LCQ Fleet Getting Connected Guide Revision A

LCQ Fleet
Getting Connected Guide
97055-97224 Revision A
September 2015
© 2015 Thermo Fisher Scientific Inc. All rights reserved.
Ion Max-S and SpectraSYSTEM are trademarks, and Accela, Ion Max, LCQ, LCQ Fleet, and Xcalibur are
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The contents of this document are subject to change without notice. All technical information in this
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Release history: Rev A, September 2015
Software version: Microsoft Windows 7 Professional (32-bit and 64-bit) SP1—Thermo Foundation 2.0 and
later, and Thermo Xcalibur 2.2 and later; Windows XP Workstation SP3—Foundation 1.0.2 SP2 or earlier,
and Xcalibur 2.1 SP1 or earlier; Thermo LTQ Tune Plus 2.7.0 and later
For Research Use Only. Not for use in diagnostic procedures.
Regulatory Compliance
Thermo Fisher Scientific performs complete testing and evaluation of its products to ensure full compliance with
applicable domestic and international regulations. When the system is delivered to you, it meets all pertinent
electromagnetic compatibility (EMC) and safety standards as described in the next section or sections by product name.
Changes that you make to your system may void compliance with one or more of these EMC and safety standards.
Changes to your system include replacing a part or adding components, options, or peripherals not specifically
authorized and qualified by Thermo Fisher Scientific. To ensure continued compliance with EMC and safety standards,
replacement parts and additional components, options, and peripherals must be ordered from Thermo Fisher Scientific
or one of its authorized representatives.
EMC Directive 2004/108/EC
EMC compliance has been evaluated by TUV Rheinland of North America.
CFR 47, FCC Part 15, Subpart B, Class A: 2015
EN 61000-4-2: 2009
CISPR 11: 2009 + A1
EN 61000-4-3: 2006 + A1 + A2
ICES-003: 2014
EN 61000-4-4: 2004 + A1
EN 55011: 2009 + A1
EN 61000-4-5: 2006
EN 61326-1: 2013
EN 61000-4-6: 2009
EN 61000-3- 2: 2006 + A1 + A2
EN 61000-4-11: 2004
EN 61000-3-3: 2008
Low Voltage Safety Compliance
This device complies with Low Voltage Directive 2006/95/EC and harmonized standard IEC/EN/CSA/UL 61010-1,
Third Edition.
FCC Compliance Statement
THIS DEVICE COMPLIES WITH PART 15 OF THE FCC RULES. OPERATION IS SUBJECT TO
THE FOLLOWING TWO CONDITIONS: (1) THIS DEVICE MAY NOT CAUSE HARMFUL
INTERFERENCE, AND (2) THIS DEVICE MUST ACCEPT ANY INTERFERENCE RECEIVED,
INCLUDING INTERFERENCE THAT MAY CAUSE UNDESIRED OPERATION.
CAUTION Read and understand the various precautionary notes, signs, and symbols contained inside
this manual pertaining to the safe use and operation of this product before using the device.
Notice on Lifting and Handling of
Thermo Scientific Instruments
For your safety, and in compliance with international regulations, the physical handling of this Thermo Fisher Scientific
instrument requires a team effort to lift and/or move the instrument. This instrument is too heavy and/or bulky for one
person alone to handle safely.
Notice on the Proper Use of
Thermo Scientific Instruments
In compliance with international regulations: This instrument must be used in the manner specified by Thermo Fisher
Scientific to ensure protections provided by the instrument are not impaired. Deviations from specified instructions on
the proper use of the instrument include changes to the system and part replacement. Accordingly, order replacement
parts from Thermo Fisher Scientific or one of its authorized representatives.
WEEE Directive
2012/19/EU
Thermo Fisher Scientific is registered with B2B Compliance (B2Bcompliance.org.uk) in the UK and with the
European Recycling Platform (ERP-recycling.org) in all other countries of the European Union and in Norway.
If this product is located in Europe and you want to participate in the Thermo Fisher Scientific Business-to-Business
(B2B) Recycling Program, send an email request to [email protected] with the following information:
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• Pick-up address and contact person (include contact information)
• Appropriate pick-up time
• Declaration of decontamination, stating that all hazardous fluids or material have been removed from the product
For additional information about the Restriction on Hazardous Substances (RoHS) Directive for the European Union,
search for RoHS on the Thermo Fisher Scientific European language websites.
IMPORTANT This recycling program is not for biological hazard products or for products that have been medically
contaminated. You must treat these types of products as biohazard waste and dispose of them in accordance with
your local regulations.
Directive DEEE
2012/19/EU
Thermo Fisher Scientific s'est associé avec une ou plusieurs sociétés de recyclage dans chaque état membre de l’Union
Européenne et ce produit devrait être collecté ou recyclé par celle(s)-ci. Pour davantage d'informations, rendez-vous sur
la page www.thermoscientific.fr/rohs.
WEEE Direktive
2012/19/EU
Thermo Fisher Scientific hat Vereinbarungen mit Verwertungs-/Entsorgungsfirmen in allen EU-Mitgliedsstaaten
getroffen, damit dieses Produkt durch diese Firmen wiederverwertet oder entsorgt werden kann. Weitere Informationen
finden Sie unter www.thermoscientific.de/rohs.
C
Contents
Preface . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . xi
Related Documentation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .xi
Cautions and Special Notices . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .xiii
Contacting Us . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .xiv
Chapter 1
Setting Up the Mass Spectrometer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Connecting the Gas Supplies. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2
Fittings, Parts, and Tools. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3
Connecting the Helium Gas Supply . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Connecting the High-Purity Nitrogen Gas Supply . . . . . . . . . . . . . . . . . . . . . 5
Connecting the Vacuum System . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5
Connecting the Mass Spectrometer to the Forepump . . . . . . . . . . . . . . . . . . . 6
Connecting the Forepump to the Lab Exhaust System . . . . . . . . . . . . . . . . . . 9
Connecting Line Power to the Forepump . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
Connecting the Data System Computer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
Connecting the Mass Spectrometer to Line Power . . . . . . . . . . . . . . . . . . . . . . 12
Chapter 2
Ion Max and Ion Max-S Ion Sources. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
API Source Housing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13
API Source Housing Drain . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 15
Chapter 3
External Peripheral Devices . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
Interface Kits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17
External Devices Controlled by a Mass Spectrometry Application . . . . . . . . . . . 18
Connecting the Contact Closure Cable . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
Selecting the Start Instrument . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19
External Devices Not Controlled by a Mass Spectrometry Application . . . . . . . 21
Connecting the Contact Closure Cable . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21
Starting a Sequence Run from the Xcalibur Data System. . . . . . . . . . . . . . . . 22
Triggering External Devices. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25
Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
Index . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
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LCQ Fleet Getting Connected Guide
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F
Figures
Figure 1.
