Hach PHC 805 pH probe User Manual
Below you will find brief information for pH probe PHC 805. This manual describes the operation, calibration, and maintenance of the PHC 805 pH probe. It is designed for use in the laboratory and can be used to measure the pH of aqueous samples.
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User Manual
PHC805
Safety information
DOC022.5
3.80436
W A R N I N G
Chemical exposure hazard. Obey laboratory safety procedures and wear all of the personal protective equipment appropriate to the chemicals that are handled. Refer to the current safety data sheets (MSDS/SDS) for safety protocols.
C A U T I O N
Personal injury hazard. Glass components can break. Handle with care to prevent cuts.
Precautionary labels
Read all labels and tags attached to the instrument. Personal injury or damage to the instrument could occur if not observed. A symbol on the instrument is referenced in the manual with a precautionary statement.
Electrical equipment marked with this symbol may not be disposed of in European domestic or public disposal systems. Return old or end-of-life equipment to the manufacturer for disposal at no charge to the user.
Specifications
Specifications are subject to change without notice.
Specifications
Probe type
Body material pH range pH resolution pH accuracy
Sodium (alkalinity) error
Slope
Details
Digital combination glass pH probe with refillable electrolyte and built-in temperature sensor
Glass pH 0 to 14
User-selectable stabilization time and resolution—Fast: 0.1, Fast: 0.01, Medium: 0.01, Slow:
0.01 or Slow: 0.001
±0.02 pH
<0.3 pH at pH 13 in 0.1 M NaOH
–59 mV/pH (85 to 115% at 25 °C (77 °F) per Nernstian theoretical value)
Isopotential point pH 7.00
Temperature compensation 30 kΩ NTC thermistor
Temperature accuracy
Operating temperature
±0.3 °C (±0.54 ° F)
0 to 80 °C (32 to 176 °F)
Storage temperature
Junction type
Reference type
Electrolyte
5 to 40 °C (41 to 104 °F)
Porous pin
Ag/AgCl
Refillable, 3 M KCl
1
Specifications
Storage solution
Minimum sample depth
Dimensions
Details
3 M KCl
18 mm (0.71 in.)
Body diameter: 12 mm (0.47 in.)
Body length: 103 mm (4.1 in.)
Total length: 200 mm (7.87 in.)
Cable length: 1 m (3.28 ft)
M12 digital output and connector compatible with HQd meters Cable connection
Product overview
The probe is a digital pH combination electrode with refillable electrolyte, a glass body and an integrated temperature sensor. The probe is for laboratory use and measures pH in general aqueous samples.
Note: Do not use the probe with organic solvents, low ionic strength, wastewater, high solids or high alkaline sample types.
A 50-mL bottle of reference electrolyte filling solution (3 M KCl solution) is included with the probe. Refer to
Figure 1 Probe overview
1 Probe soaker bottle
2 Filling-hole cap
3 Protective tape and filling-hole
4 Cable, 1 meter (3.28 ft)
5 Probe soaker bottle holder
6 Reference junction
7 Glass bulb and temperature sensor
Preparation for use
Prepare the probe before a calibration or a sample measurement.
1. Turn the probe soaker bottle cap counter-clockwise to loosen the cap.
2. Remove the soaker bottle from the probe.
3. Fully rinse the reference junction and the glass bulb with deionized water to remove all of the storage solution or possible salt particles. Dry with a no-lint cloth.
2
5. Add the filling solution to the probe as necessary (refer to Fill the probe
on page 11). The filling solution must be above the standard solution or the sample
level during measurement or calibration ( Figure 2
).
6. Make sure that the filling hole is open during measurement for the correct flow of the filling solution.
Note: For the best stabilization time, condition the probe for 2 hours in pH buffer 4.01 before use, if the probe was not used for 3 weeks or more. In low ionic strength (LIS) samples, condition the probe for a maximum of 5 minutes in the sample before use. In all other cases a condition before use is not necessary.
Figure 2 Filling solution level
1 KCl crystals
1
2 Filling solution level
1
Red Rod probes only
Calibration
3 Filling solution
4 Standard solution or sample level
Before calibration:
The probe must have the correct service-life time stamp. Set the date and the time in the meter before the probe is attached.
