Contents - Severn Sales

Contents - Severn Sales
BÜCHI Vacuum Controller V-800/V-805
Contents
Contents
1
Scope of Delivery
2
2
Safety
4
3
Function V-800
3.1 Overview program structure V-800
3.2 General function s
4
4.1
4.2
4.3
7
7
7
8
8.1
8.2
8.3
8.4
8.5
8.6
8.7
8.8
8.9
8.10
8.11
8.12
Operation V-805
Controls V-805
Connections V-805
Fundamental arrangement of the display
General information on the control keys
Manual distillation
Distillation with pressure gradient
Distillation with timer
Automatic distillation
Distillation at constant vapour temperature
Repeating the last distillation performed
Configuration
Memory of methods
24
24
24
25
25
25
27
29
30
31
32
33
34
9
Information on choosing distillation
conditions
36
Putting into operation of V-800
Point of use
Electrical connections
Fixation of the Vacuum Controller to
Rotavapor R-200/R-205
4.4 Installation with water jet pump B-764
4.5 Installation with water jet jump B-767 with
integrated cooling water valve
4.6 Installation with vacuum pump and valve
10
10
10
5
5.1
5.2
5.3
5.4
5.5
5.6
13
13
13
14
14
14
16
10 Control function in connection with
Rotavapor R-200/R-205
38
11 The ventilation valve
39
12 Remote control
39
6
Functions V-805
6.1 Overview of program structure V-805
6.2 General functions
17
17
17
13 Maintenance
40
14 Taking out of operation
43
7
7.1
7.2
7.3
21
21
21
15 Spare parts and accessories
44
16 Annex
48
7.4
7.5
7.6
7.7
Operation V-800
Controls V-800
Connections V-800
Fundamental arrangement of the display
General information on control keys
Manual distillation
Configuration
Putting into operation V-805
Point of use
Electrical connections
Fixation of Vacuum Controller to
Rotavapor R-200/R-205
Instalation of automatic dual temperature sensor
Installation with water jet pump B-764
Installation with water jet pump B-767
Installation with vacuum pump and valve unit
10
11
11
12
21
22
22
23
23
Read these instructions thoroughly before you
use the BÜCHI Vacuum Controller V-800/
V-805. Keep these instructions near the
apparatus, so that they are quickly accessible.
Chapter two contains important safety
instructions. This information is essential as
regards safe operation of the rotary evaporator.
We reserve the right to make technical modifications without
prior notice. No part of these operating instructions can be
reproduced or processed, copied or distributed using electronic or optical systems without permission in writing from BÜCHI
Labortechnik AG.
All rights reserved. © BÜCHI Labortechnik AG, 2000
en, Version H (50 pages)
V-800/V-805 Operating Instructions
Order number
96771
1
BÜCHI Vacuum Controller V-800/V-805
1 Scope of Delivery
1
Scope of Delivery
Base apparatus
V-800 Vacuum Controller
230 V / 50-60Hz
40736
V-800 Vacuum Controller
100/120 V / 50-60Hz
40737
V-805 Vacuum Controller
230 V / 50-60Hz
40738
V-805 Vacuum Controller
100/120 V / 50-60Hz
40739
Standard accessories:
Order number
Photograph of V-805
1 Mains cable
Typ CH
37551
Typ Schuko
37551
Typ GB
37589
Typ AUS
40720
Typ USA
37552
1 Operating instructions
2
German
96770
English
96771
French
96772
Italian
96773
Spanish
96774
BÜCHI Vacuum Controller V-800/V-805
1 Scope of Delivery
Facultative accessories
1 Valve unit
37968
1 Holder for valve unit
on Rotavapor R-200 /205
40810
1 Remote control
40735
1 Communication set to
rotary evaporator R-200/205
40235
Remote control
3
BÜCHI Vacuum Controller V-800/V-805
2 Safety
2
Safety
This apparatus has been built according to state-of-the-art
and recognised safety rules. Still, it can be associated with
risks and hazards:
• If the apparatus is operated by insufficiently trained
personnel;
• If the apparatus is not used properly.
2.1
Symbols
Stop
Information on hazards, which can lead to heavy material
damages, to severe or life-threatening injuries.
Warning
Information on hazards, which can lead to health damages or
to material damages.
Please note
Information, pointing to technical requirements. If these are
not complied with, disturbances, reduced economic efficiency
and product losses can result.
2.2
Requirements placed on operators
This apparatus can only be used by expert personnel or other
persons, who, because of their education or profession are
familiar with hazards, which can arise when this apparatus is
operated.
Personnel lacking this kind of training or persons, still being
trained, require thorough instructions. These operating
instructions are the basis for such training measures.
2.3
Proper use
This apparatus has been designed and built for laboratory uses.
Its proper uses include regulating and displaying vacuum in
working range 0mbar to atmospheric pressure.
The Vacuum Controller is used for:
• Distillation apparatuses, especially rotary evaporators
• Vacuum drying cabinet
4
BÜCHI Vacuum Controller V-800/V-805
2 Safety
2.4
Improper use
Applications not mentioned above are improper. Also,
applications, which do not comply with the technical data are
considered improper. The operator assumes sole risk for any
damages, attributed to such improper use.
Especially the following uses are not permitted:
• Use of the apparatus in rooms, which require protected
apparatuses
• Calibration apparatus for other apparatuses
• Work in excess pressure
2.5
Fundamental hazards
Fundamental hazards are associated with:
• Evacuated apparatuses
• Damaged glassware, which is evacuated
Covers can only be removed with conventional tools by
authorised repair personnel.
Contact with live parts is life threatening!
5
BÜCHI Vacuum Controller V-800/V-805
2 Safety
2.6
Safety measures
You must respect regional and local laws and regulations.
Basically, personal protective equipment such as protective
eye goggles, and protective clothing are to be worn.
These operating instructions must be available for operating
personnel at the point of use of the apparatus as component
of the Vacuum Controller V-800/V-805. This also applies to
additional language versions of these instructions. These
language versions can be ordered separately.
2.7
Modifications
Modifications to the apparatus or to spare parts and
accessories as well as use of other spare parts and
accessories than those mentioned in these operating
instructions are only permitted with the written consent of
Büchi Labortechnik AG.
2.8 Operator’s responsibilities
The operator is responsible for training its personnel. For this
purpose, you can be order these operating instructions in
other languages.
The operator shall inform the manufacturer immediately about
any safety relevant events, occurring during use of the
apparatus.
6
BÜCHI Vacuum Controller V-800/V-805
3 Functions
3
Functions V-800
3.1
Overview program structure V-800
BASIC STATE
MEMORY
MODE
MANUAL
TIMER
RECALL
dP
Choose hysteresis
P Set
Enter Set Point
MENU
RUN
STORE
SERVICE
CONFIGURATION
USER
SETTINGS
DELETE
COMMUNICATION
OFFSET
CALIBRATION
SERVICE
MESSAGE
TEST
Overview program structure V-800
3.2
3.2.1
General functions
Manual distillation
The set point of system pressure is input. When the distillation
starts, the system pressure is reduced to the input value and
kept constant. An input value stays in the memory even when
the apparatus is turned off. Distillation must be stopped
manually.
