Peak Scientific NM32LA Nitrogen Generator

Peak Scientific NM32LA Nitrogen Generator
NM32LA
Product Information Package
2010 Copyright Peak Scientific - Rev. 313/08/2010
peakscientific.com
NM32LA PIP
Introduction
This is the Product Information Package (PIP) for Peak Scientific Instruments’ NM32LA
Nitrogen Generator specifically designed to provide gas to LCMS Applications as
produced by most LCMS Manufacturers.
With this guide to the NM32LA we hope to provide you with a better understanding of
this Nitrogen generator model both from a sales and from a technical point of view.
The PIP- NM32LA will provide you with detailed information on:
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Though we anticipate for this PIP to be a full guide on the NM32LA we will appreciate
any feedback in terms of inclusion of other items and/ or information that will be useful
to any of our representatives in the field.
To submit feedback, please address any comments to your account manager, who
will pass the information to Peak Scientific’s Marketing Department or contact the
Marketing Department directly through [email protected]
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NM32LA PIP
Product Description
The ‘NM32LA’ Nitrogen Generator has been specifically designed to operate LCMS
manufactured by Waters Corporation, Thermo Fisher Scientific, Agilent Technologies,
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Extensively tested under supervision of Peak and LCMS Manufacturers, the ‘NM32LA’
has been approved to supply Nitrogen to their LCMS Applications.
The ‘NM32LA’ generates Nitrogen through the application of ‘Membrane Technology’.
Nitrogen membranes separate gases by the principle of selective permeation across
the nitrogen membrane wall. “Fast” gases permeate through the nitrogen membrane
wall more readily than “slow” gases, thus separating the original gas mixture into 2
streams. The purity of the desired streams can be adjusted depending on operating
conditions.
Internal air compressors further make the ‘NM32LA’ a stand- alone, self- sufficient
Nitrogen Generator, independent from external air sources.
Features & Benefits
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Peak Scientific has more than 10 years of experience in the development, production and
service of laboratory gas generators
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More cost effective than gas bottles or cylinders
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Easy to fit into your laboratory environment
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No more worries about running out of gas
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Extensively tested to ensure reliability and longevity of generator
Every generator is tested to its specifications before despatch from factory
Electronic Control System facilitates compressor cycling, resulting in longer compressor
life
Indicators for Preventative Compressor Maintenance ensure maximum uptime
Alarm function aids fault finding and prevents unnecessary downtime
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A variety of preventative maintenance plans are available from Peak Scientific
Easy access to a network of authorized partners and Peak Global Support
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NM32LA PIP
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NM32LA
Minimum Operating Ambient Temperature
5°C/ 41°F
Maximum Operating Ambient Temperature
30°C/ 86°F
Maximum relative Humidity
70%
Maximum Altitude
2,000 meters
Outlet Gas - Nitrogen Maximum Flow Rate
32L/min (1.13cfm)
Outlet Gas - Nitrogen Maximum Outlet Pressure
6.90 bar/ 100 psi
Particles
< 0.1 μm
Phthalates
None
Suspended Liquids
None
Outlet 1/4” BSP
1
Pressure Gauges
1
Start Up Time
30 minutes
Noise Level
54 dBA @ 1m
Electrical Requirements
230v ± 10%, 50/ 60 Hz, 7A
Compressors
2-Pole 6A - D curve
Fans & Controls
2- Pole 4A - C curve
Electrical Connection
Single Phase Power Cord
Dimensions WxDxH (cm/ inches)
60 x 75 x 71.2 / 23.6 x 29.5 x 28
Weight
95kg / 209lb
Shipping Weight
120kg / 264lb
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NM32LA PIP
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‘NM32LA’ was developed to provide a reliable source of nitrogen in the laboratory.
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noise, low vibration solution for the laboratory without emitting excess heat.
Nitrogen is generated from ambient air. The internal air compressors feed the air
through a nitrogen membrane which separates gases by the principle of selective
permeation across the nitrogen membranes wall. For nitrogen polymeric membranes,
the rate of permeation of each gas is determined by its solubility in the nitrogen
membrane material, and the rate of diffusion through the molecular free volume in the
nitrogen membrane wall. Gases that exhibit high solubility in the nitrogen membranes,
and gases that are small in molecular size, permeate faster than larger, less soluble
gases.