It is not necessary to calibrate again if a calibrated probe is moved from one HQd meter to another. Make sure that the additional meter is configured to use the same calibration options.
To view the calibration data, push , then select View Probe Data>View Current Calibration.
If two probes are connected, push the UP or DOWN arrow to change to the single display mode to show the Calibrate option
(available only on HQ40d and HQ440d meters).
Prepare the probe for use (refer to Preparation for use
on page 2).
Calibration notes:
• Use buffers that are two pH units apart.
• Select additional standard sets with the minimum number of calibration points in the
Calibration Options. For a two-point calibration, select: one buffer with a pH above and one buffer with a pH below the sample pH. For a one-point calibration, select the buffer nearest to the sample pH.
• The calibration is recorded in the probe and the data log. Send the calibration to a
PC, a printer or a flash memory stick if connected.
3
• Air bubbles under the sensor tip can cause a slow response or an error in the measurement. If there are bubbles under the sensor tip, carefully shake the probe to remove the bubbles.
• Make sure that the filling hole is open and above the sample solution level.
• Use a laboratory stirrer or shake the probe from side to side in the solution to refresh the reference junction.
• The meter display shows "Stabilizing" and a progress bar as the probe stabilizes in the standard. The display shows the buffer and the temperature corrected pH value when the measurement is stable.
• The calibration and sample measurement conditions must be as similar as possible
(e.g., the temperature of the solution, the stir procedure, the stir rate and the position of the probe).
•
If a calibration error occurs, refer to Troubleshooting on page 12.
Calibration procedure:
1. Connect the probe to the meter. Make sure that the cable locking nut is correctly connected to the meter. Set the meter to on.
2. Push Calibrate.
The display shows the buffers that are necessary for calibration.
3. Prepare the fresh buffers in separate beakers or applicable containers.
4. Rinse the probe with deionized water.
Dry with a no-lint cloth.
5. Put the probe in the pH buffer solution and stir lightly. Make sure to fully put the reference junction into the standard.
4
6. Push Read. Wait until the reading stabilizes.
7. Do steps 4–6 again to collect the minimum number of calibration points specified in the calibration options.
8. Push Done to view the calibration summary.
Note: The display will not show "Done" until the minimum number of calibration points is collected.
9. Push Store to accept the calibration and go back to the measurement mode.
Sample requirements
N O T I C E
Some probes are not compatible with specific sample types. Probe damage can occur.
• Samples must be aqueous. The probe can also make measurements in partially aqueous or some water-miscible solvents. Read the results with caution because the full pH scale changes when the solvent system changes.
• Probes with an Ag/AgCl reference system and a single junction are not compatible with solutions that contain silver complexing or binding agents (e.g., TRIS, proteins and sulfides). To measure in these solutions, use a double junction probe, a probe with an Ag
+
(silver ion) barrier or a Red Rod
*
probe.
• Proteins can collect on the sensing element. Make sure that the probe stays clean when these types of samples are measured.
• Do not use the probe in solutions that are out of the temperature range of the probe.
Refer to Specifications on page 1.
• For low ionic strength (LIS) or high purity samples, use an LIS chamber or a flow cell to prevent sample contamination.
Measurement
Before measurement:
The probe must have the correct service-life time stamp. Set the date and the time in the meter before the probe is attached.
If the complete traceability is necessary, enter a sample ID and an operator ID before the measurement. Refer to the HQd meter manual for more information.
A regular calibration is necessary for the best measurement accuracy (refer to
on page 3).
Prepare the probe for use (refer to Preparation for use
on page 2).
Measurement notes:
• Data is automatically stored in the data log when Press to Read or Interval is selected in the Measurement Mode. When Continuous is selected, data is only stored when Store is pushed.
• Air bubbles under the sensor tip can cause a slow response or an error in the measurement. If there are bubbles under the sensor tip, carefully shake the probe to remove the bubbles.
• For the best stabilization time, condition the probe for several minutes in the sample or in a solution comparable to the sample in terms of pH and ionic strength before the initial sample measurement.
• Do not put the probe on the bottom or sides of the container.
• Make sure that the filling hole is open and above the sample solution level.
• Use a laboratory stirrer or shake the probe from side to side in the solution to refresh the reference junction.