3.2.2
Distillation with timer function
The set point of system pressure and distillation duration are
input. When the distillation starts, the system pressure is
reduced to the input value and kept constant during the
selected period. At the end of the input distillation period, the
distillation is stopped. If configured accordingly, rotation of the
evaporating flask is stopped and the flask is lifted from the
bath (see 5.6 Configuration).
3.2.3
Working memory
The last module used and associated values remain in the
working memory after the apparatus is turned off and are
automatically recalled when the apparatus is turned on again.
7
BÜCHI Vacuum Controller V-800/V-805
3 Functions
3.2.4
Configuration - Communication
In this menu, you defined whether:
• Whether rotation of the evaporating flask is to start
automatically when the controller starts (only in connection
with Rotavapor R-200/R-205)
• Whether the evaporating flask is to be lowered into the
bath automatically when the controller starts
• Whether the evaporating flask is to be automatically lifted
from the bath when the controller stops
• Whether the apparatus is to be automatically ventilated
when the controller stops.
All of these functions can be turned on and off.
3.2.5
Set point (P Set)
Defines the value, at which the system pressure is kept
constant. An input value stays in the working memory after
the apparatus is turned off and is automatically recalled when
you start the apparatus again.
3.2.6
Hysteresis (dP)
Defines the band width, within which a chosen set point is
kept constant.
3.2.6.1 Manual hysteresis (dP = 500… 1mbar, A)
Example: set point 400 mbar, hysteresis 7 mbar
P
System pressure is reduced to 400 mbar, the vacuum
source is turned off
The system pressure increases to 7 mbar
2
407 mbar
7 mbar
400 mbar
0
0
Manual hysteresis
8
1
3
t
The vacuum source is turned on and the system pressure
is evacuated again to 400 mbar
BÜCHI Vacuum Controller V-800/V-805
3 Functions
3.2.6.2 Automatic hysteresis (dP = A)
The hysteresis is automatically adjusted to the input set point
and is 5 % of the set point, but a minimum of 2 mbar.
Example: set point is 400 mbar, automatic hysteresis
P
The system pressure is reduced to 400 mbar, the vacuum
source is turned off
2+3
420 mbar
20 mbar
400 mbar
0
0
1
The system pressure increases by 20 mbar
The vacuum source is turned on and the system pressure
is evacuated again to 400 mbar
t
Automatic hysteresis
9
BÜCHI Vacuum Controller V-800/V-805
4 Putting into operation
4
Putting into operation of V-800
Look for damages when you unpack the unit. It is important
that you detect any transport damages when you unpack. If
necessary, you must prepare a status report immediately
(informing postal company, railway company or transportation
company).
Keep the original packaging in case the unit needs to be
transported later.
4.1
Point of use
The apparatus is installed directly onto the rotary evaporator
R-200/R-205. If the controller is operated on another rotary
evaporator or apparatus, it is mounted onto a rod.
4.2
Electrical connections
Determine whether the voltage on the socket corresponds to
the voltage given on the apparatus plate.
If the Vacuum Controller is operated in connection with a
Rotavapor R-200/R-205, the controller is connected to the
rotary evaporator. The connection cable is under the cover
plate of the evaporator (see 4.3). In all other cases, connection
is done via the supplied mains cable.
4.3
Screw out screw and pull the cover plate to the back.
Lift the lower spring-loaded catch of the front plate and
remove the front plate.
Connect the display module with the flat belt cable in the
apparatus.
Connect the 2 pole cable with the display module.
Latch display module from the front to the Rotavapor and
insert it on the rear of the plug socket into the foreseen
holder as shown in the picture.
Screw the tower cover back on.
V-800/V-805 with Rotavapor R-200/R-220
10
Fixation of the Vacuum Controller to
Rotavapor R-200/R-205
The holder for the valve unit is fastened to the side of the
tower and valve unit is pushed into it.
BÜCHI Vacuum Controller V-800/V-805
4 Putting into operation
4.4
Installation with water jet pump B-764
Screw on water jet pump together with inserted sealing to
the water tap. Plug cable to valve socket of the controller.
Connect the water jet pump with the rotary evaporator
via the Woulff bottle.
Screw on cooling water valve with sieve and seal to the
water tap. Plug cable to the CW socket of the controller.
Connect cooling water tubing.
V-800/V-805 with Water jet pump B-764
4.5
Installation with water jet pump B-767 with
integrated cooling water valve
Screw on water jet pump with seal to the water tap. Plug
cable to valve socket of the controller.
Connect water jet pump to the rotary evaporator via Woulff
bottle.
Connect cooling water tubing.
V-800/V-805 with water jet pump B-767
11
BÜCHI Vacuum Controller V-800/V-805
4 Putting into operation
4.6
Installation with vacuum pump and valve unit
Connect cable of valve unit with valve socket of the
controller
Connect control cable of the pump with pump socket of
the controller
Connect cable cooling water valve (optional) with CW
socket of the controller
Connect vacuum cover V.Contr. of the valve unit to the
controller
Connect vacuum cover pump of the valve unit to the air
intake fitting of the pump
Connect vacuum cover R1 of the valve unit to the rotary
evaporator
V-800/V-805 with valve unit
12
BÜCHI Vacuum Controller V-800/V-805
5 Operation V-800
5
Operation V-800
Note that the apparatus must be properly put into operation
in accordance with the instructions in Chapter 4, Putting into
operation.
5.1
Controls V-800
Main switch
Function button, activates the respectively assigned
function
Button for permanent vacuum turns pump 100 % on
Stop button
Controls V-800
5.2
Connections V-800
Valve unit or vacuum valve Valve
Cooling water valve CW
Pump Pump
No function
Connection R for Rotavapor R-200/R-205, controls the
function ”Rotation on/off and lowering/raising” of rotary
evaporator
Connection RC for remote control
Vacuum connection
Ventilation valve
Connections V-800
13
BÜCHI Vacuum Controller V-800/V-805
5 Operation V-800
5.3
Fundamental arrangement of the display
Information on active mode
Set point
Operating state
Actual pressure
Selected unit
Graphical pressure display
Illustration of functional buttons
5.4
General information on control keys
The [OK] key closes an input and puts the new value
into the working memory.
[ESC] (Escape) always put you one step backward. Inputs, that have already been changed, but not yet
confirmed with [OK] are ignored.
5.5
5.5.1
Manual distillation
Setting the set point and start
Choose manual mode (if it is not already active)
[MENU]ð[MODE]ð[MANUAL]
Define set point ð[P Set]. You can always use the [é]
key to increase the actual value and [ê] to decrease the
actual value. Press [OK] to confirm value.
Define hysteresis ð[dP]. You can always use the [é]
key to increase the actual value and [ê] to decrease the
actual value. A = Automatic hysteresis. Press [OK] to
confirm value.
Now, the controller is ready. Use RUN to start the controller.
STOP ends the distillation and ventilates the apparatus (unless
you have configured otherwise).
14
BÜCHI Vacuum Controller V-800/V-805
5 Operation V-800
5.5.2
Possible interventions into the regulation
process
[Pé]
Increase the system pressure or interrupt pressure drop in
the start phase. The apparatus goes into the hold mode
and regulates further to the actual value. If necessary, the
apparatus is partially ventilated. [ESC] puts the apparatus
back into the RUN mode with the original set point. [OK]
puts it back into the RUN mode with the new set point.
[Pê]
Reduce system pressure.
