Hach PHC 805 pH probe User Manual

Hach PHC 805 pH probe User Manual
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Below you will find brief information for pH probe PHC 805. This manual describes the operation, calibration, and maintenance of the PHC 805 pH probe. It is designed for use in the laboratory and can be used to measure the pH of aqueous samples.

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PHC 805 pH probe User Manual | Manualzz

User Manual

PHC805

Safety information

DOC022.5

3.80436

W A R N I N G

Chemical exposure hazard. Obey laboratory safety procedures and wear all of the personal protective equipment appropriate to the chemicals that are handled. Refer to the current safety data sheets (MSDS/SDS) for safety protocols.

C A U T I O N

Personal injury hazard. Glass components can break. Handle with care to prevent cuts.

Precautionary labels

Read all labels and tags attached to the instrument. Personal injury or damage to the instrument could occur if not observed. A symbol on the instrument is referenced in the manual with a precautionary statement.

Electrical equipment marked with this symbol may not be disposed of in European domestic or public disposal systems. Return old or end-of-life equipment to the manufacturer for disposal at no charge to the user.

Specifications

Specifications are subject to change without notice.

Specifications

Probe type

Body material pH range pH resolution pH accuracy

Sodium (alkalinity) error

Slope

Details

Digital combination glass pH probe with refillable electrolyte and built-in temperature sensor

Glass pH 0 to 14

User-selectable stabilization time and resolution—Fast: 0.1, Fast: 0.01, Medium: 0.01, Slow:

0.01 or Slow: 0.001

±0.02 pH

<0.3 pH at pH 13 in 0.1 M NaOH

–59 mV/pH (85 to 115% at 25 °C (77 °F) per Nernstian theoretical value)

Isopotential point pH 7.00

Temperature compensation 30 kΩ NTC thermistor

Temperature accuracy

Operating temperature

±0.3 °C (±0.54 ° F)

0 to 80 °C (32 to 176 °F)

Storage temperature

Junction type

Reference type

Electrolyte

5 to 40 °C (41 to 104 °F)

Porous pin

Ag/AgCl

Refillable, 3 M KCl

1

Specifications

Storage solution

Minimum sample depth

Dimensions

Details

3 M KCl

18 mm (0.71 in.)

Body diameter: 12 mm (0.47 in.)

Body length: 103 mm (4.1 in.)

Total length: 200 mm (7.87 in.)

Cable length: 1 m (3.28 ft)

M12 digital output and connector compatible with HQd meters Cable connection

Product overview

The probe is a digital pH combination electrode with refillable electrolyte, a glass body and an integrated temperature sensor. The probe is for laboratory use and measures pH in general aqueous samples.

Note: Do not use the probe with organic solvents, low ionic strength, wastewater, high solids or high alkaline sample types.

A 50-mL bottle of reference electrolyte filling solution (3 M KCl solution) is included with the probe. Refer to

Figure 1 .

Figure 1 Probe overview

1 Probe soaker bottle

2 Filling-hole cap

3 Protective tape and filling-hole

4 Cable, 1 meter (3.28 ft)

5 Probe soaker bottle holder

6 Reference junction

7 Glass bulb and temperature sensor

Preparation for use

Prepare the probe before a calibration or a sample measurement.

1. Turn the probe soaker bottle cap counter-clockwise to loosen the cap.

2. Remove the soaker bottle from the probe.

3. Fully rinse the reference junction and the glass bulb with deionized water to remove all of the storage solution or possible salt particles. Dry with a no-lint cloth.

4. Remove the protective tape from the filling hole before initial use (refer to Product overview on page 2). Discard the protective tape.

2

5. Add the filling solution to the probe as necessary (refer to Fill the probe

on page 11). The filling solution must be above the standard solution or the sample

level during measurement or calibration ( Figure 2

).

6. Make sure that the filling hole is open during measurement for the correct flow of the filling solution.

Note: For the best stabilization time, condition the probe for 2 hours in pH buffer 4.01 before use, if the probe was not used for 3 weeks or more. In low ionic strength (LIS) samples, condition the probe for a maximum of 5 minutes in the sample before use. In all other cases a condition before use is not necessary.