• The meter display shows "Stabilizing" and a progress bar as the probe stabilizes in the sample. The display shows the lock icon when the measurement is stable.
•
If a measurement error occurs, refer to Troubleshooting on page 12.
Measurement procedure:
*
Radiometer Analytical’s Red Rod technology: Encapsulation of reference elements with a red protection tube.
5
1. Connect the probe to the meter. Make sure that the cable locking nut is correctly connected to the meter. Set the meter to on.
2. Condition the probe in the sample.
3. Rinse the probe with deionized water and then with the sample. Dry with a no-lint cloth.
4. Put the probe in the sample and stir lightly. Make sure to fully put the reference junction into the sample.
5. Push Read. Wait until the reading stabilizes.
6. Do steps 3–5 again to make more measurements.
7. When measurements are done, put the probe in storage (refer to
on page 11).
Run Check Standard
The Run Check Standard feature validates the instrument performance between sample measurements. Use the Run Check Standard feature for a periodic or a user-defined interval measurements of a traceable standard solution. Set the criteria for check standards from the PHC805 Settings menu.
Note: Access control must be set to off or a valid password must be used to change the Run Check
Standard options.
1. Push . The Full Access Options menu shows.
2. Select Run Check Standard.
Note: Select the correct probe if two probes are connected to the meter.
3. Use the standard solution shown on the display.
4. Rinse the probe with deionized water. Dry the probe with a no-lint cloth.
5. Put the probe in the standard solution. Make sure that the reference junction is fully in the standard. Move the probe up or down or lightly shake the probe to remove air bubbles.
6. Push Read. The display shows "Stabilizing" and a progress bar as the reading stabilizes. The display shows the value of the check standard and Check Standard
Passed or Check Standard Failed.
7. If the display shows Check Standard Passed, the check standard measurement is in the accepted limits. Select Done to continue the sample measurement.
8. If the display shows Check Standard Failed, the measurement is out of the accepted limits. A calibration is recommended. Make sure that the limits are set correctly at the
PHC805 Settings menu. If the acceptance criteria is set to "Cal Expires on Failure:
Yes", the display shows the calibration icon and a question mark until the probe is
6
Advanced operation
This section gives instructions about menu navigation and available options. Change parameter-specific settings through the Full Access Options menu.
The settings that can be changed are shown in
Table 1 Parameter-specific settings
Setting
Measurement Options
Options
• Resolution
• Upper and lower range limits
Calibration Options calibrated again. To correct the probe calibration and status indicator, calibrate the probe (refer to
on page 3).
• Buffer set
• Buffer set values (if Custom Buffer Set selected)
• Reminder
• Minimum Cal points
• Slope limit
Check Standard Options
• Standard (temperature compensated buffer or custom at 25 °C (77 °F))
• Reminder
• Acceptance criteria
• Standard value at 25 °C (77 °F) (if custom standard selected)
Units
• pH
• mV
Change measurement options
Methods are groups of default or user-defined settings related to specific applications. If the meter is set to the default method, a prompt for a new name method shows. The settings are saved with this name to identify them from the default method settings, which cannot be changed. Use a saved method as an alternative of many adjustments to the individual settings. Changes made to a user-defined method are automatically saved with the existing name. Save different methods for the same probe on each meter.
1. Make sure that a probe is connected to the meter.
2. Push and select PHC805 Settings.
3. Select Modify Current Settings.
4. Select Units. Select pH (default) or mV.
Note: Use the mV option to find the probe offset in a pH 7 buffer or to measure the slope. Both units show when the Detail Display mode is selected.
7
5. Select Measurement Options and update the settings:
Option
Resolution
Description
Set the resolution:
• 0.1 pH—Fast
• 0.01 pH—Fast (default)
• 0.01 pH—Medium
• 0.01 pH—Slow, or
• 0.001 pH—Slow
Measurement
Limits
The resolution has an effect on the number of decimal digits and the stabilization time. More stabilization time is necessary for higher resolution measurements. Slower stabilization times give higher accuracy measurements.
Set the measurement limits—Lower limit (default: 0.00 pH) or Upper limit
(default: 14.00 pH).
Set the measurement limits to agree with the permitted values for the sample. When the measurement is above the upper limit setting or below the lower limit setting, the meter shows an "Out of limits" message. This message is an alert to a possible problem with the process conditions.