The apparatus goes into the hold mode and regulates further to the actual value. [ESC] puts it back into the RUN
mode with the original set point. [OK] puts it into the RUN
mode with the new set point.
[Set] ð [dP]
Change hysteresis.
You can increase the actual value with [é] and reduce it
with [ê]. A = Automatic hysteresis. Confirm desired value
with [OK]. [ESC] puts it back into RUN mode with the
original value.
5.5.3 Choose program
[MENU]ð[MODUS]ð[TIMER]
[PROG]
Define distillation time with the buttons [é] and [ê] confirm
the value with [OK] .
Define working pressure with the buttons [é] and [ê]
confirm the value with [OK] .
5.5.4 Saving a program
Save program (if desired). [OK] is saving the program to
the recommended number, [ESC] is ignores the saving
of the program. In both cases the display changes into
the basic state of the timer function.
Now, the controller is ready. Use [RUN] to start the
controller.
15
BÜCHI Vacuum Controller V-800/V-805
5 Operation V-800
5.5.5
Recall a program from the memory
Recall the program from the memory:
[MENU] ð [MEMORY] ð [RECALL ] ð [OK].
Choose the desired program number and confirm with
[OK] .
The display is changeing into the basic state automatically..
Now, the disired program is in the working memory. Use
[RUN] to start the controller..
5.5.6
Delete a program
Recall the program from the memory:
[MENU] ð [MEMORY] ð [DELETE] ð [OK].
Choose the desired program number and confirm with
[OK] .
Back into the basic state ð [ESC] or delete further
programs according and .
5.6
Configuration
Choose configuration mode [MENU] ð
[CONFIGURATION] ð [USER SETTING]
Use [é] and [ê] to define the parameters.
Confirm desired setting with [OK].
• Language
• Ventilation ON = automatic ventilation in case of Stop
Ventilation OFF = apparatus remains evacuated in case of
stop
• Sound BUTTON ON/OFF
• Sound END ON/OFF
• Contrast: contrast of displays (30 … 100 %)
• Unit = mbar/hPa/Torr
[COMMUNICATION]
• Start rotation ON/OFF: Autostart rotation of evaporating
flask when Controller starts On/Off (only R-200/R-205)
• Stop rotation ON/OFF: Autostop of rotation of evaporating
flask when Controller stops (only R-200/R-205
• Lowering ON/OFF: automatic lowering of the evaporating
flask when the Controller starts (only R-200/R-205)
• Raising ON/OFF: automatic raising of the evaporating flask
from the bath when the controller stops
(only R=200/R-205)
16
BÜCHI Vacuum Controller V-800/V-805
6 Functions V-805
6
Functions V-805
6.1
Overview of program structure V-805
BASIC STATE
MEMORY
MODE
MANUAL
GRADIENT
TIMER
AUTODEST
dP
Choose hysteresis
P Set
Enter Set Point
MENU
RUN
TEMPERATURE
REPEAT
USER SETTING
COMMUNICATION
AUTO. DEST. PARAMETER
RECALL
STORE
SERVICE
CONFIGURATION
AUTO. DEST. CALIBRATION
DELETE
OFFSET
CALIBRATION
SERVICEINDICATION
TEST
Overview program structure V-805
6.2
6.2.1
General functions
Manual distillation
The set point of system pressure is input. When the distillation
starts, the system pressure is reduced to the input value and
kept constant. An input value stays in the memory even when
the apparatus is turned off. Distillation must be stopped
manually.
6.2.2
Distillation with pressure gradients
Programming of a pressure profile from up to 20 segments.
Each segment is defined by start pressure, end pressure and
its duration. At the end of the entire pressure profile, the
distillation is stopped. If so configured, rotation of the
evaporating flask is stopped and the flask is lifted from the
bath.
17
BÜCHI Vacuum Controller V-800/V-805
6 Functions V-805
6.2.3
Distillation with timer function
The set point of system pressure and distillation duration are
input. When the distillation starts, the system pressure is
reduced to the input value and kept constant during the
selected period. At the end of the input distillation time, the
distillation is stopped. If so configured, rotation of the rotary
evaporator is stopped and the flask is lifted from the bath.
6.2.4
AUTODEST function (only with automatic
dual temperature sensor)
Allows full automatic distillation without input of parameters until
dryness, if physically possible. As soon as the evaporating flask
is dry, distillation is stopped. If so configured, rotation of the
evaporating flask is stopped and the flask is lifted from the bath.
6.2.5
The TEMPERATURE function (only with
automatic dual temperature sensor)
Distillation is carried out on the automatically found pressure.
As soon as the vapour temperature drops, distillation is
stopped. If so configured, rotation of the evaporating flask is
stopped and the flask is lifted from the bath.
6.2.6
The REPEAT function
The last, for example, manually performed distillation can be
repeated and stored for later use (learning by doing). This is a
valuable function for difficult distillations, which must be
performed repeatedly, in which the parameters must be
experimentally determined and optimised.
6.2.7
Working memory
The last mode used and associated values are kept in the
working memory after the apparatus is turned off and are
automatically recalled when the apparatus is turned back on.
6.2.8
Memory of methods
Memory for 5 complete distillation programs. Memory
management with the help of conventional functions, Storing,
Retrieving, and Deleting.
18
BÜCHI Vacuum Controller V-800/V-805
6 Functions V-805
6.2.9
Configuration
In this menu, you define:
• Whether the rotation of the evaporator is to automatically
start when the controller starts (only in connection with
Rotavapor R-200/R-205)
• Whether the evaporating flask is to be lowered into the
bath automatically when the controller starts
• Whether the evaporating flask is to be automatically lifted
from the bath when the controller stops
• Whether the apparatus is to be automatically ventilated
when the controller stops.
Further:
• Language
• Sound (Beep)
• Contrast
• Pressure Unit
All of these functions can be turned on and off. Moreover, all
apparatus specific parameters and process parameters can
be defined for the automatic distillations.
6.2.10 Set point (P Set))
Defines the value, at which the system pressure is kept
constant. An input value stays in the working memory after
the apparatus is turned off and is automatically called when
you start the apparatus again.
6.2.11 Hysteresis (dP)
Defines the band width, within which a chosen set point is
kept constant.
6.2.11.1 Manual hysteresis (dP = 500…1mbar, A)
P
Example: set point 400 mbar, hysteresis 7 mbar
System pressure is reduced to 400 mbar, the vacuum
source is turned off
The system pressure increases to 7 mbar
2
407 mbar
7 mbar
400 mbar
0
0
1
3
The vacuum source is turned on and the system pressure
is evacuated again to 400 mbar
t
Manual hysteresis
19
6 Functions V-805
BÜCHI Vacuum Controller V-800/V-805
6.2.11.2 Automatic hysteresis (dP = A)
The hysteresis is automatically adjusted to the input set point
and is 5 % of the set point, but a minimum of 2 mbar.
Example: set point is 400 mbar, automatic hysteresis
P
The system pressure is reduced to 400 mbar, the vacuum
source is turned off
2+3
420 mbar
20 mbar
400 mbar
0
0
Automatic hysteresis
20
The system pressure increases by 20 mbar
The vacuum source is turned on and the system pressure
is evacuated again to 400 mbar
1
t
BÜCHI Vacuum Controller V-800/V-805
7 Putting into operation
7
Putting into operation V-805
Look for damages when you unpack the unit. It is important
that you detect any transport damages when you unpack. If
necessary, you must prepare a status report immediately
(informing postal company, railway company or transportation
company).