Figure 2 Filling solution level

1 KCl crystals

1

2 Filling solution level

1

Red Rod probes only

Calibration

3 Filling solution

4 Standard solution or sample level

Before calibration:

The probe must have the correct service-life time stamp. Set the date and the time in the meter before the probe is attached.

It is not necessary to calibrate again if a calibrated probe is moved from one HQd meter to another. Make sure that the additional meter is configured to use the same calibration options.

To view the calibration data, push , then select View Probe Data>View Current Calibration.

If two probes are connected, push the UP or DOWN arrow to change to the single display mode to show the Calibrate option

(available only on HQ40d and HQ440d meters).

Prepare the probe for use (refer to Preparation for use

on page 2).

Calibration notes:

• Use buffers that are two pH units apart.

• Select additional standard sets with the minimum number of calibration points in the

Calibration Options. For a two-point calibration, select: one buffer with a pH above and one buffer with a pH below the sample pH. For a one-point calibration, select the buffer nearest to the sample pH.

• The calibration is recorded in the probe and the data log. Send the calibration to a

PC, a printer or a flash memory stick if connected.

3

• Air bubbles under the sensor tip can cause a slow response or an error in the measurement. If there are bubbles under the sensor tip, carefully shake the probe to remove the bubbles.

• Make sure that the filling hole is open and above the sample solution level.

• Use a laboratory stirrer or shake the probe from side to side in the solution to refresh the reference junction.

• The meter display shows "Stabilizing" and a progress bar as the probe stabilizes in the standard. The display shows the buffer and the temperature corrected pH value when the measurement is stable.

• The calibration and sample measurement conditions must be as similar as possible

(e.g., the temperature of the solution, the stir procedure, the stir rate and the position of the probe).

If a calibration error occurs, refer to Troubleshooting on page 12.

Calibration procedure:

1. Connect the probe to the meter. Make sure that the cable locking nut is correctly connected to the meter. Set the meter to on.

2. Push Calibrate.

The display shows the buffers that are necessary for calibration.

3. Prepare the fresh buffers in separate beakers or applicable containers.

4. Rinse the probe with deionized water.

Dry with a no-lint cloth.

5. Put the probe in the pH buffer solution and stir lightly. Make sure to fully put the reference junction into the standard.

4

6. Push Read. Wait until the reading stabilizes.

7. Do steps 4–6 again to collect the minimum number of calibration points specified in the calibration options.

8. Push Done to view the calibration summary.

Note: The display will not show "Done" until the minimum number of calibration points is collected.

9. Push Store to accept the calibration and go back to the measurement mode.

Sample requirements

N O T I C E

Some probes are not compatible with specific sample types. Probe damage can occur.

• Samples must be aqueous. The probe can also make measurements in partially aqueous or some water-miscible solvents. Read the results with caution because the full pH scale changes when the solvent system changes.

• Probes with an Ag/AgCl reference system and a single junction are not compatible with solutions that contain silver complexing or binding agents (e.g., TRIS, proteins and sulfides). To measure in these solutions, use a double junction probe, a probe with an Ag

+

(silver ion) barrier or a Red Rod

*

probe.

• Proteins can collect on the sensing element. Make sure that the probe stays clean when these types of samples are measured.

• Do not use the probe in solutions that are out of the temperature range of the probe.

Refer to Specifications on page 1.

• For low ionic strength (LIS) or high purity samples, use an LIS chamber or a flow cell to prevent sample contamination.

Measurement

Before measurement:

The probe must have the correct service-life time stamp. Set the date and the time in the meter before the probe is attached.

If the complete traceability is necessary, enter a sample ID and an operator ID before the measurement. Refer to the HQd meter manual for more information.

A regular calibration is necessary for the best measurement accuracy (refer to

Calibration

on page 3).

Prepare the probe for use (refer to Preparation for use

on page 2).

Measurement notes:

• Data is automatically stored in the data log when Press to Read or Interval is selected in the Measurement Mode. When Continuous is selected, data is only stored when Store is pushed.

• Air bubbles under the sensor tip can cause a slow response or an error in the measurement. If there are bubbles under the sensor tip, carefully shake the probe to remove the bubbles.

• For the best stabilization time, condition the probe for several minutes in the sample or in a solution comparable to the sample in terms of pH and ionic strength before the initial sample measurement.

• Do not put the probe on the bottom or sides of the container.

• Make sure that the filling hole is open and above the sample solution level.

