Buchi Vacuum Pump V-100 Manual
Advertisement
Advertisement
Vacuum Pump V-100
Operation Manual
Imprint
Product Identification:
Operation Manual (Original) Vacuum Pump V-100
11593636
Publication date: 03.2019
BÜCHI Labortechnik AG
Meierseggstrasse 40
Postfach
CH-9230 Flawil 1
E-Mail: [email protected]
BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experience, especially with respect to structure, illustrations and technical details.
This manual is copyrighted. Information from it may neither be reproduced, distributed, or used for competitive purposes, nor made available to third parties. The manufacture of any component with the aid of this manual without prior written agreement is also prohibited.
BÜCHI Labortechnik AG Table of contents
Contents
Operation Manual Vacuum Pump V-100 iii
Table of contents BÜCHI Labortechnik AG
iv Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
1
About this document | 1
About this document
These operating instructions describe the Vacuum Pump V-100 at the time supplied.
They are an integral part of the product and contain important information that is necessary for safe operation and maintenance.
These operating instructions apply to all variants of the Vacuum Pump V-100 and are intended primarily for laboratory staff.
u u u
To ensure safe and trouble-free operation, read these operating instructions before starting up the device and follow the guidance they contain.
Keep the operating instructions somewhere near to the device.
Pass on the operating instructions to any subsequent owner or user.
BÜCHI Labortechnik AG accepts no liability whatsoever for any faults or damage that result from the failure to follow these operating instructions.
u If you still have any questions after reading these operating instructions, please contact BÜCHI Labortechnik AG Customer Service. Contact details for your local agents can be found on the back cover of these operating instructions or on the Internet at http://www.buchi.com.
1.1
Warning notices in this document
Warning notices warn you of dangers that can occur when handling the device. There are four danger levels, each identifiable by the signal word used.
Signal word
DANGER
WARNING
CAUTION
NOTICE
Meaning
Indicates a danger with a high level of risk which could result in death or serious injury if not prevented.
Indicates a danger with a medium level of risk which could result in death or serious injury if not prevented.
Indicates a danger with a low level of risk which could result in minor or medium-severity injury if not prevented.
Indicates a danger that could result in damage to property.
1.2
1.2.1
Symbols
The following symbols may be displayed in this instruction manual or on the device:
Warning symbols
Symbol Meaning
General warning
Symbol Meaning
Corrosive substance
Dangerous electrical voltage
Biological hazard
Breakable items
Flammable substance
Potentially explosive atmosphere
Dangerous gases
Operation Manual Vacuum Pump V-100 5/52
1 | About this document
Symbol Meaning
Hot surface
Risk of hand injury
BÜCHI Labortechnik AG
Symbol Meaning
Health-harming or irritant substances
Strong magnetism
1.2.2
Mandatory directive symbols
Symbol Meaning
Wear safety goggles
Symbol Meaning
Wear protective clothing
Wear protective gloves Heavy load, do not lift without assistance
1.2.3
1.3
1.4
Other symbols
NOTE
This symbol draws attention to useful and important information.
R This character draws attention to a requirement that must be met before the instructions below are carried out.
u This character indicates an instruction that must be carried out by the user.
5 This character indicates the result of a correctly carried out instruction.
Available languages
These operating instructions were originally produced in German and have been translated into several other languages. The translations are available on the enclosed CD or can be obtained as a PDF file via http://www.buchi.com.
Trademarks
Product names and registered or unregistered trademarks that are used in this instruction manual are used only for identification and remain the property of the owner in each case.
For example, Rotavapor® is a registered trademark of BÜCHI Labortechnik AG.
6/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
2 Safety
2.1
2.2
2.3
Safety | 2
Intended use
The Vacuum Pump V-100 has been designed and built as an item of laboratory equipment. Its intended use is the evacuation of laboratory apparatus. This is done by means of a PTFE-membrane pump – with or without regulation by a vacuum controller.
PTFE-membrane pumps are used primarily for the following applications:
Evacuating distillation apparatus, in particular rotary evaporators (Rotavapor®)
Vacuum filtration
Vacuum-drying cabinets
Drying kilns
Use other than that intended
Use of any kind other than that referred to and any application that does not comply with the technical specifications constitutes use other than that intended. The operator alone is liable for any damage brought about by use of the device in a manner other than that intended.
In particular, the following applications are not permissible:
Use in areas which require explosion-safe apparatus.
Pumping of liquids and solid particles.
Processing samples which could be caused to explode or ignite by impact, friction, heat or sparks (e.g. explosives).
Use for analysis (e.g. Kjeldahl).
Generation of positive pressure (pressurizing a system).
Operation at ambient temperatures >40 °C.
Staff qualification
Unqualified persons are unable to identify risks and are therefore exposed to greater dangers.
The device may only be operated by suitably qualified laboratory staff.
These operating instructions are aimed at the following target groups:
Users
Users are persons that meet the following criteria:
They have been instructed in the use of the device.
They are familiar with the contents of these operating instructions and the applicable safety regulations and apply them.
They are able on the basis of their training or professional experience to assess the risks associated with the use of the device.
Operation Manual Vacuum Pump V-100 7/52
2 | Safety
2.4
2.4.1
2.4.2
2.5
2.6
BÜCHI Labortechnik AG
Operator
The operator (generally the laboratory manager) is responsible for the following aspects:
The device must be correctly installed, commissioned, operated and serviced.
Only suitably qualified staff may be assigned the task of performing the operations described in these operating instructions.
The staff must comply with the locally applicable requirements and regulations for safe and hazard-conscious working practices.
Safety-related incidents that occur while using the device should be reported to the manufacturer ([email protected]).
BUCHI service technicians
Service technicians authorized by BUCHI have attended special training courses and are authorized by BÜCHI Labortechnik AG to carry out special servicing and repair measures.
Residual risks
The device has been developed and manufactured using the latest technological advances. Nevertheless, risks to persons, property or the environment can arise if the device is used incorrectly.
Appropriate warnings in this manual serve to alert the user to these residual dangers.
Dangerous vapors
Distillation can produce dangerous vapors that are capable of causing life-threatening toxic effects.
u u u u u u
Do not inhale any vapors produced during distillation.
Ensure that vapors are removed immediately by a suitable fume hood.
Only use the device in well ventilated areas.
If vapors escape from joints or connections, check the seals concerned and replace them if necessary.
Do not distill any unknown fluids.
Observe the safety data sheets for all fluids used.
Faults during operation
If a device is damaged, sharp edges or exposed electrical wires can cause injuries.
u u u
Regularly check device for visible damage.
If faults occur, switch off the device immediately, unplug the power cord and inform the operator.
Do not continue to use devices that are damaged.
Personal protective equipment
Depending on the application, hazards due to heat and/or corrosive chemicals may arise.
u u
Always wear appropriate personal protective equipment such as safety goggles, protective clothing and gloves.
Make sure that the personal protective equipment meets the requirements of the safety data sheets for all chemicals used.