‘Fast’ gases permeate through the membrane wall more readily than ‘slow’ gases, thus
separating the original gas mixture into two streams. With nitrogen being a slow gas,
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permeate through the membrane wall and are vented back to atmosphere.
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end user.
However, Peak Scientific and their local representatives offer installation of their
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is generally recommended and is highly advisable where the generator is not to be
installed adjacent to the LCMS Application.
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The ‘NM32LA’ generator is designed for indoor use only and should only be installed
adjacent to the Mass Spectrometer it is supplying. If this is not convenient then the unit
can be sited elsewhere, however, consideration should be given to the lengths of pipe
runs as pressure drops can result from extended runs of pipe.
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by ambient conditions. Continuous operation in ambient temperatures exceeding
30˚C will shorten the life of the internal air compressors and affect the generator’s
performance.
Note should also be taken to the proximity of Air Conditioning outlets. These can
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‘NM32LA’ within such pockets could also adversely affect its performance.
Please ensure sufficient air flow around the unit. It is recommended that an air gap of
75mm (3”) should be maintained down both sides, at the rear and across the top of the
unit.
The unit must always be placed on a level surface. Failure to do so will affect the
performance of the generator.
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With the ‘NM32LA’ installed, disconnect the outlet port from the instrument (ensuring
that any internal pressure has been safely dissipated) and switch generator on. The
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the tubing to the output ports on the rear of the generator.
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NM32LA PIP
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1.
2.
3.
4.
Fans at the rear of the generator will start after 3 seconds
Solenoid valve will energise to vent any residual pressure from the compressor
heads after 2 seconds
Compressor No 1 will start after 1 second
Compressor No 2 will start after a further second
The total time for start up is 7 seconds.
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internal storage tanks. This can be monitored by watching the output pressure gauge
on the front panel climb. This will climb to the factory set pressure as noted in the
generator specifications.
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tank upper pressure limits is reached and the compressor has run for a period of 3
minutes (or more).
The compressors will then rest until the internal tank lower pressure limit is reached.
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cycling is normal and will continue throughout the operation of the Generator.
When the system has been operated for a period of 30 minutes, all the internal pipework and storage tanks will have been purged with clean Nitrogen.
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intervention.
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thoroughly checked for being leak- tight. Even the slightest leak in the gas supply
between the generator and the Mass Spectrometer can lead to a reduction in efficiency.
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6mm Push Fit Tube Fitting
1/4” Compression Tube Fitting
2m 6mm Grey Tubing
4m 1/4” Teflon Tubing
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The ‘NM32LA’ Laboratory Gas Generator is designed specifically to minimize operator
involvement. Given that the system is installed as described in the user manual and
is serviced in accordance with the specified maintenance recommendations, then it
should simply be a matter of turning the generator on.
The generator will automatically produce the factory default flow and pressure:
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and been set to allow for pressure drops between the generator and the instrument,
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These settings have been approved by LCMS Manufacturers.
The ‘NM32LA’ produces gas on demand. If the Mass Spectrometer is operating and
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NM32LA PIP
Spectrometer.
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from the Mass Spec starts again, the generator will detect the demand for gas and will
automatically start again to suit the demand.
The ‘NM32LA’ is designed for the internal compressors to cycle. This cycling reduces
the duty (run time) on the compressors. The rate at which they cycle will be dependent
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the maximum gas flow of the ‘NM32LA’, the compressor duty will be higher. If the Mass
Spec demand is lower than the maximum gas flow, then the duty on the compressors
will decrease. If the generator is installed in an extreme environment or is subjected to
low supply voltage or high altitude the compressors may undergo periods where they
do not cycle.
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If at any time the generator begins to emit excessive noise or vibration, then it should
be switched off and you should contact your authorised service provider or Peak
Scientific as soon as possible.
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Please ensure that the drain port at the rear of the compressor is led to a suitable
connection or container. It should be noted that the generator will expel considerable
amounts of water from this port. If a container is used it should be emptied at regular
intervals.
Note: The container must not have an airtight seal.
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Ensure that the generator is serviced in accordance with the maintenance
recommendations. The information is also made available as a download from the Peak
Scientific Website on:
www.peakscientific.com
Maintenance
Due to the simplicity of the design and the small number of moving parts in the
‘NM32LA’, the generator will have a long and trouble free life. However, the components
mentioned below should be replaced to maintain optimum performance levels and
maximum runtime.