Figure 2.
Figure 3.
Figure 4.
Figure 5.
Figure 6.
Figure 7.
Figure 8.
Figure 9.
Figure 10.
Figure 11.
Figure 12.
Thermo Scientific
Gas connections on the back of the LCQ Fleet MS . . . . . . . . . . . . . . . . . . . . . . . 2
Connector assembly for the helium tubing . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Vacuum hose assembly (P/N 97055-60135) . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Connections between the MS vacuum port, forepump, and lab exhaust system . . 8
Power panel for the LCQ Fleet MS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 10
API source housing connection . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
API source drain assembly and waste container . . . . . . . . . . . . . . . . . . . . . . . . . 15
Peripheral Control and Analog Input terminals . . . . . . . . . . . . . . . . . . . . . . . . . 19
Run Sequence dialog box showing the default start instrument. . . . . . . . . . . . . 20
Change Instruments In Use dialog box showing the default start instrument . . . 20
Run Sequence dialog box with the mass spectrometer as the start instrument . . . 23
Change Instruments In Use dialog box without a specified start instrument . . . . 23
LCQ Fleet Getting Connected Guide
ix
Figures
x
LCQ Fleet Getting Connected Guide
Thermo Scientific
P
Preface
The LCQ Fleet Getting Connected Guide describes how to connect the Thermo Scientific™
LCQ™ Fleet™ mass spectrometer (MS) to line power (ac mains power system), the data system
computer, the external vacuum system, the waste exhaust system, and external peripheral
devices. External devices include those that are controlled from or are independent of Thermo
mass spectrometry applications, such as the Thermo Xcalibur™ data system.
Contents
• Related Documentation
• Cautions and Special Notices
• Contacting Us
 To suggest changes to the documentation or to the Help
Complete a brief survey about this document by clicking the button below.
Thank you in advance for your help.
Related Documentation
The LCQ Fleet mass spectrometer includes complete documentation. In addition to this
guide, you can also access the following documents as PDF files from the data system
computer:
• LCQ Fleet Preinstallation Requirements Guide
• LCQ Fleet Getting Started Guide
• LCQ Fleet Hardware Manual
Thermo Scientific
LCQ Fleet Getting Connected Guide
xi
Preface
• Ion Max and Ion Max-S API Source Hardware Manual
• Safety and Regulatory Guide
The LCQ Fleet also ships with a printed copy of the Safety and Regulatory Guide. This
guide contains important safety information about Thermo Scientific liquid
chromatography (LC) and mass spectrometry (MS) systems. Make sure that all lab
personnel have read and have access to this document.
 To view the product manuals
From the Microsoft™ Windows™ taskbar, choose Start > All Programs > Thermo
Instruments > Manuals > LCQ Fleet, and then open the PDF file to view it.
 To view the data system Help
• From the application window, choose Help from the menu bar.
• If information about setting parameters is available for a specific view, page, or dialog
box, click Help or press the F1 key for information about setting parameters.
 To download user documentation from the Thermo Scientific website
1. Go to www.thermoscientific.com.
2. In the Search box, type the product name and press ENTER.
3. In the left pane, select Documents & Videos, and then under Refine By Category, click
Operations and Maintenance.
4. (Optional) Narrow the search results or modify the display as applicable:
• For all related user manuals and quick references, click Operator Manuals.
• For installation and preinstallation requirements guides, click Installation
Instructions.
• For documents translated into a specific language, use the Refine By Language
feature.
• Use the Sort By options or the Refine Your Search box (above the search results
display).
5. Download the document as follows:
a. Click the document title or click Download to open the file.
b. Save the file.
xii
LCQ Fleet Getting Connected Guide
Thermo Scientific
Preface
Cautions and Special Notices
Make sure you follow the cautions and special notices presented in this guide. Cautions and
special notices appear in boxes; those concerning safety or possible system damage also have
corresponding caution symbols.
This guide uses the following types of cautions and special notices.
CAUTION Highlights hazards to humans, property, or the environment. Each CAUTION
notice is accompanied by an appropriate CAUTION symbol.
IMPORTANT Highlights information necessary to prevent damage to software, loss of
data, or invalid test results; or might contain information that is critical for optimal
performance of the system.
Note Highlights information of general interest.
Tip Highlights helpful information that can make a task easier.
The LCQ Fleet Getting Connected Guide contains the following caution-specific symbols
(Table 1).
Table 1. Caution-specific symbols and their meaning (Sheet 1 of 2)
Symbol
Meaning
Chemical hazard: Observe Good Laboratory Practices (GLP) when
handling chemicals. Only work with volatile chemicals under a fume
or exhaust hood.Wear gloves and other protective equipment, as
appropriate, when handling toxic, carcinogenic, mutagenic, corrosive,
or irritant chemicals. Use approved containers and proper procedures
to dispose of waste oil and when handling wetted parts of the
instrument.
Risk of eye injury: Eye injury could occur from splattered chemicals or
airborne particles. Wear safety glasses when handling chemicals or
servicing the instrument.
Thermo Scientific
LCQ Fleet Getting Connected Guide
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Preface
Table 1. Caution-specific symbols and their meaning (Sheet 2 of 2)
Symbol
Meaning
Hot surface: Allow heated components to cool before touching or
servicing the instrument.
Sharp object: Avoid handling the tip of the syringe needle.
Trip obstacle: Be aware of cords, hoses, or other objects located on the
floor.
