525_Broch_Discover S..

SPECIFICATIONS
o
HEATING RATE
2-6 C/second
TEMPERATURE
-80 to 300 oC
PRESSURE
0-30 bar (0-435 psi)
ActiVent Self-Venting Technology included for pressure relief during or after reaction
REFLUX REACTION COMPLIANT
Open vessel option included for reflux reactions
POWER
0-300 W
TEMPERATURE MEASUREMENT
Infrared for volume-independent non-invasive temperature measurement
Fiber optic probe for direct feedback
OPERATING VOLUME
0.2 – 75 mL
0.2 – 50 mL pressurized
REACTION AGITATION
Electromagnetic stirring with adjustable speeds
AIR COOLING
≥25 psi (20 L/min flow) user-supplied
For Simultaneous Cooling (PowerMAX) and reaction quenching
AUTOMATION
12-position [up to 12 (10 mL) vessels or 6 (35 mL) vessels ]
48-position [up to 48 (10 mL) vessels or 24 (35 mL) vessels]
72-position [up to 72 (10 mL) vessels or 36 (35 mL) vessels]
96-position [up to 96 (10 mL) vessels or 48 (35 mL) vesselss]
AVAILABLE ACCESSORIES
Mobile Interface
Camera
Sub-ambient reactions (CoolMate Sub-Ambient Microwave System)
Gas Addition kit
Flow Cell
Peptide Synthesis
Enzymatic Digest
WEIGHT
38 lbs. (17.3 kg)
DIMENSIONS
14.2”W x 16.9”D x 11.2”H
(36.1 cm x 42.9 cm x 28.4 cm)
CEM Corporation
World Headquarters
PO Box 200
Matthews, NC 28106
Tel: 800-726-3331
Tel: 704-821-7015
Fax: 704-821-7894
Email: info@cem.com
www.cem.com
SUBSIDIARIES
United Kingdom
Italy
Japan
CEM Microwave Technology Ltd.
2 Middle Slade
Buckingham Industrial Estate
Buckingham MK181WA
Tel: (44) 1280-822873
Fax: (44) 1280-822873
Email: info.uk@cem.com
www.cemmicrowave.co.uk
CEM S.R.L.
Via Dell’ Artigianato, 6/8
24055 Cologno al Serio (Bg)
Tel: (39) 35-896224
Fax: (39) 35-891661
Email: info.srl@cem.com
www.cemmicroonde.com
CEM Japan K.K.
2-18-10 Takanawa
Minato-ku, Tokyo
108-0074
Tel: +81-3-5793-8542
Fax: +81-3-5793-8543
Email: info@cemjapan.jp
www.cemjapan.jp
Germany
CEM μWave S.A.S.
Immeuble Ariane
Domaine Technologique de Saclay
4, rue Rene’ Razel
91892 ORSAY Cedex
Tel: +33 (01) 69 35 57 80
Fax: +33 (01) 60 19 64 91
Email: info.fr@cem.com
www.cemfrance.fr
CEM GmbH
Carl-Friedrich-Gauss-Str.9
47475 Kamp-Lintfort
Tel: (49) 2842-9644-0
Fax: (49) 2842-9644-11
Email: info@cem.de
www.cem.de
France
©2012 CEM Corporation
Discover SP™, ActiVent™, Synergy™, PowerMAX™ and CoolMate™ are trademarks of CEM Corporation.
Discover ® and Explorer ® are registered trademarks of CEM Corporation.
Ireland
CEM Technology (Ireland) Ltd.
Sky Business Centre
9a Plato Business Park
Damastown
Dublin 15
Tel: +353 (0) 1 885 1752
Fax: +353 (0) 1 885 1601
Email: info.ireland@cem.com
www.cemmicrowave.co.uk
B087.2
THE BEST-SELLING MICROWAVE SYNTHESIS PLATFORM
takes another leap forward with Discover SP. This new system has all of the
features for which the Discover series is known, plus an enhanced heating
capability, and CEM’s new ActiVent Technology, all in one compact simple-tooperate system. As the most advanced technology designed for microwave
synthesis, the Discover SP provides superior flexibility with easily interchangeable
accessories that enable you to customize a system so you can do your chemistry,
your way.