6. If prompted, enter a name for the new method settings. Other changes made to the settings of an existing method are automatically saved with the same method name.
7. Push EXIT until the meter goes back to the measurement mode.
Change calibration options
1. Make sure that a probe is connected to the meter.
2. Push and select PHC805 Settings.
3. Select Modify Current Settings.
4. Select Calibration Options and update the settings:
Option
Buffer Set
Description
Sets the temperature compensated buffer set for calibration:
• Color Coded—4.01, 7.00, 10.01 (default)
• IUPAC—4.01, 7.00, 10.01, 12.45
• DIN—4.65, 9.23
• IUPAC—4.01, 6.86, 10.01, 12.45
• IUPAC—4.01, 6.86, 9.18, 12.45
• IUPAC—4.01, 7.00, 9.18, 12.45
• Custom Buffer Set (refer to
Custom buffer sets are characterized at 25 °C (77 °F).
Buffer set values show on the Calibration Options screen.
Note: Measure only the minimum calibration points specified in Minimum
Cal Points to complete a calibration.
Sets the buffer values if Custom Buffer Set is selected (refer to
Buffer Set
Values
Minimum Cal
Points
Slope Limit
Sets the minimum number of calibration points that are necessary to complete a calibration—1 (default), 2 or 3.
Sets the slope limit—1% to 20% (acceptable slope criteria, default = 15%).
Set the slope between the set limits for a correct calibration.
8
5. Select the Calibration Reminder and update the settings:
Option
Reminder
Repeat
Expires
Description
The meter makes a sound when a calibration is necessary and at the selected interval—Off (default), 2 h, 4 h, 8 h, 2 d, 5 d or 7 d.
Calibration expires after the selected time—Immediately, Reminder +
30 min, Reminder + 1 h, Reminder + 2 h or Continue Reading.
Note: The meter cannot read samples after calibration has expired unless
Continue Reading is selected.
6. If prompted, enter a name for the new method settings. Other changes made to the settings of an existing method are automatically saved with the same method name.
7. Push EXIT until the meter goes back to the measurement mode.
Table 2 Custom buffer sets
Description Buffer set values
Std1 to
Std5
Option
1.09 pH—25 °C Pre-set temperature compensated buffer values.
1.68 pH—25 °C
4.01 pH—25 °C
4.65 pH—25 °C
6.86 pH—25 °C
7.00 pH—25 °C
9.18 pH—25 °C
9.23 pH—25 °C
10.01 pH—
25 °C
12.45 pH—
25 °C
Note: It is necessary for selected standards to be different by a minimum of 2 pH units. For example, if
1.09 pH is selected for the first standard, the second standard must be different by at least 2 pH.
Standards that do not meet this minimum will show gray on the screen and will not be selectable.
Custom Buffer Custom buffer value.
Range = 2.000 pH to 14.000 pH.
Custom buffer values are not temperature compensated. Custom buffers must be read at
25 °C (77 °C).
No Buffer Select this option for undefined standards.
Change check standard options
1. Make sure that a probe is connected to the meter.
2. Push and select PHC805 Settings.
3. Select Modify Current Settings.
9
4. Select Check Standards Options and update the settings:
Option
Standard
Description
Sets the temperature compensated buffer value for check standard—
• 4.01 pH—25 °C
• 4.65 pH—25 °C
• 6.86 pH—25 °C
• 7.00 pH—25 °C
• 9.18 pH—25 °C
• 9.23 pH—25 °C
• 10.01 pH—25 °C
• 12.45 pH—25 °C
• Custom
Standard
Value
The standard value shows on the Check Standard Options screen.
No temperature compensation for custom buffers.
When the Standard is set to Custom, enter the standard value with the up/down arrow keys.
5. Select Check Standard Reminder and update the settings:
Option Description
Reminder Repeat Sets the time interval for the check standard reminder—Off, 30 minutes,
2 h, 4 h, 8 h, 12 h or 24 h.
Allow Defer
Lets the postponement of check standard reminders—Yes or No.
6. Select Acceptance Criteria and update the settings:
Option
Acceptance Limits
Description
Sets the tolerance limits for check standard—0.005 pH (default) to
1.000 pH.