7.1
Point of use
The apparatus is installed directly onto the rotary evaporator
R-200/R-205. If the controller is operated in connections with
other apparatuses , it is mounted onto a rod.
7.2
Electrical connections
Determine whether the voltage on the socket corresponds to
the voltage given on the apparatus plate.
If the Vacuum Controller is operated in connection with a
Rotavapor R-200/R-205, the controller is connected to the
rotary evaporator. The connection cable is under the cover
plate of the evaporator (see 7.3). In all other cases, connection
is done via the supplied mains cable.
7.3
Screw out screw and pull the cover plate to the back.
Lift the lower spring-loaded catch of the front plate and
remove the front plate
Connect the display module with the flat belt cable in the
apparatus
Connect the 2 pole cable with the display module.
Latch display module from the front to the Rotavapor and
insert it on the rear of the plug socket into the foreseen
holder as shown in the picture.
Screw the tower cover back on.
Fixation of the Vacuum Controller to
Rotavapor R-200/R-205
The holder for the valve unit is fastened to the side of the
tower and valve unit is pushed into it.
Fixation of the Vacuum Controller to Rotavapor R-200/R-205
21
7 Putting into operation
BÜCHI Vacuum Controller V-800/V-805
7.4
Installation and adjusting of automatic dual
temperature sensor
Insert the long end of the temperature sensor into the
condenser, through the screw neck melted to the top of
the condenser between the inner condenser coil and
centrally melted vacuum tube in the condenser. Position
the sensor, so that it is in the front part of the condenser.
The tip of the sensor is located about at the height of the
highest condenser coil . Tightened screw cap.
Install the short end of the temperature sensor to the cooling
water outlet with the help of the supplied T piece.
Plug temperature sensor into the AS socket of the
controller.
Connect cooling water tubing.
Adjusting (before putting into operation for the first time):
Submerge both sensor tips as far as possible into water of
approximately 30 °C, until all of 3 measuring points are covered by water.
Wait 2 to 3 minutes, and occasionally stir the water.
Adjust the apparatus:
[MENU] ð [CONFIGURATION] ð
[ADJUST CALIBR.] ð [OK]
7.5
Installation with water jet pump B-764
Screw water jet pump together with the seal onto the
water tap. Plug cable to valve socket of the controller.
Connect water jet pump with the rotary evaporator via
the Woulff bottle.
Screw on cooling water valve together with sieve and seal.
Plug cable to CW socket of the controller.
Connect cooling water tubing.
Installation with water jet pump B-764
22
BÜCHI Vacuum Controller V-800/V-805
7 Putting into operation
7.6
Installation with water jet pump B-767
(with integrated cooling water valve)
Screw on water jet pump together with seal to the water
tap. Plug cable to valve socket of the controller.
Connect water jet pump to the rotary evaporator via Woulff
bottle.
Connect cooling water tubing.
Installation with water jet pump B-767 (with integrated cooling water valve)
7.7
Installation with vacuum pump and valve unit
Connect cable of valve unit with valve socket of the
controller
Connect control cable of the pump with pump socket of
the controller
Connect cable cooling water valve (optional) with CW
socket of the controller
Connect vacuum cover V.Contr. of the valve unit to the
controller
Connect vacuum cover pump of the valve unit to the air
intake fitting of the pump
Connect vacuum cover R1 of the valve unit to the rotary
evaporator
Installation with vacuum pump and valve unit
23
8 Operation V-805
BÜCHI Vacuum Controller V-800/V-805
8
Operation V-805
Note that the apparatus must be properly put into operation
in accordance with the instructions in Chapter 7, Putting into
operation.
8.1
Controls V-805
Main switch
Control keys, activating assigned function
Key for permanent vacuum, turns the pump 100 % on
Stop key
Controls V-805
8.2
Connections V-805
24
Connections V-805
Valve unit or vacuum valve Valve
Cooling water valve CW
Pump Pump
Automatic dual temperature sensor AS
Connection R for Rotavapor R-200/R-205, controls the
function ”Turn on rotation and lower flask” of the rotary
evaporator
Connection RC for remote control
Vacuum connection
Ventilation valve
BÜCHI Vacuum Controller V-800/V-805
8 Operation V-805
8.3
Fundamental arrangement of the display
Information on active mode
Set point
Operating state
Actual pressure
Selected unit
Graphical pressure display
Illustration of control keys
8.4
General information on the control keys
The key [OK] closes an input and puts the new value into
the working memory.
The key [ESC] (Escape) always take you one step
backward. Inputs that have already been changed, but
not yet confirmed with [OK] are ignored.
8.5
8.5.1
Manual distillation
Setting set values and start
Choose manual mode (if it is not already active)
[MENU] ð [MODE] ð [MANUAL]
Define set point ð [P Set]. You can always use the key
[é] to increase the actual value and [ê] to decrease the
value. Confirm the desired value with OK.
Define hysteresis ð [dP]. You can always use the key
[é] to increase the actual value and [ê] to decrease the
value. A = Automatic hysteresis. Confirm the desired value
with OK.
Now, the controller is ready. Press RUN to start the controller.
STOP ends the distillation and ventilates the apparatus (if it
has not already been configured).
25
BÜCHI Vacuum Controller V-800/V-805
8 Operation V-805
8.5.2
Possible interventions into the regulating
process
[Pé]
Increase the system pressure or interrupt pressure drop in
the start phase. The apparatus goes into the hold mode
and regulates further to the actual value. If necessary, the
apparatus is partially ventilated. [ESC] the apparatus puts
back into the RUN mode with the original set point. [OK]
it puts back into the RUN mode with the new set point.
[Pê]
Reduce system pressure.
The apparatus goes into the hold mode and regulates further to the actual value. [ESC] puts it back into the RUN
mode with the original set point. [OK] puts it into the RUN
mode with the new set point.
[Set] ð [dP]
Change hysteresis.
You can increase the actual value with [é] and reduce it
with [ê] A = Automatic hysteresis. Confirm desired value
with [OK]. [ESC] puts it back into RUN mode with the
original value.
Installation of the automatic dual temperature sensor (Version V)
26
Transfer manually started distillation to automatic mode. The
distillation is continuously optimised by the automatism, and,
if physically possible, is carried out to dryness. At the end of
distillation, if so configured, rotation of evaporating flask is
stopped and the evaporating flask is lifted from the bath.
BÜCHI Vacuum Controller V-800/V-805
8 Operation V-805
8.6
8.6.1
Distillation with pressure gradient
Setting of the set point and Start,
preparing a new program
Choose gradient mode (if it is not already active)
[MENU]ð[MODE]ð[GRADIENT]ð[PROG]ð[NEW].
The first segment can now be programmed. Each segment
is defined by a start pressure, its end pressure and the
duration.
Define start pressure. Use the [é] key to increase the
value and the [ê] to decrease the value. Confirm desired
value with [OK].
Defines end pressure. Use the [é] key to increase the
value and the [ê] to decrease the value. Confirm desired
value with [OK].
Define duration of segment. Use the [é] key to increase
the value and the [ê] to decrease the value. Confirm
desired value with [OK].