ENERGY EFFICIENT
Why use more power than you really need? Instead of following the conventional
approach of applying more power to heat reaction mixtures more rapidly, we
improved the cavity of the Discover SP and made it even more efficient.
This enhancement gives the Discover SP the best heating cavity using the least
amount of microwave power input.
INNOVATIVE ENGINEERING
FOR SIMPLE OPERATION
Discover SP is engineered
for superior performance.
Intuitive software and quick
programming make Discover
SP the easiest to operate
microwave synthesis system
you’ll ever use.
ACCESSORIES
CoolMateTM
The CoolMateTM is the only commercially available microwave system designed
to perform reactions at sub-ambient temperatures. Reactions such as lithiation,
carbohydrate synthesis, and other temperature-sensitive chemistries can now
benefit from the use of microwave energy. Use the power of microwave
energy to accelerate reactions even at temperatures as low as -80 oC.
Gas Addition
The Gas Addition accessory is the only system specially designed for reactions
with gaseous reagents. Perform hydrogenations, carbonylations, or other
reactions with gaseous reagents or simply use the vessel to ensure an inert
atmosphere during microwave irradiation. This system allows you to purge
the reaction vessel and back-fill it with a gas. During the reaction, the gas
source is completely shut off from the microwave, thereby ensuring your
safety at all times.
Camera
The optional Integrated Camera allows you to see the changes occurring during
your reaction. It’s the perfect tool for documentation and publication support.
Fiber Optic Temperature
Control provides the most
precise temperature
measurement available by
directly measuring the
temperature inside the
reaction vessel. It can be used
with 10-mL reaction vessels
designed for this purpose, as
well as with the 80-mL vessel.
Other accessories, including
the CoolMate™ and Gas
Addition Kit use this type of
temperature measurement.
EXPLORER SP
AUTOMATION
SUPERIOR DESIGN FOR
SIMPLE OPERATION
Optimize your reactions
and expand the capabilities
of your laboratory without
expanding your lab space.
Explorer modules for the
Discover SP platform provide
fully automated reaction
handling capabilities and are
an ideal solution to support
small groups of chemists as a
shared resource.
CEM’s patented ActiVent caps
for pressure vessels offer a
secure seal without the need
for crimping tools.
Mobile Interface
Run your system and manipulate data with CEM’s new flexible, easy-to-use, and
powerful Mobile Interface option for the Discover SP Series. The interface can
easily be mounted on the Discover to free up benchspace or placed away from
the chemicals in the fume hood depending on your needs. Take the interface
to your office to analyze data, create new methods, or transfer data into another
program. The interface features a large, full color, 10.1” touchscreen, with a
mountable dock, which also serves as a charging station. The Mobile Interface
also connects wirelessly to Discover Systems running the full version of CEM’s
Synergy™ software.
New ActiVentTM Technology
Control your reaction in more ways than ever before.
CEM’s patented ActiVent™ Technology is the latest advance in automated
pressure control and the safest way to perform pressurized reactions. The
ActiVent pressure control system was designed to work exclusively with
ActiVent vessels and caps to give you greater flexibility in pressure control
and optimum results.
Vent as your reaction progresses or after it is complete
Perform high temperature/high pressure reactions using
either parameter to safely and effectively control the reaction
without venting.
Automatically program the system to release a gaseous byproduct
as it forms.
Ultimate programmability for your reaction. Any material that is
released is vented safely through exhaust tubing to a location
specified by you.
Vent more effectively during a reaction
Explorer 48, 72, & 96
EXPLORER 12
All of the benefits of a large format
autosampler within the footprint of
the world’s smallest manual reactor.
This twelve position autosampler
accommodates both the 10- and 35-mL
vessels and is the best value of any
autosampler commercially available.
