS 24/40 Distillation spider with 20 sleeves
RV 10.606
RV 10.607
NS 29/32 Distillation spider with 5 flasks 50 ml
NS 29/32 Distillation spider with 5 flasks 100 ml
RV 10.608
RV 10.609
NS 24/29 Distillation spider with 5 flasks 50 ml
NS 24/29 Distillation spider with 5 flasks 100 ml
RV 10.2032
RV 10.2033
NS 29/42 Distillation spider with 5 flasks 50 ml
NS 29/42 Distillation spider with 5 flasks 100 ml
RV 10.2034
RV 10.2035
NS 24/40 Distillation spider with 5 flasks 50 ml
NS 24/40 Distillation spider with 5 flasks 100 ml
RV 10.3000
Extension plate
RV 10.4001
RV 10.4002
RV 10.4003
RV 10.5001
RV 10.5002
RV 10.5003
Solenoid valve (central vacuum system) (1)
Solenoid valve (laboratory vacuum system) (2)
Pump controller, including solenoid valve (3)
Water regulator valve (4), only for use on water supply line!
Filter (5)
Pressure control valve (6)
032010
3859400a_RV10c_032010:Layout­1­­15.04.10­­14:10­­Seite­57
RV 06.13
RV 06.15
Seal FKM, PTFE-coated (1)
Seal PTFE (2)
PC 1.1
Cable
2
1
labworldsoft ®
Error codes
Any malfunctions during operation will be identified by an error message on the display.
Once a serious error message has been displayed, the lift moves to the top end position and the device can no longer be operated. The lift can
be operated again.
Proceed as follows in such cases:
 Switch off device using the main switch
 Carry out corrective measures
 Restart device
Error
Effect
Communication
error bath
Distillation canceled in "Auto-distillation" mode IR interface obstructed
Heating bath switched off
- Press ESC to confirm
- Switch on heating bath
- Check and clean IR interface
Distillation stopped,
no rotary drive
- Switch device off and on at mains switch
No rotation
Cause
Rotary drive does not start or
exhibits very large speed variation
No temperature Distillation canceled in "Auto-distillation" mode No differential temperature increase of
difference
cooling water
Correction
- Press ESC to confirm
- Check flow of cooling water
- Check that the cooling water hoses are fitted
correctly
Temperature
out of range
Distillation stopped
Differential temperature outside
measurement range (> 7 K)
- Press ESC to confirm
- Check that the cooling water hoses are fitted
correctly
No vacuum
Distillation stopped
Vacuum cannot be controlled
Vacu um target value not reached
- Press ESC to confirm
- Check that the glassware and hose connections
are properly sealed
- Switch on the pump
- Check the solenoid valve connections
No venting
Vacuum cannot be vented
No venting of condenser
- Switch off the device
- Vacuum sensor faulty
- Manually vent the glassware using the stop
valve
Water valve
not closed
Water runs continuously into cooling circuit
Water valve not closed
- Press ESC to confirm
- Check the connection
Flow rate
out of range
Distillation canceled in "Auto-distillation" mode Flow rate of cooling water out of range
- Readjust flow rate
- Press ESC to confirm
- Switch off flow rate control
(for dry ice coolers)
Condenser
overload
Distillation stopped
Distillate may be able to enter th e vacuum
pump
Condenser overload
- Press ESC to confirm
- Change process parameters, e.g.
- Increase pressure
- Reduce bath temperature
- Increase condenser flow rate within specified range
Distillation
dry
Distillation stopped
The system detected that there was no
more medium in the evaporating flask
during the distillation.
- Press ESC to confirm
- Alternatively, activate the “Drying” option
in the “Settings” menu
Distillation stopped
Lift motor switches off
Obstruction in path of lift
- Press ESC to confirm
- Check the path of the lift.
- Remove any obstructions.
Calibration error
Calibration reset to factory setting
Out of calibration range (max. +/-0.5 K)
- Press ESC to confirm
- Check that the sensor is connected correctly
- Carry out a new calibration procedure
Memory error
Calibration parameter for vacuum reset to
factory setting
Error by che cking contents of memory
Vacuum must be recalibrated
Distillation stopped
Leak in vacuum system
Press ESC to confirm
Locate leak
Lift not in
end position
Vacuum leak
If the actions described fail to resolve the fault or another error code is displayed then take one of the following steps:
- Contact the service department,
- Send the device for repair, including a short description of the fault.