Contacting Us
There are several ways to contact Thermo Fisher Scientific for the information you need. You
can use your smartphone to scan a QR code, which opens your email application or browser.
Contact us
xiv
LCQ Fleet Getting Connected Guide
Customer Service and Sales
Technical Support
(U.S.) 1 (800) 532-4752
(U.S.) 1 (800) 532-4752
(U.S.) 1 (561) 688-8731
(U.S.) 1 (561) 688-8736
us.customer-support.analyze
@thermofisher.com
us.techsupport.analyze
@thermofisher.com
Thermo Scientific
Preface
Contact us
Customer Service and Sales
Technical Support
 To find global contact information or customize your request
1. Go to www.thermoscientific.com.
2. Click Contact Us, select the Using/Servicing a Product option, and then
type the product name.
3. Use the phone number, email address, or online form.
 To find product support, knowledge bases, and resources
Go to www.thermoscientific.com/support.
 To find product information
Go to www.thermoscientific.com/lc-ms.
Note To provide feedback for this document:
• Send an email message to Technical Publications ([email protected]).
• Complete a survey at www.surveymonkey.com/s/PQM6P62.
Thermo Scientific
LCQ Fleet Getting Connected Guide
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Preface
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LCQ Fleet Getting Connected Guide
Thermo Scientific
1
Setting Up the Mass Spectrometer
This chapter describes how to connect the LCQ Fleet mass spectrometer to the gas supplies,
vacuum system, data system computer, and line power (ac mains power system).
Note
• A Thermo Fisher Scientific field service engineer must install the mass spectrometer.
• The Glossary defines some of the terms used in this guide.
• For instructions about setting up the application parameters for tuning, calibrating,
and testing, refer to the LCQ Fleet Getting Started Guide.
Contents
• Connecting the Gas Supplies
• Connecting the Vacuum System
• Connecting the Data System Computer
• Connecting the Mass Spectrometer to Line Power
Thermo Scientific
LCQ Fleet Getting Connected Guide
1
1
Setting Up the Mass Spectrometer
Connecting the Gas Supplies
Connecting the Gas Supplies
Table 2 lists the required gases and specifies their function.
Table 2. Summary of required gas types
Gas type
Gas function
Helium:
• Ultra high purity (UHP), 99.999%
• 275 ±70 kPa (40 ±10 psi)
collision gas and damping gas
Nitrogen:
• High purity (HP), 99%
• 690 ±140 kPa (100 ±20 psi)
auxiliary gas, collision gas, sheath gas, and
sweep gas
Figure 1 shows the location of the gas inlets on the back of the instrument.
Figure 1.
Gas connections on the back of the LCQ Fleet MS
Nitrogen In
Helium In
Note
• Make sure that the lab already has the gas supply lines installed, properly terminated,
and ready to connect to the MS. For information about the gas supply lines, refer to
the LCQ Fleet Preinstallation Requirements Guide.
• If your system includes additional devices that require their own gas connections, refer
to the connection instructions in the appropriate manuals for those devices.
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LCQ Fleet Getting Connected Guide
Thermo Scientific
1
Setting Up the Mass Spectrometer
Connecting the Gas Supplies
Fittings, Parts, and Tools
Table 3 lists the parts required to connect the LCQ Fleet MS to the gas delivery system.
Connections and gas delivery systems might vary. You are responsible for supplying any
additional fittings or connections necessary during installation.
The following kits that shipped with the instrument contain the tubings and fittings listed in
Table 3:
• MS Setup Kit (P/N 70111-62033)
• MS Accessory Kit (P/N 97055-62055)
• Special Accessory Kit for the LCQ Fleet (P/N 97055-62060)
Table 3. Shipped gas plumbing hardware
Gas type
Part description
Part number
Helium
Ferrule, two-piece set, brass, 1/8 in. ID
00101-02500 (back)
00101-08500 (front)
Swagelok™-type nut, brass, 1/8 in. ID
00101-15500
Tubing, copper, pre-cleaned, 1/8 in. OD,
3 m (10 ft) long
00301-22701
You might need an additional length of tubing
for the installation.
Nitrogen,
HP
Connection for the other end of the tubing to
the helium gas source
–a
Ferrule, two-piece set, brass, 1/4 in. ID
00101-04000 (back)
00101-10000 (front)
Swagelok-type nut, brass, 1/4 in. ID
00101-12500
Tubing, Teflon™ PFA, 1/4 in. OD, 4.6 m (15 ft) 00101-50100
long
You might need an additional length of tubing
for the installation.
Connection for the other end of the tubing to
the nitrogen gas source
a
Thermo Scientific
–a
Customer-supplied item
LCQ Fleet Getting Connected Guide
3
1
Setting Up the Mass Spectrometer
Connecting the Gas Supplies
Connecting the Helium Gas Supply
The helium gas must be UHP (99.999%) with less than 1.0 ppm each of total hydrocarbons,
oxygen, and water. The required gas pressure is 275 ±70 kPa (40 ±10 psi). Terminate the
helium gas supply line with the parts listed in Table 3 on page 3.
 To connect the helium supply to the instrument
Note Use the appropriate 1/8 in. fittings and parts listed on page 3.
1. Cut an appropriate length of the precleaned, copper tubing.
If you prefer, you can use stainless steel tubing.
2. Connect the Swagelok-type nut to one end of the tubing, followed by the two-piece
ferrule set (Figure 2), and then connect this end of the tubing to the Helium In gas inlet
on the back of the instrument (Figure 1 on page 2).
Figure 2.
Gas tubing
Connector assembly for the helium tubing
Back ferrule
Front ferrule
Swagelok-type nut
3. On the other end of the tubing, connect an appropriate fitting for the gas supply.
4. Connect the tubing to the UHP helium gas supply.
IMPORTANT
• After you start using the LCQ Fleet MS, do not shut off the helium gas. Optimum
performance requires a continuous flow of helium.
• If you intend to use helium for sparging your LC solvents, you must have a second
tank and regulator.