• Use a laboratory stirrer or shake the probe from side to side in the solution to refresh the reference junction.

• The meter display shows "Stabilizing" and a progress bar as the probe stabilizes in the sample. The display shows the lock icon when the measurement is stable.

If a measurement error occurs, refer to Troubleshooting on page 12.

Measurement procedure:

*

Radiometer Analytical’s Red Rod technology: Encapsulation of reference elements with a red protection tube.

5

1. Connect the probe to the meter. Make sure that the cable locking nut is correctly connected to the meter. Set the meter to on.

2. Condition the probe in the sample.

3. Rinse the probe with deionized water and then with the sample. Dry with a no-lint cloth.

4. Put the probe in the sample and stir lightly. Make sure to fully put the reference junction into the sample.

5. Push Read. Wait until the reading stabilizes.

6. Do steps 3–5 again to make more measurements.

7. When measurements are done, put the probe in storage (refer to

Storage

on page 11).

Run Check Standard

The Run Check Standard feature validates the instrument performance between sample measurements. Use the Run Check Standard feature for a periodic or a user-defined interval measurements of a traceable standard solution. Set the criteria for check standards from the PHC805 Settings menu.

Note: Access control must be set to off or a valid password must be used to change the Run Check

Standard options.

1. Push . The Full Access Options menu shows.

2. Select Run Check Standard.

Note: Select the correct probe if two probes are connected to the meter.

3. Use the standard solution shown on the display.

4. Rinse the probe with deionized water. Dry the probe with a no-lint cloth.

5. Put the probe in the standard solution. Make sure that the reference junction is fully in the standard. Move the probe up or down or lightly shake the probe to remove air bubbles.

6. Push Read. The display shows "Stabilizing" and a progress bar as the reading stabilizes. The display shows the value of the check standard and Check Standard

Passed or Check Standard Failed.

7. If the display shows Check Standard Passed, the check standard measurement is in the accepted limits. Select Done to continue the sample measurement.

8. If the display shows Check Standard Failed, the measurement is out of the accepted limits. A calibration is recommended. Make sure that the limits are set correctly at the

PHC805 Settings menu. If the acceptance criteria is set to "Cal Expires on Failure:

Yes", the display shows the calibration icon and a question mark until the probe is

6

Advanced operation

This section gives instructions about menu navigation and available options. Change parameter-specific settings through the Full Access Options menu.

The settings that can be changed are shown in

Table 1 .

Table 1 Parameter-specific settings

Setting

Measurement Options

Options

• Resolution

• Upper and lower range limits

Calibration Options calibrated again. To correct the probe calibration and status indicator, calibrate the probe (refer to

Calibration

on page 3).

• Buffer set

• Buffer set values (if Custom Buffer Set selected)

• Reminder

• Minimum Cal points

• Slope limit

Check Standard Options

• Standard (temperature compensated buffer or custom at 25 °C (77 °F))

• Reminder

• Acceptance criteria

• Standard value at 25 °C (77 °F) (if custom standard selected)

Units

• pH

• mV

Change measurement options

Methods are groups of default or user-defined settings related to specific applications. If the meter is set to the default method, a prompt for a new name method shows. The settings are saved with this name to identify them from the default method settings, which cannot be changed. Use a saved method as an alternative of many adjustments to the individual settings. Changes made to a user-defined method are automatically saved with the existing name. Save different methods for the same probe on each meter.

1. Make sure that a probe is connected to the meter.

2. Push and select PHC805 Settings.

3. Select Modify Current Settings.

4. Select Units. Select pH (default) or mV.

Note: Use the mV option to find the probe offset in a pH 7 buffer or to measure the slope. Both units show when the Detail Display mode is selected.

7

5. Select Measurement Options and update the settings:

Option

Resolution

Description

Set the resolution:

• 0.1 pH—Fast

• 0.01 pH—Fast (default)

• 0.01 pH—Medium

• 0.01 pH—Slow, or

• 0.001 pH—Slow

Measurement

Limits

The resolution has an effect on the number of decimal digits and the stabilization time. More stabilization time is necessary for higher resolution measurements. Slower stabilization times give higher accuracy measurements.

Set the measurement limits—Lower limit (default: 0.00 pH) or Upper limit

(default: 14.00 pH).