Modifications
Unauthorized modifications may impair safety and lead to accidents.
8/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG Safety | 2 u u
Use only genuine BUCHI accessories, spare parts and consumables.
Technical modifications to the device or accessories should only be carried out with the prior written approval of BÜCHI Labortechnik AG and only by authorized
BUCHI technicians.
BUCHI accepts no liability whatsoever for damage arising as a result of unauthorized modifications.
Operation Manual Vacuum Pump V-100 9/52
3 | Product description
3 Product description
3.1
BÜCHI Labortechnik AG
Description of function
The Vacuum Pump V-100 is intended for evacuating laboratory apparatus to a terminal vacuum of 10 mbar (± 2 mbar).
Once switched on, the V-100 runs in continuous mode unless it is connected to the
Interface I-100 unit. In unregulated continuous mode, the pump runs at a maximum speed of 1280 rpm and generates a terminal vacuum of 10 mbar (± 2 mbar). The time required for evacuation depends on the size (volume) of the vessel.
After 1 hour of operation, the V-100 switches automatically to ECO mode. In ECO mode, the V-100 runs at 70 % capacity but still generates the same terminal vacuum of 10 mbar (± 2 mbar).
The pump can be operated either as a standalone device or combined with optional
accessories (see Chapter 3.3 "Specifications supplied", page 14).
3.2
3.2.1
Configuration
Front view
10/52
Fig. 1: Design of V-100
1 Carrying handle
2 Pump top cover
3 On/Off master switch
Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
3.2.2
Rear view
Product description | 3
Fig. 2: Rear view of V-100
1 Knurled-head screws
2 Pump outlet
3 Type plate
4 Pump intake (vacuum)
5 Mini-DIN connection
6 Power supply connection
7 Lashing eye (for securing against earthquakes)
Operation Manual Vacuum Pump V-100 11/52
3 | Product description
3.2.3
Internal view
1
2
BÜCHI Labortechnik AG
3
6
7
4
5
Fig. 3: Internal view of V-100 showing pump head and pump-head connection piece
1 Torx key (TX10)
2 Pump top cover
3 Torx key (TX25)
4 Pump outlet
5 Pump-head metal cover
6 GL14 cap nut
7 Pump-head connection piece
12/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
3.2.4
Product description | 3
Typical application
The V-100 is used for evacuating laboratory apparatus such as tubes, flasks and other apparatus.
Recirculating
Chiller F-100
Fig. 4: Typical application for the V-100 in a laboratory
1 Recirculating Chiller F-100
2 Rotavapor R-100
3 Vacuum Pump V-100 with Interface I-100
Evacuation changes the physical and chemical properties of materials. The V-100 is ideally suited to connection to a Rotavapor R-100 in combination with a Recirculating
Chiller F-1xx. With that combination of apparatus controlled by a controller such as the Interface I-100, ideal distillation configurations for all commonly used solvents can be created.
Operation Manual Vacuum Pump V-100 13/52
3 | Product description
3.2.5
Type plate
The type plate is on the rear of the Vacuum Pump V-100.
BUCHI Operations India Pvt Ltd
394230 Surat / India
Type: V-100
SN: 1000000000
Volt: 100 – 240 VAC
Frequ.: 50/60 Hz
Power: 150 W
Built: 2014
Designed by BUCHI in Switzerland,
Made in India
1
4
5
6
2
3
7
8
9
3.3
11 10
Fig. 5: Type plate (example)
1 Company name and address
2 Device name
3 Serial number
4 Input voltage
5 Frequency
6 Maximum power rating
Specifications supplied
BÜCHI Labortechnik AG
7 Year of manufacture
8 Country of manufacture
9 Approvals
10 Symbol for "Do not dispose of as household waste"
11 Product code
Vacuum Pump V-100
Vacuum tubing (2 m)
Power supply cable
Silencer
Tubing connections (set)
Interface I-100
Woulff bottle
Condensation unit
Communication cables
* As per order code
*
*
*
*
1
1
1
1
V-100
1
14/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
3.4
3.4.1
3.4.2
3.4.3
Product description | 3
Technical data
Vacuum Pump V-100
Dimensions (W x H x D)
Weight
Power supply voltage
Power consumption
Power consumption in ECO mode
Terminal vacuum (absolute)
Pump capacity
Vacuum connection
Motor
Rotation speed
Rotation speed in ECO mode
Noise level
Overvoltage category
Pollution degree
Enclosure rating
Certificates
180 x 275 x 210 mm
5.6 kg
100 – 240 V, 50/60 Hz
150 W
70 W
10 mbar (± 2 mbar)
1.5 m 3 /h
GL-14
Brushless DC motor
1280 rpm max.
II
2
70 % of max. capacity
32 to 57 dBA
57 dBA: with 100% load
IP 20
CE
Ambient conditions
Max. altitude above sea level
Ambient temperature
Maximum relative humidity
2000 m
5 - 40 °C
80 % for temperatures up to 31 °C decreasing linearly to 50 % at 40 °C
The Vacuum Pump V-100 may only be used in indoor areas.
Materials
Component
Pump heads
Drive unit body
Housing
Membranes
Valve plate
Valve head
Pump-head connection piece
Vacuum tubing
Non-return valve O-rings
Material
PPS
Aluminium
PBT
PTFE/rubber
PEEK
PEEK
FEP
Silicone/natural rubber
FFKM
Operation Manual Vacuum Pump V-100 15/52
4 | Transport and storage
4 Transport and storage
4.1
BÜCHI Labortechnik AG
Transport
NOTICE
Risk of breakage due to incorrect transportation u u
Make sure that all parts of the device are safely packed in such a way as to prevent breakage, ideally in the original box.
Avoid sharp movements during transit.
4.2
u u u
After transportation, check the device for damage.
Damage that has occurred in transit should be reported to the carrier.
Keep packing for future transportation.
Storage
u u u
Make sure that the ambient conditions are complied with (see Chapter 3.4 "Technical data", page 15).
Wherever possible, store the device in its original packaging.
After storage, check the device, all seals and tubing for damage and replace if necessary.
16/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
4.3
Removing transit fixings
Transport and storage | 4
Fig. 6: Transit fixings on the rear of the Vacuum Pump V-100
1 Transit fixings 2 GL14 cap nuts
Before the V-100 is set up and put into service, the transit fixings (red) have to be removed.
u u u
On the rear of the V-100, unscrew the GL14 cap nuts (2) from the pump intake and pump outlet.
Pull off the red transit fixings (1).
Screw the cap nuts back on.
Operation Manual Vacuum Pump V-100 17/52
5 | Installation
5
5.1
BÜCHI Labortechnik AG
Installation
Important considerations prior to commissioning
WARNING
Risk of irritation of mucous membranes and poisoning from inhalation of hazardous gases and vapors.
In the process of evacuation it is possible that hazardous substances may be pumped out at the same time and released into the atmosphere. In addition, it is possible for such substances to collect as condensation at leaking connections.
u u u u
Operate the pump inside a fume hood.