Answer question about program end (Yes/No). Yes ends
the program, No pushes it to the next segment. Use [OK]
to confirm answer..
Store segment, Yes/No. Use [OK] to confirm selection.
Yes stores the values and leads program to next segment
(or ends program), if you answer No, the segment stays in
the display and the values can be corrected by over writing.
Store program (if desired). [OK], the program is stored
under suggested number, [ESC], saving is ignored. In
both cases, the display changes in the basic state for the
gradient course.
Now, the controller is ready and can be started with [RUN].
[SHOW] displays the start width or current program in
graphical representation.
[PROG] shows the start width or current program in graphical
representation.
[STOP] ends distillation and ventilates the apparatus (unless
you have configured otherwise).
27
BÜCHI Vacuum Controller V-800/V-805
8 Operation V-805
8.6.2
Possible interventions in the regulating
process (gradient mode)
Increase the system pressure or interrupt pressure drop in
the start phase ð [Pé]. The apparatus goes into the
hold mode and regulates further to the actual value. If
necessary, the apparatus is partially ventilated. [ESC] it
puts back into the RUN mode with the original set point.
[OK] puts it back into the RUN mode with the new set
point.
Holds program course ð [HOLD]. The apparatus changes
into the hold mode and regulates further to the actual
value.
[GO] sends the apparatus back into the RUN mode and
continues the program.
[SHOW] displays the hold program and the actual time
graphically.
[MAN] changes the apparatus into the manual mode.
8.6.3
Changing an existing program
(gradient mode)
Request the program to be changed from the memory (if
it is not already active) [MENU] ð [MEMORY] ð
[RECALL]. Use [OK] to confirm desired program number.
Choose editing mode [PROG] ð [EDIT]
Change desired value by overwriting as described in
preparing a new program (see 8.6.1).
After you have modified the program, store the program
(see 8.6.1).
28
BÜCHI Vacuum Controller V-800/V-805
8 Operation V-805
8.7
8.7.1
Distillation with timer
Setting the set point and start
Choose timer mode (if it is not already active)
[MENU] ð [MODE] ð [TIMER] ð [PROG]
Define distillation time. Use [é] to increase the actual value
and [ê] to decrease the actual value. Use [OK] to confirm
the desired value.
Define set point. Use [é] to increase the actual value and
[ê] to decrease the actual value. Use [OK] to confirm
the desired value.
Store Program (if desired) [OK]
Now, the controller is ready. Use [RUN] to start the controller.
[STOP] ends the distillation and ventilates the apparatus
(unless you have configured otherwise).
8.7.2
Possible interventions into the regulating
process
Increase the system pressure or interrupt pressure drop in
the start phase ð [Pé]. The apparatus goes into the
hold mode and regulates back to the actual value. If
necessary, the apparatus is partially ventilated. [ESC] it
puts back into the RUN mode with the original set point.
[OK] puts its back into the RUN mode with the new set
point.
Reduce system pressure ð [P Set] ð [Pê]. The
apparatus goes into the hold mode and regulates further
to the actual value. If necessary, the apparatus is partly
ventilated. [ESC] it puts back into the RUN mode with
the original set point. [OK] puts its back into the RUN
mode with the new set point.
Change hysteresis ð [dP]. Use [é] to increase the actual
value and [ê] to decrease the actual value. A = Automatic
hysteresis. Confirm desired value with [OK]. [ESC] puts
it back into RUN mode with the original value.
Changes into the manual mode ð [Man]. The timer
function is turned off.
29
BÜCHI Vacuum Controller V-800/V-805
8 Operation V-805
8.8
8.8.1
Automatic distillation (only with connected
auto sensor)
Preconditions for an automatic distillation
The automatic dual temperature sensor is based on a balance
adjustment of the temperature in the condenser with
consideration of the cooling material temperature. For troublefree distillation until dryness, the following conditions must exist:
• minimum solvent quantity 50 … 100 ml.
• Boiling point differences in the case of solvent mixtures is
not greater than 45…50°C. Greater differences lead to
back evaporation from the receiving flask and stopping of
the apparatus.
• Temperature difference between heating bath and cooling
35…45°C.
It is difficult to evaporate solvent mixtures with very large boiling
point and/or evaporation heat difference in automatic mode.
This includes many aqueous solvent mixtures.
You cannot add anything to the evaporating flask in the
automatic mode. To do this, the controller must be changed
into the manual mode, the material added to the evaporating
flask and then the apparatus must be changed back into the
automatic mode.
8.8.2
Performing automatic distillation
Choose the autodist function [MENU] ð [MODE] ð
[AUTODEST.] (if it is not already active). The display changes
to the READY state. You do not have to input any other
parameters.
Now, the controller is ready. Use [RUN] to start it.
[STOP] ends the distillation and ventilates the apparatus
(unless configured otherwise).
30
BÜCHI Vacuum Controller V-800/V-805
8 Operation V-805
8.8.3
Possible interventions into the regulating
process
Increase the system pressure or interrupt pressure drop in
the start phase ð [Pé]. he apparatus goes into the hold
mode and regulates further to the actual value. If necessary,
the apparatus is partially ventilated. [ESC] puts back into
the RUN mode with the original set point. [OK] puts back
into the RUN mode with the new set point. Use [AUTO]
to put distillation back into the automatic mode.
Change into the manual mode ð [MAN]. Now, distillation
can be continued manually (for example, if the distillation is
too slow). You can change back to the automatic mode
at any time.
8.9
8.9.1
Distillation at constant vapour temperature
(Mode TEMPERATURE)
Performing temperature distillation
Choose the temperature mode (if it is not already active)
[MENU] ð[MODE] ð[TEMPERATURE]
Now, the controller is ready and you can use [RUN] to start it.
[STOP] ends the distillation and ventilates the apparatus
(unless configured otherwise).
31
BÜCHI Vacuum Controller V-800/V-805
8 Operation V-805
8.9.2
Possible interventions into the regulating
process
Increase the system pressure or interrupt pressure drop in
the start phase ð[Pé]. The apparatus goes into the hold
mode and regulates further to the actual value. If necessary,
the apparatus is partially ventilated. [ESC] puts back into
the manual RUN mode with the original set point.
[OK] puts back into the manual RUN mode with the new
set point. Use [AUTO] to put distillation back into the
automatic mode.
Change into the manual mode ð[MAN]. Now, distillation
can be continued manually.
8.10 Repeating the last distillation performed
The last manual distillation performed is automatically saved
in active working memory.
8.10.1 Performing the distillation
Choose repeat mode [MENU] ð[MODE] ð[REPEAT]
ð[OK].
The display automatically goes into the basic state of the
repeat function.
Now, the controller is ready and you can use [RUN] to start
it.
[SHOW] displays the pressure course graphically.
[STOP] ends the distillation and ventilates the apparatus
(unless configured otherwise).
The program can be saved from the basic state for applications
later: [MENU] ð [MEMORY] ð [STORE] ð [OK] (program
is saved as gradient).
32
BÜCHI Vacuum Controller V-800/V-805
8 Operation V-805
8.10.2 Possible interventions into the regulating
process
Increase the system pressure or interrupt pressure drop in
the start phase ð [Pé]. he apparatus goes into the hold
mode and regulates further to the actual value. If necessary,
the apparatus is partially ventilated. [ESC] puts back into
the RUN mode with the original set point. [OK] puts back
into the RUN mode with the new set point. Use [AUTO]
to put distillation back into the automatic mode.