Set the measurement limits to agree with the permitted values for the sample. When the measurement is above the upper limit setting or below the lower limit setting, the meter shows an "Out of limits" message. This message is an alert to a possible problem with the process conditions.

6. If prompted, enter a name for the new method settings. Other changes made to the settings of an existing method are automatically saved with the same method name.

7. Push EXIT until the meter goes back to the measurement mode.

Change calibration options

1. Make sure that a probe is connected to the meter.

2. Push and select PHC805 Settings.

3. Select Modify Current Settings.

4. Select Calibration Options and update the settings:

Option

Buffer Set

Description

Sets the temperature compensated buffer set for calibration:

• Color Coded—4.01, 7.00, 10.01 (default)

• IUPAC—4.01, 7.00, 10.01, 12.45

• DIN—4.65, 9.23

• IUPAC—4.01, 6.86, 10.01, 12.45

• IUPAC—4.01, 6.86, 9.18, 12.45

• IUPAC—4.01, 7.00, 9.18, 12.45

• Custom Buffer Set (refer to

Table 2 )

Custom buffer sets are characterized at 25 °C (77 °F).

Buffer set values show on the Calibration Options screen.

Note: Measure only the minimum calibration points specified in Minimum

Cal Points to complete a calibration.

Sets the buffer values if Custom Buffer Set is selected (refer to

Table 2 ).

Buffer Set

Values

Minimum Cal

Points

Slope Limit

Sets the minimum number of calibration points that are necessary to complete a calibration—1 (default), 2 or 3.

Sets the slope limit—1% to 20% (acceptable slope criteria, default = 15%).

Set the slope between the set limits for a correct calibration.

8

5. Select the Calibration Reminder and update the settings:

Option

Reminder

Repeat

Expires

Description

The meter makes a sound when a calibration is necessary and at the selected interval—Off (default), 2 h, 4 h, 8 h, 2 d, 5 d or 7 d.

Calibration expires after the selected time—Immediately, Reminder +

30 min, Reminder + 1 h, Reminder + 2 h or Continue Reading.

Note: The meter cannot read samples after calibration has expired unless

Continue Reading is selected.

6. If prompted, enter a name for the new method settings. Other changes made to the settings of an existing method are automatically saved with the same method name.

7. Push EXIT until the meter goes back to the measurement mode.

Table 2 Custom buffer sets

Description Buffer set values

Std1 to

Std5

Option

1.09 pH—25 °C Pre-set temperature compensated buffer values.

1.68 pH—25 °C

4.01 pH—25 °C

4.65 pH—25 °C

6.86 pH—25 °C

7.00 pH—25 °C

9.18 pH—25 °C

9.23 pH—25 °C

10.01 pH—

25 °C

12.45 pH—

25 °C

Note: It is necessary for selected standards to be different by a minimum of 2 pH units. For example, if

1.09 pH is selected for the first standard, the second standard must be different by at least 2 pH.

Standards that do not meet this minimum will show gray on the screen and will not be selectable.

Custom Buffer Custom buffer value.

Range = 2.000 pH to 14.000 pH.

Custom buffer values are not temperature compensated. Custom buffers must be read at

25 °C (77 °C).

No Buffer Select this option for undefined standards.

Change check standard options

1. Make sure that a probe is connected to the meter.

2. Push and select PHC805 Settings.

3. Select Modify Current Settings.

9

4. Select Check Standards Options and update the settings:

Option

Standard

Description

Sets the temperature compensated buffer value for check standard—

• 4.01 pH—25 °C

• 4.65 pH—25 °C

• 6.86 pH—25 °C

• 7.00 pH—25 °C

• 9.18 pH—25 °C

• 9.23 pH—25 °C

• 10.01 pH—25 °C

• 12.45 pH—25 °C

• Custom

Standard

Value

The standard value shows on the Check Standard Options screen.

No temperature compensation for custom buffers.

When the Standard is set to Custom, enter the standard value with the up/down arrow keys.

5. Select Check Standard Reminder and update the settings:

Option Description

Reminder Repeat Sets the time interval for the check standard reminder—Off, 30 minutes,

2 h, 4 h, 8 h, 12 h or 24 h.

Allow Defer

Lets the postponement of check standard reminders—Yes or No.