Direct vapors from the pump outlet into the fume hood.
If necessary, wear a face mask and safety goggles.
If necessary, only handle pump and accessories with protective gloves.
WARNING
Risk of fire or explosion from flammable solvent vapors.
In the process of evacuation, it is possible for solvent vapors to get into the inside of the pump and catch fire or explode due to the electric current.
u u u
Follow the guidance notes for the solvents used.
Connect a Woulff bottle upstream of the pump intake.
Operate the pump inside a fume hood.
CAUTION
Health risks when handling corrosive substances.
u When working with strong acids or caustic solutions, always wear personal protective equipment (safety goggles, protective clothing, protective gloves).
18/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
5.2
Installation | 5
Installation site
u Before setting up the V-100 and putting it into service, remove the transit fixings
(red) on the rear of the device (see Chapter 4.3 "Removing transit fixings", page 17).
NOTICE
Risk of property damage from falling equipment (e.g. in an earthquake) u Secure the Vacuum Pump against falling by means of the lashing eye on the rear
of the device (see Chapter 3.2.2 "Rear view", page 11).
5.3
The installation site must meet the following requirements:
Firm and level surface: at least 200 mm x 300 mm (W x D)
Height: at least 300 mm
Set up inside a fume hood or feed the pump outlet into the fume hood
Sufficient air supply to the pump cooler
Connecting laboratory equipment
1 2
Fig. 7: Vacuum Pump (V-100) with transit fixings
1 Pump outlet 2 Pump intake (vacuum)
Operation Manual Vacuum Pump V-100 19/52
5 | Installation BÜCHI Labortechnik AG
The V-100 is connected by a vacuum tubing to the laboratory apparatus to be evacuated. The vacuum tubing leads via a GL14 connection from the pump intake (2) to the outlet of the laboratory device concerned.
Precondition:
R
Transit fixings have been removed (see Chapter 4.3 "Removing transit fixings", page 17).
u Fit tubing to pump intake (2) using the GL14 cap nut.
If vapors are to be expected during evacuation, we recommend the following: u u
Connect the tubing to the Woulff bottle intake using a GL14 cap nut.
For details of connecting the V-100 to a rotary evaporator (e.g. Rotavapor® R-100) see the relevant section of the device's operating instructions.
For more information on the use of the V-100, see Chapter 3.2.4 "Typical application", page 13.
20/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
5.4
Connecting the silencer
Installation | 5
2
3
4
Fig. 8: Silencer on pump outlet of V-100
1 GL14 cap nut
2 Flow direction marker
3 Silencer
4 Silencer outlet
The silencer can be connected directly to the pump or to the outlet of the secondary condenser.
Connecting silencer directly to V-100 u u
Fit the silencer (3) onto the pump outlet so that the flow direction marker (2) on the silencer points away from the pump.
Slide forwards the GL14 cap nut (1) on the top connection of the silencer and screw it onto the GL14 thread of the pump outlet.
Connecting the silencer to the outlet of the secondary condenser
1
Fig. 9: Connection for the silencer
1 Secondary condenser outlet u Position the silencer inlet on the secondary condenser outlet (1).
Operation Manual Vacuum Pump V-100 21/52
5 | Installation BÜCHI Labortechnik AG u Slide forwards the GL14 cap nut on the silencer inlet and screw it onto the thread of the condenser outlet.
22/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
5.5
Connecting a Woulff bottle
Installation | 5
6
7
8
9
10
1
2
3
4
5
Fig. 10: Connecting a Woulff bottle to the V-100
1 GL14 cap nut
2 Woulff bottle outlet
3 Top outlet for connecting Interface
I-100
4 Woulff bottle inlet
5 Woulff bottle glass component
6 Pump intake
7 Connection piece
8 Screw
9 Mounting rail for holder
10 Woulff bottle holder
The Woulff bottle is connected to the pump intake on the rear of the V-100.
Tools required: Torx key (fitted in pump top cover) u u u u u
Fix the mounting rail (9) for the holder below the pump intake (6) using the screw
(8).
Fit the holder (10) onto the mounting rail.
Unscrew the GL14 screw-cap from the pump intake (6).
Fit the connection piece (7) from the outlet of the Woulff bottle onto the pump intake. Screw the GL14 cap nut (1) on the end of the tubing onto the pump intake thread.
Press the Woulff bottle into the holder.
Connecting an Interface I-100 via a Woulff bottle u u
If necessary connect the Woulff bottle to the Interface I-100 as follows: Fit the connection piece to the top outlet (3) of the Woulff bottle.
For details of connecting the connection piece to the interface unit and the setup, also refer to the operating instructions for the I-100.
Operation Manual Vacuum Pump V-100 23/52
5 | Installation
5.6
Connecting a secondary condenser
BÜCHI Labortechnik AG
1
Fig. 11: Connecting secondary condenser to V-100
1 Secondary condenser
2 Pump outlet
3 Holder
4 Screw
NOTE
Connecting a secondary condenser is advised particularly in cases where the pump outlet cannot be connected to a fume hood or the solvent concentration in the vapor is too high. The secondary condenser reduces the amount of vapor emitted.
The secondary condenser is connected directly to the pump outlet (2) on the rear of the V-100.
Fitting holder for secondary condenser
Tools required: Torx key (fitted in pump top cover – see Chapter 3.2.3 "Internal view", page 12).
u Position the holder (3) below the pump outlet (2) and fix to the pump housing by means of two screws (4).
24/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
Fitting secondary condenser into the holder and connecting up
Installation | 5
4
1
2
3
5
6
Fig. 12: V-100 with secondary condenser connected
1 Connection piece
2 GL14 cap nut
3 Pump outlet
4 Secondary condenser outlet
5 Ball joint clamp
6 Receiving flask u u u u
Push secondary condenser together with connection piece (1) and GL14 cap nut
(2) fully home into holder from above.
Fit the unattached end of the connection piece into the pump outlet (3).
Screw the GL14 cap nut (2) on the connection piece onto the thread on the pump outlet.
Fit receiving flask (6) underneath the secondary cooling cold trap and fix with ball joint clamp (5).
Operation Manual Vacuum Pump V-100 25/52
5 | Installation
5.7
Connecting a secondary cooling cold trap
BÜCHI Labortechnik AG
5
6
7
Fig. 13: Cold trap for V-100
1 Cover
2 Secondary cooling cold trap
3 Secondary cooling cold trap inlet with connecting tubing
4 Holder for secondary cooling cold trap
5 Secondary cooling cold trap outlet
6 Ball joint clamp
7 Receiving flask
Connecting a secondary cooling cold trap upstream of the pump outlet reduces the amount of residual vapor released into the atmosphere.
Fitting to pump outlet
Tools required: Torx key (fitted in pump top cover – see Chapter 3.2.3 "Internal view", page 12).
u u u u u u u
Position the holder (4) for the secondary cooling cold trap below the pump outlet and fix it to the housing using two screws.