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LCQ Fleet Getting Connected Guide
Thermo Scientific
1
Setting Up the Mass Spectrometer
Connecting the Vacuum System
Connecting the High-Purity Nitrogen Gas Supply
The nitrogen gas must be HP (99%). The required gas pressure is 690 ±140 kPa
(100 ±20 psi).
 To connect the HP nitrogen supply to the instrument
Note Use the appropriate 1/4 in. fittings and parts listed on page 3.
1. Cut an appropriate length of the Teflon PFA tubing.
2. Connect the Swagelok-type nut to one end of the tubing, followed by the two-piece
ferrule set (Figure 2 on page 4), and then connect this end of the tubing to the HP
nitrogen gas supply.
3. Push the other end of the tubing into the Nitrogen In gas inlet on the back of the
instrument (Figure 1 on page 2).
Connecting the Vacuum System
The LCQ Fleet MS requires one forepump (or roughing pump) to maintain the internal
vacuum pressure.
CAUTION For forepump operation and maintenance, refer to the operating instructions
provided with the pump. In particular, note the following:
• Prevent the forepump from over-heating by ensuring that there is sufficient air
clearance around the pump.
• Maintain the exhaust pressure from atmospheric pressure minus 15 mbar to 1.15 bar
absolute (0.15 bar relative).
• Follow the instructions for adding and changing the oil.
To connect the vacuum system, follow these procedures:
• Connecting the Mass Spectrometer to the Forepump
• Connecting the Forepump to the Lab Exhaust System
• Connecting Line Power to the Forepump
Thermo Scientific
LCQ Fleet Getting Connected Guide
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1
Setting Up the Mass Spectrometer
Connecting the Vacuum System
Connecting the Mass Spectrometer to the Forepump
The LCQ Fleet MS requires one forepump. Figure 3 shows the vacuum hose assembly that
consists of the parts provided in the Vacuum Hose Accessory Kit (Table 4) and provided with
the forepump (Table 5).
IMPORTANT To ensure the best pumping performance, limit the length of the vacuum
hose to no more than 2.4 m (8 ft).
Figure 3.
Vacuum hose assembly (P/N 97055-60135)
Connects to the instrument.
(2.16 in. OD adapter)
Connects to the forepump.
(1.5 in. OD adapter)
Table 4. Assembly parts in the Vacuum Hose Accessory Kit (Sheet 1 of 2)
6
Image
Part description
Part number
—
Vacuum hose, reinforced PVC, 1.5 in. ID,
2.4 m (8 ft) long
00301-24163
Centering ring with O-ring, nitrile and
aluminum, NW40
00108-02-00005
Hose adapter, aluminum, 1.5–2.2 in. OD
(connects to the instrument)
97055-20714
Hose adapter, aluminum, 1.5 in. OD
(connects to the forepump)
70111-20210
LCQ Fleet Getting Connected Guide
Thermo Scientific
1
Setting Up the Mass Spectrometer
Connecting the Vacuum System
Table 4. Assembly parts in the Vacuum Hose Accessory Kit (Sheet 2 of 2)
Image
Part description
Part number
Hose clamp, high-torque, stainless steel,
1.25–2.125 in.
00201-99-00056
Swing clamp, aluminum, NW40
00108-02-00004
Table 5. Assembly parts supplied with the forepump
Image
Part description
Part number
Centering ring with O-ring, Viton™ and
aluminum, NW25
00108-02011
Swing clamp, aluminum, NW25
00102-10020
 To connect the forepump to the instrument
1. Connect the vacuum hose to the instrument as follows:
a. Place the NW40 centering ring on the flange of the vacuum port located on the back
of the instrument.
b. Using the NW40 swing clamp, secure the end of the vacuum hose that has the
instrument adapter to the vacuum port.
2. Connect the other end of the vacuum hose to the forepump as follows:
a. Place a NW25 centering ring on the flange of the forepump inlet port.
b. Using a NW25 swing clamp, secure the vacuum hose to the forepump.
Figure 4 show the connections for the LCQ Fleet vacuum system.
Thermo Scientific
LCQ Fleet Getting Connected Guide
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1
Setting Up the Mass Spectrometer
Connecting the Vacuum System
Figure 4.
Connections between the MS vacuum port, forepump, and lab exhaust system
Back of the MS
Vacuum port connects to the forepump.
Optional oil
mist filter
EDWARDS
30
Forepump
8
LCQ Fleet Getting Connected Guide
Blue hose (connects to
the lab exhaust system)
Thermo Scientific
1
Setting Up the Mass Spectrometer
Connecting the Vacuum System
Connecting the Forepump to the Lab Exhaust System
To operate the forepump properly requires an efficient fume exhaust system. Most
atmospheric pressure ionization (API) applications contribute to solvents accumulating in the
forepump. While Thermo Fisher Scientific recommends that you periodically open the gas
ballast valve (on the top of the pump) to purge the accumulated solvents, opening the valve
might allow a large volume of volatile solvent waste to enter the fume exhaust system. Because
the optional oil mist filter connects to the ballast port, be aware that opening the valve also
drains the oil mist filter. Choose an exhaust system that can accommodate the periodic
purging of these solvents. The frequency of the purging depends on the throughput of the
system—never operate a pump continuously with the gas ballast valve open.
CAUTION Because the forepump exhaust is a health hazard, make sure that it vents to an
appropriate external exhaust system.
Table 6 lists the parts required to connect the forepump to the lab exhaust system. These parts
are in the MS Setup Kit (P/N 70111-62033) and the Mechanical Pump Accessory Kit
(P/N 70111-62048).
Table 6. Shipped forepump exhaust system hardware
Image
Part description
Quantity
Part number
Exhaust hose, blue, 1 in. ID,
6.1 m (20 ft) long
1
00301-08301
Hose clamp, high-torque, stainless steel,
1.25–2.125 in.
2
00201-99-00056
 To connect the forepump to the lab exhaust system
1. Using a hose clamp, secure the blue exhaust hose to the forepump exhaust port.
2. Using a hose clamp, secure the other end of the hose to the lab exhaust system.
Figure 4 on page 8 shows the blue exhaust hose connection.