6. Select Acceptance Criteria and update the settings:

Option

Acceptance Limits

Description

Sets the tolerance limits for check standard—0.005 pH (default) to

1.000 pH.

Cal Expires on Failure Recalibration is necessary if check standard fails—Yes or No.

7. If prompted, enter a name for the new method settings. Other changes made to the settings of an existing method are automatically saved with the same method name.

8. Push EXIT until the meter goes back to the measurement mode.

Maintenance

Clean the probe

Clean the probe when there is contamination on the sensor. Symptoms of contamination are:

• Readings are not accurate or consistent.

• The stabilization time is slow.

• A calibration error occurs.

• Contamination is visible on the probe (e.g., dirt).

1. Rinse the probe with deionized water. Blot dry with a no-lint cloth.

2. Soak the glass bulb of the probe in the applicable cleaning agent. Refer to

Table 3 .

Note: Remove KCl salt build-up from the probe with warm deionized water.

3. Rinse or soak the probe for 1 minute in deionized water.

4. Soak the probe in pH 4 buffer for 20 minutes.

5. Rinse the probe with deionized water.

6. Blot dry with a no-lint cloth.

10

Contaminant

General contaminants

Mineral deposits

Fats, grease and oils

Protein deposits

Inorganic buildup

Table 3 Cleaning agent

Cleaning agent

Electrode cleaning solution

0.1 N HCl solution

Warm, mild detergent solution

Pepsin cleaning solution

EDTA solution

Soak time

12–16 hours

10–15 minutes

2 hours (maximum)

3 hours (maximum)

3 hours (maximum)

Replace the filling solution

Replace the filling solution and KCl crystals (if applicable) when either occurs:

• The filling solution becomes contaminated.

• The KCl crystals in a Red Rod probe no longer move freely through the liquid when the probe is inverted.

1. Use a syringe or small pipette to remove as much filling solution from the probe as possible.

2. For Red Rod probes, if KCl crystals are still in the probe:

a. Fill the probe half full with the filling solution.

b. With a finger over the filling hole, shake the probe until the crystals become loose.

c. If the crystals will not loosen, fill the probe with filling solution. Put the probe into a warm water bath for approximately 10 minutes (up to 60 °C (140 °F)).

d. Do step 1 again.

3. For Red Rod probes, add approximately 0.5 cm (0.2 in.) of KCl crystals to the probe through the filling hole. For measurements at temperatures more than 60 °C (140 °F), more crystals are necessary. Refer to

Preparation for use

on page 2.

4. Fill the probe. Refer to Fill the probe on page 11.

Fill the probe

Add filling solution to the probe when the filling solution level is low (refer to Preparation for use

on page 2) or is replaced (refer to Replace the filling solution on page 11). Refer

to Specifications on page 1 for the applicable filling solution.

1. If the filling hole is closed, remove the filling-hole cap from the filling hole (refer to

Product overview on page 2).

2. Remove the cap from the tip of the filling solution bottle.

3. Hold the bottle so that the tip is down. Put the tip of the bottle in the filling hole.

4. Slowly squeeze the bottle and fully fill the probe.

Note: Fully fill the probe for the best performance.

5. Put the probe into storage if not used immediately (refer to

Storage

on page 11).

6. Keep the filling solution bottle and cap for later use.

Note: If the dispensing tip becomes clogged, remove the dispensing tip and soak the tip in warm water. Fully dry and assemble the tip.

Storage

Short-term and long-term storage

For the best probe performance, do not let the reference junction become dry.

Note: Keep the probe in a sample for a maximum of 2 hours if the sample pH is not too high.

11

1. Put the filling-hole cap in the filling hole (refer to

Product overview on page 2).

2. Rinse the probe with deionized water. Dry the probe with a no-lint cloth.

3. Fill the probe soaker bottle half full with the applicable Storage Solution (refer to

Specifications

on page 1) .

4. Loosen the soaker bottle cap and put the soaker bottle on the probe.

5. Turn the soaker bottle cap clockwise to tighten the soaker bottle cap.

6. Make sure that the solution in the soaker bottle fully covers the glass bulb and the reference junction.

Rehydration

If the glass bulb becomes dry:

1. Soak the probe tip in the 4.01 and 7.00 buffers each for 5 minutes.

2. Rinse the probe with deionized water. Blot dry with a no-lint cloth.

3. Calibrate the probe.

Troubleshooting

Message or symptom

Probe not supported

Possible cause

Software not updated

Action

To download the most current version of the software, refer to the applicable product page on the manufacturer's website.