Unscrew the GL14 cap nut from the pump outlet and slide it narrow-end first over the connecting tubing on the inlet (3) of the secondary cooling cold trap.
Fit the unattached end of the connecting tubing (3) into the pump outlet.
Screw the GL14 cap nut on the connecting tubing back onto the thread on the pump outlet.
Push secondary cooling cold trap (2) fully home into holder.
Fit receiving flask (7) into the bottom outlet of the secondary cooling cold trap and fix with the aid of a ball joint clamp (6).
From the outlet (5) of the secondary cooling cold trap, feed another connecting tubing directly into a waste drum.
26/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
5.8
Electrical connections
Installation | 5
4
Fig. 14: Electrical connections on the V-100 (left) and the Interface I-100 (right)
1 Mini-DIN connection (Interface I-100) 3 Mini-DIN connection (vacuum pump)
2 Power supply for Interface I-100 4 Power supply for vacuum pump u u u u u
Make sure that the available power supply matches the rating indicated on the type plate.
Join the mini-DIN socket (1) of the V-100 to the mini-DIN socket (3) of the Interface I-100 with a communication cable.
Plug the mains power cord supplied into the power supply socket (4) on the V-100.
Plug the mains power cord into a grounded mains power socket.
Connect the power adapter for the Interface I-100 to the socket (2) for the power supply.
Operation Manual Vacuum Pump V-100 27/52
5 | Installation
5.9
5.9.1
Fitting and connecting the Interface I-100
Fitting an interface unit to the Vacuum Pump V-100
Fitting the holder
BÜCHI Labortechnik AG
2
3
4
Fig. 15: Fitting the holder for the Interface I-100
1 Screw
2 Holder for Interface I-100
3 Rubber plug (in thread for screw)
4 Lower hinge of holder
The Torx key required for fitting the holder is included in the specifications supplied.
u u u
Remove rubber plug (3).
Fit the holder (2) onto the pump top cover from behind and secure it with the screw (1).
Make sure that the hinge (4) of the holder is engaged in the slot on the rear of the
V-100.
28/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
Fitting the interface unit
Installation | 5
2
3
5.9.2
Fig. 16: Fitting the Interface I-100
1 Interface I-100
2 Holder
3 T-screw u u
Fit the interface unit (1) onto the holder (2).
Tighten the T-screw (3) on the back of the interface unit by turning it clockwise.
Connecting interface unit to Vacuum Pump V-100
The V-100 is connected to the Interface I-100 by means of a communication cable
in Chapter 5.5 "Connecting a Woulff bottle", page 23). For more information on con-
necting the tubing and communication cable, refer to the section "Commissioning" in the operating instructions for the Interface I-100.
Operation Manual Vacuum Pump V-100 29/52
6 | Operation
6
6.1
6.2
BÜCHI Labortechnik AG
Operation
Operating V-100 with Interface I-100
The Vacuum Pump V-100 can be controlled by an Interface I-100. Control encompasses the following parameters and functions:
Setting the required vacuum
Timer
Details of controlling the V-100 and the other laboratory equipment involved in evacuation can be found in the operating instructions for the Interface I-100.
Operating V-100 without Interface I-100
1 2
30/52
Fig. 17: V-100
1 Pump outlet 2 Pump intake (vacuum)
If not controlled by an Interface I-100, the vacuum pump runs in continuous mode and
switches to ECO mode after one hour, see Chapter 3.1 "Description of function", page 10.
Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
7
Cleaning and servicing | 7
Cleaning and servicing
NOTE
Users may only carry out the servicing and cleaning operations described in this section.
Any servicing and repair work which involves opening up more than the pump top cover may only be carried out by authorized service technicians.
u u
Use only genuine BUCHI consumables and spare parts in order to ensure correct operation of the device and preserve the warranty.
Before carrying out any servicing work, switch off the device and disconnect it from the power cable.
7.1
7.1.1
Cleaning
Important considerations when cleaning
WARNING
Risk of fatal injury from electric shock.
If the pump is opened up while it is running there is a risk of dangerous electric shocks.
u Before carrying out any cleaning or servicing work, always shut down the device and disconnect the power cable.
7.1.2
7.1.3
u u u u u u u u u
Cleaning the pump
Disconnect all connections to the device.
Place a collecting vessel under the pump outlet.
Switch on the Vacuum Pump V-100 and allow it to run.
Spray ethanol into the pump intake.
Hold your finger over the pump intake so that a vacuum is created for a short time.
Remove your finger from the pump intake again.
Allow the pump to run until there is no more liquid inside the pump heads.
Repeat the procedure if necessary.
Switch off the pump and reconnect the apparatus.
After working with strong acids
After distilling strong acids or corrosive solutions the pump should be flushed out in order to increase its service life.
u u u u u u u
Detach tubing connections to other laboratory equipment.
If present, remove Woulff bottle from pump intake and secondary condenser or cold trap from pump outlet and clean them.
Place a bowl or glass collection vessel under the pump outlet.
Switch on the pump and pour 5 to 10 mL of water into the pump intake.
Test the pH level of the water collected at the pump outlet.
Repeat the flushing process until the discharged water has a pH level of between
3 and 9.
Allow the pump to run for two to three minutes to dry out.
Operation Manual Vacuum Pump V-100 31/52
7 | Cleaning and servicing
7.1.4
BÜCHI Labortechnik AG
Cleaning the housing
NOTICE
Risk of acid damage
The housing of the unit is made of plastic. Escaping acid may damage the material.
u Immediately remove any drops of acid with a damp cloth.
32/52
7.1.5
7.1.6
7.1.7
u u
Only use a damp cloth to clean the device.
To clean the housing, only use ethanol or soapy water.
Cleaning glass components
The V-100 does not itself contain any glass components but the accessories (Woulff bottle, secondary cooling cold trap, secondary condenser) consist mainly of glass and must always be inspected and cleaned before and after use.
As the glass components are under vacuum when in use, they are subjected to high stress.
u u u u
Before use, check all glass components for cracks, chipping and any other damage.
Replace any damaged glass components.
Rinse out glass components with water and a conventional cleaning agent (e.g.
mild soap and water solution).
Wherever possible, clean glass components by hand.
NOTE
Feeding a thin copper wire into the cooling coil of the secondary condenser or cold trap reduces the amount of dirt deposited.
Cleaning tubing
After evacuation, there may still be residual fluid in the tubing from condensed vapors.
The pump can largely dry itself out when running idle.
u u
Detach connections to other laboratory equipment and allow the pump to run in continuous mode.
Switch off the pump after three to five minutes.
To clean the connecting tubing inside the pump between the two pump heads it is necessary to open up the pump as follows:
Precondition:
R Pump has been shut down.
u u u u u
Remove the pump top cover and take out the pump tubing (see Chapter 7.2.5
Rinse out the tubing with clean water. If necessary, remove residues inside the tubing with a copper wire.