Cal Expires on Failure Recalibration is necessary if check standard fails—Yes or No.
7. If prompted, enter a name for the new method settings. Other changes made to the settings of an existing method are automatically saved with the same method name.
8. Push EXIT until the meter goes back to the measurement mode.
Maintenance
Clean the probe
Clean the probe when there is contamination on the sensor. Symptoms of contamination are:
• Readings are not accurate or consistent.
• The stabilization time is slow.
• A calibration error occurs.
• Contamination is visible on the probe (e.g., dirt).
1. Rinse the probe with deionized water. Blot dry with a no-lint cloth.
2. Soak the glass bulb of the probe in the applicable cleaning agent. Refer to
Note: Remove KCl salt build-up from the probe with warm deionized water.
3. Rinse or soak the probe for 1 minute in deionized water.
4. Soak the probe in pH 4 buffer for 20 minutes.
5. Rinse the probe with deionized water.
6. Blot dry with a no-lint cloth.
10
Contaminant
General contaminants
Mineral deposits
Fats, grease and oils
Protein deposits
Inorganic buildup
Table 3 Cleaning agent
Cleaning agent
Electrode cleaning solution
0.1 N HCl solution
Warm, mild detergent solution
Pepsin cleaning solution
EDTA solution
Soak time
12–16 hours
10–15 minutes
2 hours (maximum)
3 hours (maximum)
3 hours (maximum)
Replace the filling solution
Replace the filling solution and KCl crystals (if applicable) when either occurs:
• The filling solution becomes contaminated.
• The KCl crystals in a Red Rod probe no longer move freely through the liquid when the probe is inverted.
1. Use a syringe or small pipette to remove as much filling solution from the probe as possible.
2. For Red Rod probes, if KCl crystals are still in the probe:
a. Fill the probe half full with the filling solution.
b. With a finger over the filling hole, shake the probe until the crystals become loose.
c. If the crystals will not loosen, fill the probe with filling solution. Put the probe into a warm water bath for approximately 10 minutes (up to 60 °C (140 °F)).
d. Do step 1 again.
3. For Red Rod probes, add approximately 0.5 cm (0.2 in.) of KCl crystals to the probe through the filling hole. For measurements at temperatures more than 60 °C (140 °F), more crystals are necessary. Refer to
on page 2.
4. Fill the probe. Refer to Fill the probe on page 11.
Fill the probe
on page 2) or is replaced (refer to Replace the filling solution on page 11). Refer
to Specifications on page 1 for the applicable filling solution.
1. If the filling hole is closed, remove the filling-hole cap from the filling hole (refer to
2. Remove the cap from the tip of the filling solution bottle.
3. Hold the bottle so that the tip is down. Put the tip of the bottle in the filling hole.
4. Slowly squeeze the bottle and fully fill the probe.
Note: Fully fill the probe for the best performance.
5. Put the probe into storage if not used immediately (refer to
on page 11).
6. Keep the filling solution bottle and cap for later use.
Note: If the dispensing tip becomes clogged, remove the dispensing tip and soak the tip in warm water. Fully dry and assemble the tip.
Storage
Short-term and long-term storage
For the best probe performance, do not let the reference junction become dry.
Note: Keep the probe in a sample for a maximum of 2 hours if the sample pH is not too high.
11
1. Put the filling-hole cap in the filling hole (refer to
2. Rinse the probe with deionized water. Dry the probe with a no-lint cloth.
3. Fill the probe soaker bottle half full with the applicable Storage Solution (refer to
on page 1) .
4. Loosen the soaker bottle cap and put the soaker bottle on the probe.
5. Turn the soaker bottle cap clockwise to tighten the soaker bottle cap.
6. Make sure that the solution in the soaker bottle fully covers the glass bulb and the reference junction.
Rehydration
If the glass bulb becomes dry:
1. Soak the probe tip in the 4.01 and 7.00 buffers each for 5 minutes.
2. Rinse the probe with deionized water. Blot dry with a no-lint cloth.
3. Calibrate the probe.
Troubleshooting
Message or symptom
Probe not supported
Possible cause
Software not updated
Action
To download the most current version of the software, refer to the applicable product page on the manufacturer's website.
Refer to the HQd Series meter documentation for more information.