Refer to the HQd Series meter documentation for more information.

Contact technical support.

Connect a probe or probe requires service pH reading and/or mV reading is same for all solutions

HQd meter does not sense the

IntelliCAL

®

probe

Probe not connected correctly

Software not updated

Large number of methods stored on probe

Damaged probe

Soaker bottle not removed

Electrical issue

Standard not recognized error Soaker bottle not removed

Incorrect buffer or contamination in the buffer solution

Contamination in the filling solution

Disconnect, then connect the probe. Tighten the locking nut.

To download the most current version of the software, refer to the applicable product page on the manufacturer's website.

Refer to the HQd Series meter documentation for more information.

If the probe has a large number of stored methods, more time is necessary for connection. Do not disconnect the probe, continue to let the probe connect.

Make sure that there is connectivity with another probe or meter to confirm isolated issue with probe. Contact technical support.

Remove the soaker bottle.

Contact technical support.

Remove the soaker bottle.

Use fresh buffer solution as specified in the method.

Drain and replace the filling solution with fresh solution.

12

Message or symptom

Slow stabilization time

Calibration errors

Possible cause

Tape not removed from the filling-hole

Contamination in the glass sensor

Contamination in the filling solution

Filling hole closed

Poor contact between reference junction and solution

LIS sample

Low sample temperature or temperature difference between samples

Air bubbles around inner reference electrode

Dehydrated glass bulb

Not sufficient electrolyte flow

1 pH probe too old (membrane degradation)

Calibration not done correctly

Contaminated glass sensor

Slope exceeds the criteria for % of theoretical (as defined in the method slope limit)

Action

Remove the tape.

Clean the probe. Refer to Clean the probe

Drain and replace the filling solution with fresh solution.

Make sure that the filling hole is open and above the solution level.

Shake the probe in the solution from side to side to refresh the reference junction.

Soak the probe in the sample for 10 to 15 minutes before the initial measurement or use a LIS chamber or flowthrough cell.

Examine the sample temperature. The lower the temperature or the higher difference of temperatures between samples, the longer the stabilization time will be.

Carefully tap the probe with hand or shake the probe downward to remove any air bubbles.

Rehydrate the probe. Refer to Storage on page 11.

Open the sleeve junction.

Replace the probe.

Calibrate again with fresh pH buffers.

Clean the probe. Refer to Clean the probe

calibration settings and method.

on page 10.

on page 10.

1.

Adjust the slope limits by changing the PHC805

2.

Calibrate again the probe.

3.

Make a check standard to examine the performance of the probe.

13

Message or symptom

Drifting/Inaccurate readings

Out of range

Out of limits

Temperature out of range

Possible cause

Contaminated glass bulb

CO

2

absorption (for low ionic strength or high purity sample)

Clogged reference

Improper storage conditions/

Dehydrated glass bulb

Measured temperature is out the range of the probe

Check standard temperature value is out of range

Action

Clean the probe. Refer to Clean the probe

on page 10.

Use the LIS chamber for LIS/high purity samples to prevent sample contamination.

Make sure that the filling hole is not covered. Rinse the reference junction holes with deionized water. Carefully tap the probe with hand or shake the probe to remove air bubbles. If there are salt crystals around the junction, soak the electrode tip in a 60 ºC (140 ºF) water bath for

10 minutes.

Clean or condition the probe and calibrate again. The probe can not operate correctly if the probe was left dry

for a long time. Rehydrate the probe. Refer to Storage

on page 11.

Colloidal and/or particulates in the filling solution

Air bubbles around inner reference electrode

Not sufficient electrolyte flow

Not sufficient stirring

1

Replace the filling solution, calibrate and test again.

Carefully tap the probe with hand or shake the probe to remove air bubbles.

Open the sleeve junction.

Stir the standards and samples at a slow and steady rate to prevent the formation of a vortex.

Make sure that the sample is in the range of the probe.

Measurement value is out of range

Check Standard value is out of limits in the current method

Make sure that the standard is in the limits of the current method.

Measurement value is out of measurement limits in the current method

Do another method that expands the acceptable limits.