Refit the pump tubing (see Chapter 7.2.5 "Replacing tubing", page 40).
Switch on the pump and allow it to run in continuous mode until the inside of the tubing is dried out.
Refit the pump top cover.
Cleaning valve heads
Dirt contamination of the valve heads is evidenced by the V-100 failing to achieve the terminal vacuum of 10 mbar (± 2 mbar) even though components are intact and connections air-tight. To clean them, proceed as follows:
Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
7.1.8
7.1.9
Cleaning and servicing | 7 u u u u u u u
Detach all connections (tubing and communication cable) from the pump.
Place a collecting vessel under the pump outlet.
Switch on the pump.
Spray a small amount of acetone (approx. 10 mL) into the pump intake.
Wait until the sound of the pump changes back to what it was before the acetone was injected.
Repeat this procedure four times.
Re-attach the connections to the pump and check whether the terminal vacuum is now achieved.
If the V-100 is still unable to achieve the required performance even after the valve heads have been cleaned, both pump heads must be dismantled and manually
cleaned (see Chapter 7.2.2 "Dismantling and reassembling pump head", page 35).
Cleaning non-return valve
The V-100 operates with a total of four non-return valves. There is one valve with an
O-ring in the connection on each of the two ports on each pump head. To clean the valves, the pump heads have to be dismantled as follows: u
Remove the pump top cover and dismantle the pump heads (see Chapter 7.2.2
"Dismantling and reassembling pump head", page 35).
Cleaning the membrane
After evacuation, there may still be residual fluid on the membrane from condensed vapors. The pump can largely dry itself out when running idle.
u u
Detach connections to other laboratory equipment and allow the pump to run in continuous mode.
Switch off the pump after three to five minutes.
If the membrane is contaminated by residues, the pump heads must first be dismantled and the membranes then unscrewed and cleaned.
u u u u u
Unscrew the membranes (see Chapter 7.2.3 "Replacing the membrane", page 38).
Wipe down membranes with a damp cloth.
Refit the membranes (see Chapter 7.2.3 "Replacing the membrane", page 38).
7.2
7.2.1
Servicing
Notes on servicing
WARNING
Risk of fatal injury from electric shock.
If the pump is opened up while it is running there is a risk of dangerous electric shocks.
u Before carrying out any cleaning or servicing work, always shut down the device and disconnect the power cable.
Operation Manual Vacuum Pump V-100 33/52
7 | Cleaning and servicing BÜCHI Labortechnik AG
NOTICE
Risk of pump damage and loss of warranty entitlement.
Unauthorized opening up of the lower part of the pump may permanently impair the function of the pump.
u Only allow authorized BUCHI service technicians to open up the lower part of the pump.
34/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
7.2.2
Dismantling and reassembling pump head
Removing pump top cover
Cleaning and servicing | 7
Fig. 18: V-100 with pump top section opened up
1 Rubber surrounds
Precondition:
R Pump has been shut down.
u u
Unscrew the two knurled-head screws on the rear of the V-100 and remove the pump top cover.
Remove the rubber surrounds (1) from the pump intake and pump outlet.
Removing pump-head connection piece
2
3
4
Fig. 19: Pump-head connection piece with union nuts between the two pump heads
1 Screw (elbow connection)
2 Elbow connection
3 Pump-head connection piece
4 GL14 cap nut u u u
Unscrew two screws (1) from each of the two pump heads, and remove the elbow connections (2) together with the pump-head connection piece (3) from the pump heads.
Unscrew the GL14 cap nuts (3) from the elbow connections.
Pull the GL14 cap nuts off the pump-head connection piece (4).
Operation Manual Vacuum Pump V-100 35/52
7 | Cleaning and servicing
Removing the pump head
BÜCHI Labortechnik AG
36/52
Fig. 20: Pump head opened up showing membrane underneath
1 Allen-head screws
2 Metal cover
3 Pump head u u u
Lie the pump on its side.
Unscrew the four Allen-head screws (1) and remove the metal cover (2).
Remove the pump head (3).
Dismantling the pump head
1
5
6
2
2
3
4
Fig. 21: View of completely dismantled pump head
1 Membrane
2 O-rings
3 GL14 cap nut
4 Elbow connection
5 Straight connection
6 Non-return valves
6
Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG Cleaning and servicing | 7
The pump head has two ports, attached to each of which is a connection (4, 5) with a non-return valve (6) and an O-ring (2). The straight connection (5) leads to the pump intake/pump outlet. The elbow connection (4) leads to the opposite pump head via the pump-head connection piece.
u u u
Unscrew the fixing screws on the straight connections (5) and remove the connections.
Remove the O-rings (2) from the connections.
Remove the non-return valves (6) from the connections.
Reassembling and refitting the pump head u u u u u u
Insert the non-return valves (6) and O-rings (2) inside the connections (4 and 5).
Fit the straight connections (5) on the pump heads (the elbow connections are refitted later together with the pump-head connection piece).
Position the pump head on the membrane and fix in place with the four Allen-head screws.
Fit the elbow connections (4) together with the pump-head connection piece and the GL14 cap nuts between the two pump heads.
Refit the rubber surrounds on the pump intake and pump outlet inside the housing.
Refit the pump top cover and fix in place with the knurled-head screws.
Operation Manual Vacuum Pump V-100 37/52
7 | Cleaning and servicing
7.2.3
BÜCHI Labortechnik AG
Replacing the membrane
The membranes of the V-100 are located on the left and right behind the pump head.
Fig. 22: Membrane
1 Membrane
Precondition:
R Pump has been shut down.
u u u u u Remove the top cover of the V-100 and remove the pump head (see Chap-
ter 7.2.2 "Dismantling and reassembling pump head", page 35).
Grip membrane with clamp and turn counter-clockwise.
Remove old membrane and insert new membrane.
Tighten new membrane by turning clockwise with clamp.
38/52
Fig. 23: Membrane and clamp
Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
7.2.4
Replacing valve
Cleaning and servicing | 7
5
3
2
1
2
3
4
Fig. 24: Dismantling the pump head
1 O-rings
2 Non-return valves
3 Screws for connections
4 Elbow connection
5 Straight connection u u u u u u
Remove the pump head (see Chapter 7.2.2 "Dismantling and reassembling pump head", page 35).
Unscrew the screws (3) from the connections (4, 5).
Remove the elbow connection and the straight connection from the pump head.
Remove the O-rings (1) and the non-return valves (2) from inside the connections.
Insert new O-rings and valves into the connections. NOTICE! When inserting the non-return valves, pay attention to the airflow direction: the air enters on the funnel-shaped side of the non-return valve. See also the schematic diagram on the inside of the housing above the pump intake and pump outlet.
Refit the connections to the pump head.
Operation Manual Vacuum Pump V-100 39/52
7 | Cleaning and servicing
7.2.5
Replacing tubing
BÜCHI Labortechnik AG
2
3
4
Fig. 25: Pump-head connection piece with GL-14 union nuts between the two pump heads
1 Screws for connections
2 Elbow connection
3 Pump-head connection piece
4 GL14 cap nut
Precondition:
R Pump has been shut down.
u u u u u u u u u
Unscrew the two knurled-head screws and remove the pump top cover.