Contact technical support.
Connect a probe or probe requires service pH reading and/or mV reading is same for all solutions
HQd meter does not sense the
IntelliCAL
®
probe
Probe not connected correctly
Software not updated
Large number of methods stored on probe
Damaged probe
Soaker bottle not removed
Electrical issue
Standard not recognized error Soaker bottle not removed
Incorrect buffer or contamination in the buffer solution
Contamination in the filling solution
Disconnect, then connect the probe. Tighten the locking nut.
To download the most current version of the software, refer to the applicable product page on the manufacturer's website.
Refer to the HQd Series meter documentation for more information.
If the probe has a large number of stored methods, more time is necessary for connection. Do not disconnect the probe, continue to let the probe connect.
Make sure that there is connectivity with another probe or meter to confirm isolated issue with probe. Contact technical support.
Remove the soaker bottle.
Contact technical support.
Remove the soaker bottle.
Use fresh buffer solution as specified in the method.
Drain and replace the filling solution with fresh solution.
12
Message or symptom
Slow stabilization time
Calibration errors
Possible cause
Tape not removed from the filling-hole
Contamination in the glass sensor
Contamination in the filling solution
Filling hole closed
Poor contact between reference junction and solution
LIS sample
Low sample temperature or temperature difference between samples
Air bubbles around inner reference electrode
Dehydrated glass bulb
Not sufficient electrolyte flow
1 pH probe too old (membrane degradation)
Calibration not done correctly
Contaminated glass sensor
Slope exceeds the criteria for % of theoretical (as defined in the method slope limit)
Action
Remove the tape.
Clean the probe. Refer to Clean the probe
Drain and replace the filling solution with fresh solution.
Make sure that the filling hole is open and above the solution level.
Shake the probe in the solution from side to side to refresh the reference junction.
Soak the probe in the sample for 10 to 15 minutes before the initial measurement or use a LIS chamber or flowthrough cell.
Examine the sample temperature. The lower the temperature or the higher difference of temperatures between samples, the longer the stabilization time will be.
Carefully tap the probe with hand or shake the probe downward to remove any air bubbles.
Rehydrate the probe. Refer to Storage on page 11.
Open the sleeve junction.
Replace the probe.
Calibrate again with fresh pH buffers.
Clean the probe. Refer to Clean the probe
calibration settings and method.
on page 10.
on page 10.
1.
Adjust the slope limits by changing the PHC805
2.
Calibrate again the probe.
3.
Make a check standard to examine the performance of the probe.
13
Message or symptom
Drifting/Inaccurate readings
Out of range
Out of limits
Temperature out of range
Possible cause
Contaminated glass bulb
CO
2
absorption (for low ionic strength or high purity sample)
Clogged reference
Improper storage conditions/
Dehydrated glass bulb
Measured temperature is out the range of the probe
Check standard temperature value is out of range
Action
Clean the probe. Refer to Clean the probe
on page 10.
Use the LIS chamber for LIS/high purity samples to prevent sample contamination.
Make sure that the filling hole is not covered. Rinse the reference junction holes with deionized water. Carefully tap the probe with hand or shake the probe to remove air bubbles. If there are salt crystals around the junction, soak the electrode tip in a 60 ºC (140 ºF) water bath for
10 minutes.
Clean or condition the probe and calibrate again. The probe can not operate correctly if the probe was left dry
for a long time. Rehydrate the probe. Refer to Storage
on page 11.
Colloidal and/or particulates in the filling solution
Air bubbles around inner reference electrode
Not sufficient electrolyte flow
Not sufficient stirring
1
Replace the filling solution, calibrate and test again.
Carefully tap the probe with hand or shake the probe to remove air bubbles.
Open the sleeve junction.
Stir the standards and samples at a slow and steady rate to prevent the formation of a vortex.
Make sure that the sample is in the range of the probe.
Measurement value is out of range
Check Standard value is out of limits in the current method
Make sure that the standard is in the limits of the current method.
Measurement value is out of measurement limits in the current method
Do another method that expands the acceptable limits.
Make sure that the sample is in the limits of the current method.
Temperature value is out of range
Make a new method with an expanded range.
Make sure that the sample temperature is in the range of the probe.