Make sure that the sample is in the limits of the current method.

Temperature value is out of range

Make a new method with an expanded range.

Make sure that the sample temperature is in the range of the probe.

Make sure that the temperature sensor works correctly.

Make sure that the standard temperature is in the range of the probe.

Make sure that the temperature sensor works correctly.

Make sure that the check standard temperature is in the range of the probe.

1

Only applicable for probes with sleeve junction.

Consumables and accessories

Description

Electrode filling solution, 3 M KCl

Hach electrode storage solution, 3 M KCl

Hach Electrode Cleaning Solution

EDTA standard solution, 0.20N

Soaker bottle

LIS chamber assembly

Quantity

50 mL

500 mL

500 mL

500 mL

1

1

Item Number

2756559

2756549

2965249

102149

5192900

5189900

14

Consumables and accessories (continued)

Description

Color-coded pH standards (buffers)

pH 4.01 ±0.02 at 25 °C (77 °F), 500 mL pH 7.00 ±0.02 at 25 °C (77 °F), 500 mL pH 10.01 ±0.02 at 25 °C (77 °F), 500 mL pH 4.01 ±0.02 at 25 °C (77 °F), 4 L pH 7.00 ±0.02 at 25 °C (77 °F), 4 L pH 10.01 ±0.02 at 25 °C (77 °F), 4 L pH 4.01 ±0.02 at 25 °C (77 °F), 20 L pH 7.00 ±0.02 at 25 °C (77 °F), 20 L pH 10.01 ±0.02 at 25 °C (77 °F), 20 L

IUPAC series certified pH standards (buffers)

1 pH 4.005 ±0.010 at 25 °C (77 °F), 500 mL pH 6.865 ± 0.010 at 25 °C (77 °F), 500 mL pH 7.000 (Radiometer Analytical) ±0.010 at 25 °C (77 °F), 500 mL pH 9.180 ± 0.010 at 25 °C (77 °F), 500 mL pH 10.012 ± 0.010 at 25 °C (77 °F), 500 mL pH 12.45 ± 0.05 at 25 °C (77 °F), 500 mL

Technical grade pH standards (buffers)

pH 4.65 at 25 °C (77 °F), 500 mL pH 9.23 at 25 °C (77 °F), 500 mL

1

Certified standards ship with certificates for traceability to Standard Reference Materials

Quantity

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

Item Number

2283449

2283549

2283649

2283456

2283556

2283656

2283461

2283561

2283661

S11M002

S11M003

S11M004

S11M006

S11M007

S11M008

S11M010

S11M011

15

HACH COMPANY World Headquarters

P.O. Box 389, Loveland, CO 80539-0389 U.S.A.

Tel. (970) 669-3050

(800) 227-4224 (U.S.A. only)

Fax (970) 669-2932 [email protected]

www.hach.com

HACH LANGE GMBH

Willstätterstraße 11

D-40549 Düsseldorf, Germany

Tel. +49 (0) 2 11 52 88-320

Fax +49 (0) 2 11 52 88-210 [email protected]

www.hach-lange.de

HACH LANGE Sàrl

6, route de Compois

1222 Vésenaz

SWITZERLAND

Tel. +41 22 594 6400

Fax +41 22 594 6499

©

Hach Company/Hach Lange GmbH, 2014. All rights reserved. Printed in U.S.A. 01/2014, Edition 1

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Key Features

  • Digital combination glass pH probe
  • Refillable electrolyte
  • Built-in temperature sensor
  • pH range 0 to 14
  • User-selectable stabilization time and resolution
  • ±0.02 pH accuracy
  • Storage solution 3 M KCl
  • Minimum sample depth 18 mm (0.71 in.)
  • Cable length 1 m (3.28 ft)

Frequently Answers and Questions

What is the pH range of the PHC 805 pH probe?
The pH range of the PHC 805 pH probe is 0 to 14.
What is the accuracy of the PHC 805 pH probe?
The accuracy of the PHC 805 pH probe is ±0.02 pH.
What is the minimum sample depth for the PHC 805 pH probe?
The minimum sample depth for the PHC 805 pH probe is 18 mm (0.71 in.)
What is the cable length of the PHC 805 pH probe?
The cable length of the PHC 805 pH probe is 1 m (3.28 ft)

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