advertisement
HANDLING, INSTALLATION, STORAGE AND TRANSIT INFORMATION
5.1.3 Mechanical Handling
5.1.3.1 Weights, Dimensions and Lifting Points
Description NET Dimensions
Weight kg
(width x height x depth)
cm
Centre of gravity
Kappa goniometer
106 43 x 64 x 47 Offset from centre of unit towards side of
X-ray tube mount
Lifting points
At four corners
(DO NOT lift from below)
40 48 x 22 x 69 Centre of unit X-ray generator
Enclosure
Electronics rack
15
60
115 x 100 x 100
80 x 85 x 80
N/A
Centre of unit
From the sides and below
N/A
By hand from top four corners, otherwise from below
KMW200CCD 55
KMW3000C
Helijet
Cryojet
56
10
15
38 x 54 x 75
38 x 54 x 96
Centre of unit
Centre of unit
At the four corners and from below
At the four corners and from below
30 x 25 x 10 (head only) Centre of component parts
From below with transfer tube removed
15 x 35 x 15 (head only) Centre of component parts
From below or using handles whilst supporting transfer tube.
ILM210
ITC502
GFC1
5
5
12
44 x 10 x 30
44 x 10 x 30
45 x 26 x 38
Centre of unit
Centre of unit
Centre of unit
By hand from below
By hand from below
Front panel handles
Version 1.4 Xcalibur_Manual_v1.4
Page 24
Xcalibur
USER MANUAL
advertisement
Related manuals
advertisement
Table of contents
- 10 1. Health and Safety Information
- 10 1.1 General
- 11 1.2 Electrical Safety
- 11 1.2.1 Potential Electrical Hazards
- 11 1.2.2 Recommended Precautions
- 11 1.2.3 First Aid
- 12 1.3 Mechanical Handling Safety
- 12 1.4 Safe Mechanical Practice
- 12 1.5 Moving Parts
- 12 1.6 X-ray Radiation
- 13 1.7 Extreme Temperatures
- 14 1.8 Vacuum
- 14 1.9 High Pressures
- 14 1.10 Hazardous or Toxic Materials
- 14 1.11 Modifications and Service
- 15 2. Introduction
- 15 2.1 Scope
- 15 2.2 How To Use This Manual
- 15 2.3 System Overview
- 16 3. Specifications
- 16 3.1 Environmental Requirements
- 16 3.2 Services
- 16 3.2.1 Electrical Supply
- 16 3.2.2 Water Cooling
- 17 3.2.3 Helium Gas Supply (where applicable)
- 17 3.3 Performance Data
- 17 3.3.1 X-ray Tube (Typical Operating Conditions)
- 18 3.3.2 Sapphire 2 CCD Detector
- 19 3.3.3 Sapphire 3 CCD Detector
- 20 3.3.4 Onyx CCD Detector
- 20 Onyx CCD Detector Theta and Resolution Ranges
- 21 3.3.5 PC CCD Interface
- 21 3.3.6 Four-circle Kappa Geometry X-ray Goniometer
- 22 4.4 Electrical Data
- 23 4. Technical Description
- 23 4.1 Overview
- 24 4.2 CCD Detector Technology
- 25 4.2.1 Beryllium Window
- 26 4.2.2 Phosphor
- 26 4.2.3 Taper
- 26 4.2.4 CCD
- 26 4.2.5 Readout Speed
- 26 4.2.6 Binning
- 27 4.2.7 Dark Current and MPP Mode
- 27 4.2.8 Radiation Damage
- 27 4.2.9 Full Well Depth and 18-bit Digitisation
- 27 4.2.10 Anti-blooming
- 27 4.2.11 Vacuum
- 27 4.2.12 Fast Shutter
- 28 4.2.13 Zingers and Cosmic Ray Events
- 28 4.3 Four-Circle Kappa Geometry Goniometer
- 29 4.4 X-ray Generator
- 30 4.5 Software
- 30 4.5.1 Directory Structure
- 31 4.5.2 Basic Menu Philosophy
- 31 4.6 KMW200CCD Chiller
- 31 4.7 KMW3000C Chiller
- 31 4.8 Low Temperature Option
- 31 4.9 Safety Features
- 32 5. Handling, Installation, Storage and Transit Information
- 32 5.1 Reception and Handling
- 32 5.1.1 Delivery
- 32 5.1.2 Unpacking
- 33 5.1.3 Mechanical Handling
- 33 5.1.3.1 Weights, Dimensions and Lifting Points
- 34 Delivery
- 34 5.2 Installation and Setting to Work
- 34 5.2.1 Preparation of Site and Services
- 34 5.2.1.1 Environmental Requirements
- 34 5.2.1.2 System Layout
- 35 5.2.1.3 Electrical Services
- 36 5.2.1.4 Water Supply
- 36 5.2.1.5 Low Temperature Option
- 36 5.2.1.6 CCD Camera Pumping
- 36 5.2.1.7 Helijet Option
- 37 5.2.2 Setting to Work
- 37 5.2.2.1 Equipment Required
- 37 5.2.2.2 Personnel Required for Installation
- 37 5.2.2.3 Setting up Procedures
- 39 Storage
- 40 6. Operation
- 40 6.1 Controls and Indicators
- 41 6.2 Initial Switch on Procedure