CEM manufactures autosamplers to accommodate both 10- and 35-mL sealed
vessels. Run either size or a combination of both easily. Intelligent rack design
allows the autosampler to recognize the vessel type without user input and the
integrated robotics ensure that switching between 10-mL and 35-mL reaction
vessels occurs seamlessly, freeing your time for other things.
10-mL Vessels
35-mL Vessels
Explorer 48
Up to 48
Up to 24
Explorer 72
Up to 72
Up to 36
Explorer 96
Up to 96
Up to 48
Mix and match reaction vessel sizes for the ultimate in flexible reaction setup.
Release unexpected pressure quickly and safely, allowing the
reaction to proceed to completion.
Safely remove unneeded gaseous by-products and help shift the
equilibrium of your reaction to generate more product, quickly.
Perform the reaction in a completely sealed environment.
Generate a gas in-situ and consume it as a normal reagent.
ActiVent safely releases the pressure after the reaction is
complete without intervention.
It’s your choice.
Your chemistry, your way.
DISCOVER SP INNOVATIVE FEATURES
ActiVentTM
Pressure Device
Self-Tuning Cavity
EASIEST-TO-USE
VESSELS
Simple Integrated
Attenuator Design
allows full access to the Discover
cavity to simplify cleaning process
and provide the ultimate flexibility
in vessel selection.
takes all of the guesswork out of ensuring that
your reaction is positioned correctly every time,
no matter which vessel you use. As the reaction
progresses, the microwave energy distribution
adjusts automatically for optimum performance
and reproducibility.
Perform either pressurized
or non-pressurized reactions
YOU CAN’T GET ANY EASIER THAN
CEM’S ActiVentTM CAPS.
NO TOOLS REQUIRED
300-mL Cavity
Discover has the largest
single-mode cavity available,
providing unprecedented
access and vessel flexibility.
Focused
Microwave Cavity
is the core of the Discover
System. Built around the
largest single mode cavity
available, the Discover System
provides the ultimate flexibility
in reaction selection and vessel
compatibility.
CoolMate vessel
Air Cooling for Simultaneous
Heating and Reaction Quenching
quickly reduces the overall reaction temperature
to quench the reaction upon completion. Air
cooling is also the critical component behind
PowerMAX™ Technology.
Volume Independent
IR Temperature Sensor
provides the simplest means to measure
the temperature in a reaction in a noninvasive manner. No need for multiple
reaction vessels or large minimum volumes
with the IR mounted on the bottom.
10-mL flow cell
OPEN VESSEL REACTIONS
Electromagnetic Stirring
to ensure maximum agitation for your
reaction mixture. Adjust the speed to
guarantee your sample mixes each and
every time.
PowerMAX™ Simultaneous Cooling
maximizes the benefits of microwave energy. One of
the reasons microwave energy works so well for driving
synthetic reactions is because it heats kinetically, not
thermally. Localized superheating raises the temperature
of the reactant mixture, but energy is actually transferred
kinetically. CEM’s patented PowerMAX technology uses
compressed gas to cool the reactant mixture while
simultaneously applying more energy than would normally
be used. Reactions proceed much more quickly than
normal and do not have time to form side products. This
technology is ideal for reactions that require a substantial
amount of energy, but may be temperature-sensitive.
Discover SP is the only single-mode microwave
synthesis system capable of also performing open
vessel reactions using standard laboratory glassware
and condensers. Discover SP accepts up to a 125-mL
round-bottom flask and allows reagent addition and
overhead stirring. It can be used with or without a
reflux condenser.
Durable Design
An advanced membrane design and specially formulated
coating protects parts from solvents and reagents.
Easiest to Clean
Discover SP is designed with a removable spill cup, as well as
a drain tray for easy clean up. There’s nothing to disassemble,
just clean out the cup and the tray and you’re ready to run
another reaction.