Failure to follow the prescribed maintenance will invalidate the product warranty.
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NM32LA PIP
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Servicing and/ or repair of the generator should only be undertaken by a
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Service Interval
12 months
Component
Part No
2x Coalescer Filter Element
00-4499
1x Compressor Inlet Filter Element
02-4640
1x Reverse Active Carbon Filter Element
00-4425
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whilst giving the added benefit of cost saving over buying the parts separately.
Purchase Interval
Component
Part No
12 months
Annual Service Kit NM32LA
08-4780
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Peak Scientific has programmed their generators to indicate the Compressor Service
Stages.
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The NM32LA Gas Generator monitors and counts the accumulative run- time (in hours)
for the internal compressors and Peak Scientific has programmed the generator to go
through the following Service Indication Stages:
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in the front of the generator will light.
This is to make the user aware that a service of the generator is due and should be
planned at the earliest convenience. The generator will continue to operate as normal
with the LED on.
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compressors reach a total of 4,000 hours, the service LED indicator (yellow) will start
to flash.
This is to make the user aware that the service of the generator is now overdue and
must be completed immediately to ensure the continuous operation of the generator.
Service Interval
Component
Part No
every 4,000 hours or 12
months
Compressor Service Kit
06-5529
Compressor Replacement Assembly
08-8141
Please note that this service/ replacement interval may be shortened by extreme
ambient conditions, such as heat, high relative humidity, altitude and excessive use of
the generator, being the most prominent examples.
Compressors can be re- fitted as an alternative to replacements up to a maximum of 3
times, this is a more cost effective solution however a degree of technical expertise is
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NM32LA PIP
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Though Peak Scientific anticipates that the Spare Parts used to fulfil the generators
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‘NM32LA’, it may be advisable for any authorized service staff to have the following
parts available.
Part Description
P/N
Part Description
P/N
Compressor Inlet Filter Element
02-4640
Silencer
02-1016
Coalescer Filter Element
00-4499
Power Supply, 24 VDC 211A
04-4543
Reverse Active Carbon Filter Element
00-4425
Pressure Relief Valve
02-1220
Annual Service Kit (contains items
08-4779
3-2 Solenoid Valve, universal, 24
02-5494
Large THI Compressor Service Kit
06-5529
2-2 Solenoid Valve, 24 VDC
02-5504
Large THI Replacement Compressor
06-5522
Non Return Valve
02-5473
Large Compressor Anti- Vib Mounts
06-6173
Nitrogen Membrane
06-4418
Replacement Compressor Assembly
08-8141
Non Return Valve
02-4546
Elbow 1/4 BSP
02-4402
Filter, Carbon
02-4552
Capacitor
04-4472
Filter, Coalescing
02-5432
Elbow 10MM
02-5451
Pressure Regulator
02-1110
Compressor Braided Hose
02-1105
Pressure Release Valve, 11 bar
02-4544
Reducing Bush
02-1051
Flow Controller Valve
02-4207
Pressure Switch, 24V
04-4526
Indicator LED (red)
04-4550
Pressure Gauge (0-200psi)
02-4598
Indicator LED (yellow)
04-4551
PLC, 24 VDC
04-4557
120mm Fan
04-1021
PLC Display
04-4558
Compressor Socket
04-4449
Relay Base
04-4533
Exhaust Silencer
02-4287
Connector Triple Deck
04-1010
Compressor Inlet Filter
02-4639
10A Relay
04-4534
Circuit Breaker 4A
04-4559
Timer Relay
04-1071
Earth Connector
04-4415
Buzzer 24 VDC
04-4562
Motor Contactor
04-4544
Circuit Breaker 6A
04-4560
Elbow 1/4 BSP M-M
02-4403
Compressor Plug
04-4450
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NM32LA PIP
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the running condition of the internal compressors and illuminates when they have been
operating continually for a period of 8 hours.