CAUTION Run the exhaust hose at floor level for at least 2 m (6.6 ft). This hose acts as a
trap for exhaust fumes that would otherwise recondense in the forepump oil.
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LCQ Fleet Getting Connected Guide
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1
Setting Up the Mass Spectrometer
Connecting the Vacuum System
Connecting Line Power to the Forepump
This section describes how to connect the forepump to line power (ac mains power system).
The forepump receives 230 Vac power through its connection to the Forepump receptacle on
the right side of the instrument (Figure 5).
IMPORTANT Do not connect the forepump to a wall outlet.
Figure 5.
Power panel for the LCQ Fleet MS
Ethernet port
Forepump receptacle
 To connect line power to the forepump
1. Turn off (0) the power switches on both the instrument and the forepump.
2. Connect the forepump’s nondetachable power supply cord to the Forepump receptacle.
IMPORTANT Do not turn on the forepump until after you complete all of the system
connections and connect the instrument to line power.
CAUTION Trip hazard. After completing the forepump connections, move the pump to
the floor, either under or to the side of the workbench. Do not place it on the workbench.
Route the hose so that it is not a trip hazard.
10
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1
Setting Up the Mass Spectrometer
Connecting the Data System Computer
Connecting the Data System Computer
The data system for the LCQ Fleet MS includes a computer, a monitor, and an Ethernet
switch. You can also add a printer. The instrument communicates with the data system
computer through an Ethernet network.
Table 7 lists the parts required to connect the data system computer to the instrument. These
parts are in the MS Setup Kit (P/N 70111-62033).
Table 7. Shipped data system connection hardware
Description
Quantity
Part number
Ethernet cable, Category 5, 2.1 m (7 ft) long
2
00302-01838
Fast Ethernet switch, 10T/100Base-TX, 5-port
1
00825-01-00024
CAUTION Safety and EMC regulations require the use of Category 5 shielded Ethernet
communication cables, maximum 3 m (10 ft) long.
 To connect the instrument to the data system computer
1. Connect one Ethernet cable from a port on the Ethernet switch to the Ethernet port on
the right side of the instrument (see page 10).
2. Connect the second Ethernet cable from a port on the Ethernet switch to the Ethernet
network card (labeled LC/MS) in the data system computer.
3. Connect a power supply cord from the Ethernet switch to a wall outlet, and then turn on
the Ethernet switch.
4. If the Ethernet switch has an ECO button (for power conservation), make sure that it is
in the Off position to maintain the communication link between the instrument and data
system computer.
5. Connect another power supply cord from the computer to a wall outlet, and then turn on
the computer.
Tip For troubleshooting purposes, you might want to record which devices connect to
which Ethernet ports.
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1
Setting Up the Mass Spectrometer
Connecting the Mass Spectrometer to Line Power
Connecting the Mass Spectrometer to Line Power
Note For information about the line power requirements, refer to the LCQ Fleet
Preinstallation Requirements Guide.
 To connect the instrument to line power
1. Turn off (0) the main power switch.
2. Place the electronics service switch to Service Mode (down position).
3. Connect the power supply cord to the Power In receptacle on the right side of the
instrument, and then plug the cord into a 230 Vac wall outlet.
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2
Ion Max and Ion Max-S Ion Sources
This chapter briefly describes the Ion Max™ and Ion Max-S™ ion source assemblies and the
source drain connection to the LCQ Fleet MS.
Note For information about available ionization modes, and how to install or remove the
API source housing, refer to the Ion Max and Ion Max-S API Source Hardware Manual.
Contents
• API Source Housing
• API Source Housing Drain
API Source Housing
The Ion Max or Ion Max-S API source housing holds the ESI, HESI-II, or APCI probe. The
Ion Max has two features that the Ion Max-S does not have: an adjustable probe port and a
front door with a window. Aside from these two features, these two source housings have the
same functionality and mount to the LCQ Fleet MS in the same way. No tools are needed to
remove or install the API source housing or source drain. For information about installing or
removing the API source housing, refer to the LCQ Fleet Getting Started Guide and the
Ion Max and Ion Max-S API Source Hardware Manual.
Figure 6 shows the API source mounting assembly located on the front of the instrument (left
drawing) and the back view of the API source housing (right drawing). The API source
housing receives power for the heater, high-voltage safety interlock, and readback through the
housing connector.
CAUTION Hot surface. While the mass spectrometer is in operation, the external surface
of the API source housing can become extremely hot. Let the API probe and housing cool
to room temperature (approximately 20 minutes) before you touch them.
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2
Ion Max and Ion Max-S Ion Sources
API Source Housing
Figure 6.
API source housing connection
API source housing
connector
Guide pins on the instrument
mount assembly
14
LCQ Fleet Getting Connected Guide
Guide pin holes on the back
of the API source housing
Thermo Scientific
2
Ion Max and Ion Max-S Ion Sources
API Source Housing Drain
API Source Housing Drain
When installing the API source, connect the drain at the bottom of the API source housing to
the solvent waste container (Figure 7). For instructions, refer to the Ion Max and Ion Max-S
API Source Hardware Manual.
Figure 7.
API source drain assembly and waste container
Source drain adapter
API source drain
Tygon tubing, 1 in. ID
(at least 1 m [3 ft])
Reducing connector
Tygon tubing, 0.5 in. ID
Tygon tubing, 0.5 in. ID,
connects to the cap.
To an external vent
Solvent waste container
Table 8 lists the components of the solvent waste system. During the initial installation of the
instrument, a Thermo Fisher Scientific field service engineer installs the solvent waste system.
Thermo Scientific
LCQ Fleet Getting Connected Guide
15
2
Ion Max and Ion Max-S Ion Sources
API Source Housing Drain
Table 8. Solvent waste system parts
Description
Part number
Kit
Cap, filling/venting
00301-57022
MS Setup Kit
Container, Nalgene™, heavy-duty, 4 L
00301-57020
MS Setup Kit
Reducing connector, single barbed fitting,
1 to 0.5 in. ID
00101-03-00001
MS Setup Kit
Source drain adapter, Teflon
70111-20971
MS Accessory Kit
Tubing, Tygon™, 0.5 in. ID, 3/4 in. OD
00301-22920
MS Setup Kit
Tubing, Tygon PVC, 1 in. ID, 1-3/8 in. OD
00301-22922
MS Setup Kit
Use these guidelines for the API source drain:
• Use the PVC tubing provided with the solvent waste container to connect the solvent
waste container to a fume exhaust system. Do not connect silicone tubing to the API
source drain. If silicone tubing connects to the outlet drain, you might observe
background ions at m/z 536, 610, and 684.