- 42 6.3 X-ray Tube Warm-up Procedure
- 43 6.4 Software
- 43 6.4.1 Software Updates
- 44 6.4.2 Software Installation
- 44 6.4.2.1 MGC interface software
- 45 6.4.2.2 CrysAlis Software
- 45 6.4.3 Changing Machine Correction and Set-up Files
- 46 6.5 Normal Operation
- 46 6.5.1 General Commands
- 48 6.5.2 Changing Xcalibur Settings
- 52 6.5.3 Standard Diffraction Experiment
- 52 6.5.3.1 Crystal Mounting and Alignment
- 54 6.5.3.2 Diffraction Photographs to Determine Crystal Quality
- 55 6.5.3.3 Unit Cell Determination
- 57 6.5.3.4 Data Collection
- 58 6.5.3.5 Data Processing and Reduction
- 59 6.5.3.5.1 Orientation Matrix
- 60 6.5.3.5.2 Run List
- 61 6.5.3.5.3 Scan Width
- 61 6.5.3.5.4 Background Evaluation
- 62 6.5.3.5.5 Special Corrections
- 63 6.5.3.5.6 Outlier Rejection
- 64 6.5.3.5.7 Output Format
- 65 6.5.3.6 Changing the Output Format from Data Reduction
- 66 6.5.3.7 Absorption Correction
- 74 6.5.3.8 GRAL - Space Group Determination
- 80 6.5.3.9 Structure Solution and Refinement
- 80 6.5.4 Ewald explorer
- 86 6.5.5 Dc Movie - Replay of Data Collection Movie
- 87 6.5.6 Reconstruction of Precession Photographs
- 91 6.5.7 Dc opti - Optimisation of Data Collection Strategy
- 96 6.5.8 Indexing and Data Reduction of Incommensurate Samples
- 97 6.5.9 Indexing and Data Reduction of Twinned Samples
- 99 6.5.10 Extracting Data from Powder Samples
- 100 6.5.11 Refining of Machine Parameter File
- 103 6.5.12 Glossary of CrysAlis Commands
- 110 6.6 Normal Shutdown
- 110 6.7 Emergency Shutdown
- 111 6.7.1 Emergency Shutdown Procedure
- 112 7. Mechanical Changeover of Detectors and X-ray Sources
- 112 7.1 Interchange of CCD Detectors
- 112 7.1.1 Installation of a Sapphire 2 and Sapphire 3 CCD detectors
- 113 7.1.2 Removal of a Sapphire 2 and Sapphire 3 CCD detectors
- 113 7.1.3 Installation of the Onyx CCD camera
- 116 7.1.4 Removal of the Onyx CCD camera
- 117 7.2 Procedure for Interchange of the Molybednum and Copper Enhance X-ray Source
- 121 8. Maintenance Schedules
- 121 8.1 Introduction
- 121 8.2 Weekly Maintenance Schedule
- 121 8.3 Monthly Maintenance Schedule
- 122 8.4 Six Monthly Maintenance Schedule
- 122 8.5 Yearly Maintenance Schedule
- 123 8.6 10,000 Hours Maintenance Schedule
- 124 9. Maintenance Instructions
- 124 9.1 Special Tools
- 124 9.2 Refining the Machine Parameter File
- 125 9.3 Changing the X-ray Tube of Enhance
- 126 9.4 Changing the X-ray Tube of Enhance ULTRA
- 128 9.5 X-ray Beam Stop Alignment
- 129 9.6 Changing the Collimator of Enhance
- 130 9.7 Changing the Collimator of Enhance Ultra
- 130 9.8 Aligning the X-ray Collimator of Enhance
- 130 9.9 Aligning the Enhance X-ray Source
- 133 9.10 Aligning the Enhance Ultra X-ray Source
- 133 9.10.1 X-ray Beam Alignment of Enhance Ultra
- 135 9.10.2 Optic Alignment of Enhance Ultra
- 136 9.10.3 Collimator Alignment of Enhance Ultra
- 136 9.10.4 Aligning the beam to the centre of the goniometer – Enhance Ultra
- 137 9.11 Checking the Door Safety Interlocks
- 137 9.12 Checking the Emergency stop
- 138 9.13 Checking the X-ray Radiation Levels
- 138 9.14 CCD Detector – Pumping Out Vacuum
- 140 9.15 Dismantling Xcalibur
- 143 10. Trouble Shooting
- 146 11. Spares
- 148 12. Disposal Instructions
- 148 12.1 X-ray Tube and CCD Detector
- 148 12.2 Third Party Equipment
- 149 13. Additional Information
- 149 13.1 Third Party Information
- 150 13.2 Drawings
- 150 13.2.1 Mechanical Drawings
- 150 Xcalibur Suggested Layout
- 150 System and Component Dimensions
- 152 13.2.2 Electrical Drawings
- 154 14. CE Conformity notice
- 155 Appendices
- 155 Appendix 1 X-ray Tubes Wave Lengths
- 155 Appendix 2 Standard Crystal Parameters
- 155 Appendix 3 Temperature Scales Conversion
- 155 Appendix 4 Maintenance Records
- 160 Appendix 5 Example of Local Rules for the Xcalibur System Set Up at Oxford Diffraction