There are a number of extreme conditions that can affect the duty cycling of
the compressors inside the ‘NM32LA’. These extremes include very high ambient
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high altitude. Any of these or a combination of a number of these extremes can be
evident in a customer site. While the ‘NM32LA’ generator is designed to operate fully
in these conditions it should be noted that the effect of these extremes can force
the compressors to run continually. The compressors are fully capable of running
continually with no detrimental effect. However, it should be noted that if this is the
case it will increase their duty and they will reach the 3000 hour recommended service
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If the compressors have been operating continually for a period of 8 hours the indicator
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‘NM32LA’ generator has been operating for a significant period of time, then suddenly
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as an external leak of imminent compressor failure.
You should contact Peak Scientific or any of our authorized service providers.
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Peak Scientific has been rewarded with a good reputation as a first class provider of
sales and after- sales to our partners and customers world- wide.
Country
Telephone
eMail
UK & ROW
+44 (0)845 258 2943
[email protected]fic.com
North America
+1 866 732 5427
[email protected]fic.com
India
+91 9885 28 6875
[email protected]fic.com
Sub- Saharan Africa
+27 (0)83 296 4516
[email protected]fic.com
Page 11
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NM32LA PIP
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Peak Scientific offers Product Training for a variety of gas generators, including the
‘NM32LA’.
Since adopting the training program for Peak Scientific, we have certified over 300
Field Service Engineers as “Peak Authorized Service Engineer”.
Where the Peak branded technician training program comes into its own, it provides
an in- depth understanding of the gas generator and all its individual components.
As a result, all students are fully conversant with the servicing protocols, spare parts
and anything else from unpacking the generator, to installation, maintenance and fault
finding.
Peak Scientific branded product training is available in- house in our facilities in
Scotland and takes place 6 times a year.
Though in- house training is always the preferred option, allowing trainees to gain
valuable hands- on experience on units, we appreciate that the busy schedule of
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offer training courses to take place at the site of our partners, covering all aspects of
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To compete and meet your business objectives and achieve a healthy bottom line,
its critical to maximize uptime. The training we offer will help you achieve your
performance goals.
After the training your engineers will be certified to service Peak products and will
receive a certificate acknowledging their achievement.
For more information or to arrange free of charge training, please contact Peak
Scientific at [email protected]
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‘Complete’.
The ‘Complete’ Service Plan is an all- inclusive package which ensures your customer
will receive complete care throughout the duration of their service plan with no
unexpected additional cost. During the course of the year a Peak Engineer or an
authorized representative will carry out preventative maintenance visits and all call- out
charges, labour charges and parts are included in the initial Service Plan price. In the
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and your customer will further benefit from a priority response time.
The ‘Standard’ Service Plan offered by Peak Scientific is a more basic package. The
Peak Engineer, or authorized representative, will carry out a service visit, when they
will change consumable parts. Any other spare parts and breakdowns are, however, not
included in this plan, though a discount may be applied to any charges.
The response time will only be prioritised over non- plan customers.
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for the NM32LA, please contact Peak Scientific.
Page 12
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NM32LA PIP
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The ‘NM32LA’ is part of a product family suitable for most LC/MS Applications and as
such forms part of a sell- up strategy.
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systems, such as the NM60L, can provide suitable alternative solutions to the ‘NM32LA’
for the customer.
NM32L
NM32LA
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NM60-420L
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for any LCMS
for any LCMS
for any LCMS
for multiple LCMS
‘hi flo’ option available
for Agilent Jetstream
applications
(unit with internal
compressor)
Clinical
Environments
catering for any LCMS
Model
(unit with internal
compressor)
Typically, the recommendation of any generator model is dependent on the following:
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peakscientific.com
Peak Scientific UK
Fountain Crescent
Inchinnan Business Park
Inchinnan
1"3&
4DPUMBOE6,
Peak Scientific North America
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Suite #8
Billerica, MA 01862
64"
Peak Scientific India
202, Amsri Shamira
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0QQ4U.BSZT%FHSFF$PMMFHF
4%3PBE4FDVOEFSBCBE
500 025, India
Peak Scientific Africa
#MPDL%6OJU%
The Grove Business Park
0ME1BBSEFWMFJ3PBE
Somerset West, 7137
South Africa
Tel: +44 (0)141 812 8100
Fax: +44 (0)141 812 8200
Tel: +1 866 647 1649
Fax: +1 978 608 9503
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Fax: +49 (0)69 677 33 200
Tel: +86 21 2890 9652
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