Unscrew two screws (1) from each elbow connection (2).
Remove the two elbow connections together with the pump-head connection piece
(3) from the pump heads.
Unscrew the GL14 cap nuts (4) on each end of the pump-head connection piece counter-clockwise and remove the connections (2).
Pull the GL14 cap nuts off the pump-head connection piece.
Feed a new pump-head connection piece through the union nuts.
Screw the GL14 cap nuts onto the connections. Make sure that the FEP pipe seals under the GL14 cap nuts are in proper contact with the pump-head connection piece and are not damaged.
Fit the connections together with the pump-head connection piece on the pump heads.
Refit the pump top cover and fix in place.
40/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
8 Help with faults
8.1
Help with faults | 8
Faults, possible causes and remedies
Fault Possible cause
Device does not work.
Master switch is off.
System is not air-tight and cannot achieve terminal vacuum.
Device is not connected to a power supply.
Pipe clips not properly fitted or are damaged.
Tubing leaking (and brittle)
Membrane and/or valves dirty
Remedy u Switch on master switch.
u Check power supply.
u u
Check pipe clips (see Chap-
ter 7.2.5 "Replacing tubing", page 40).
Replace tubing (see Chap-
ter 7.2.5 "Replacing tubing", page 40).
u Clean or replace membrane and/or valves (see Chap-
ter 7.2.3 "Replacing the membrane", page 38 and
Chapter 7.2.4 "Replacing valve", page 39).
Pump fails to start.
Valve O-rings are leaking.
Switch on pump top cover not closing.
u Replace O-rings (see Chap-
ter 7.2.4 "Replacing valve", page 39).
u Check seating of pump top cover and correct if necessary. The cover is fixed by two knurled-head screws.
Operation Manual Vacuum Pump V-100 41/52
8 | Help with faults
8.2
BÜCHI Labortechnik AG
Customer service
Repairs to the device may only be carried out by authorized service technicians. The service technicians have been comprehensively technically trained and are aware of the potential hazards that can arise from the device.
The addresses of the official BUCHI Customer Service offices can be found on the
BUCHI website at: www.buchi.com. If you have any questions regarding technical issues or faults, please contact those offices.
Customer Services can offer you:
supply of spare parts
repairs
technical advice
42/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
9
Taking out of service and disposal | 9
Taking out of service and disposal
9.1
9.2
u u u
Taking out of service
Remove all tubing and communication cables from the device.
Run the pump to dry out tubing and diaphragms inside the pump.
Switch off the pump and disconnect it from the mains power supply.
Disposal
The operator is responsible for proper disposal of the Vacuum Pump.
u When disposing of equipment observe the local regulations and statutory requirements regarding waste disposal.
Operation Manual Vacuum Pump V-100 43/52
10 | Appendix BÜCHI Labortechnik AG
10 Appendix
Solvent
10.1
Solvent table
Formula Molar mass in g/ mol
Evaporation energy in J/g
58.1
88.1
553
595
Boiling point in °C at 1013 mbar
56
37
Density in g/cm 3
0.790
0.814
Vacuum in mbar for
40 °C boiling point
556
11
Acetone n -Amyl alcohol, n -pentanol
CH
3
H
6
O
C
5
H
12
O
Benzene n -butanol
Tert butyl alcohol (2methyl-2-propanol)
C
6
H
6
C
4
H
10
O
C
4
H
10
O
Chlorobenzene
Chloroform
Cyclohexane
Diethyl ether
C
6
H
5
Cl
CHCl
3
C
6
H
12
C
4
H
10
O
1,2-dichloroethane C
2
H
4
Cl
2 cis -1,2-dichloroethylene
C
2
H
2
Cl
2 trans -1,2dichloroethylene
Di-isopropyl ether
Dioxane
C
2
H
2
Cl
2
C
6
H
14
O
C
4
H
8
O
2
C
3
H
7
NO DMF (dimethylformamide)
Acetic acid
Ethanol
Ethylacetate
Heptane
Hexane
Isopropylalcohol
Isoamylalcohol (3methyl-1-butanol)
Methylethylketone
Methanol
C
4
H
8
O
CH
4
O
CH
2
CI
2
Methylene chloride, dichloromethane
Pentane n -propylalcohol
C
5
H
12
C
3
H
8
O
Pentachloroethane C
2
HCl
5
C
2
H
4
O
2
C
2
H
6
O
C
4
H
8
O
2
C
7
H
16
C
6
H
14
C
3
H
8
O
C
5
H
12
O
78.1
74.1
74.1
112.6
119.4
84.0
74.0
99.0
97.0
97.0
102.0
88.1
73.1
60.0
46.0
88.1
100.2
86.2
60.1
88.1
72.1
32.0
84.9
72.1
60.1
202.3
548
620
590
377
264
389
389
335
322
314
318
406
–
695
879
394
373
368
699
595
473
1227
373
381
787
201
48
80
65
40
80
118
82
132
62
81
35
84
60
68
101
153
118
79
77
98
69
82
129
36
97
162
0.877
0.810
0.789
1.257
0.724
1.034
0.949
1.049
0.789
0.900
0.684
0.660
0.786
0.809
1.106
1.483
0.779
0.714
1.235
1.284
0.805
0.791
1.327
0.626
0.804
1.680
236
25
130
44
175
240
120
360
137
14
36
474
235
850
210
479
751
375
107
11
243
337
850
850
67
13
44/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
Solvent Formula
1,1,2,2-tetrachloroethane
Trichloroethylene
Water
Xylene (mixture) o m p
-xylene
-xylene
-xylene
C
2
H
2
Cl
C
7
H
8
C
2
HCl
3
H
2
O
C
8
H
10
C
8
H
10
C
8
H
10
C
8
H
10
4
Carbon tetrachloride CCl
4
1,1,1-trichloroethane C
2
H
3
Cl
3
Tetrachloroethylene C
2
Cl
4
THF (tetrahydrofurane)
C
4
H
8
O
Toluene
Appendix | 10
Molar mass in g/ mol
Evaporation energy in J/g
167.9
247
Boiling point in °C at 1013 mbar
146
Density in g/cm 3
1.595
Vacuum in mbar for
40 °C boiling point
20
153.8
133.4
165.8
72.1
92.2
131.3
18.0
106.2
106.2
106.2
106.2
226
251
234
–
427
264
2261
389
–
–
–
77
74
121
67
111
87
100
–
144
139
138
1.594
1.339
1.623
0.889
0.867
1.464
1.000
–
0.880
0.864
0.861
–
–
77
183
72
25
–
271
300
53
374
Operation Manual Vacuum Pump V-100 45/52
10 | Appendix BÜCHI Labortechnik AG
10.2
Spare parts and accessories
u Use only genuine BUCHI consumables and spare parts in order to ensure correct, safe and reliable operation of the system.