Change into the manual mode ð [MAN]. Now, distillation
can be continued manually
[SHOW] displays the pressure profile and the momentary
time graphically. [ESC] puts the system back into the
normal RUN display.
8.11 Configuration
Choose configuration mode [MENU] ð
[CONFIGURATION] ð [USER SETTING]
Use [é] and [ê] to define the parameters.
Confirm desired setting with [OK].
• Language
• Ventilation ON = automatic ventilation in case of Stop
• Ventilation OFF = apparatus remains evacuated in case of
stop
• Sound BUTTON ON/OFF = Buzzer On/Off
• Sound END ON/OFF = Buzzer On/Off
• Contrast: contrast of displays (30 … 100 %)
[COMMUNICATION]
• Start rotation ON/OFF: Autostart rotation of evaporating
flask when Controller starts On/Off (only R-200/R-205)
• Stop rotation ON/OFF: Autostop of rotation of evaporating
flask when Controller stops (only R-200/R-205
• Lowering ON/OFF: automatic lowering of the evaporating
flask when the Controller starts (only R-200/R-205)
• Raising ON/OFF: automatic raising of the evaporating flask
from the bath when the controller stops
(only R=200/R-205)
• Unit = mbar/hPa/Torr
33
8 Operation V-805
BÜCHI Vacuum Controller V-800/V-805
8.12 Method memory
8.12.1 General information
Gradient programs and time programs can be saved in the
methods memory. Manual distillation can only be saved via the
repeat function. The save function . The save function includes
conventional functions like saving, opening and deleting.
8.12.2 Saving programs
Normally, you save gradient, time and temperature programs
immediately after you have prepared them. You are prompted
to do so automatically. However, you can also save a program from the working memory into the methods memory
later. Proceed as follows:
Program is in the working memory (basic state in the
display)
Call up save function
[MENU] ð [MEMORY] ð [STORE] ð [OK].
Confirm save ð [OK]
Back to the basis state ð [ESC]
8.12.3 Retrieving a program from the memory
Retrieve save function
[MENU] ð [MEMORY] ð [RECALL] ð [OK].
Choose desired program number and use [OK] to confirm.
The display automatically changes to the basis state.
Now, the desired program is in the working memory and you
can use [RUN] to start it.
34
BÜCHI Vacuum Controller V-800/V-805
8 Operation V-805
8.12.4 Deleting a program from the memory
Call up memory function
[MENU] ð [MEMORY] ð [DELETE] ð [OK].
Choose desired program number and confirm with [OK].
Back to basis state ð [ESC] or other program according
to or delete.
35
BÜCHI Vacuum Controller V-800/V-805
9 Distillation conditions
9
Information on choosing
distillation conditions
To achieve optimum distillation conditions when rotary
evaporators are used, the energy, supplied for distillation from
the heating bath, must be removed via the condenser. To
guarantee this, operations should be performed according to
this rule of thumb.
∆T2 (min. 20°C)
∆T
1
(mi
n. 2
0°C
Cooling water
max. 20°C
)
Vapour
40°C
Bath
60°C
How can you achieve these conditions?
• Set the bath temperature to 60 °C
• Set cooling water, temperature no higher than 20°C
• Allow cooling water to flow through the condenser at
approximately 40 – 50 l/h
• The working vacuum is to be chosen, so that the boiling
point of the solvent is 40 °C. You can get the corresponding
pressure from the Solvent Table (next page).
Advantages associated with 60 °C bath temperature:
45: “20-40-60”
• The evaporating flask can be replaced without risk of
scalding.
• The evaporation rate of the water from the heating bath is
not very high (energy loss).
• The heating bath energy is employed at a good degree of
efficiency.
This rule can also be applied to lower bath temperatures, for
example:
Cooling water
max. 0°C
Vapour
20°C
Bath
40°C
Optimising distillation:
Depending on distilled solvent, distillation may have to be
optimised again. However, before you optimise distillation again,
the heating bath must have reached 60 °C.
/
/
2
3
2
3
The following applies: condensation of solvent should be 2/3
to 3/4 of the existing condenser coil.
There are basically two possibilities for optimising distillation:
1. Slowly reduce pressure again
Bath must have reached 60 °C (Boiling point is reduced,
increase of ∆T1, resulting in increase of distillation capacity) or
2. increasing bath temperature
(Increase of ∆T1, resulting in increase of distillation capacity).
By increasing the bath temperature, not all of the additional
energy is supplied to distillation, but more is also discharged
into the environment. This is due to the increase temperature
difference between bath and environmental temperature.
Condensation range
36
BÜCHI Vacuum Controller V-800/V-805
9 Distillation conditions
Solvent table
Solvent
Formula
Molar Mass
in g/mol
Evaporation
energy in J/g
Boiling point
at 1013 mbar
Density
in g/cm3
Vacuum in mbar for
boiling point at 40°C
Acetone
C3H6O
58.1
553
56
0.790
556
n-amylalcohol, n-pentanol
C5H12O
88.1
595
37
0.814
11
C6H6
78.1
548
80
0.877
236
n-butanol, tert.butanol
C4H10O
74.1
620
118
0.810
25
(2-methyl-2-propanol)
C4H10O
74.1
590
82
0.789
130
Chlorobenzene
C6H5Cl
112.6
377
132
1.106
36
Chloroform
CHCl3
119.4
264
62
1.483
474
Cyclohexane
C6H12
84.0
389
81
0.779
235
Diethylether
C4H10O
74.0
389
35
0.714
Atmospheric
1,2-dichloroethane
C2H4Cl2
99.0
335
84
1.235
210
1,2-dichloroethylene (cis)
C2H2Cl2
97.0
322
60
1.284
479
1,2-dichloroethylene (trans)
C2H2Cl2
97.0
314
48
1.257
751
Diisopropyl ether
C6H14O
102.0
318
68
0.724
375
Dioxane
C4H8O2
88.1
406
101
1.034
107
DMF (dimethyl-formamide)
C3H7NO
73.1
153
0.949
11
Acetic acid
C2H4O2
60.0
695
118
1.049
44
Ethanol
C2H6O
46.0
879
79
0.789
175
Benzene
Ethylacetate
C4H8O2
88.1
394
77
0.900
240
Heptane
C7H16
100.2
373
98
0.684
120
Hexane
C6H14
86.2
368
69
0.660
335
Isopropylalcohol
C3H8O
60.1
699
82
0.786
137
3-methyl-1- butanol
C5H12O
88.1
595
129
0.809
14
Methylethylketone
C4H8O
72.1
473
80
0.805
243
Methanol
CH4O
32.0
1227
65
0.791
337
CH2Cl2
84.9
373
40
1.327
Atmospheric
Pentane
C5H12
72.1
381
36
0.626
Atmospheric
n-propylalcohol
C3H8O
60.1
787
97
0.804
67
Pentachloroethane
C2HCl5
202.3
201
162
1.680
13
C2H2Cl4
167.9
247
146
1.595
35
Isoamylalcohol,
Methylene chloride,
dichloromethane
1,1,2,2-tetra-chloroethane
Tetrachlorocarbon
CCl4
153.8
226
77
1.594
271
1,1,1-trichloroethane
C2H3Cl3
133.4
251
74
1.339
300
Tetra-chloro-ethylene
C2Cl4
165.8
234
121
1.623
53
THF (tetrahydrofurane)
C4H8O
72.1
67
0.889
357
C7H8
92.2
427
111
0.867
77
C2HCl3
131.3
264
87
1.464
183
100
1.000
72
Toluene
Trichloroethylene
Water
H2O
18.0
2261
Xylene (mixture)
C8H10
106.2
389
0-xylene
C8H10
106.2
144
0.880
25
m-xylene
C8H10
106.2
139
0.864
p-xylene
C8H10
106.2
138
0.861
37
10 Control function with R-200/R-205
BÜCHI Vacuum Controller V-800/V-805
10 Control function in connection
with Rotavapor R-200/R-205
10.1 Start of rotation
The Vacuum Controller V-800/V-805 makes it possible to
automatically start rotation of the evaporating flask. This
function is activated and deactivated in the configuration menu.