CAUTION Do not vent the PVC drain tube (or any vent tubing connected to the
waste container) to the same fume exhaust system that connects to the forepump.
Vent the waste container to a dedicated fume exhaust system. The exhaust system for
the API source must accommodate a flow rate of up to 30 L/min (64 ft3/h).
• Use the Teflon source drain adapter (see Table 8). Do not connect Tygon tubing directly
to the API source drain. At high temperatures, Tygon releases volatile contaminates.
f
CAUTION When you reconnect the API source drain tubing to the bottom of the API
source housing, make sure that you first connect the Teflon source drain adapter. This
adapter can withstand the high temperatures produced by the H-ESI or APCI source.
• To prevent solvent waste from backing up into the mass spectrometer, make sure that all
tubing is above the level of liquid in the waste container as follows:
16
–
Tygon tubing from the mass spectrometer to the solvent waste container
–
PVC tubing from the waste container to the exhaust system
LCQ Fleet Getting Connected Guide
Thermo Scientific
3
External Peripheral Devices
This chapter provides information on how to control an external device that connects to the
LCQ Fleet MS through a contact closure cable. Control of external devices might or might
not be through one of the Thermo Scientific mass spectrometry applications, such as the
Xcalibur data system.
Note For information about connecting LC devices that are controlled by a layered
application, refer to the appropriate manual provided on the LC Devices software DVD.
Contents
• Interface Kits
• External Devices Controlled by a Mass Spectrometry Application
• External Devices Not Controlled by a Mass Spectrometry Application
Interface Kits
Table 9 lists the kits that connect the instrument to various external devices.
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3
External Peripheral Devices
External Devices Controlled by a Mass Spectrometry Application
Table 9. Data system interface kits
Description
Part Number
Xcalibur Ethernet Communication Kit (Agilent 1200 Series LC):
OPTON-30012
•
•
•
•
•
Contact closure cable with 15-pin connector
Contact closure PCB
Ethernet Category 5 shielded cables (2)
Ethernet switch, 10T/100Base-TX, 5-port
Agilent G1369A LAN card
Xcalibur JetDirect™ Ethernet Control Kit (Agilent™ 1100 Series LC):
•
•
•
•
•
OPTON-30018
Contact closure cable with 15-pin connector
Contact closure PCB
Ethernet Category 5 shielded cables (2)
Ethernet switch, 10T/100Base-TX, 5-port
HP™ JetDirect 400N print server PCB
Mass Spectrometer Contact Closure Cable (for devices not controlled by OPTON-21705
the Xcalibur data system):
• 2-wire trigger cable
• 8-position screw connector
External Devices Controlled by a Mass Spectrometry Application
Thermo mass spectrometry applications, such as the Xcalibur data system, control external
devices (for example, autosamplers, pumps, and detectors) from several manufacturers
including Thermo Fisher Scientific, Agilent Technologies, and Waters™ Corporation.
The LCQ Fleet MS can start data acquisition upon receiving a contact closure (start) signal
from an external device, which is typically an autosampler. This external device connects to
the contact closure pins (Start In ±) by using the contact closure cable provided with the LC
device. For instructions, refer to the instrument manual.
CAUTION The external device providing the start signal must have proper earth
grounding. Ground loops can cause problems and create a safety hazard. The
complementary metal-oxide-semiconductor (CMOS) integrated circuits that are mounted
on the internal input/output (I/O) printed circuit board (PCB) fail if they receive more
than 5 V or 5 mA.
To connect and set up the external device, follow these procedures:
1. Connecting the Contact Closure Cable
2. Selecting the Start Instrument
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3 External Peripheral Devices
External Devices Controlled by a Mass Spectrometry Application
Connecting the Contact Closure Cable
Thermo Fisher Scientific provides instructions for connecting supported LC systems to a
Thermo Scientific mass spectrometer. You can access the appropriate manual from the data
system computer by choosing Start > All Programs > Thermo Instruments > Manuals >
LC Devices and so on to find the applicable manual for your specific device.
The contact closure connector (Start In pins) for the instrument is on the right side
(Figure 8).
Figure 8.
Peripheral Control and Analog Input terminals
Inlet device
2-wire contact
closure cable
Selecting the Start Instrument
You can now turn on the data system computer, Ethernet switch, forepump, mass
spectrometer, and LC system. By default, the Xcalibur data system, for example, selects the
configured autosampler as the start instrument for a sequence run. The following procedure
shows you how to verify this setting and, if necessary, change the selection.
 To select the external start instrument
1. Open the Xcalibur data system, and then choose View > Sequence Setup View to open
the Sequence Setup window.
2. Open the sequence that you want to run as follows:
a. Click the Open button and browse to the appropriate folder.
b. Select the sequence (SLD) file and click Open.
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External Peripheral Devices
External Devices Controlled by a Mass Spectrometry Application
3. Choose Actions > Run Sequence or Actions > Run This Sample to open the Run
Sequence dialog box (Figure 9).
The Yes in the Start Instrument column indicates that the default start instrument for the
sequence run is the Thermo Scientific Accela Open Autosampler.
Figure 9.
Run Sequence dialog box showing the default start instrument
4. If you must change the start instrument, do the following:
a. Click Change Instruments to open the Change Instruments In Use dialog box
(Figure 10).
Figure 10. Change Instruments In Use dialog box showing the default start instrument
20
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3 External Peripheral Devices
External Devices Not Controlled by a Mass Spectrometry Application
b. In the Start Instrument column, click the blank field to the right of the appropriate
triggering device (typically an autosampler) to move the word Yes to this field.
c. Click OK.