Make sure that the temperature sensor works correctly.
Make sure that the standard temperature is in the range of the probe.
Make sure that the temperature sensor works correctly.
Make sure that the check standard temperature is in the range of the probe.
1
Only applicable for probes with sleeve junction.
Consumables and accessories
Description
Electrode filling solution, 3 M KCl
Hach electrode storage solution, 3 M KCl
Hach Electrode Cleaning Solution
EDTA standard solution, 0.20N
Soaker bottle
LIS chamber assembly
Quantity
50 mL
500 mL
500 mL
500 mL
1
1
Item Number
2756559
2756549
2965249
102149
5192900
5189900
14
Consumables and accessories (continued)
Description
Color-coded pH standards (buffers)
pH 4.01 ±0.02 at 25 °C (77 °F), 500 mL pH 7.00 ±0.02 at 25 °C (77 °F), 500 mL pH 10.01 ±0.02 at 25 °C (77 °F), 500 mL pH 4.01 ±0.02 at 25 °C (77 °F), 4 L pH 7.00 ±0.02 at 25 °C (77 °F), 4 L pH 10.01 ±0.02 at 25 °C (77 °F), 4 L pH 4.01 ±0.02 at 25 °C (77 °F), 20 L pH 7.00 ±0.02 at 25 °C (77 °F), 20 L pH 10.01 ±0.02 at 25 °C (77 °F), 20 L
IUPAC series certified pH standards (buffers)
1 pH 4.005 ±0.010 at 25 °C (77 °F), 500 mL pH 6.865 ± 0.010 at 25 °C (77 °F), 500 mL pH 7.000 (Radiometer Analytical) ±0.010 at 25 °C (77 °F), 500 mL pH 9.180 ± 0.010 at 25 °C (77 °F), 500 mL pH 10.012 ± 0.010 at 25 °C (77 °F), 500 mL pH 12.45 ± 0.05 at 25 °C (77 °F), 500 mL
Technical grade pH standards (buffers)
pH 4.65 at 25 °C (77 °F), 500 mL pH 9.23 at 25 °C (77 °F), 500 mL
1
Certified standards ship with certificates for traceability to Standard Reference Materials
Quantity
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Item Number
2283449
2283549
2283649
2283456
2283556
2283656
2283461
2283561
2283661
S11M002
S11M003
S11M004
S11M006
S11M007
S11M008
S11M010
S11M011
15
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P.O. Box 389, Loveland, CO 80539-0389 U.S.A.
Tel. (970) 669-3050
(800) 227-4224 (U.S.A. only)
Fax (970) 669-2932 [email protected]
www.hach.com
HACH LANGE GMBH
Willstätterstraße 11
D-40549 Düsseldorf, Germany
Tel. +49 (0) 2 11 52 88-320
Fax +49 (0) 2 11 52 88-210 [email protected]
www.hach-lange.de
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1222 Vésenaz
SWITZERLAND
Tel. +41 22 594 6400
Fax +41 22 594 6499
©
Hach Company/Hach Lange GmbH, 2014. All rights reserved. Printed in U.S.A. 01/2014, Edition 1
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Key Features
- Digital combination glass pH probe
- Refillable electrolyte
- Built-in temperature sensor
- pH range 0 to 14
- User-selectable stabilization time and resolution
- ±0.02 pH accuracy
- Storage solution 3 M KCl
- Minimum sample depth 18 mm (0.71 in.)
- Cable length 1 m (3.28 ft)
Frequently Answers and Questions
What is the pH range of the PHC 805 pH probe?
What is the accuracy of the PHC 805 pH probe?
What is the minimum sample depth for the PHC 805 pH probe?
What is the cable length of the PHC 805 pH probe?
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Table of contents
- 1 Safety information
- 1 Precautionary labels
- 1 Specifications
- 2 Product overview
- 2 Preparation for use
- 3 Calibration
- 4 Sample requirements
- 5 Measurement
- 6 Run Check Standard
- 7 Advanced operation
- 7 Change measurement options
- 8 Change calibration options
- 9 Change check standard options
- 10 Maintenance
- 10 Clean the probe
- 11 Replace the filling solution
- 11 Fill the probe
- 11 Storage
- 12 Troubleshooting
- 14 Consumables and accessories