The rotation speed corresponds to the respective rotary button
setting of the rotary evaporator. In spite of the activated
autostart function, you can also rotate the evaporating flask
at any time without start of controller. For this purpose, you
simply turn slightly on the respective regulating button of the
evaporator.
Configuration possibility: start rotation On/Off
10.2 Stop rotation
If the function is activated, when the controller stops, rotation
of the evaporating flask is automatically stopped. This function
is turned on and off in the configuration menu.
Configuration possibility: Stop rotation On/Off
10.3 Automatic lowering of the evaporating flask
When configured accordingly, when the controller starts, the
evaporating flask is automatically lowered into the bath. It is
essential that the lower end catch is correctly set in the quickaction jack of the rotary evaporator. Hand operation of the
quick-action jack is already priority effective.
Configuration possibility: Lowering ON/OFF
10.4 Automatic raising of the evaporating flask
This function is also only active when configured accordingly.
When the controller stops, the evaporating flask is automatically
lifted from the heating bath to the upper end catch. Hand
operation of the quick-action jack is always priority active.
Configuration possibility: Lifting ON/OFF
38
BÜCHI Vacuum Controller V-800/V-805
11 Ventilation valve/12 Remote control
11 The ventilation valve
Automatic ventilation
With standard configuration ex factory, when the controller
stops, the connected apparatus is ventilated immediately and
the valve remains open even after the apparatus has been
turned off. As a result, accidental excess pressure situations
are avoided.
However, you can also configure the controller so that hen
the system stops the apparatus is not ventilated. In this case,
you must puss on the Stop key again to ventilate the apparatus.
Attention: Excess pressure situations can arise when the second operating mode is used. Thus, always remove the
evaporating flask immediately and drain receiving flask!
Configuration possibility: ventilation ON/OFF
12 Remote control
(optional accessory)
Plug remote control to connection RC. Now, remote control
is ready and when the Vacuum Controller is turned on, you
can use it to control all controller functions. The function keys
F1 to F4 correspond to the menu driven keys (visual contact
with Vacuum Controller is precondition).
You can also operate the apparatus even if the remote control
is connected to the Vacuum Controller.
Remote control (optional accessory)
39
BÜCHI Vacuum Controller V-800/V-805
13 Maintenance
13 Maintenance
You must observe all instructions, aimed at keeping the
Rotavapor functional. This includes periodically cleaning and
checking for damages.
13.1 Cleaning
Attention: Before cleaning, make sure that the apparatus is
unplugged from the current mains.
Housing
Use a moist cloth to clean the housing. Never use solvents as
cleaning agents. Check the housing for defects (controls, plugs).
13.2 Functional test
Test the following functions after each intervention or in regular
intervals during the year:
Turn on apparatus: display shows the basis state of the
last distillation. If the connected apparatus is ventilated,
the device shows the actual atmospheric pressure.
Press RUN: ventilation valve turns on and can be heard,
pump runs, vacuum valve opens, display shows RUN mode.
Stop apparatus: ventilation valve switches in an way that
can be heard (if ventilation OFF is configured, the valve
only switched when you press the STOP key a second
time), pump stops, vacuum valve closes, display changes
to the basic mode.
13.3 Water jet pump
The water jet pump is equipped with a low-impact valve.
Diaphragms built into such valves have a small opening, which,
for example, can be clogged by furring or dirt. In such cases,
the valve no longer closely completely.
Water jet pump
40
Screw off valve coil
Remove diaphragm
Push needle through opening 0.5 mm
Needle
Reassemble the valve.
BÜCHI Vacuum Controller V-800/V-805
13 Maintenance
13.4 Customer service
Only authorised service personnel can perform work on or in
the apparatus. These persons have a comprehensive technical
training and knowledge about hazards, resulting when safety
stipulations are not complied with. BÜCHI Customer Service
Office have apparatus specific Service Manual, which can
only be obtained by authorised personnel.
Addresses of official BÜCHI Customer Service Offices are given
on the last page of these operating instructions. If your
apparatus malfunctions or you have technical questions or
application problems, contact one of these offices.
BÜCHI Customer Service offers the following services:
• Spare parts
• Repairs
• Maintenance
• Technical advise.
13.5 Error messages on Vacuum Controller
SW Version 1.02:
Error—1
Error—2
Pressure sensor not calibrated
RAM (battery suppeorted) not initilized
Error—3
Automatic distillation wrong/leak is
too high
(only 805)
Error—4
Automatic temperature sensor defective
or not connected
(only 805)
Pressure sensor defective
Error—5
Call customer service
Call customer service
Call customer service
41
BÜCHI Vacuum Controller V-800/V-805
13 Maintenance
13.6 Troubleshooting
Malfunction
Possible cause
Remedy
No display
No current to apparatus
Turn mains switch on
Check mains connections
Frequent switching of valve or pump
System is untight
Control all sealing points (tubes and
their connections)
Choose larger hysteresis (if end
vacuum is greater than 700 mbar, set
to automatic hysteresis)
Hysteresis is too small
Valve does not switch
Valve does not close
Valve coil is dirty
Valve cable is not plugged in
No vacuum
Tubing incorrec
Incorrectly cabled
See Chapter 4, Installation
See 5.1 Controls
Vacuum is not reached
Back evaporation Rotavapor
Water pressure to water jet pump is
too low
Empty receiving flask
Completely open water tap
Auto distillation has ”abated”
Manually decrease pressure until the distillation starts again, then, if so desired,
return to the automatic function.
Distillation has ended
despite not dried out completely
a) Back evaporation from the receiving flask is too strong (especially
solvent mixtures), drain receiving flask and start distillation again
b) Malfunction in distillation procedure is not exactly defined (for example,
sudden cooling, heat flow is too low, etc.). Decrease pressure manually until
the distillation starts again, then return to automatic function (V-805)
Rest moisture is too high after
auto distillation
Control to end dryness by manually decreasing pressure of product
42
BÜCHI Vacuum Controller V-800/V-805
14 Taking out of operation
14 Taking out of operation
You must remove dangerous substances and thoroughly clean
the apparatus. As a result, people will not be injured from
contact with dangerous substances.
14.1 Storage/transportation
Clean the apparatus thoroughly. Residues of chemicals must
be removed completely and glass components must be
cleaned.
Keep and transport the apparatus in its original packaging..