NOTE
Any modifications of spare parts or assemblies are only allowed with the prior written permission of BUCHI.
10.2.1
Accessories
Secondary condensers
Secondary condenser C. Cold trap, P+G, incl. holder
Condenses vapor before getting into the pump. In use with ice or dry ice. Contents: 500 mL receiving flask, connection piece, holder for the vacuum pump
047190
Secondary condenser V. Vertical condenser, incl. insulator, holder
Condenses vapor before getting into the pump. Used with recirculating chiller or tap water. Contents: 500 mL receiving flask, connection piece, holder for the vacuum pump
047180
Tubing
FEP, Ø6/8mm, transparent, per m
Utilization: Vacuum, cooling media
Natural rubber, Ø6/16mm, red, per m
Utilization: Vacuum
Nyflex, PVC-P, Ø8/14mm, transparent, per m
Utilization: Vacuum, cooling media, feeding (industrial Rotavapor)
PTFE, Ø8/10mm, white, per m
Utilization: Vacuum, feeding (industrial Rotavapor)
Silicone rubber, Ø6/9mm, transparent, per m
Utilization: Cooling media
Communication cables
Mini-DIN, 0.6m
Connection between interface and vacuum pump
Mini-DIN, Y-shielded, 650mm
Used when connecting vacuum pump with two vacuum controllers
Receiving flasks
Glass, BJ35/20, 250mL
Glass, BJ35/20, 250mL, P+G
Glass, BJ35/20, 500mL
Glass, BJ35/20, 500mL, P+G
027900
017622
004113
027277
004133
11060882
031920
000423
11060907
000424
025264
46/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG
Further accessories
Manometer with needle valve. Incl. holder for pump, valve, vacuum gauge
For manual vacuum adjustment
Manometer with needle valve. Incl. valve, vacuum gauge, not incl.
holder
Valve unit. Incl. Woulff bottle, 125mL, P+G, holder
The valve is only to use in combination with a vacuum controller/interface
Woulff bottle. 125mL, P+G, incl. holder
For trapping particles and droplets and for pressure equalization
Woulff bottle. 3-neck, 800mL, P+G
For trapping particles and droplets and for pressure equalization
047291
047391
047160
047170
025519
10.2.2
Wear parts
Seals
For cap nut, GL14, FEP
Set. 10pcs, for hose barbs, GL14, EPDM, black
Set. 10pcs, for hose barbs, GL14, FPM, green
Set. 20pcs, for hose barbs, GL14, silicone, red
038225
040029
040040
040023
Hose barbs
Bent, GL14, incl. silicone seal
Set. 3pcs, bent, GL14, silicone seal
Content: Hose barbs, seals
Set. 4pcs, bent, GL14, EPDM seal
Content: Hose barbs, cap nuts, seals
Set. 4pcs, bent, GL14, FEP seal
Content: Hose barbs, cap nuts, seals
Set. 4pcs, bent, GL14, silicone seal, incl. cap nut
Content: Hose barbs, cap nuts, seals
Set. 4pcs, bent, GL14, silicone seal, incl. cap nut
Content: Hose barbs, cap nuts, seals
Set. 4pcs, straight, GL14, EPDM seal
Content: Hose barbs, cap nuts, seals
Set. 4pcs, straight, GL14, silicone seal
Content: Hose barbs, cap nuts, seals
Set. 6pcs, bent (4), straight (2), GL14, silicone seal
Content: Hose barbs, cap nuts, seals
Appendix | 10
018916
041987
043129
040295
037287
043128
040296
037642
038000
Further wear parts
Membrane. For pump head, incl. clamp, support ring
Membranes, set. 10pcs, for pump head, incl. clamp, support ring
O-ring. For secondary condenser, FKM/FEP, Ø28.2/2.6mm
O-rings, set. 4pcs, FFKM, Ø15.4/1.55mm, white
047153
11055214
11057661
11057136
Operation Manual Vacuum Pump V-100 47/52
10 | Appendix BÜCHI Labortechnik AG
Check valves, set. 4pcs, incl. O-ring
Check valves, set. 4pcs, without O-rings
Screw caps, set. 5pcs, GL14
Cap nuts, set. 10pcs, screw cap with hole, GL14, incl. FEP seal
Content: Hose barbs, cap nuts, seals
Cap nuts, set. 10pcs, cap nuts with hole, GL14
10.2.3
Spare parts
Connection piece. Straight, for pump head
Content: Connection straight, valve, O-ring, cap nut, GL14, FEP seal
Connection piece. Bent, for pump head
Content: Connection bent, valve, O-ring, cap nut, GL14, FEP seal
Lid. For cold trap, Ø68mm
Insulator. For secondary condenser
Prevents formation of condensed water
Ball joint clamp. For BJ35/20
Secondary condenser V. Vertical condenser
Condenses remaining vapors after the vacuum pump outlet. Used along with a recirculating chiller or tap water
Secondary condenser V. Vertical condenser
Condenses remaining vapors after the vacuum pump outlet. Used along with a recirculating chiller or tap water
Pump head. For Vacuum Pump V-100/V-700/V-710
Pump head, set. For Vacuum Pump V-100
Content: Pump head, set connection piece straight, set connection piece angled
Silencer. Incl. cap nut, GL14, FEP seal
For Vacuum Pump V-100 / V-700 or V-710
Tubing. Silicone rubber, Ø6/16, red, 2m
Utilization: Vacuum
Support secondary condenser V. Incl. holder, FEP seal, connection piece
Support condenser V/C. Holder
Connection piece. PTFE, Ø6/8mm, 162mm
Tubing between vacuum controller/interface and Woulff bottle
Connection piece. PTFE, Ø6/8mm, 77mm
Tubing between vacuum pump and Woulff bottle
Packaging. V-100/V-700, with glass assembly
Packaging. V-100/V-700, without glass assembly
047156
11058389
040624
041999
041956
11061580
11061579
047193
047183
003275
047181
11061840
11061578
11061577
047090
040459
11055584
047182
047154
047066
045617
045616
48/52 Operation Manual Vacuum Pump V-100
BÜCHI Labortechnik AG Appendix | 10
10.3
List of abbreviations
Abbreviation Meaning
ADR Accord européen relatif au transport international des marchandises dangereuses par route (European Agreement concerning the
International Carriage of Dangerous Goods by Road)
DKD
EPDM
Deutscher Kalibrierdienst (German Calibration Service)
Ethylene propylene diene monomer
FEP
FFKM
FPM
GGVE
GGVS
Fluorinated ethylene propylene
Perfluoro-elastomer
Fluorinated propylene monomer
Gefahrgutverordnung Eisenbahn (German Hazardous Goods Regulations for Railways)
Gefahrgutverordnung Strasse (German Hazardous Goods Regulations for Road Transport)
PBT
PEEK
PP
PTFE
RID
Polybutylene terephthalate
Polyetheretherketone
Polypropylene
Polytetrafluoroethylene
Règlement concernant le transport international ferroviaire de marchandises dangereuses (Regulations concerning the International Carriage of Dangerous Goods by Rail)
10.4
Health and safety approval
To guarantee the health and safety of our staff and to comply with the law and the regulations for handling hazardous materials, for the purposes of health and safety at work and safe disposal of waste, no products may be sent back to BÜCHI Labortechnik AG or repaired unless we have received the declaration below, completed and signed.