Technical Data
Operating voltage range
Rated voltage
Frequence
Power input without heating bath
Power input operation “stand by”
Speed
Speed display
032010
Vac
Vac
Hz
W
W
rpm
100 - 230 + 10%
100 - 230
50 / 60
100
3,3
20-280
digital
­57
3859400a_RV10c_032010:Layout­1­­15.04.10­­14:10­­Seite­58
Dimensions of visible display area (W x H)
Display
Multiple languages
Right and left movement/ interval operation
Smooth start
Lift
Lifting speed
Stroke
Setting of lower end stop
Head angle adjustable
Timer
Interval
Integrated vacuum controller
Measurement range
Adjustment range
Measurement accuracy
Adjustment accuracy
Measurement range of differential temperature
Offset balancing range
Interface
Ramp programming
Distillation processes programmable
Remote control
Cooling surface (Standard condenser RV 10.1,10.10,10.2,10.20)
Minimum cooling water flow rate
Maximum cooling water flow rate
Cooling water pressure
Cooling water temperature range
Fuse
Perm. On- time
Perm. ambient temperature
Perm. humidity
Protection acc. to DIN EN 60529
Protection class
Overvoltage category
Contamination level
Weight (no glassware; no heating bath)
Dimensions (W x D x H)
Operation at a terrestrial altitude
mm
mm/s
mm
mbar (hPa)
mbar (hPa)
mbar
mbar
K
K
cm2
l/h
l/h
bar
°C
%
°C
%
kg
mm
m
70 x 52
TFT-Display
yes
yes
yes
automatic
50
140
60 mm, contactless
0° - 45°
1-199 minutes
1-60 sec
yes
1050 - 1
1050 - 1
+ 2 (+ 1 Digit) if calibritation is done at a constant temperature
adjustable hysteresis
6
+0,5
USB, RS 232
yes
yes
with accessory labworldsoft ®
1200
30
100
0,5
18 - 22, constantly
2 x T1,6A 250V 5x20
100
5-40
80
IP 20
I
II
2
18,6
500 x 440 x 430
max. 2000
Subject to technical changes!
Solvent table (excerpt)
Solvent
Formula
Pressure for
boiling point
40 °C in mbar
Acetic acid
Acetone
Acetonitrile
N-Amylalcohol,
n-Pentanol
n-Butanol
tert. Butanol,
2-Methyl-2-Propanol
Butylacetate
Chlorobenzene
Chloroform
Cyclohexane
Dichloromethane,
Methylenechloride
Diethylether
1,2,-Dichloroethylene (trans)
Diisopropylether
Dioxane
Dimethylformamide (DMF)
Ethanol
C2H4O2
C3H6O
C2H3N
C5H12O
44
556
226
11
C4H10
C4H10O
25
130
C6H12O2
C6H5CI
CHCI3
C6H12
CH2CI2
39
36
474
235
atm.press.
C4H10O
C2H2CI2
C6H14O
C4H8O2
C3H7NO
C2H6O
atm.press.
751
375
107
11
175
Ethylacetate
Ethylmethylketone
Heptane
Hexane
Isopropylalcohol
Isoamylalcohol,
3-Methyl-1-Butanol
Methanol
Pentane
n-Propylalcohol
Pentachloroethane
1,1,2,2,-Tetrachloroethane
1,1,1,-Trichloroethane
Tetrachloroethylene
Tetrachloromethane
Tetrahydrofurane (THF)
Toluene
Trichloroethylene
Water
Xylene
C4H8O2
C4H8O
C7H16
C6H14
C3H8O
C5H12O
240
243
120
335
137
14
CH4O
C5H12
C3H8O
C2HCI5
C2H2CI4
C2H3CI3
C2CI4
CCI4
C4H8O
C7H8
C2HCI3
H2O
C8H10
337
atm.press.
67
13
35
300
53
271
357
77
183
72
25
Warranty
In accordance with IKA warranty conditions, the warranty period is
24 months. For claims under the warranty please contact your local
dealer. You may also send the machine direct to our factory, enclosing the delivery invoice and giving reasons for the claim. You will
be liable for freight costs.
­58
The warranty does not cover worn out parts, nor does it apply to
faults resulting from improper use, insufficient care or maintenance
not carried out in accordance with the instructions in this operating
manual.
032010
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