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3 Technical data
3 Technical data
This chapter introduces the reader to the instrument specifications. It contains the scope of delivery, technical data, requirements and performance data.
3 .1 Scope of delivery
Check the scope of delivery according to the order number.
NOTE
For detailed information on the listed products, see www.buchi.com or contact your local dealer.
3 .1 .1 Basic instrument
Order number:
2 3
0
x x x x x x
Rotavapor R-210
11
R-210/215 Operation Manual, Version E
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Table of contents
- 6 About this manual
- 6 Reference documents
- 6 1.2 Trademarks
- 6 1.3 Abbreviations
- 7 2 Safety
- 7 User qualification
- 7 Proper use
- 7 Improper use
- 8 Warning notices used in this manual
- 8 Product safety
- 8 2.5.1 Instrument-related hazards
- 9 2.5.2 Other hazards
- 9 2.5.3 Safety measures
- 9 2.5.4 Safety elements
- 10 General safety rules
- 11 Technical data
- 11 Scope of delivery
- 11 3.1.1 Basic instrument
- 12 3.1.2 Standard accessories
- 19 3.1.3 Optional accessories
- 22 3.1.4 Upgrade
- 22 Materials used
- 23 Technical data overview
- 24 Solvent table
- 25 Description of function
- 25 Functional principle of a Rotavapor
- 25 4.1.1 Functional principle considering the V assembly as example
- 26 4.1.2 Controls of Rotavapor R
- 27 4.1.3 Rear connections of the Rotavapor
- 27 Motorized quick-action jack
- 28 Heating bath
- 28 Combi Clip
- 29 Vapor temperature sensor
- 29 Protective shield (optional)
- 30 Valve unit
- 30 Woulff bottle
- 30 Combination of Rotavapor and vacuum controller
- 31 4.10 Infrared interface
- 32 Putting into operation
- 32 Installation site
- 32 Electrical connections
- 32 Commissioning the heating bath
- 33 5.3.1 Heating Bath B
- 34 5.3.2 Heating medium
- 35 Glass assembly
- 35 Installing the condenser and the seal
- 36 Installing the reflux insert
- 36 Mounting the support rod (optional accessory)
- 37 Tube connections
- 37 5.8.1 Connection scheme
- 38 5.8.2 Cooling water tubes
- 38 5.8.3 Vacuum tubes
- 39 5.8.4 Tube connections to the valve unit
- 40 Installing the vacuum controller
- 40 5.10 Cable connections to the Rotavapor
- 41 5.11 Installing the vapor temperature sensor
- 41 5.12 Functional test
- 42 6 Operation
- 42 Settings at the heating bath
- 42 6.1.1 Setting the heating bath temperature
- 42 6.1.2 Switching the B-491 from water bath mode to oil bath mode
- 43 6.1.3 Switching the B-491 from oil bath mode to water bath mode
- 43 6.1.4 Selecting the set temperature
- 43 6.1.5 Changing / switching off the set temperature
- 44 Immersion angle of the evaporating flask into the heating bath
- 45 Lowering and raising the evaporating flask into and out of the heating bath
- 45 Selecting the distillation conditions
- 46 6.5 Distilling
- 47 Optimizing the distillation conditions
- 48 When the distillation “dies out
- 49 7 Maintenance
- 49 7.1 Housing
- 49 Tube connections and joints
- 49 Sealing system
- 50 7.3.1 Cleaning the seals
- 50 7.3.2 Replacing the seals
- 50 Heating bath
- 50 Glass components
- 51 8 Troubleshooting
- 51 Malfunctions and their remedy
- 54 Customer service
- 55 Shutdown, storage, transport and disposal
- 55 Storage and transport
- 55 9.2 Disposal
- 56 Health and safety clearance form
- 57 10 Spare parts
- 58 10.1 Glass assembly A
- 59 10.2 Glass assembly V
- 60 10.3 Glass assembly C
- 62 10.4 Glass assembly S
- 64 10.5 Glass assembly CR
- 66 10.6 Glass assembly E
- 68 10.7 Glass assembly BY
- 69 10.8 Sealing system
- 70 10.9 Various glass parts
- 73 10.10 Miscellaneous
- 76 11 Declarations and requirements
- 76 11.1 FCC requirements (for USA and Canada)
- 77 11.2 Declaration of conformity