5. In the Run Sequence dialog box, complete the remaining selections.
6. Click OK.
External Devices Not Controlled by a Mass Spectrometry Application
When an external device is not controlled by a Thermo mass spectrometry application, such
as the Xcalibur data system, you must properly connect it to send its contact closure (start)
signal. In addition, the Xcalibur Run Sequence dialog box must indicate the appropriate
instrument as the start instrument.
The LCQ Fleet MS can start data acquisition upon receiving a contact closure (start) signal
from an external device, typically an autosampler. This external device connects to the contact
closure pins (Start In ±) by using a contact closure cable.
To connect and set up the external device, follow these procedures, as applicable:
1. Connecting the Contact Closure Cable
2. Starting a Sequence Run from the Xcalibur Data System on page 22
Connecting the Contact Closure Cable
Before proceeding, verify that the external device is suitable for use with the instrument.
Note To start data acquisition, the output (start) signal from the external device must be
Normally Hi (5 V) and momentarily go to Low (less than 2.5 V). If you cannot configure
the external device to go from Normally Hi to Low momentarily, you cannot use it with
the instrument.
If the Xcalibur data system does not control your external device, use the supplied contact
closure mating connector to assemble a two-wire contact closure cable. This cable connects
the Start In pins on the instrument (Figure 8 on page 19) to your device. However, you are
responsible for providing the cable for the Ready Out and Start Out pin connections, which
are described in Table 10.
The Analog Input terminal (Figure 8) converts the signal from an analog external input device
to a digital signal for the LCQ Fleet MS. Analog devices are typically those that are not
controlled by a mass spectrometry application.
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3
External Peripheral Devices
External Devices Not Controlled by a Mass Spectrometry Application
The 1 V Max and 10 V Max inputs are 12-bit analog-to-digital converters (ADCs) that
acquire a 1 V or 10 V input signal from the connected external device. The output signals
from the ADCs are low resolution and suitable for qualitative data acquisition. The 1 V Max
input accepts a 0–1 V signal and the 10 V max input accepts a 0–10 V signal. For a high
resolution ADC output signal suitable for quantitative data acquisition, use an external high
resolution analog converter.
Table 10. Pin-out descriptions for an external device contact closure connection
Peripheral control pin
Description
Start In +
A digital latch circuit (TTL) that sends a 5 V signal to the
connected external device, which must be able to pull the
signal to less than 2.5 V.
Start In –
Earth ground.
Ready Out (2 pins)
Provides ready status.
The relay switch circuit sends a programmable output signal
to the external receiving device. Rated maximum 3 A,
switching 60 W.
Start Out (2 pins)
Provides a connection for an external device that requires a
programmable start signal, such as a fraction collector.
The relay switch circuit sends a programmable output signal
to the external receiving device. Rated maximum 3 A,
switching 60 W.
 To connect the contact closure cable
1. Connect the contact closure cable to the Start In pins on the right side of the instrument
(Figure 8 on page 19).
2. Connect the other end of the cable to the external device according to its manual.
Starting a Sequence Run from the Xcalibur Data System
You can now turn on the data system computer, Ethernet switch, forepump, mass
spectrometer, and LC system. When the Xcalibur data system, for example, does not control
the autosampler, it selects the mass spectrometer as the start instrument for a sequence run.
Therefore, you must change the start instrument as part of the sequence run setting.
 To start the sequence run
1. Open the Xcalibur data system, and click the Sequence Setup icon to open the Sequence
Setup window.
2. Open the sequence that you want to run as follows:
a. Click the Open button and browse to the appropriate folder.
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3 External Peripheral Devices
External Devices Not Controlled by a Mass Spectrometry Application
b. Select the sequence (.sld) file and click Open.
3. Choose Actions > Run Sequence or Actions > Run This Sample to open the Run
Sequence dialog box (Figure 11).
The Yes in the Start Instrument column indicates that the default start instrument for the
sequence run is the mass spectrometer.
Figure 11. Run Sequence dialog box with the mass spectrometer as the start instrument
4. Click Change Instruments to open the Change Instruments In Use dialog box
(Figure 12).
Figure 12. Change Instruments In Use dialog box without a specified start instrument
The instrument is not selected as
the start instrument.
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External Peripheral Devices
External Devices Not Controlled by a Mass Spectrometry Application
5. Do one of the following:
• If Yes appears in the Start Instrument column for the mass spectrometer, click Yes to
clear this device as the start instrument.
• If Yes does not appear in the Start Instrument column for the mass spectrometer,
click OK.
6. Under Acquisition Options, select the Start When Ready check box, and then click OK.
The instrument method downloads to the instrument, and the Status page displays the
following message:
Waiting - Contact Closure
7. If the Xcalibur Roadmap page does not display the Info View pane, click the
Information View button, and then click the Status tab.
8. Start the external device.
Acquisition from the instrument begins after the external device sends the contact closure
(start) signal.
In situations where the Xcalibur data system does not control external devices such as
autosamplers, control might be through a third-party system or a built-in control system.
For example, you can control the Thermo Scientific SpectraSYSTEM™ AS3000
autosampler from its front-panel command center.
Note The SpectraSYSTEM LC modules are external devices because Thermo Fisher
Scientific does not provide Xcalibur-compatible device drivers for them. You can control
the SpectraSYSTEM LC modules from their front-panel control modules.
24
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3
External Peripheral Devices
Triggering External Devices
Triggering External Devices
You can use Thermo Scientific mass spectrometry applications, such as the Xcalibur data
system, to trigger (activate or deactivate) an external device, such as a fraction collector, when
the LCQ Fleet MS detects a specified target.
A contact closure signal that triggers an external device can occur when one or more external
trigger activation masses are present in the mass spectrum, or the base peak intensity exceeds a
preset threshold.
To select the first option, specify the external trigger activation masses for each sample in the
Sequence Setup view in the columns for predefined user labels: ETMW (external trigger
molecular weight) or MWFC (molecular weight for fraction collection). The data system
automatically tests for the presence of external trigger activation masses and the presence of
these masses with common solvent adducts. When the external trigger activation mass is no
longer present in the scan or when the base peak intensity is less than the preset threshold, the
contact closure is deactivated.