Use round-bottom
flask up to 125-mL
Open Vessel
Attenuator
80-mL vessel
DISCOVER SP INNOVATIVE FEATURES
ActiVentTM
Pressure Device
Self-Tuning Cavity
EASIEST-TO-USE
VESSELS
Simple Integrated
Attenuator Design
allows full access to the Discover
cavity to simplify cleaning process
and provide the ultimate flexibility
in vessel selection.
takes all of the guesswork out of ensuring that
your reaction is positioned correctly every time,
no matter which vessel you use. As the reaction
progresses, the microwave energy distribution
adjusts automatically for optimum performance
and reproducibility.
Perform either pressurized
or non-pressurized reactions
YOU CAN’T GET ANY EASIER THAN
CEM’S ActiVentTM CAPS.
NO TOOLS REQUIRED
300-mL Cavity
Discover has the largest
single-mode cavity available,
providing unprecedented
access and vessel flexibility.
Focused
Microwave Cavity
is the core of the Discover
System. Built around the
largest single mode cavity
available, the Discover System
provides the ultimate flexibility
in reaction selection and vessel
compatibility.
CoolMate vessel
Air Cooling for Simultaneous
Heating and Reaction Quenching
quickly reduces the overall reaction temperature
to quench the reaction upon completion. Air
cooling is also the critical component behind
PowerMAX™ Technology.
Volume Independent
IR Temperature Sensor
provides the simplest means to measure
the temperature in a reaction in a noninvasive manner. No need for multiple
reaction vessels or large minimum volumes
with the IR mounted on the bottom.
10-mL flow cell
OPEN VESSEL REACTIONS
Electromagnetic Stirring
to ensure maximum agitation for your
reaction mixture. Adjust the speed to
guarantee your sample mixes each and
every time.
PowerMAX™ Simultaneous Cooling
maximizes the benefits of microwave energy. One of
the reasons microwave energy works so well for driving
synthetic reactions is because it heats kinetically, not
thermally. Localized superheating raises the temperature
of the reactant mixture, but energy is actually transferred
kinetically. CEM’s patented PowerMAX technology uses
compressed gas to cool the reactant mixture while
simultaneously applying more energy than would normally
be used. Reactions proceed much more quickly than
normal and do not have time to form side products. This
technology is ideal for reactions that require a substantial
amount of energy, but may be temperature-sensitive.
Discover SP is the only single-mode microwave
synthesis system capable of also performing open
vessel reactions using standard laboratory glassware
and condensers. Discover SP accepts up to a 125-mL
round-bottom flask and allows reagent addition and
overhead stirring. It can be used with or without a
reflux condenser.
Durable Design
An advanced membrane design and specially formulated
coating protects parts from solvents and reagents.
Easiest to Clean
Discover SP is designed with a removable spill cup, as well as
a drain tray for easy clean up. There’s nothing to disassemble,
just clean out the cup and the tray and you’re ready to run
another reaction.
Use round-bottom
flask up to 125-mL
Open Vessel
Attenuator
80-mL vessel
EXPLORER SP
AUTOMATION
SUPERIOR DESIGN FOR
SIMPLE OPERATION
Optimize your reactions
and expand the capabilities
of your laboratory without
expanding your lab space.
Explorer modules for the
Discover SP platform provide
fully automated reaction
handling capabilities and are
an ideal solution to support
small groups of chemists as a
shared resource.
CEM’s patented ActiVent caps
for pressure vessels offer a
secure seal without the need
for crimping tools.
Mobile Interface
Run your system and manipulate data with CEM’s new flexible, easy-to-use, and
powerful Mobile Interface option for the Discover SP Series. The interface can
easily be mounted on the Discover to free up benchspace or placed away from
the chemicals in the fume hood depending on your needs. Take the interface
to your office to analyze data, create new methods, or transfer data into another
program. The interface features a large, full color, 10.1” touchscreen, with a
mountable dock, which also serves as a charging station. The Mobile Interface
also connects wirelessly to Discover Systems running the full version of CEM’s
Synergy™ software.