Products sent to us will not be accepted for repair or DKD calibration until we have received this declaration.
u u u u u
Copy the form overleaf and complete it.
Make sure that you know the full details of the substances with which the device has been in contact and the all questions have been answered fully and correctly.
Send the completed from to us in advance by post or fax. The declaration must reach us before the device.
Enclose a copy of the declaration with the device.
If the product is contaminated, inform the carrier (in accordance with GGVE/
GGVS/RID/ADR).
If the declaration is missing or the procedure described is not followed, the repairs will be delayed. We ask for your understanding and cooperation with regard to these measures.
Operation Manual Vacuum Pump V-100 49/52
10 | Appendix BÜCHI Labortechnik AG
10.5
Health and safety
Declaration regarding the safety, hazards and safe disposal of waste
To guarantee the health and safety of our staff and to comply with the law and the regulations for handling hazardous materials, regarding health and safety at work, and to comply with safety regulations, health and safety requirements and requirements for safe disposal of waste such as chemical waste, chemical residues or solvents, the form below must be fully completed and signed whenever devices or faulty components are to be sent back to our factory.
Products or components will not be accepted if this declaration has not been provided.
Device
Model: Part/Device no.:
Declaration for non-hazardous materials
We hereby assure that the products returned have not been used in the laboratory and are new.
have not been in contact with toxic, corrosive, biologically active, explosive, radioactive or other hazardous materials.
are not contaminated. The solvents or residues of the substances pumped have been removed.
Declaration for hazardous materials
In respect of the products returned, we hereby assure that all substances (toxic, corrosive, biologically active, explosive, radioactive or otherwise hazardous) that have been pumped by the products or have otherwise been in contact with the products are listed below.
the products have been cleaned, decontaminated, sterilised inside and outside and all inlets and outlets are sealed.
List of hazardous materials that have been in contact with the products:
Chemical, material Hazard category
Final declaration We hereby declare that
we are fully conversant with the substances that have been in contact with the products and have answered all questions correctly.
we have taken all measures necessary to prevent potential hazards in respect of the products returned.
Company name or stamp:
Place, date:
Name (block letters), position
(block letters):
Signature:
50/52 Operation Manual Vacuum Pump V-100
Quality in your hands
BUCHI Affiliates:
Europe
Switzerland/Austria
BÜCHI Labortechnik AG
CH – 9230 Flawil
T +41 71 394 63 63
F +41 71 394 64 64 [email protected]
www.buchi.com
Italy
BUCHI Italia s.r.l.
IT – 20010 Cornaredo (MI)
T +39 02 824 50 11
F +39 02 575 12 855 [email protected]
www.buchi.com/it-it
Benelux
BÜCHI Labortechnik GmbH
Branch Office Benelux
NL – 3342 GT Hendrik-Ido-Ambacht
T +31 78 684 94 29
F +31 78 684 94 30 [email protected]
www.buchi.com/bx-en
Russia
BUCHI Russia/CIS
Russia 127287 Moscow
T +7 495 36 36 495 [email protected]
www.buchi.com/ru-ru
France
BUCHI Sarl
FR – 94656 Rungis Cedex
T +33 1 56 70 62 50
F +33 1 46 86 00 31 [email protected]
www.buchi.com/fr-fr
United Kingdom
BUCHI UK Ltd.
GB – Oldham OL9 9QL
T +44 161 633 1000
F +44 161 633 1007 [email protected]
www.buchi.com/gb-en
Germany
BÜCHI Labortechnik GmbH
DE – 45127 Essen
T +800 414 0 414 0 (Toll Free)
T +49 201 747 49 0
F +49 201 747 49 20 [email protected]
www.buchi.com/de-de
Germany
BÜCHI NIR-Online
DE – 69190 Walldorf
T +49 6227 73 26 60
F +49 6227 73 26 70 [email protected]
www.nir-online.de
America
Brazil
BUCHI Brasil Ltda.
BR – Valinhos SP 13271-200
T +55 19 3849 1201
F +55 19 3849 2907 [email protected]
www.buchi.com/br-pt
USA/Canada
BUCHI Corporation
US – New Castle, DE 19720
T +1 877 692 8244 (Toll Free)
T +1 302 652 3000
F +1 302 652 8777 [email protected]
www.buchi.com/us-en
Asia
China
BUCHI China
CN – 200233 Shanghai
T +86 21 6280 3366
F +86 21 5230 8821 [email protected]
www.buchi.com/cn-zh
India
BUCHI India Private Ltd.
IN – Mumbai 400 055
T +91 22 667 75400
F +91 22 667 18986 [email protected] www.buchi.com/in-en
Indonesia
PT. BUCHI Indonesia
ID – Tangerang 15321
T +62 21 537 62 16
F +62 21 537 62 17 [email protected]
www.buchi.com/id-in
Japan
Nihon BUCHI K.K.
JP – Tokyo 110-0008
T +81 3 3821 4777
F +81 3 3821 4555 [email protected]
www.buchi.com/jp-ja
Korea
BUCHI Korea Inc.
KR – Seoul 153-782
T +82 2 6718 7500
F +82 2 6718 7599 [email protected]
www.buchi.com/kr-ko
Malaysia
BUCHI Malaysia Sdn. Bhd.
MY – 47301 Petaling Jaya,
Selangor
T +60 3 7832 0310
F +60 3 7832 0309 [email protected]
www.buchi.com/my-en
BUCHI Support Centers:
South East Asia
BUCHI (Thailand) Ltd.
TH-Bangkok 10600
T +66 2 862 08 51
F +66 2 862 08 54 [email protected]
www.buchi.com/th-th
Middle East
BÜCHI Labortechnik AG
UAE – Dubai
T +971 4 313 2860
F +971 4 313 2861 [email protected]
www.buchi.com
Singapore
BUCHI Singapore Pte. Ltd.
SG – Singapore 609919
T +65 6565 1175
F +65 6566 7047 [email protected]
www.buchi.com/sg-en
Latin America
BUCHI Latinoamérica
S. de R.L. de C.V.
MX – Mexico City
T +52 55 9001 5386 [email protected]
www.buchi.com/es-es
Thailand
BUCHI (Thailand) Ltd.
TH – Bangkok 10600
T +66 2 862 08 51
F +66 2 862 08 54 [email protected]
www.buchi.com/th-th
We are represented by more than 100 distribution partners worldwide.
Find your local representative at: www.buchi.com

Public link updated
The public link to your chat has been updated.
Advertisement