Note For additional information about triggering an external device, refer to the Tune
Plus Help.
Thermo Scientific
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External Peripheral Devices
Triggering External Devices
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Thermo Scientific
G
Glossary
A
B
C
D
E
F
G
H
I
J
K
L M N O
A
API source The sample interface between the liquid
chromatograph (LC) and the mass spectrometer
(MS).
atmospheric pressure chemical ionization (APCI) A
soft ionization technique done in an ion source
operating at atmospheric pressure. Electrons from a
corona discharge initiate the process by ionizing the
mobile phase vapor molecules, forming a reagent gas.
atmospheric pressure ionization (API) Ionization
performed at atmospheric pressure by using
atmospheric pressure chemical ionization (APCI),
heated-electrospray ionization (H-ESI), or nanospray
ionization (NSI).
auxiliary gas The outer-coaxial gas (nitrogen) that
assists the sheath (inner-coaxial) gas in dispersing
and/or evaporating sample solution as the sample
solution exits the APCI, ESI, or HESI nozzle.
C
collision gas A neutral gas used to undergo collisions
with ions.
computer data system See data system.
Thermo Scientific
P
Q
R
S
T
U
V W X
Y
Z
contact closure connection The cable connection is
from the external peripheral device to the mass
spectrometer contact closure pins (Start In ±). The
external device sends the contact closure (start) signal
to the mass spectrometer.
D
damping gas Helium gas introduced into the ion trap
mass analyzer that slows the motion of ions entering
the mass analyzer so that the ions can be trapped by
the rf voltage fields in the mass analyzer.
data system Consists of a computer, a monitor, a
keyboard, a mouse, an Ethernet switch, and an
optional printer.
E
electrospray (ESI) A type of atmospheric pressure
ionization that is currently the softest ionization
technique available to transform ions in solution into
ions in the gas phase.
electrospray ionization (ESI) See electrospray (ESI).
F
forepump The pump that evacuates the foreline. A
rotary-vane pump is a type of forepump. It might
also be referred to as a backing, mechanical, rotaryvane, roughing, or vacuum pump.
LCQ Fleet Getting Connected Guide
27
Glossary: heated-electrospray (H-ESI)
H
heated-electrospray (H-ESI) A type of atmospheric
pressure ionization that converts ions in solution into
ions in the gas phase by using electrospray ionization
(ESI) in combination with heated auxiliary gas.
heated-electrospray ionization (H-ESI) See heatedelectrospray (H-ESI).
I
ion source A device that converts samples to gas-phase
ions.
N
nanoelectrospray (nanoNSI or NSI) A type of
electrospray (ESI) that accommodates very low flow
rates of sample and solvent at 1–20 nL/min (for
static nanospray) or 100–1000 nL/min (for dynamic
nanospray).
S
sheath gas The inner coaxial gas (nitrogen), which is
used in the API source to help nebulize the sample
solution into a fine mist as the sample solution exits
the ESI or APCI nozzle.
source See API source.
sweep gas Nitrogen gas that flows out from behind
the sweep cone in the API source. Sweep gas aids in
solvent declustering and adduct reduction.
28
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Thermo Scientific
I
Index
A
Agilent Technologies 18
API source
ionization modes 13
solvent waste container, connecting 15
API source drain 15
API source drain adapter, caution 16
auxiliary power receptacle 10
C
Change Instruments In Use dialog box 20, 23
communication connections, Ethernet 11
compliance
EMC 11
FCC iv
regulatory iii
computer
See data system computer
contact closure cable
connecting, without MS control 21
description 18
contact closure connectors
drawing 19
pin-outs 22
contact closure signal 18, 21
contacting us xiv
customer responsibility 2–3, 21
downloading documents xii
drain, API source housing 15
E
electromagnetic compatibility iii
electronics service switch 10, 12
EMC compliance iii, 11
Ethernet
port 10
switch, connecting 11
exhaust hose, connecting 9
F
FCC compliance iv
figures, list of ix
forepump
fume exhaust system
connecting 9
exhaust hose 9
fume exhaust systems
description 9
line power 10
operating instructions 5
vacuum hose
connecting 7
description 6
fume exhaust systems 9
D
G
data acquisition 18, 21
data system computer
connecting to the MS 11
description 11
directive, WEEE v
documentation
accessing xii
additional xi
gas ballast valve 9
gas supplies
connecting 5
description 2
fittings and parts 3
pressures 2
Thermo Scientific
LCQ Fleet Getting Connected Guide
29
Index: H
gases
See helium gas or nitrogen gas
grounding method, caution 18
H
hardware, gas plumbing provided 3
hardware, shipped
Ethernet communications 11
forepump fume exhaust system 9
vacuum system 6–7
helium gas
connecting 4
note 4
plumbing hardware 3
grounding 18
output signal 21
power
See line power
power panel 10
power switch, main 10
pump
See forepump
R
receptacle, auxiliary power 10
regulatory compliance iii
relay switch circuit 22
Run Sequence dialog box 20, 23
K
S
kits
MS Accessory 3
MS Setup 3, 9, 11
shipped with instrument 3
Xcalibur Ethernet Control, Agilent 1200 Series LC 18
Xcalibur JetDirect Ethernet Control, Agilent 1100
Series LC 18
safety standards iii
sequence run, starting 22
solvent waste
API applications 9
routing 15
start instrument, configuring
with Xcalibur control (example) 19
without Xcalibur control 22
start signal
See contact closure signal
switches
electronics service 10, 12
main power 10
L
LC devices
manuals 17, 19
SpectraSYSTEM 24
LC solvents 4
line power
data system computer 12
forepump 10
mass spectrometers 12
M
T
Thermo Scientific website, user documents xii
trigger cable
See contact closure cable
triggering external devices 25
mass spectrometers
line power 12
power panel 10
mass spectrometry applications 17
V
N
W
nitrogen gas
connecting 5
plumbing hardware 3
waste container 15
Waters Corp. 18
WEEE directive v
vacuum hose, connecting 7
P
peripheral devices
description 17
30
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Thermo Scientific

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