New ActiVentTM Technology
Control your reaction in more ways than ever before.
CEM’s patented ActiVent™ Technology is the latest advance in automated
pressure control and the safest way to perform pressurized reactions. The
ActiVent pressure control system was designed to work exclusively with
ActiVent vessels and caps to give you greater flexibility in pressure control
and optimum results.
Vent as your reaction progresses or after it is complete
Perform high temperature/high pressure reactions using
either parameter to safely and effectively control the reaction
without venting.
Automatically program the system to release a gaseous byproduct
as it forms.
Ultimate programmability for your reaction. Any material that is
released is vented safely through exhaust tubing to a location
specified by you.
Vent more effectively during a reaction
Explorer 48, 72, & 96
EXPLORER 12
All of the benefits of a large format
autosampler within the footprint of
the world’s smallest manual reactor.
This twelve position autosampler
accommodates both the 10- and 35-mL
vessels and is the best value of any
autosampler commercially available.
CEM manufactures autosamplers to accommodate both 10- and 35-mL sealed
vessels. Run either size or a combination of both easily. Intelligent rack design
allows the autosampler to recognize the vessel type without user input and the
integrated robotics ensure that switching between 10-mL and 35-mL reaction
vessels occurs seamlessly, freeing your time for other things.
10-mL Vessels
35-mL Vessels
Explorer 48
Up to 48
Up to 24
Explorer 72
Up to 72
Up to 36
Explorer 96
Up to 96
Up to 48
Mix and match reaction vessel sizes for the ultimate in flexible reaction setup.
Release unexpected pressure quickly and safely, allowing the
reaction to proceed to completion.
Safely remove unneeded gaseous by-products and help shift the
equilibrium of your reaction to generate more product, quickly.
Perform the reaction in a completely sealed environment.
Generate a gas in-situ and consume it as a normal reagent.
ActiVent safely releases the pressure after the reaction is
complete without intervention.
It’s your choice.
Your chemistry, your way.
THE BEST-SELLING MICROWAVE SYNTHESIS PLATFORM
takes another leap forward with Discover SP. This new system has all of the
features for which the Discover series is known, plus an enhanced heating
capability, and CEM’s new ActiVent Technology, all in one compact simple-tooperate system. As the most advanced technology designed for microwave
synthesis, the Discover SP provides superior flexibility with easily interchangeable
accessories that enable you to customize a system so you can do your chemistry,
your way.
ENERGY EFFICIENT
Why use more power than you really need? Instead of following the conventional
approach of applying more power to heat reaction mixtures more rapidly, we
improved the cavity of the Discover SP and made it even more efficient.
This enhancement gives the Discover SP the best heating cavity using the least
amount of microwave power input.
INNOVATIVE ENGINEERING
FOR SIMPLE OPERATION
Discover SP is engineered
for superior performance.
Intuitive software and quick
programming make Discover
SP the easiest to operate
microwave synthesis system
you’ll ever use.
ACCESSORIES
CoolMateTM
The CoolMateTM is the only commercially available microwave system designed
to perform reactions at sub-ambient temperatures. Reactions such as lithiation,
carbohydrate synthesis, and other temperature-sensitive chemistries can now
benefit from the use of microwave energy. Use the power of microwave
energy to accelerate reactions even at temperatures as low as -80 oC.
Gas Addition
The Gas Addition accessory is the only system specially designed for reactions
with gaseous reagents. Perform hydrogenations, carbonylations, or other
reactions with gaseous reagents or simply use the vessel to ensure an inert
atmosphere during microwave irradiation. This system allows you to purge
the reaction vessel and back-fill it with a gas. During the reaction, the gas
source is completely shut off from the microwave, thereby ensuring your
safety at all times.
Camera
The optional Integrated Camera allows you to see the changes occurring during
your reaction. It’s the perfect tool for documentation and publication support.