14.2 Disposal
So that the apparatus can be disposed of in an environmentally
friendly manner, there is a list of materials used in Chapter 13,
Annex. This helps to ensure that the components are
separated and recycled.
Please observe valid regional and local laws concerning
disposal.
43
BÜCHI Vacuum Controller V-800/V-805
15 Spare parts and accessories
15 Spare parts and accessories
Only BÜCHI original accessories and spare parts guarantee
safety and that the apparatus functions correctly. You can
only use spare parts and accessories from other companies if
BÜCHI consents. During assembling and disassembling the
general safety rules and Chapters 4 and 7 are to be respected.
Before placing the apparatus into operation, check to make
sure that it operates correctly according to Chapter 11.2
Manufacturing according to this Manual is prohibited.
Copyright remains at Büchi AG.
15.1 Spare parts
Name
Hose nipple GL 14 complete, 4 pieces
Order number
37287
Table 7: Spare parts hose nipple
Hose nipple GL14 complete
15.2 Accessory
Name
15860
Order number
Water jet pump B-764
31358
Set with 5 sieves and 10 seals
15860
Kalrez PP membrane
23347
Set of four O rings
37607
Table 8: Accessory B-764
23347
Water jet pump for creating vacuum.
Is controlled via the V-805. When the set vacuum is reached,
this water jet pump turns off and, thus, saves up to 400 l
water/h.
The integrated backstroke valve prevents back suction of water
into the system.
Water jet pump B-764
44
BÜCHI Vacuum Controller V-800/V-805
15 Spare parts and accessories
Name
15860
03560
23347
Order number
Water jet pump B-767
31357
Set with 5 sieves and 10 seals
15860
Kalrez PP membrane
23347
Set of four O rings
37607
Table 9: Accessory B-767
Just like B-764, B-767 is also equipped with a cooling water
valve, thus, you need only one water connection for vacuum
and cooling water.
Water jet pump B-767
Name
15860
Order number
Cooling water valve
31356
Set with five sieves and 10 seals
15860
Table 10: Accessory cooling water valve
The Vacuum Controller controls this cooling water valve. It
opens it only when cooling water is needed. This also helps to
save water and reduce control efforts.
Cooling water valve
Name
Order number
In line valve 24 VDC
Ø 2,4 mm to 1 litre Rotavapor
(with 00394 Y-piece)
31353
Ø 4 mm to 20 litre Rotavapor
31354
Ø 4 mm to 50 litre Rotavapor
31355
Table 11: Accessory in line valve
The in line valve is used in connection with in-house vacuum
systems or continuous operating vacuum pumps. It controls
opening and closing of the vacuum line.
In line valve to 1 litre Rotavapor
45
BÜCHI Vacuum Controller V-800/V-805
15 Spare parts and accessories
Name
Order number
Valve unit, complete
37968
The valve unit combines the function of the Woulff bottle with
that of the vacuum valve.
Valve unit, complete
Name
Order number
Automatic dual temperature sensor
Complete for glass assemblies V and S
(including T piece, only for V-805)
40741
Table 12: ZAccessory automatic dual temperature sensor
For automatic distillation (only V-805).
Automatic dual temperature sensors
Name
Glass T piece complete
For automatic distillation (only V-805).
T-piece
46
Order number
37751
BÜCHI Vacuum Controller V-800/V-805
15 Spare parts and accessories
Name
15860
Order number
Water control valve ½” complete
(01308 + 03560 + 15860)
11606
Set with 5 sieves and 10 seals
15860
Water control valve, complete
Name
Order number
Vacuum tube 16/6 mm
17622
Nylex tube 14 x 8
(alternative to 17622)
04113
Vacuum tube
Name
Woulff bottle, complete
Order number
25519
Woulff bottle
47
BÜCHI Vacuum Controller V-800/V-805
16 Annex
16 Annex
16.1 Technical data
V-800 / V-805
Dimensions casing (W x L x D)
110 x110 x 70 mm
Weight
0.9 kg
Electrical supply
230 V / 50/60 Hz
100 - 120 V / 50/60 Hz
Power consumption
16 W
Ambient conditions
for indoor use only, altitude up to 2000 m, 5 - 40 °C
maximum relativ humidity 80% for temperatures up to 30°C
Magnetic valve supply
24V
Regulating range
1 mbar/torr to atmospheric pressure
Max regulating range deviation
+/- 0.5% f.s.
Display range
0 - 1400 mbar
Hysteresis
Automatic or 1 – 500 mbar
Installation category
II
Pollution degree
2
16.2 Materials used
Component
Material
Abbreviation
Pressure foil
Polyester
PES
Casing
Polybutylterephthalate
PBT
Printed board
Glass fibre reinforced epoxi resin
Cable
Polyvinyl chloride
48
PVC
BÜCHI Vacuum Controller V-800/V-805
16 Annex
16.3 Declaration of conformity
We,
BÜCHI Labortechnik AG
Postfach, CH-9230 Flawil, Switzerland
Declare, solely under our responsibility, that the product:
BÜCHI Vacuum Controller V-800/V-805
On which this declaration is based, complies with the following standards:
EN 61326-1: 1997
Electrical equipment for measurement technique, control and laboratory use
EMC requirements
EN 55011:1991/B (~VDE 0875/B, VDE 0871/B)
Limit values and measuring methods for interference of industrial, scientific and medical high frequency instruments
EN 61000-3-2: 1995/1996
Limits for harmonic current emissions
EN 61000-3-3: 1995
Limitation of voltage fluctuations and flicker
In accordance with specifications of the EU Directive:
73/23/EEC (Electrical equipment/low voltage directive)
89/336/EEC (Electromagnetic compatibility)
Flawil, 16.01.2001
BÜCHI Labortechnik AG
Meierseggstrasse 40
9230 Flawil
Schweiz
Tel +41 (0)71 394 63 63
Fax +41 (0)71 394 65 65
[email protected]
www.buchi.com
Guido Worch
Qualitymanager
49
16 Annex
BÜCHI Vacuum Controller V-800/V-805
16.4. FCC Deklaration
English:
This equipment has been tested and found to comply with the limits for a Class A digital device, pusuant to both Part 15 of
the FCC Rules and the radio interference regulations of the Canadian Department of Communications. These limits are
designed to provide reasonable protection against harmful interference when the equipment is operated in a commercial
environment.
This equipment generates, uses and can radiate radio frequency energy and, if not installed and used in accordance with
the instruction manual, may cause harmful interference to radio communications. Operation of this equipment in a residential
area is like to cause harmful interference in which case the user will be required to correct the interference at his own
expense.
Français:
Cet appareil a été testé et s'est avéré conforme aux limites prévues pour les appareils numériques de classe A et à la partie
15 des règlementation FCC à la règlementation des radio-interférences du Canadian Department of communications. Ces
limites sont destinées à fournir une protection odéquate contre les interférences nétastes lorsque l'appareil est utilisé dans
un environnement commercial.
Cet appareil génère, utilise et peut radier une énergie à fréquence radioélectrique, il est en outre susceprible d'engendrer
des interferences avec les communications radio, s'il n'est pas installé et utilisé conformément aux instructions du mode
d'emploi. L'utilisation de cet appareil dans les zones résidentielles peut causer des interférences nèfastes, auquel cas
l'exploitant sera amené à prendre les dispositions utiles pour polier aux interférences à ses propres frais.
50
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