Fiber Optic Temperature
Control provides the most
precise temperature
measurement available by
directly measuring the
temperature inside the
reaction vessel. It can be used
with 10-mL reaction vessels
designed for this purpose, as
well as with the 80-mL vessel.
Other accessories, including
the CoolMate™ and Gas
Addition Kit use this type of
temperature measurement.
SPECIFICATIONS
o
HEATING RATE
2-6 C/second
TEMPERATURE
-80 to 300 oC
PRESSURE
0-30 bar (0-435 psi)
ActiVent Self-Venting Technology included for pressure relief during or after reaction
REFLUX REACTION COMPLIANT
Open vessel option included for reflux reactions
POWER
0-300 W
TEMPERATURE MEASUREMENT
Infrared for volume-independent non-invasive temperature measurement
Fiber optic probe for direct feedback
OPERATING VOLUME
0.2 – 75 mL
0.2 – 50 mL pressurized
REACTION AGITATION
Electromagnetic stirring with adjustable speeds
AIR COOLING
≥25 psi (20 L/min flow) user-supplied
For Simultaneous Cooling (PowerMAX) and reaction quenching
AUTOMATION
12-position [up to 12 (10 mL) vessels or 6 (35 mL) vessels ]
48-position [up to 48 (10 mL) vessels or 24 (35 mL) vessels]
72-position [up to 72 (10 mL) vessels or 36 (35 mL) vessels]
96-position [up to 96 (10 mL) vessels or 48 (35 mL) vesselss]
AVAILABLE ACCESSORIES
Mobile Interface
Camera
Sub-ambient reactions (CoolMate Sub-Ambient Microwave System)
Gas Addition kit
Flow Cell
Peptide Synthesis
Enzymatic Digest
WEIGHT
38 lbs. (17.3 kg)
DIMENSIONS
14.2”W x 16.9”D x 11.2”H
(36.1 cm x 42.9 cm x 28.4 cm)
CEM Corporation
World Headquarters
PO Box 200
Matthews, NC 28106
Tel: 800-726-3331
Tel: 704-821-7015
Fax: 704-821-7894
Email: info@cem.com
www.cem.com
SUBSIDIARIES
United Kingdom
Italy
Japan
CEM Microwave Technology Ltd.
2 Middle Slade
Buckingham Industrial Estate
Buckingham MK181WA
Tel: (44) 1280-822873
Fax: (44) 1280-822873
Email: info.uk@cem.com
www.cemmicrowave.co.uk
CEM S.R.L.
Via Dell’ Artigianato, 6/8
24055 Cologno al Serio (Bg)
Tel: (39) 35-896224
Fax: (39) 35-891661
Email: info.srl@cem.com
www.cemmicroonde.com
CEM Japan K.K.
2-18-10 Takanawa
Minato-ku, Tokyo
108-0074
Tel: +81-3-5793-8542
Fax: +81-3-5793-8543
Email: info@cemjapan.jp
www.cemjapan.jp
Germany
CEM μWave S.A.S.
Immeuble Ariane
Domaine Technologique de Saclay
4, rue Rene’ Razel
91892 ORSAY Cedex
Tel: +33 (01) 69 35 57 80
Fax: +33 (01) 60 19 64 91
Email: info.fr@cem.com
www.cemfrance.fr
CEM GmbH
Carl-Friedrich-Gauss-Str.9
47475 Kamp-Lintfort
Tel: (49) 2842-9644-0
Fax: (49) 2842-9644-11
Email: info@cem.de
www.cem.de
France
©2012 CEM Corporation
Discover SP™, ActiVent™, Synergy™, PowerMAX™ and CoolMate™ are trademarks of CEM Corporation.
Discover ® and Explorer ® are registered trademarks of CEM Corporation.
Ireland
CEM Technology (Ireland) Ltd.
Sky Business Centre
9a Plato Business Park
Damastown
Dublin 15
Tel: +353 (0) 1 885 1752
Fax: +353 (0) 1 885 1601
Email: info.ireland@cem.com
www.cemmicrowave.co.uk
B087.2
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